Petronas Technical Standards: Radiographic Testing
Petronas Technical Standards: Radiographic Testing
Radiographic Testing
   PTS 15.30.01
   October 2014
FOREWORD
PETRONAS Technical Standards (PTS) has been developed based on the accumulated knowledge,
experience and best practices of the PETRONAS group supplementing National and International
standards where appropriate. The key objective of PTS is to ensure standard technical practice across
the PETRONAS group.
Compliance to PTS is compulsory for PETRONAS-operated facilities and Joint Ventures (JVs) where
PETRONAS has more than fifty percent (50%) shareholding and/or operational control, and includes
all phases of work activities.
Contractors/manufacturers/suppliers who use PTS are solely responsible in ensuring the quality of
work, goods and services meet the required design and engineering standards. In the case where
specific requirements are not covered in the PTS, it is the responsibility of the
Contractors/manufacturers/suppliers to propose other proven or internationally established
standards or practices of the same level of quality and integrity as reflected in the PTS.
In issuing and making the PTS available, PETRONAS is not making any warranty on the accuracy or
completeness of the information contained in PTS. The Contractors/manufacturers/suppliers shall
ensure accuracy and completeness of the PTS used for the intended design and engineering
requirement and shall inform the Owner for any conflicting requirement with other international
codes and technical standards before start of any work.
PETRONAS is the sole copyright holder of PTS. No part of this document may be reproduced, stored
in a retrieval system or transmitted in any form or by any means (electronic, mechanical, recording or
otherwise) or be disclosed by users to any company or person whomsoever, without the prior written
consent of PETRONAS.
The PTS shall be used exclusively for the authorised purpose. The users shall arrange for PTS to be
kept in safe custody and shall ensure its secrecy is maintained and provide satisfactory information to
PETRONAS that this requirement is met.
ANNOUNCEMENT
Please be informed that the entire PTS inventory is currently undergoing transformation exercise from
2013 - 2015 which includes revision to numbering system, format and content. As part of this change,
the PTS numbering system has been revised to 6-digit numbers and drawings, forms and requisition
to 7-digit numbers. All newly revised PTS will adopt this new numbering system, and where required
make reference to other PTS in its revised numbering to ensure consistency. Users are requested to
refer to PTS 00.01.01 (Index to PTS) for mapping between old and revised PTS numbers for clarity. For
further inquiries, contact PTS administrator at ptshelpdesk@petronas.com.my
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                                                              Table of Contents
1.0   INTRODUCTION ..................................................................................................... 5
      1.1      SCOPE ............................................................................................................................. 5
      1.2      GLOSSARY OF TERM ....................................................................................................... 5
      1.3      SUMMARY OF CHANGES ................................................................................................ 6
2.0   SPECIFICATION REQUIREMENTS............................................................................. 7
      2.1      PERSONNEL QUALIFICATION .......................................................................................... 7
      2.2      RADIATION SAFETY ......................................................................................................... 7
      2.3      PROCEDURE .................................................................................................................... 8
      2.4      EQUIPMENT .................................................................................................................... 8
      2.5      RADIOGRAPHIC FILMS .................................................................................................. 10
      2.6      LOCATION MARKERS .................................................................................................... 11
      2.7      SYSTEM OF IDENTIFICATION ........................................................................................ 11
      2.8      IMAGE QUALITY INDICATOR (IQI)................................................................................. 12
      2.9      DIAGNOSTIC FILM LENGTH (DFL) ................................................................................. 13
      2.10     RADIOGRAPHIC TESTING TECHNIQUES ........................................................................ 13
      2.11     QUALITY OF RADIOGRAPHS.......................................................................................... 14
      2.12     GEOMETRIC UNSHARPNESS ......................................................................................... 15
      2.13     BACK SCATTER RADIATION CHECK ............................................................................... 16
      2.14     DENSITY (TRANSMITTED H&D DENSITY) ...................................................................... 16
      2.15     SENSITIVITY................................................................................................................... 16
      2.16     FILM PROCESSING ........................................................................................................ 17
      2.17     VIEWING FACILITIES ..................................................................................................... 18
      2.18     ACCEPTANCE CRITERIA ................................................................................................. 18
      2.19     RECORDS AND REPORTS............................................................................................... 18
      2.20     PACKING OF FILM ......................................................................................................... 19
3.0   BIBLIOGRAPHY .................................................................................................... 20
4.0   APPENDIX 1: SAMPLE LOCATION MARKER ARRANGEMENT .................................. 22
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1.0 INTRODUCTION
        This PTS provides minimum requirements for Radiographic Testing of materials and fusion
        welds based on PETRONAS lessons learnt and best practices. This PTS was developed to ensure
        the safe and reliable operations of the equipment at PETRONAS assets.
1.1 SCOPE
i. Pressure vessels
1.1.2   This PTS excludes the acceptance / rejection criteria of Radiographic Testing (RT) for each
        equipment type. This shall be stated in other applicable PTSs
        Refer to PTS Requirements, General Definition of Terms, Abbreviations & Reading Guide PTS
        00.01.03 for General Definition of Terms & Abbreviations.
          No           Term                               Definition
                                                          Corporate, private or public entity which
            1          Employer                           employs personnel for wages, salary, fees or
                                                          other considerations.
                                                          Education, level of training, demonstrated skill,
                                                          training knowledge and experience required for
            2          Qualification
                                                          personnel to properly perform the duties of a
                                                          specific job.
                                                          Programme developed to impart knowledge
            3          Training
                                                          and skills necessary for qualification.
                                                          Specific requirements which define the
                                                          employer's procedure for the qualification and
            4          Written Practice
                                                          certification of non-destructive testing
                                                          personnel.
                                      Table 1: Specific Definition of Terms
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          No     Abbreviation                      Description
            1    AELB                              Atomic Energy Licensing Board, Malaysia
        All Radiographers and Assistant Radiographers shall be licensed by the Atomic Energy
        Licensing Board (AELB), Malaysia or equivalent for other countries.
2.1.1 Radiographer
              i.    The Contractor personnel shall have proven adequate training, experienced and
                    qualified Radiographic Interpreter certified by the employer to JPK Level II, or
                    CSWIP 3.4, or PCN 3.4 or equivalent certification as approved by the Owner.
              i.    The employer of the radiographers shall submit his Written Practice to the Owner
                    for review, approval and audit.
              ii.   At the Owner's sole discretion, mock-up tests shall be carried out to prove the
                    competency of the proposed radiographers and interpreters.
2.2.1 With regards to Radiation Safety, the following requirements shall be adhered to:-
              i.    Atomic Energy Licensing Act 1984 (Act 304) and its subsequent regulations for
                    work in Malaysia. For work outside Malaysia, the respective country's statutory
                    requirements shall apply.
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2.2.2   The Contractor shall submit his Radiation Safety Procedure and Emergency Plan to the Owner
        for approval prior to the commencement of work.
2.2.3   The Contractor shall hold valid licenses from AELB for the activities involving handling and
        management of radioactive sources and irradiating equipment for work in Malaysia. For work
        outside Malaysia, the respective country's statutory requirement shall apply.
2.2.4   The Contractor shall provide each radiographer with a Film Badge or TLD and an electronic
        Dosimeter and each team, comprising of a Radiographer and an Assistant Radiographer, a
        Survey Meter and a radiation alarm warning device (e.g. beeper). All battery operated
        radiation gadgets shall be of intrinsically safe type when working in hazardous areas.
2.2.5   The Survey Meter and electronic Dosimeter used in the RT work shall have valid calibration
        certificate. Calibration interval shall not exceed 12-month. Calibration shall be done by a
        laboratory certified by AELB or equivalent for other countries.
2.3 PROCEDURE
2.3.1   The Contractor shall submit to the Owner a written procedure developed specific for the job
        for approval prior to commencement of work. The radiographic techniques (as specified in the
        procedure) for the various thickness and diameter ranges shall be qualified by producing
        satisfactory standard test radiographs.
2.3.2   The procedure shall include, as a minimum the following: (refer ASME V T-221.1 a-g)
               i.   Material type and thickness range
2.4 EQUIPMENT
2.4.1   The Contractor shall provide the Radiographers with all the equipment, tools and consumable
        necessary to carry out the RT such as:-
iii. Emergency handling tools e.g. lead shot bags, tongs, lead pot and assorted tools.
v. X-ray machines
             ix.    Radiation warning signs, rope barriers, buntings, flashing warning lights, hand
                    crank claxon, etc.
xiii. Beeper
2.4.2   The Owner reserves the right to inspect these items/equipment for their suitability for the
        intended purpose and to check their safe working condition.
Hasteloy <25 mm
Inconel <30 mm
Incoloy <25 mm
Monel <25 mm
                                Titanium                     <50 mm
            Table 3: Recommended Material Thicknesses Limit to be Tested Using Ir-192
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i. X-ray Machine
                          a) The maximum voltage used in RT shall not exceed the values shown in ISO
                             5579 Figure 1 for the respective materials.
2.5.1 Type
                i.    Unless otherwise agreed by the Owner, only double coated industrial films having
                      low-speed, very fine grain, very high contrast (ASTM film type 1) or medium
                      speed, fine grain, high contrast (ASTM film type 2) suitable for use with lead
                      screens or fluorometallic intensifying screens shall be used.
               ii.    Contractor may use F6 film or equivalent or phosphorous cassette (digital film) to
                      speed up the work.
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2.5.2 Storage
All unexposed films shall be stored in a clean dry store where they will not be subjected to:
        Every box or roll of film shall be checked for fog density. If it is greater than 0.30 H & D (Hurter
        and Driffield), as measured with a densitometer calibrated against a National Bureau of
        Standards, the whole box or roll shall be rejected.
2.6.1   Location lead markers which are to appear as radiographic images on film shall be placed on
        the component and their locations shall be marked on the surface of the component being
        radiographed to provide traceability.
2.6.2 Location markers for the various techniques shall be in accordance with Appendix 1.
2.7.1   A system shall be used to produce permanent identification on the radiograph with at least
        the following information:
i. Contract
ii. Component
v. Date of radiography
2.8.1 Make
2.8.2 Type
               i.    The ASTM or ISO wire type IQI shall be used to provide a guide to the quality of
                     the radiographs produced.
ii. Other types of IQI may be used upon prior approval by the Owner.
               i.    A wire type IQI shall be placed on the source side with the smallest wire outward
                     and at the least density expected of the area of interest (diagnostic film length).
                     In addition, for weld inspection, the wires shall be placed across and
                     perpendicular to the weld axis. Where placement of IQI on the source side is
                     impracticable, it may be placed on the film side provided the following condition
                     is met:-
                          a) Set up a test piece of the same dimensions as the production weld to be
                             radiographed on which IQIs can be placed on both source and film sides.
                          b) Place a lead letter 'F' next to the film side IQI.
                          c) Take a test radiograph using the same radiographic technique that will be
                             used on the production weld.
                          d) Use the source side IQI to achieve the contractual sensitivity and, for
                             correlation with the radiographic sensitivity for production welds, record
                             the corresponding sensitivity on the film side IQI.
                          e) However, at all circumstances IQI shall be placed on the source side for
                             double wall double image technique.
2.9.1   In order to meet the density requirements and to allow for the fall-off in flaw sensitivity
        towards the ends of the radiograph due to an increase in penetrated thickness and to
        geometric effects, the Diagnostic Film Length (DFL) shall be limited to thickness not more than
        110% of the penetrated/thickness at the center of the radiograph.
2.10.1 In the procedure submitted to the Owner, the Contractor shall formulate and incorporate
       detailed radiographic techniques, including sketches that are to be used in the inspection.
       Standard test radiographs shall be produced based on the parameters of the approved
       techniques.
        In this technique, the radiation passes through only one wall of the object. An adequate
        number of exposures (multiple) shall be made to ensure that the required coverage has been
        obtained.
When it is not practical to use a Single Wall Exposure Technique, the following shall be used:-
i. Single-wall Viewing
                        a) In this technique, the radiation passes through two walls, but only the
                           material or weld near the film side is viewed. An adequate number of
                           exposures shall be made to ensure that the required coverage has been
                           obtained. For complete coverage of a circumferential weld or materials,
                           a minimum of three exposures at 120 degrees to each other shall be
                           made.
             iii.   Composite viewing of multiple films exposure in not permitted unless written
                    approval by the Owner has been obtained.
2.11.1 All radiographs shall be free from mechanical, chemical or other blemishes to ensure that they
       shall not mask or be confused with the image of any flaw in the area of interest within the
       produced radiograph. Such blemishes, include, but are not limited to:
i. Fog
iii. Scratches, finger marks, crimps, dirtiness, static marks, smudges or tears
2.12.1 Formula
2.12.2 Limitations
                                                          Cobalt 60            0.35
               Table 4: Geometric Unsharpness (Ug) Limit of Produced Radiographs
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2.13.1 As a check on back scattered radiation, a lead symbol "B" with minimum dimensions of
       12.7mm high x 1.6mm thick (½ in. high x 1/16 in. thick) shall be attached to the back of each
       film holder.
2.13.2 If a light image of "B" appears on the darker background of the radiograph, the protection
       from back scatter is insufficient and the radiograph shall be rejected. However, a dark image
       of "B" on a lighter background is not a cause for rejection.
        The transmitted H&D density at adjacent to the designated wire IQI and the whole area of
        interest shall be minimum 1.8 - 4.0 and 2.0 - 4.0 for X-ray and gamma ray sources respectively.
        The maximum density variation at anywhere of the area of interest shall be minus 15% or plus
        30% from the adjacent to the designated wire IQI.
        The transmitted H&D density shall comply with 2.14.1 above except for the requirement for
        density variation.
2.14.3 Pipeline
        The transmitted H&D density at adjacent to the designated wire IQI and the whole area of
        interest shall be 1.8 – 4.0
2.15 SENSITIVITY
2.15.1 Sensitivity is usually taken a measure of image quality and is expressed as a percentage in the
       following equation:-
        Unless otherwise agreed by the Owner, the sensitivity, using wire type IQI, shall be less than
        or equal to 2%. In sensitivity computation, the source side IQI shall be used.
a) The nominal single wall thickness adjacent to the film of the specimen.
2.15.4 For weldment radiography, the thickness used for sensitivity computation shall include the
       thickness of the weld reinforcement as permitted in the applicable code/standard/
       specification.
2.16.1 Contractor shall describe detailed film processing procedure including equipment and
       accessories used to produce quality radiograph to the Owner for approval. Contractor shall
       consult the film and processing chemicals manufacturers for detailed recommendations for
       film processing.
       Developing time varies with temperature. It is therefore imperative that the film
       manufacturer's recommended developing time and temperature shall be adhered to. The
       fixing time shall be twice the time needed to clear an unexposed film. An acid stop bath shall
       be used between the developer and fixer. Developed films shall be washed thoroughly for a
       minimum for ten minutes in running water and twenty minutes in still water.
2.16.3 Drying
       Films shall be dried in a dryer which is in good, safe condition or a drying cabinet, at
       temperature not exceeding 55ºC. When there is no urgency, films may be dried in a dry, dust
       free room. No films shall be subjected to continued exposure to a temperature higher than
       40ºC.
                i.   The automatic processor shall be able to handle the work load and speed
                     required.
             ii.     The processor shall maintain the chemical solutions at the proper temperature
                     agitate and replenish the solutions automatically and transport the films
                     mechanically at a carefully controlled speed throughout the processing cycle. It is
                     imperative that the processor, films and chemicals are compatibly matched.
                i.   Films shall be processed to ensure their integrity for at least five (5) years under
                     normal storage conditions.
ii. Films also can be transformed to digital image for the purpose of archiving.
                     Note: Films with mechanical scratch or water/chemical mark would not be able
                     to be validated on digital image.
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2.17.1 Viewing room shall provide subdued background lighting of an intensity that will not cause
       troublesome reflections, shadows or glare on the radiographs.
2.17.2 Viewers shall provide variable light intensities to view radiographs up to 4.0 H & D density.
2.17.3 All radiographs shall be viewed, interpreted and evaluated in the properly dried condition.
2.18.1 The acceptance and rejection criteria shall be in accordance with the specific contract
       specification, codes and standards.
2.18.2 The Owner shall have the final decision on the interpretation and evaluation of radiographs.
2.19.1 The Contractor shall submit records and reports in accordance with the following:-
               i.    Films and objects (e.g. welds) radiographed shall be clearly identified in a manner
                     approved by the Owner so that the radiograph and the weld to which it pertains
                     to can be immediately located.
              ii.    A summary of all objects radiographed and the results of the inspection i.e. cut-
                     out, grind and repair, etc., in accordance with the Owner's requirements, shall be
                     furnished to the Owner daily.
              iii.   The records of all objects radiographed including those of rejected welds, repairs
                     and any reshoots shall be properly catalogued and filled to permit ready retrieval
                     and identification during and after construction.
2.20.1 All sheet films shall be inserted in the paper sleeves and packed into their original boxes after
       evaluation.
2.20.2 All roll films (Rollpac) shall be rolled up properly and packed into suitable boxes after
       evaluation. On completion of the projected these boxes shall be packed into cartons suitable
       for archiving as instructed by the Owner.
2.20.3 Suitable markings shall be provided on the boxes and cartons for easy retrieval including
       proper documentation as requires by the Owner.
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3.0 BIBLIOGRAPHY
       MALAYSIA STANDARDS
                                                                                   Laws of Malaysia
       Atomic Energy Licensing Act and Regulations
                                                                                            Act 304
       AMERICAN STANDARDS
                                                                                            CP-189
       ASNT Standard for Qualification and Certification of Nondestructive
       Testing Personnel
                                                                                          ASTM E95
       Standard guide for radiographic examination
                                                                                        ASTM E1815
       Standard test method for classification of film systems for industrial
       radiography
                                                                                       ANSI/ASME V
       Non-destructive examination.
                                                                                          SNT-TC-1A
       The American Society for Nondestructive Testing (ASNT)
       Recommended Practice
       GERMAN STANDARDS
                                                                                   DIN 54109 Part 1
       Non-destructive testing; image quality of radiographs; concepts,
       image quality indicators, determination of image quality value.
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BRITISH STANDARDS
                                                                      BS EN 1435
Non-destructive of welds
ISO STANDARDS