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14 Agitator

The document discusses agitation and mixing of liquids. It defines agitation as an induced circulatory motion within a container, while mixing involves random distribution of phases into one another. Good mixing achieves uniformity with minimum power and cost. Factors like vessel type, agitator design, and fluid properties affect mixing. Common agitator types include paddles, propellers, turbines, and helical designs. Dimensionless numbers like Reynolds and Froude are used to calculate power requirements based on fluid properties and agitator speed. Baffles control fluid flow patterns. Mechanical seals prevent leaks at the agitator shaft.

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Harshil Parmar
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0% found this document useful (0 votes)
609 views51 pages

14 Agitator

The document discusses agitation and mixing of liquids. It defines agitation as an induced circulatory motion within a container, while mixing involves random distribution of phases into one another. Good mixing achieves uniformity with minimum power and cost. Factors like vessel type, agitator design, and fluid properties affect mixing. Common agitator types include paddles, propellers, turbines, and helical designs. Dimensionless numbers like Reynolds and Froude are used to calculate power requirements based on fluid properties and agitator speed. Baffles control fluid flow patterns. Mechanical seals prevent leaks at the agitator shaft.

Uploaded by

Harshil Parmar
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as PDF, TXT or read online on Scribd
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Agitator

Mihir P.Shah
DDU
22-Sep-18 MPS,DDU 1
AGITATION & MIXING OF LIQUIDS

“Many processing operations depend for their success on the effective


agitation & mixing of fluids” ……McCabe

Agitation
 It is an induced motion of a material in a specified way.
 the pattern is normally circulatory.
 it is normally taken place inside a container.

Mixing
 Random distribution, into & through one another
of two or more initially separate phases

22-Sep-18 2
22-Sep-18 MPS,DDU 3
Why to go for mixing?
• Heart of the chemical industry
• Uniformity of composition
• Desired flow pattern
• To control the quality of the product
• To maintain the heat transfer at highest
possible rate.
• To separate two phase mixture effectively.

22-Sep-18 MPS,DDU 4
Where is it required?
• Blending of miscible liquids
• Solid suspension
• Gas absorption
• Dispersion
• Dissolution
• Crystallization
• Heat transfer
• Chemical Reaction
• Extraction

22-Sep-18 MPS,DDU 5
A good mixing should achieve
• Minimum power requirement.
• Efficient mixing in optimum time.
• Best possible economy.
• Minimum maintenance, durable and trouble
free operation.
• Compactness.

22-Sep-18 MPS,DDU 6
Factors affecting the designing of the
agitator
• Type of vessel
• Circulation pattern.
• Location of the agitator
• Shape and size of the vessel
• Diameter and width of the agitator
• Method of baffling
• Power required
• Shaft overhang
• Type of stuffing box or seal, bearing, drive system etc

22-Sep-18 MPS,DDU 7
Types of agitator
– Paddle
– Propeller
– Turbine
– Helical
– Toothed / disc type
– Cone

22-Sep-18 MPS,DDU 8
22-Sep-18 MPS,DDU 9
Impeller Technology

22-Sep-18 MPS,DDU 10
22-Sep-18 MPS,DDU 11
Vortex
If solid particles present within tank; it tends to
throw the particles to the outside by centrifugal
force.
Power absorbed by liquid is limited.
At high impeller speeds, the vortex may be so deep
that it reaches the impeller.
Method of preventing vortex
- baffles
- impeller in an angular off-center position

22-Sep-18 12
22-Sep-18 MPS,DDU 13
Flow Around Baffles

22-Sep-18 MPS,DDU 14
(ii) Impeller in an angular off-center position

Mount the impeller away from the center of the vessel & tilted in the direction
perpendicular to the direction of flow.

Flow pattern with off-center propeller

22-Sep-18 15
Agitator Drive system
• Electric motor supplies the power.
• If rpm of motor shaft and agitator shaft is
similar then gear box is not required.
• Gear box transmits power of electric motor
shaft to agitator shaft directly or sometimes to
the other shaft which is attached to agitator
shaft.
• Coupling is used to connect two shafts.
• This power transmission system creates power
losses up to 20% of agitator power
consumption.
22-Sep-18 MPS,DDU 16
Drive
(Motor-Gearbox)
Assembly
Shaft seals
• During the process, liquid vapors or gases should not leak
through agitator shaft nozzle.
• There should not be any exchange either from inside to outside
or vise versa.
• Like in case of vacuum reaction
• Most common method for sealing shaft is with stuffing box
and gland.
• If P > 10kgf/cm2, T > 120C and N > 300rpm, one can not use
stuffing box.
• Mechanical seal will be preferred in above conditions.
• The losses occurred to loose type of fitting between shaft and
seal is considered to be 10% of agitator power consumption.

22-Sep-18 MPS,DDU 18
Stuffing box

Bolt Gland sleeve

Gland
Packing

Stuffing box

22-Sep-18 MPS,DDU 19
Mechanical Seal

22-Sep-18 MPS,DDU 20
Power consumption in agitated vessels

For an effective mixing, the volume of fluid


circulated in a vessel via an impeller must be
sufficient to sweep out the entire vessel in a
reasonable time.
Stream velocity leaving the impeller must be
sufficient to carry currents to the remotest part
of the vessel.

22-Sep-18 21
POWER REQUIREMENT
Factors affecting power requirement
• Properties of fluid to be agitated
• Height of the liquid
• Tank size and dimensions
• Agitator type and size
• Speed of agitator

Power number is ratio of drag force acting on unit area of impeller


to internal stress
22-Sep-18 MPS,DDU 22
Power Number
Pg c
NP  3 5
n Da 
• Where
– P = Power required for agitation
–  = Density of liquid solution agitated
– N = rotational speed of agitator in rps.
– Da = diameter of agitator

N P  f ( N Re , N Fr , S )
22-Sep-18 MPS,DDU 23
Dimensionless Numbers
• Reynolds's Number = Inertial stress/Viscous Stress
Da2 n
N RE 

• Froude Number = Inertial stress to gravitational stress
n 2 Da
N Fr 
g
• Shape Factor is related to linear dimension of vessel.
For turbine type agitator,
Dt E L W J H
S1  ; S2  ; S3  ; S4  ; S5  ; S5 
Da Da Da Da Dt Dt
22-Sep-18 24
Froude Number
• Considered when vertex is formed.
• In baffled tank, no vertex formation, so Np (NFr).
• In un-baffled tank with Nre < 300, no vertex
formation, so Np (NFr).
• In un-baffled tank with Nre > 300, vertex formation
takes place so Np =(NFr).
a  log 10 N Re
m
N P ( Corrected)  N P  N m
Fr b
Turbine a b
Three blades 1.7 18

22-Sep-18 Six blades MPS,DDU 1 40 25


Dimensionless Correlations

22-Sep-18 26
Fig 1

Curve A = vertical blades, W/Da = 0.2 Curve C = pitched blade


Curve B = vertical blades, W/Da = 0.125 Curve D = unbaffled tank
22-Sep-18 27
Power number NP vs. Reynolds number Re for turbines and impellers

22-Sep-18 28
Power number NP vs. Reynolds number Re for marine propellers and helical ribbons

22-Sep-18 29
Power correlation for a 6-blade turbine in pseudoplastic liquids

22-Sep-18 30
Power required for complete suspension of solids
in agitated tanks using pitched-blade turbines

22-Sep-18 31
22-Sep-18 MPS,DDU 32
Example
A flat-blade turbine with six blades is installed
centrally in a vertical tank. The tank is 1.83 m in
diameter, the turbine is 0.61 m in diameter & is
positioned 0.61 m from the bottom of the tank.
The turbine blades are 127mm wide. The tank is
filled to a depth of 1.83m with a solution of 50%
caustic soda at 65.6oC, which has a viscosity of
12cP and a density of 1498 kg/m3. The turbine
is operated at 90 rpm. What power will be
required to operate the mixer if the tank was
baffled?

22-Sep-18 33
Solution (a) baffled
n = 90rpm / 60 s = 1.5 r/s
Da = 0.61m
µ = 12cP = 12x10-3 kg/ms

N RE 
Da2 n

0.61 (1.5)(1498)
2
 69600
 1210 3

For Re > 10000, Np = KT = 5.8 from curve A for baffle (NRe = 69600),
NP = 5.8 (or from table 2 given before)

NPn 3
Da 
5
P
gc
3 5
 (5.8)(1.5) (0.61) (1498)  2476.6 mN / s 
2476.6W
22-Sep-18 34
Solution (b) unbaffled n = 90rpm / 60 s = 1.5 r/s
Da = 0.61m
From Fig 1, curve D (NRe =
µ = 12cP = 12x10-3 kg/ms
69600), NP = 1.07
Froude number,
N RE  69600

n 2 Da (1.5) 2 (0.61)
N Fr    0.14
g 9.81
From Table 1, the constants a & b are 1.0 & 40.0 respectively

a  log 10 N Re 1.0  log10 69600


m   0.096
b 40

22-Sep-18 35
From curve D, the power number for NRe = 69600 is 1.07
So the corrected value of NP,

N P (Corrected)  N P  N Fr
m
 1.070.140.096  1.29

Thus power,

N P n3 Da5 
P  (1.29)(1.5)3 (0.61)5 (1498)
gc
 550mN / s  550 W

22-Sep-18 36
SHAFT DESIGN
 Shaft can be attached to the vessel in vertical,
horizontal or angular positions.
 It is preferable to use the bearing either at top of
the vessel or at bottom. It can be placed externally
or internally to the vessel.
 DESIGNING CAN BE DONE BY 3 WAYS
• Based on torque
• Based on Bending moment calculations
• Based on the critical speed of the agitator.

