2
Grain Size Distribution: The Sieve Analysis
Introduction
        In order to classify a soil for engineering purposes, one needs to know the
distribution of the size of grains in a given soil mass. Sieve analysis is a method used to
determine the grain size distribution of soils and in the classification of sands and gravels.
Sieves are made of woven wires with square openings. Note that as the sieve number
increases, the size of the openings decreases. Table 2.1 gives a list of the U.S. standard
sieve numbers with their corresponding size of openings. For all practical purposes, the
No. 200 sieve is the sieve with the smallest opening that should be used for the test. The
sieves that are most commonly used for soil tests have a diameter of 8 in. (203 mm). A
stack of sieves is shown in Fig. 2.1.
        The method of sieve analysis described here is applicable for soils that are mostly
granular with some or no fines. Sieve analysis does not provide information as to shape
of particles.
                                Table 2.1 U.S. Sieve Sizes
                             Sieve     Opening        Sieve           Opening
                              No.        (mm)          No.             (mm)
                               4            4.75           35           0.500
                               5            4.00           40           0.425
                               6            3.35           45           0.355
                               7            2.80           50           0.300
                               8            2.36           60           0.250
                              10            2.00           70           0.212
                              12            1.70           80           0.180
                              14            1.40          100           0.150
                              16            1.18          120           0.125
                              18            1.00          140           0.106
                              20            0.85          200           0.075
                              25            0.71          270           0.053
                              30            0.60          400           0.038
                                      Grain Size Distribution: The Sieve Analysis        2
    Fig 2.1 A stack of sieves with a pan at the bottom and a cover on the top.
Equipment
  1. Sieves, a bottom pan, and a cover
      Sieve numbers 4, 10, 20, 40, 60, 140, and 200 are generally used for most
      standard sieve analysis work.
  2. A scale sensitive up to 0.1 g.
  3. Mortar and rubber-tipped pestle.
  4. Oven.
  5. Mechanical sieve shaker.
Procedure
  1. Collect a representative oven dry sample. Samples having largest particles of the
     size of No.4 sieve openings (4.75 mm) should be about 500 grams. For soils
     having largest particles of size greater than 4.75 mm, larger weights are needed
     (Fig. 2.2)
                                  Grain Size Distribution: The Sieve Analysis              3
                                 Fig. 2.2 Soil Sample.
2. Break the soil sample into individual particles using a mortar and a rubber-tipped
   pestle. (The idea is to break up the soil into individual particles, not to break the
   particles themselves.)
3. Determine the mass of the sample accurately to 0.1 g (W).
4. Prepare a stack of sieves. A sieve with larger openings is placed above a sieve with
   smaller openings. The sieve at the bottom should be No. 200. A bottom pan should
   be placed under sieve No. 200. As mentioned before, the sieves that are generally
   used in a stack are Nos. 4, 10, 20, 40, 60, 140, and 200; however, more sieves can
   be placed in between.
5. Pour the soil prepared in Step 2 into the stack of sieves from the top.
6. Place the cover on the top of the stack of sieves.
7. Run the stack of sieves through a sieve shaker (Fig. 2.3) for about 10 to 15
   minutes.
                Fig. 2.3 The sieve shaker with a stack of sieves.
                                 Grain Size Distribution: The Sieve Analysis              4
8. Stop the sieve shaker and remove the stack of sieves. (Fig. 2.4)
                   Fig. 2.4 Sieves separated and bottom pan.
9. Weigh the amount of soil retained on each sieve and the bottom pan.
10. If a considerable amount of soil with silty and clayey fractions is retained on the
   No. 200 sieve, it has to be washed. Washing is done by taking the No.200 sieve
   with the soil retained on it and pouring water through the sieve from a tap in the
   laboratory (Fig. 2.5).
                Fig. 2.5 Washing the soil retained on No. 200 sieve.
   When the water passing through the sieve is clean, stop the flow of water. Transfer
   the soil retained on the sieve at the end of washing to a porcelain-evaporating dish
   by back washing. Put it in the oven to dry to a constant weight. (This step is not
   necessary if the amount of soil retained on the No. 200 sieve is small.). Determine
                                                                         Grain Size Distribution: The Sieve Analysis                        5
                          the mass of the dry soil retained on the No. 200 sieve. The difference between this
                          mass and that retained on the No. 200 sieve determined in step 9 is the mass of soil
                          that has washed through.
