METROLOGY 101
Infrared Thermometer Calibration
                                                  By Frank Liebmann
    Training Objective: The objective of this article is to give laboratory personnel a basis to set up a calibration program
    for infrared thermometers. While this information is not a complete set of instructions, it contains a number of factors that
    commonly result in errors to people who are calibrating these devices.
    What Is an Infrared                                                     Field-of-View
    Thermometer Measuring?                                                      Handheld IR thermometers usually come equipped with
                                                                            a laser pointer. This serves as a guide to show where the
       An infrared thermometer is a non-contact thermometer,                infrared thermometer is pointed. However, these pointers
    since it doesn’t touch the surface being measured. It                   can be misleading in two respects. First, the laser provides
                                                                            a finite point. In fact, the infrared thermometer is typically
    measures thermal radiation in the infrared region of the
                                                                            measuring a non-finite area or spot which will be discussed
    electromagnetic spectrum beyond where the eye can see.
                                                                            shortly. Second, typically the laser center does not represent
    A common spectral band for measuring temperatures from
                                                                            the center of the spot.
    below ambient up to 500 °C or 1000 °C is the 8 – 14 µm
                                                                                Using IEC terminology, the measure for the size of
    band. This is partly because at room temperature, the peak
                                                                            this spot is field-of-view [3]. In a nutshell, field-of-view
    energy occurs just below 10 µm.
                                                                            specifies that the infrared thermometer will measure a
       As temperatures get higher, this peak wavelength
                                                                            certain percentage of energy within a specified diameter
    becomes shorter. Most people have seen a “red hot” piece
                                                                            at a given distance. What about the energy measured
    of metal. This is because the human eye can see this thermal            outside of this diameter? This is called scatter, and the
    radiation. The metal is red hot because the radiation has               infrared thermometer is measuring it as well. Most infrared
    a significant enough amount of energy in the shorter                    thermometers come with a diagram, or a specification of
    wavelengths where the human eye can see, between 0.3                    distance to size ratio (D:S). The diameter specified by this
    and 0.7 µm. This occurs at some point above 600 °C. The                 ratio only contains a certain percentage of the radiation
    Sun’s surface temperature is at a temperature between 5000              received by the infrared thermometer. For a measurement,
    and 5500 K. The peak wavelength for these temperatures                  it is best to have at least two times this ratio in diameter [1]
    is roughly 0.5µm, right in the middle of the range visible              as is shown in Figure 2. For calibration, the diameter of the
    to the human eye.                                                       source should be at least three times this diameter [4]. For
                                                                            this reason, a flat-plate is often used as a thermal radiation
    Pitfalls in Infrared                                                    source instead of a cavity. At a minimum, the measuring
    Thermometer Measurement                                                 distance and diameter of the source should be stated on
                                                                            the calibration certificate.
      There are a number of factors which can increase                                                                                              Effects of Emissivity Change (Tamb = 23°C, ε = 0.95)
    uncertainty and cause errors when using infrared                                                                                       8
                                                                         Change in Measured Temperature (0.01 change in emissivity) (°C)
    thermometers. An adequate uncertainty budget should                                                                                    7
    help point these out. There are two which cause people                                                                                 6
    more problems than others, emissivity and size-of-source.
                                                                                                                                           5
    Emissivity                                                                                                                             4
       Emissivity is a material’s ability to radiate compared to                                                                           3
    a perfect blackbody. It can have a value from anywhere                                                                                 2
    from 0.0 to 1.0. Bare metal tends to have a low emissivity;
    oxidized metal tends to have a moderate emissivity; non                                                                                1
    metals tend to have high emissivity [1]. Typically, it is                                                                              0
    difficult to control a surface’s emissivity to within ±0.01                                                                            -1
    [2]. In the 8 – 14 µm band, an uncertainty in emissivity of
    0.01 translates to a uncertainty of 0.6 K at 100 °C and 3.4 K                                                                          -2
                                                                                                                                                0   200               400               600                800   1000
    at 500 °C. This is illustrated in Figure 1.                                                                                                                    Source Temperature (°C)
                                                                               Figure 1. Effect of emissivity error.
    Cal Lab: The International Journal of Metrology                 20                                                                                                                   Jul • Aug • Sep 2011
	                                                   METROLOGY 101
    Figure 2. Proper measurement size-of-source.
    Equipment Needed for Calibration                                       Calibration of the Thermal Radiation Source
                                                                             There are two methods to calibrate the radiation source.
      Table 1 provides a list of equipment for infrared                    One is using a contact transfer and the other a radiometric
    thermometer calibration [5].                                           transfer. The contact calibration has the advantage in
                                                                           that it is not wavelength dependant. The contact transfer
     Mandatory Equipment
                                                                           does not account for the ‘heat exchange’ error [6]. When
                                   Two Types:                              a flat-plate source is used, it also may result in a large
                                     •	 Cavity (preferred)
     Thermal Radiation Source                                              uncertainty for emissivity [5]. The radiometric transfer
                                     •	 Flat-plate (large size-of-
                                        source)                            has the advantage in that it accounts for the errors caused
                                   Two Types:
                                                                           by heat exchange (between the reference probe and
     Transfer Standard               •	 Contact thermometer                the radiation source’s surface) and for not well defined
                                     •	 Radiation thermometer              emissivity. The radiometric transfer standard must be of the
     Ambient Temperature           Monitors laboratory                     same wavelength as the infrared thermometer’s calibrated
     Thermometer                   temperature.                            using the thermal radiation source [5].
                                   Tripod, fixture, or technician’s
     Mounting Device
                                   hand.
                                                                           Basic Infrared Thermometer Calibration
     Distance Measuring            Can be a by ruler, tape
     Device                        measure, or fixturing.
                                                                           Procedure
     Optional Equipment
                                                                             Before calibrating an infrared thermometer, the
                                   Needed only if requested                infrared thermometer should be allowed to reach room
     Aperture                      by user or required by                  temperature. This is especially important when moving an
                                   manufacturer.
                                                                           infrared thermometer from one environment to another.
                                     •	 Cold Temperatures:                 Typically, 30 minutes is sufficient.
                                        Prevents ice or dew
                                        build-up
                                                                             The basic infrared thermometer procedure for a
     Purge Device                    •	 High Temperatures:                 calibration point should include the following steps [5]:
                                        Prevents oxidation                   1.	    If a purge device is used, set up the purge.
                                     •	 May also improve
                                        temperature gradients                2.	    Allow the thermal radiation source to stabilize at
                                                                                    its set-point.
    Table 1. Mandatory and optional calibration equipment.
    Jul • Aug • Sep 2011                                              21           Cal Lab: The International Journal of Metrology
	                                                  METROLOGY 101
      3.	   If available, set the infrared thermometer’s reflected          •	 BIPM CCT-WG5: http://www.bipm.org/wg/CCT/CCT-
            temperature setting to the reflected temperature.                   WG5/Allowed/Miscellaneous/Low_T_Uncertainty_
      4.	   Set the infrared thermometer’s emissivity to the                    Paper_Version_1.71.pdf
            emissivity of the thermal radiation source.                     •	 MSL TG22: http://www.msl.irl.cri.nz/sites/all/files/
      5.	   Set the measuring distance of the infrared                          training-manuals/tg22-july-2009v2.pdf
            thermometer.
      6.	   Align the infrared thermometer so that it is centered           References
            on the thermal radiation source.
      7.	   Perform the measurement.                                        [1] ASTM E2758 - 10 Standard Guide for Selection and Use of
      8.	   Repeat these steps for repeatability if needed.
                                                                            Wideband, Low Temperature Infrared Thermometers, ASTM,
       There are a few notes and exceptions to consider when                West Conshohocken, PA, 2010.
    performing these steps. First, most infrared thermometers
    do not have a reflected temperature setting. Instead, the               [2] F. Liebmann, “Quality Control for Emissive Surfaces,”
    reflected temperature is detected within the instrument.
                                                                            Proceedings of the National Conference of Standards
    Second, some infrared thermometers do not have an
    adjustable emissivity setting. In these cases, if the emissivity        Laboratories International, 2009.
    setting of the infrared thermometer does not match the
    emissivity of the thermal radiation source, mathematical                [3] IEC/TS 62492-1 Ed. 1.0 Industrial Process Control Devices
    corrections may be made.                                                - Radiation Thermometers - Part 1: Technical data for radiation
       When using a handheld infrared thermometer, it is
                                                                            thermometers, IEC, Geneva, 2008.
    typical to initiate a measurement by pulling a trigger. The
    trigger should be held a significant amount of time longer
    than the infrared thermometer’s specified response time.                [4] F. Liebmann, “Determining Size of Source for Hand-
    Finally, the number of set points measured should be                    held Infrared Thermometers – Theory and Practice,” Pro-
    driven by the customer. If the infrared thermometer is only             ceedings of the Measurement Science Conference, 2008.
    used over a narrow temperature range, one or two points
    may be sufficient. If the infrared thermometer is used over
    a wide range, three or more points may be necessary. This               [5] ASTM WK27665 - New Procedure for Accuracy Verifica-
    should be driven by the customer. However, the calibration              tion of Wideband Infrared Thermometers, ASTM, West Con-
    laboratory should be ready to offer advice.                             shohocken, PA, not yet published.
    Where to go for more information?                                       [6] J. Fischer, P. Saunders, M. Sadli, M. Battuello, C. W.
                                                                            Park, Z. Yuan, H. Yoon, W. Li, E. van der Ham, F. Sakuma,
    Reading
                                                                            Y. Yamada, M. Ballico, G. Machin, N. Fox, J. Hollandt, S.
    •	 Radiometric Temperature Measurements, Vol. 1:
        Fundamentals, eds. Z. Zhang, B. Tsai, G. Machin (2009,              Ugur, M. Matveyev and P. Bloembergen, “Uncertainty
        Academic Press)                                                     budgets for calibration of radiation thermometers below
    •	 Theory and Practice of Radiation Thermometry by D.P.                 the silver point”, CCT-WG5 working document CCT-
        DeWitt and Gene D. Nutter (John Wiley & Sons)                       WG508-03, Sèvres, France, May 2008.
    •	 Radiation Thermometry: Fundamentals and Application in
        the Petrochemical Industry by Peter Saunders (SPIE)
    Courses
    •	 Radiation Thermometry Short Course (NIST) – Held                     Frank Liebmann is a Senior Design Engineer for
        once a year in Gaithersburg, MD                                     Fluke Calibration.
    •	 Snell Thermography Courses – Held at various locations
        in the US and Canada
    •	 Fluke Infrared Thermometry Metrology Seminar – Held
        once a year in American Fork, UT
    Standards Organizations
    •	 ASTM: http://www.astm.org/; http://irthermometry.
        blogspot.com/
    Cal Lab: The International Journal of Metrology                    22                                           Jul • Aug • Sep 2011