LABORATORY REPORT
SKU1033
SESSION            2023/2024
EXPERIMENT
                   DILUTION OF CONCENTRATED ACID SOLUTION
TITLE
                   1)   MOHAMAD        HASPIRULLAH         BIN      R.HAPESIDON
STUDENT’S NAME &
                   (E20221030576)
MATRIC NO.
                   2)MUHAMMAD IMRAN HAIKAL BIN OTHMAN
LECTURE GROUP      A
LECTURER NAME      ChM. Dr. Mohamad Idris Saidin
                                                    CHECKLIST                   Marks
                                                   Grammar/spelling       10
                                                       Format             10
                                                     Introduction         10
                                                     Materials &          10
                                                     Apparatus
                                                      Methods             10
                                                       Results            10
                                                     Discussion &         10
                                                      conclusion
                                                      References          10
                                                     Conceptual           20
                                                    understanding
                                                   TOTAL MARKS            100
EXPERIMENT 3
DILUTION OF CONCENTRATED ACID SOLUTION
OBJECTIVES
Upon completion of this experiment, students should be able to prepare a series of acid solution at
different concentration.
INTRODUCTION
 Dilution is the process of decreasing the strength of an acid or base. We know that acids and bases
produce H3O+ and OH- ions in water. When they are diluted (by having more amount of water), the
concentration of H3O+ or OH- ions per unit volume decreases. This results in decrease of the strength
of the acid. pH value can be measured by using various methods, such as universal indicator and pH
meter. pH value depends on the concentration of H3O+ in the solution.
                                         Figure 3.1: pH meter
CHEMICALS AND APPARATUS
Chemicals
Hydrochloric acid (37 %w/w)
Apparatus
Pipette
Volumetric flask (50 mL, 500mL)
Dropper
Glass rod Filter
funnel pH meter
3.4    PROCEDURE
Part A: Preparation of stock solution: 0.5 M Hydrochloric acid from HCl (37 %w/w)
1. Molarity of hydrochloric acid (37 %w/w) is determined by completing Part A table in Data Sheet.
2. 0.5 M hydrochloric acid is prepared in 500 mL volumetric flask from hydrochloric acid
   (37%w/w).
Part B: Dilution of 0.5 M Hydrochloric acid, HCl
1.    solution of 0.1 M, 0.01 M, 0.001 M and 0.0001 M is prepared in 50 mL volumetric flask using
     dilution technique.
2.   pH value are observed and recorded using pH meter.
DISCUSSION BASED ON THE FOLLOWING QUESTIONS
Part A: Preparation of stock solution: 0.5 M Hydrochloric acid from HCl (37 %w/w)
        Pour hydrochloric acid solution (37% w/w) in a beaker.next,transfer 20.49 ml hydrochloric
acid (37% w/w) solution into 500 ml volumetric flask.then add distilled water into the volumetric flask
and then use dropper to fill until it reaches meniscus level.
Part B: Dilution of 0.5 M Hydrochloric acid
         HCL with solution 0.1M has the highest concentration thus having the lowest ph scale at
     1.11.next ,HCL solution that has the lowest concentration,0.0001M has the highest ph value at
     3.96.both hcl solution with 0.01M and 0.001M concentration has ph value at 2.09 and 3.13
     accordingly.we can say the higher concentration is,the lower ph value of acid solution which is more
     acidic.
         Dilution is the process in which water or any other solvent is added to the solution to decrease
     the concentration, in this case,ion hidroxide,OH-.Basic solution has more hydroxide ion than
     hydrogen ion. Addition of water to an acidic or basic solution causes change of pH. This results in
     the increase of pH of alkali towards 7. This makes the solution more alkaline. That means the pH
     increase on diluting an alkaline solution
REFERENCES
1.     How to           Dilute Copper Sulfate.        (2017, April). Retrieved        from
       https://sciencing.com/dilute-copper-sulfate-8089464.html
2.     Safe Handling of Hydrochloric Acid. (2006, November). Retrieved from
       http://www.jsia.gr.jp/data/handling_02e.pdf
3.     Preparing         and      diluting       solutions        (2012). Retrieved    from
       http://lrrpublic.cli.det.nsw.edu.au/lrrsecure/sites/lrrview/13897/13897_pop16.html
3.7    DATA SHEET
Part A: Preparation of stock solution: Hydrochloric acid, HCl (37% w/w)
        Mass (g) of HCl in 100 g                                            37
        Density of HCl (g/mL)                                               1.2
                                                                       3783.33
        Mass (g) of HCl in 1 mL
        Molar mass of HCl (g/mol)                                          36.46
        Molarity of hydrochloric acid (37 %w/w)
                                                                          12.178
        (M)
        Mass of HCl needed (g)                                             6.089
Part B: Dilution of 0.5 M hydrochloric acid
      The concentration of HCl before
      dilution (mol/L)                                               0.5
      The volume of the volumetric flask
      (mL) for dilution                                              50
      Volume needed to prepare 0.1 M
      HCl (mL)                                                       10
      Volume needed to prepare 0.01 M
      HCl (mL)                                                        5
 pH value of HCl solution for four (4) different concentrations
                                            The concentration of HCl (M)
      pH value              0.1                0.01                0.001             0.0001
                           1.11                2.09                3.13               3.96
___________________    _____________________________
DATE                  LECTURER’S SIGNATURE/STAMP