             Sample Data
             Description of Soil: Sand with some fines
             Weight of oven dry sample, W = 502 grams
             Table 2.1
                                                                  Wt. of Sieve                         % mass of soil   Cumulative
          Sieve                         Sieve         Wt. of                       Mass of soil                                          % Finer,
 Sieve                                                                with                              retained on     % retained
         Opening                       Opening        Sieve                        retained on
Number                                                            aggregate                                                              100- ΣRn
           (in)                         (mm)           (g)                        each sieve (g)       each sieve, Rn      ΣRn
                                                                       (g)
   4      0.187                             4.750     757.2          782.8            25.6                  5.1             5.1            94.9
  16      0.047                             1.191     602.9          711.3            108.4                21.6            26.7            73.3
  30      0.024                             0.599     584.0          685.1            101.1                20.1            46.8            53.2
  60      0.010                             0.249     300.4          376.0            75.6                 15.1            61.9            38.1
 140      0.004                             0.106     318.4          458.0            139.6                27.8            89.7            10.3
 200      0.003                             0.075     339.4          364.3            24.9                  5.0            94.7             5.3
 Pan      N.A.                               N.A.     373.5          400.2            26.7                  5.3           100.0             0.0
                                                                                  = 501.9 = W 1          = 100.0
             Mass loss during Sieve analysis = 0.02 %
                                                                        Percent Finer vs. Grain Size
                                      100
                                      90
                                      80
                                      70
                  Percent Finer (%)
                                      60
                                      50
                                      40
                                      30
                                      20
                                      10
                                       0
                                            10                             1                             0.1                      0.01
                                                                                  Grain Size, D (mm)
                                                 Fig. 2.6 Plot of Percent Finer vs. grain size from the table 2.1
          D10 = 0.104                                          Cu = D60/D10 = ( 0.75)/(0.104) = 7.2
          D30 = 0.19                                           Cc = (D30)2/(D60xD10) = (0.19)2/(0.75*0.104) = 0.46
          D60 = 0.75
                                         Grain Size Distribution: The Sieve Analysis               6
    Calculations
   1. Mass of soil retained on each sieve (g) = Wt. of Sieve w/ aggregate – Wt. of Sieve (g)
   2. Percent mass of soil retained on each sieve, Rn (%) =
               = [Mass of soil retained/ Wt. of oven dry sample] x 100 (%)
                                                                           i=n
   3. Cumulative percent of soil retained on the nth sieve, Rn (%) =      Σ R(nth) (%)
                                                                           i=1
   4. Cumulative percent of soil passing through the nth sieve (% finer), 100 -Rn =
                                          i=n
               = percent finer = 100 -   Σ R(nth) (%)
                                          i=1
   5. Mass loss of soil during sieve analysis (g) =
               = [(Wt. of sample - mass of soil retained) / Wt. of sample] x 100
               = (W – W1) / (W) x 100 (%) (O.K. if less than 2%)
Note: If soil retained on No. 200 sieve is washed, the dry unit weight determined after
washing (step 10) should be used to calculate percent finer (than No. 200 sieve). The
weight lost due to washing should be added to the weight of the soil retained on the pan.
   6. The grain-size distribution obtained from the sieve analysis is plotted in a semi-
       logarithmic graph paper with grain size plotted on the log scale and percent finer
       plotted on the natural scale. Figure 2.6 is a grain-size distribution plot for the data
       and calculations shown in Table 2.1. The grain-size distribution plot helps to
       estimate the percent finer than a given sieve size which might not have been used
       during the test.
       From the grain-size distribution curve, grain sizes such as D10, D85, D60, etc. can b
obtained. The D refers to the grain size, or apparent diameter, of the soil particles and the
subscript (10, 85, 60) denotes the percent that is smaller. For example, D10 = 0.104 mm
from the distribution curve means that 10 percent of the sample grains are smaller than
0.104 mm. The diameter, D10, is also referred to as effective size. The effective size is
used for several empirical correlations, such as coefficient permeability. The coefficient of
gradation, Cc, is a parameter which indicates the range of distribution of grain sizes in a
given soil specimen. If Cc is relatively large, it indicates a well-graded soil. If Cc is nearly
                                       Grain Size Distribution: The Sieve Analysis              7
equal to one, it means that the soil grains are of approximately equal size, and the soil may
be referred to as a poorly graded soil.
The following formula is used to calculate Cc:
   7. Cu = (D60 / D10)
   8. Cc = (D30)2 / (D60xD10)
   The parameter Cc is also referred to as the coefficient of curvature. For sand, if Cu is
greater than 6 and Cc is between 1 and 3, it is considered well graded. However, for a
gravel to be well-graded, Cu should be greater than 4 and Cc must be between 1 and 3.
The D15 and D85 sizes are used for design of filters. The D50 size is used for correlation of
the liquefaction potential of saturated granular soil during earthquakes.
Conclusions
       The conclusion should answer the following questions:
1. Of what significance is the sieve analysis to a geotechnical engineer?
2. How much soil mass was lost in the analysis? What are some possible sources for error?
3. What do D10, D85, D60 signify?
4. What do the coefficient of uniformity, Cu, and the coefficient of concavity, Cc indicate
  about the test soil?
                                            Grain Size Distribution: The Sieve Analysis                 8
                                            Data Sheet
                      Grain Size Distribution: The Sieve Analysis
          Group: ___________          Date: ______________           Location: _____________
          Soil Description: _______________________________________________________
                                                      Mass of soil
          Sieve     Sieve    Wt. of    Wt. of Sieve                     % of mass       Cumulative   % Finer,
 Sieve                                                retained on
         Opening   Opening   Sieve         with                      retained on each   % retained     100-
Number                                                each sieve
           (in)     (mm)      (g)     aggregate (g)                    sieve, R(nth)      ΣRnth       ΣRnth
                                                           (g)
   4
  16
  30
  60
 140
 200
 Pan
                                                       =           =
          Notes: