Granular Materials Modulus Correlation
Granular Materials Modulus Correlation
h i g h l i g h t s
 A new regression model for the estimation of resilient modulus value for granular materials.
 Potentials use of reclaimed asphalt pavement.
 Statistical analysis for the strength and significance of the correlation.
a r t i c l e i n f o a b s t r a c t
Article history:                                       The resilient modulus (MR) value of unbound aggregates has been widely accepted as the principal
Received 2 July 2017                                   mechanical property required in the mechanistic-empirical design/analysis of pavement structures.
Received in revised form 15 September                  Resilient modulus measured through repeated triaxial load test is highly desirable to characterise gran-
2017
                                                       ular materials. However, because of the complexities encountered with this test, other laboratory tests
Accepted 8 October 2017
                                                       would be desirable if a reliable correlation could be established.
                                                         Reclaimed asphalt pavement (RAP) and recycled concrete aggregate (RCA) have potential to be used as
                                                       base and subbase material in substantial percentage to achieve economy and to minimise the undesirable
Keywords:
Pavement structure
                                                       environmental effects linked to the use of virgin aggregates. This paper presents a correlation developed
Recycled material                                      between MR value and constrained modulus (MC) value on the basis of experimental results obtained for
Material properties                                    32 reconstituted granular samples containing virgin aggregates, RAP and RCA materials. Proposed model
Empirical correlation                                  considers the effect of stress state through the experimentally determined MC value while model param-
Laboratory experimentation                             eters are correlated to the percentage of RAP materials in the reconstituted blends. Statistical analysis of
                                                       the suggested correlation by t-test demonstrates encouraging results in terms of its strength and
                                                       significance.
                                                                                                                         Ó 2017 Elsevier Ltd. All rights reserved.
https://doi.org/10.1016/j.conbuildmat.2017.10.047
0950-0618/Ó 2017 Elsevier Ltd. All rights reserved.
                                                    M. Arshad / Construction and Building Materials 159 (2018) 440–450                                     441
Correlations obtained through this approach are of varying com-                       blend (0, 50, and 75% RAP) were stored in wrapped plastic bags
plexity and acceptability [54,65–67].                                                 until they were required for different types of testing in the
                                                                                      laboratory.
3.3. Resilient modulus constitutive models                                               It should be noted that procedures for classification of RAP
                                                                                      materials are quite varied across the world. The only characteriza-
   In this approach, MR values for a particular soil is obtained by                   tion that is common to the various standards and procedures is the
taking into account the various types of stress invariant, for exam-                  particle size distribution curves (gradation curves). However
ple bulk stress [53]; bulk stress and atmospheric pressure [68];                      Tebaldi et al., [76,77] have proposed that a detailed description
bulk stress, atmospheric pressure and deviator stress [69]; confin-                   would require a series of testing including but not limited to:
ing pressure and deviator stress [70]; atmospheric pressure, octa-                    determination of particle sizes (as RAP and of recovered aggre-
hedral normal stress and octahedral shear stress [56]; bulk                           gates); determination of active binder content in RAP; shape
stress, atmospheric pressure and octahedral shear stress [71]. MR                     description of recovered aggregates; cleanliness of RAP and
values obtained through this approach are more reliable when                          homogeneity.
compared with those obtained through the first two approaches
however, this approach requires extensive efforts with higher eco-                    4.1. Grain size distribution characteristics
nomic cost.
                                                                                         The grain size distribution characteristics were obtained
3.4. Resilient modulus based on constitutive equation                                 according to AASHTO Designation T27-99 [78] for all materials/
                                                                                      blends. Fig. 1 shows the gradation curves for the virgin aggregates,
    Most of the State Highway Agencies around the world and par-                      RCA and RAP materials. Each curve corresponds to the average of
ticularly in the USA do not routinely measure MR value in the lab-                    two independent tests. Based on the gradation curves, virgin aggre-
oratory but estimate the design MR either from experience or other                    gate A is finer than other virgin aggregate materials (F & W) while
material properties. The potential benefit of estimating MR value                     the virgin W is the most coarser among them. Similarly, RAP(3) is
from soil physical properties is that the seasonal variations in the                  coarser when compared with other RAP materials and RAP(4)
MR value can be determined from seasonal changes in the mate-                         being the most finer among them. RCA was derived from plain con-
rial’s properties; however, the effect of stress sensitivity is not cap-              crete aggregate designed for 25 MPa compressive strength after 28
tured. In order to capture the effects of stress sensitivity and                      days having limestone as crushed aggregate, ordinary Portland
physical properties on design MR, Von Quintos and Killingsworth                       cement and coarse sand.