22-Sep-18 MPS,DDU 37
Design properties of shaft
• Sufficient strength
• Low sensitivity to stress concentration
• Ability to withstand heat, wear resistance
• Good machinability
Fabrication method
 Hot rolling
 Cold drawing
 Turning
 Grinding from through bars

22-Sep-18 MPS,DDU 38
Shaft Design
• Two loads
– Torsonal load
– Bending load
• Shafts are generally made from carbon steel and is
heat treated to impart high mechanical strength up
to 8000kg/cm2.
• Total power required for agitator (X)= power
required for shaft + transmission losses + fitting
losses

22-Sep-18
hp  X 1.11.2
MPS,DDU 39
Loadings on shaft
• During start up the shaft has to withstand higher torque.
• During running condition, other than torque, forces like
hydraulic force due to turbulence in liquid or
asymmetrical construction of agitator and baffles.
• Centrifugal force will also present if agitator is not
balanced.
• Possibilities of agitators being chocked when tipping bags
or containers added to vessel.
• Worst possible conditions are assumed to be equivalent
to those in which agitator blade will be jammed at 75%
of its length.

22-Sep-18 MPS,DDU 40
Based on torque (shear stress)
• Continuous average rated torque on shaft
hp * 750 * 60 hp * 60
Tc  N.m  kgf.m
2N 2N
where N  speed in rpm
• Maximum torque developed in shaft
Tm  1.5 to 2.5 TC 
• Polar modulus of section of shaft cross section
 Tm
Zp  d 3
s fs    s ,allow
16 Zp
22-Sep-18 MPS,DDU 41
Based on Moment Calculation
Worst possible conditions are assumed to be equivalent to those in which agitator
blade will be jammed at 75% of its length.

M  Fm   where   shaft length


Tm
Fm  where R b  width of blade
0.75Rb
1

M e  M  M 2  TM2
2

Me 
fb   fJ Z d 3
s
32
Z
22-Sep-18 MPS,DDU 42
Based on Critical Speed
• It is difficult to calculate the unbalanced forces due
to asymmetric construction of agitator.
• Fixing certain counter balance weight in the opposite
direction to it can easily eliminate this.
• It is necessary to control the deflection of shaft by
adequate support
• The speed at which the shaft vibrates violently is
called as the critical speed of the shaft.
• Range of 70% to 130% of critical speed should be
avoided
• Diameter should be so chosen that the normal
working speed should not fall in this range.
22-Sep-18 MPS,DDU 43
Based on Critical Speed

3
Fm 
 , cm
3EI
60 * 4.987
d 4
Nc  rpm
I s
 
12
22-Sep-18
64 MPS,DDU 44
HUB & BLADES
• Hub is attached to shaft by Keys & Bolts.
• The load on the blade is assumed to act as
75% of the agitator radius.
• This will create a bending moment in blade,
which will be maximum at the point where
the blade is attached to the hub.
M max  F m(0.75Rb  Rh )
max B.M Fm 0.75Rb  Rh  Tm
f   2
 2
22-Sep-18
Z b
MPS,DDU
t * bw / 6 bt * bw /6 45
HuB
• The hub is fixed to the shaft by key, which
transmits the shaft torque to the impeller.
• The hub is subjected to the bending moment
due to force on the blade and to shear force
due to the torque.
• It is assumed the outside hub diameter as
twice the shaft diameter and check the shear
stress due to torque.

22-Sep-18 MPS,DDU 46
Impellers

Pitched Blade Turbine (PBT) Rushton Turbine (RT

22-Sep-18 MPS,DDU 47
Impeller with Shaft, Hub and Key

22-Sep-18 MPS,DDU 48
22-Sep-18 MPS,DDU 49
Hub and key

• Hub diameter = 2 * shaft diameter


• Hub length = 2.5*shaft diameter
• Key length (ℓ) = 1.5*shaft diameter

Tm t
 bf s  f c
ds 2 2

22-Sep-18 MPS,DDU 50
Other parts
• Stuffing box
• Gland
• Coupling
• Stabilizer
• Bearing
• Shaft seals
• Drives for agitator

22-Sep-18 MPS,DDU 51

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