REQUISITION FORM FOR XPS MEASUREMENTS
Materials Research Centre, MNIT, Jaipur
No.: Date of submission:
IMPORTANT
NOTES:
i. Samples in the form of powder or gel or those which can degas in ultra-high vacuum will strictly not be
allowed. Sample(s) should not contain radioactive isotopes.
ii. There will be a vacuum check of samples prior to loading inside the XPS chamber. The sample(s) must be
handed over to the lab the previous evening for vacuum check.
iii. The sample composition and how it is prepared must positively be mentioned in section 2.
iv. A peer‐reviewed reference mentioning XPS result(s) on similar sample(s) must also be provided for
guidance.
1. User’s Profile
Name of the User: ______________________________________ Tel. / Mob. No.: _____________
Roll No. / EC: _____________________ Department / Centre: ____________________________
Name of the Institute / College / Industry _________________________________________________________
2. Sample Details
Composition/Formula: _____________________ No. of Sample ____
Form (please tick): Solid (bulk) Pellet Thin Film
Method of Preparation (in brief):
Reference (hard copy attached): Journal _______________________ Volume ______ Page ________
Any other detail: ______________________________________________________________________________
3. Desired Options (please tick)
a. Surface cleaning by sputtering: Yes No
b. Mode: Surface
Survey(XPS) Depth Profile Maximum depth = _____ nm
AES UPS Charge Neutralizer
c.
Element‐specific Scan: Yes Elements: __________________________________ No
d.Any specific feature expected? Please write.
Amount to be paid:
Mode MNIT Users Other Academic Industry
XPS (Surface Survey)
360/ Sample + Charge 720/ Sample + Charge 1800/ Sample + Charge
Neutralizer 200/ Sample Neutralizer 400/ Sample Neutralizer 800/ Sample
Depth Profile 720/ Sample 1440/ Sample 3600/ Sample
Auger Spectroscopy 300/ Sample 600/ Sample 1500/ Sample
UPS 900/ Sample 1800/ Sample 4500/ Sample
Surface Survey (+ 4 Elements HR scan included)Rs 100 will be charged for each extra element HR
scan
Signature of the user ___________________ E‐mail: ____________________________________
Name & Signature of the Supervisor (for Students/RS/Project Staff) ________________________________
Declaration by the user
1. The results recorded, if communicated for publication, will must acknowledge “Materials Research Centre"
Malaviya National Institute of Technology, Jaipur.
Signature of the user
To be filled up at the XPS Laboratory
Please allot time and complete the work.
In‐Charge XPS Laboratory
Name of the Operator: ______________________________________________
Vacuum check status: ______________________________________________
Date of Measurement: ______________________________________________
Signature of the Operator
N.B.: 1.Users are advised to submit a hard copy of the form with the reference in the XPS lab.
2. Please collect the sample and data (bring a CD) on the next working day after the measurement. The data and the
samples cannot be retained in the lab after that.
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The user will be informed about the date and time of experiment via e‐mail. He/she is expected to be present in
the lab during the measurement.
Details of payment: Demand Draft Payable in favor of ‘Registrar, MNIT Jaipur’.
* Charge Neutralization : For Non -Conducting Sample
Any Other information if necessary:
Faculty Incharge Head