[72], Dai and Zollars [73], Santha [74] and Mohammad et al. [75],
among others, have developed prediction equations for MR value                        4.2. Physical properties of recovered bitumen binder
by regressing the coefficients of selected constitutive equations
relating them to soil physical properties.                                               The RAP samples were washed with tap water to eradicate for-
                                                                                      eign materials, and the samples were put in the oven at a temper-
4. Material characterization                                                          ature of 140 °C to lose the aggregate from the binder agent.
                                                                                      Recycled binder contents for different RAP types were extracted
    For this research work index properties tests, shear strength                     from the RAP samples by solvent extraction method using a rota-
tests, resilient modulus tests, one-dimensional constrained modu-                     tional viscometer apparatus. The recovered bitumen contents
lus tests (1D) were conducted to evaluate the influence of RAP con-                   ranging from 4.3 to 3.3% were characterised in terms of penetra-
tent on the resilient properties of the various blends prepared by                    tion (ASTM D5-06), viscosity (ASTM D4402-06) and softening
mixing RAP contents (designated as ‘RAP(1)’, ’RAP(2)’, ‘RAP(3)’ &                     points (ASTM D36-06).
‘RAP(4)’) with virgin aggregates (granular) samples (designated
as ’A’, ‘F’ & ‘W’) and RCA material. Each of the virgin aggregate sam-                4.3. Compaction characteristics
ples, as well as RAP materials, were containing crushed limestone
of angular to sub-angular particles in terms of shape while flat and                     Results of the Modified Proctor Compaction tests (AASHTO
elongated particles in the samples/materials were limited to 6% as                    T180) [79] were used to get the compaction characteristics of all
per ASTM D 4791. Table 2 shows the matrix of the testing program                      the tested materials. The optimum moisture contents (wopt) of
designed for resilient modulus test and constrained modulus test.
    Virgin aggregates (A, F and W), RAC and RAP samples were                                                           100
transported to the laboratory, air-dried at ambient laboratory tem-
perature (typically 23 ± 2 °C), then carefully mixed before being                                                       90
divided into equal parts by using a standard rifle box. After propor-
                                                                                        Material passing by mass (%)
                                                                                                                        80
tioning and blending the materials, suitable quantities of each                                                         70
                                                                                                                        60
Table 2
                                                                                                                        50
Matrix of testing program.
                                                                                                                        40
  Virgin aggregate/RCA       RAP      Minimum number       Minimum number                                                                                    virgin (A)
                                      of resilient         of constrained                                               30                                   virgin (F)
                                                                                                                                                             virgin (W)
                                      modulus tests        modulus tests                                                                                     RCA
                                                                                                                        20                                   RAP(1)
  Virgin aggregate A, F, W   –        3                    3                                                                                                 RAP(4)
  RCA                        –        1                    1                                                            10                                   RAP(2)
                                                                                                                                                             RAP(3)
  Virgin aggregate A, F, W   4  2*   3  2  4 = 24       3  2  4 = 24
                                                                                                                         0
  RCA                        4  2*   24=8                24=8                                                         0.01   0.1         1         10                  100
  Total                               36                   36                                                                         Diameter (mm)
  *
    Blended samples were prepared by mixing 50% and 75% (by weight) of each RAP
type with the virgin aggregates and RCA.                                              Fig. 1. Particle size distribution curves for virgin aggregates (A, F, W), RCA and RAP
                                                                                      materials.
                                                      M. Arshad / Construction and Building Materials 159 (2018) 440–450                                               443
Fig. 2. Typical shape of applied repeated load cycles and the generated accumulative strain curve.
                                                                                         that includes a 0.1s load duration and a 0.9 s rest period. The
Table 3
Compaction characteristics of the tested materials.                                      repeated axial load is applied on top of a cylindrical specimen
                                                                                         under specified confining pressure. The total recoverable axial
  Material                    Maximum dry                     Optimum moisture
                                                                                         deformation response of the specimen is measured and used to cal-
                              density                         content
                                                                                         culate the resilient modulus. AASHTO T 307 [83] involves the use of
                              kN/m3                           (%)
                                                                                         a load cell and deformation devices mounted outside the triaxial
  virgin (A)                  21.9                            7.1
  virgin (F)                  22.5                            5.7                        chamber. Air is used as the confining fluid, and the specimen size
  virgin (W)                  23.3                            5.5                        is required to have a minimum diameter to length ratio of 1:2.
  RCA                         20.7                            7.5                        For the current study a closed-loop, servo-controlled electro-
  RAP(1)                      21.4                            6.9                        hydraulic MTS testing machine was used in conjunction with a
  RAP(2)                      20.6                            6.4
  RAP(3)                      20.9                            6.5
                                                                                         function generator that is capable of applying repeated cycles of
  RAP(4)                      19.7                            9.1                        haversine-shapes load pulse following a load history supplied by
                                                                                         the microcomputer control software. A typical variation of applied
granular and RCA were found in the range of 5.5% and 7.5%. The
maximum dry unit weight varied from 20.7 to 23.3 kN/m3, with
granular W having the highest maximum dry unit weight and
RCA the lowest. The values of wopt for the RAP were in the range
of 6.4–9.1% while the maximum dry unit weight remained
between 19.7 and 21.4 kN/m3 as shown in Table 3. Even though
the proctor compaction tests for blends of virgin aggregates with
RAP were not performed, it was assumed that the wopt values of
the blends with different RAP contents would be in the range of
5.5–7.5%.
   Resilient modulus tests were performed as per AASHTO T 307                            Fig. 3. Apparatus for the constrained modulus test. Key: 1, loading frame; 2, load
[83] which requires a haversine-shaped loading waveform. The                             measuring gauge; 3, deflection gauge; 4, mould containing test specimen; 5,
load cycle duration, when using a hydraulic loading device, is 1 s                       hydraulic pump.
444                                                                         M. Arshad / Construction and Building Materials 159 (2018) 440–450
load impulse and the accumulated strain with the passage of time                                               distinct levels of axial stress (ra) at which unloading of the sample
is shown in Fig. 2.                                                                                            was performed. The maximum vertical pressure in the condition-
    AASHTO T 307 protocol completes the MR testing with 15 load-                                               ing stage is selected as 205 kPa, which is, in fact, equal to the axial
ing series consisting of different combinations of confining stress,                                           stress in the conditioning stage of the resilient modulus testing.
cyclic axial stress and contact stress. For the first series, the maxi-                                        Ten number of cycles of loading-unloading were applied to the
mum axial stress was set at 3 psi (21.0 kPa) and the confining pres-                                           specimen by the manual control hydraulic piston at the average
sure was 3 psi (21.0 kPa). One hundred repetitions of load cycles                                              loading rate in the range of 100–150 kPa/min before the data
were applied during each series of the loading. The readings of                                                ofloading and settlement were recorded. Fig. 4 shows the typical
each LVDT and the load cell for the last five cycles of each loading                                           loading-unloading cycles corresponding to four different levels of
sequence were considered to calculate the corresponding resilient                                              axial stress. The slope of the average trend line drawn for each loop
moduli. Under a unique stress condition, 100 cycles of loads were                                              gives a calculated value of the constrained modulus at the particu-
applied while conditioning stage was completed with 750 number                                                 lar stress level [84].
of load cycles. Further details about the sample preparation, sam-
ple installation, loading sequence and data acquisition system                                                 5. Development of correlation between MR and MC
can be found in the related AASHTO guide and same has been doc-
umented by Arshad and Ahmed [84].
                                                                                                               5.1. General form of correlation
4.6. Constrained modulus test
                                                                                                                  To develop a correlation between MR and Mc values the test
4.6.1. General description                                                                                     results of 36 samples were analysed. For each sample, four values
   A series of one-dimensional (1D) constrained compression/-                                                  of the constrained modulus Mc were calculated at four selected
modulus tests were carried out using a 30 cm diameter and 30                                                   levels of axial stress. For all these samples the angle of internal fric-
cm high mould. This mould can accumulate materials with a max-                                                 tion ð/Þ was assumed to be 40° to estimate the coefficient of earth
imum particle size of approximately 40–50 mm. The constrained                                                  pressure at rest (Ko) using Jacky’s equation:
modulus, which reflects the compressibility and hence the stiffness
                                                                                                               K 0 ¼ 1  sinð/Þ                                                                                                             ð1Þ
of a material can be obtained from these tests.
                                                                                                                  The bulk stress (rbulk = h = r1 + r2 + r3) in the 1D compression
4.6.2. Loading system and data acquisition                                                                     test can be determined at the selected axial stress (ra) levels, with
    Fig. 3 shows the test setup of 1D cyclic compression test for the                                          the results being summarised in Table 5.
constrained modulus. The deformation of the sample is measured                                                    Fig. 5 shows the variation of resilient modulus and constrained
using three dial gages fixed at 120 relative to each other. Appar-                                             modulus value with bulk stress. From this figure, it can be inter-
ently, such an arrangement of the dial gauges provides ‘‘best” esti-                                           preted that both of the resilient modulus and constrained modulus
mate for the average deformation even when the loading plate has                                               values increase with the increase in bulk stress level (h) and the
a slight tilt. A load cell is used to measure the load that is controlled                                      percentage of RAP material in the blends. In addition to that MR
manually using a hydraulic pump.
    During the 1D compression test, the sample was unloaded at
                                                                                                                                                                  Table 5
different stress levels to obtain the unloading characteristics and                                                                                               Estimation of bulk stress corresponding to the axial stress
the constrained modulus of the material. Table 4 shows the four                                                                                                   during constrained modulus test.
                                                                                                                                                        450
                                                                                                                                                                                                        y = 9.7243x0.5713
                                                                                                                                                                     Virgin (W)
                                                                                                                  Resilient/constrained modulus (MPa)
                                                                                                                                                        400                                               R² = 0.9625
                       450                                                                                                                                           25%virgin(W)+75%RAP(1)
                                                                                                                                                        350
                       400                                                                                                                                           50%virgin(W)+50%RAP(1)                             y = 10.097x0.5498
                                                                                                                                                        300                                                               R² = 0.9773
                       350
                       300                                                                                                                              250
  Axial stress (kPa)
                                                                                                                                                                                                  y = 5.1683x0.6369
                       250                                                                                                                              200
                                                                                                                                                                                                    R² = 0.9923
                       200                                                                                                                              150
                                                                                                                                                                   MR
                                                                                                                                                                                                                                 Mc
                       150                                                                                                                              100        vs θ
                                                                                                                                                                                                                                 vs θ
                                                                                           Cycle 1
                       100                                                                 Cycle 2                                                       50
                       50                                                                  Cycle 3
                                                                                           Cycle 4                                                        0
                        0                                                                                                                                     0           100     200   300      400      500         600      700      800
                             0           0.002          0.004         0.006           0.008          0.01                                                                                  Bulk stress (Kpa)
                                                             Strain (%)
                                                                                                               Fig. 5. Variation of resilient modulus and constrained modulus value with bulk
 Fig. 4. Typical stress-strain loop for the estimation of the constrained modulus.                             stress.
                                                      M. Arshad / Construction and Building Materials 159 (2018) 440–450                                                 445
             300                                                                              between these two quantities, although the data points are very
                                                                                              scattered. As the first order approximation, MR can be estimated
                                                                                              as approximately 2–4 times of the value of Mc. In addition, it can
             200
                                                              R² = 0.1624                     be concluded that both MR and Mc value depend on not only the
                                                                                              stress state but also on the nature of the virgin aggregates and
             100
                                                                                              the RAP/RCA.
                                                                                                  One of the most widely utilised relationships for the estimation
               0                                                                              of resilient modulus value for an unbound granular material is the
                   0   100       200       300          400         500        600
                                        MR (MPa)                                              one proposed by Hicks and Monismith [18] as follows:
Table 6
Evaluation of regression model parameters (a, b) used in Eq. (3).
Table 6 (continued)
Table 6 (continued)
    The values of regression constants, a and b depend on the mate-                      ficient of correlation remained in the range of 0.95 to 0.99, which
rial properties and laboratory test procedure such as AASHTO                             in return reveals that 95–99% values of the dependent variable
T-307 [83]. Seed et al. [85] have also suggested a similar K–h model                     (MR) are dependent on the employed independent variable
(relation) for the estimation of resilient modulus in terms of bulk                      (Mc for the current study) [86]. Fig. 7 compares the measured MR
stress.                                                                                  values (experimentally) to those calculated (estimated) on the
    For the study under consideration, a functional relationship                         basis of Eq. (3), using the specific regression model parameters
between MR and Mc values of the selected materials/blends was                            for each sample tested. From this figure, it can be observed that
demonstrated through the power relation as shown in Eq. (3):                             all the data points remain in a narrow band about the line of unity
                                                                                         with an approximate variation of ±25 MPa.
M Rðcorrelated:Þ ¼ aðM c Þb                                                  ð3Þ
where a and b are the model parameters.                                                  5.2. Generalised values of the model parameters (a,b) for the
   Table 6 summarises the values of these model parameters                               estimation of MR values
obtained using the computer software package ‘‘SOLVER” for each
sample tested in this study. Four distinct levels of bulk stresses, as                       Virgin aggregates and the RAP materials cover a wide range of
given in Table 6, were used in the above regression analysis. The                        gradation characteristics as shown in Figure 1 and moreover, there
coefficient of determination (R2), that is in fact square of the coef-                   is no unique way to characterise these materials, so it is difficult to
                                                                                         attach a single value of regression coefficients for all the tested
                                                                                         samples (virgin aggregates and blended materials). A careful anal-
                                                                                         ysis of the experimental data reveals that tested samples can be
                                                                                         categorised by the percentage of RAP content such that:
                                                                                             Fig. 8 shows the performance of the Eq. (3) when three separate
                                                                                         sets of regression constants (each one for a particular category) are
                                                                                         used which have been developed using a computer software tool
                                                                                         ‘SOLVER’. Furthermore, the regression constant ‘a’ has been gener-
                                                                                         alised in term of percentage of RAP content as shown in Table 7
                                                                                         such that, ‘a’ can be treated as dependent variables while the per-
        Fig. 7. Comparison between measured and estimated values of MR.                  centage of RAP content can pretend as an independent variable.
448                                                                              M. Arshad / Construction and Building Materials 159 (2018) 440–450
                                                                                                                                 Pn
                                                                                                                                                                      
                                     600                                                                                              i¼1 ðui  ui Þðt i  t i Þ
                                                                                             R² = 0.593                    R ¼ qffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi
                                                                                                                                                                                 ffi                  ð4Þ
                                                                                                                                Pn
                                                                                                                                          ½ðu   i     u i Þ2
                                                                                                                                                               ðt  i     ti Þ2 
                                     500                                                                                             i¼1
              MR(estimated) (MPa)
                                     400
                                                                                                                           where ui and t i are the experimental and predicted/estimated val-
                                                                                                                           ues; respectively; u  i or t i is the average of the respective values
                                     300
                                                                                                                           and n is the size of sample.
                                     200
                                                                                                                               The numerical value of R may range from 1 to +1, whereas
                                                                                                                           positive value represents an uphill correlation and negative value
                                     100
                                                                                                                           corresponds to a downhill correlation. Additionally, the strength
                                                                                                              (a)          of the linear relationship can be categorised as very strong, moder-
                                          0
                                                                                                                           ately strong and fair for R values in the range 0.8–1.0, 0.6–0.8 and
                                              0    100      200          300           400             500           600   0.3–0.5, respectively [86]. However, if R = 0.0, doesn’t mean that
                                                                  MR(measured) (MPa)                                       the two variables are unrelated. Hence it is often mandatory to per-
                                                                                                                           form a statistical test of significance to talk about the strength of a
                                    500                                                                                    relationship indicated by the correlation coefficient [88]. For this
                                                                                           R² = 0.5912                     study, three different types of statistical tests were performed to
                                                                                                                           evaluate the significance of the developed correlation presented
                                    400
                                                                                                                           in Eq. (3) and Table 7.
       MR(estimated) (MPa)
                               400
                                                                                                                           Whereas, the standardised t statistic on the basis of R can be written
                               300                                                                                         as:
                                                                                                                                    sffiffiffiffiffiffiffiffiffiffiffiffiffiffi
                               200                                                                                                    N2
                                                                                                                           t¼R                                                                      ð5Þ
                                                                                                                                        1  R2
                               100
                                                                                                              (c)
                                                                                                                           where N is the number of paired observations in the given
                                     0
                                          0       100      200         300           400           500              600    population.
                                                                                                                              The null hypothesis is evaluated by comparing t statistic of Eq. (5)
                                                              MR(measured) (MPa)
                                                                                                                           with t-critical obtained from t distribution having N  2 degree of
Fig. 8. Comparison between measured and correlated values of MR for: (a) blended                                           freedom.
samples containing 75% RAP; (b) blended samples containing 50% RAP and (c)
samples containing virgin aggregates/RCA.                                                                                       Case 2: Direct comparison of R-value with R-critical value at a
                                                                                                                                particular degree of freedom and level of significance [90].
5.3. Statistical analysis of the proposed model                                                                                 Case 3: To perform a standard t-test for paired samples at a par-
                                                                                                                                ticular degree of freedom and level of significance [90,91].
   To evaluate the performance of the proposed models, Pearson
correlation coefficient ‘R’ as given by Eq. (4), which is a measure                                                           Table 8 summarise the statistical analysis of the above three
of the strength of the relationship between or among variables is                                                          cases for the three categories of tested samples (group) investi-
used [1,84,87].                                                                                                            gated in this study.
Table 7
Generalised model parameters on the basis of percentage of RAP content.
Table 8
Summary of the statistical analysis for the validation of proposed model for the estimation MR value.
6. Conclusions and recommendations                                                         Author also acknowledges the valuable comments and suggestions
                                                                                           of the reviewers for the improvement of this article.
    The RAP/RCA materials have substantial potential to be used in
unbound granular base/subbase layers of the pavements. Most of                             References
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