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Heseries 2993658665

This technical manual provides instructions for installing, operating, and maintaining DRI-LAB vacuum boxes from Vacuum/Atmospheres Company. The DRI-LAB system consists of a sealed glove box with an attached antechamber and viewing window. It is used to create and maintain an inert atmosphere nearly free of moisture, oxygen, and nitrogen for sensitive materials. Users access the glove box interior through gloves mounted in the viewing window and transfer materials in/out using the antechamber and sliding tray. The manual covers system components, installation and leak testing, atmosphere control procedures, routine maintenance, troubleshooting, and parts lists.

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Văn Phúc Lê
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© © All Rights Reserved
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0% found this document useful (0 votes)
62 views46 pages

Heseries 2993658665

This technical manual provides instructions for installing, operating, and maintaining DRI-LAB vacuum boxes from Vacuum/Atmospheres Company. The DRI-LAB system consists of a sealed glove box with an attached antechamber and viewing window. It is used to create and maintain an inert atmosphere nearly free of moisture, oxygen, and nitrogen for sensitive materials. Users access the glove box interior through gloves mounted in the viewing window and transfer materials in/out using the antechamber and sliding tray. The manual covers system components, installation and leak testing, atmosphere control procedures, routine maintenance, troubleshooting, and parts lists.

Uploaded by

Văn Phúc Lê
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
You are on page 1/ 46

DRI-LAB

TECHNICAL MANUAL
GBX, HE & DLX SERIES

DRI-LAB-R1-10/98

VACUUM ATMOSPHERES COMPANY


4652 ROSECRANS AVE., P.O. BOX 1043 • HAWTHORNE, CA 90250-6896
TELEPHONE: (310) 644-0255 • FAX: (310) 970-0980
http://www.vac-atm.com • email: tfitz@vac-atm.com
_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ Vacuum/Atmospheres

Contents

List of Figures iv
List of Tables iv
INTRODUCTION v

1• OVERVIEW • • 1-1
Application • 1-1
Functional Description 1 -1

2. INSTALLATION. · 2-1
General · 2-1
Customer-Furnished Items · 2-1
utility Requirements . · 2-1
Electrical · 2-1
Vacuum Line · 2-2
Gas Supply o 2-2
Installing the Gloves • 2-2
Leak Testing · 2-2
Leak In Gloves · 2-5
Oxygen and Moisture Testing · 2-6
Electric Lightbulb Test · 2-6
Welding Chamber Test · 2-6
Titanium Tetrachloride Test · 2-7
Diethylzinc Test · 2-7

3. OPERATIONS · 3-1
General · 3-1
Establishing An Inert Atmosphere . · 3-1
Antechamber . · 3-2
Evacuate/Refill Procedure • 3-2
Glove Box · 3-2
Passing Materials In/Out of Dri-Lab · 3-3

ii Dri-Lab-08/85
_ _ _ Vacuum/Atmospheres

Contents (Cont'd)

4. MAINTENANCE AND TROUBLESHOOTING · 4-1


General · 4-1
Periodic Mainten·ance · 4-1
Safety Glass Panels · 4-1
Lexan Panels . · 4-1
Dri-Lab · 4-2
Antechamber · 4-2
Replacing Old Gloves · 4-2
Accessories · 4-3
Troubleshooting · 4-3

5. PARTS AND ACCESSORIES · 5-1


Replacement Policy · 5-1
Spare Parts . · 5-1
Accessories . · 5-1

APPENDIXES
A. Specifications and Dimensions · A-1
B. Special Schematics or Diagrams . · B-1
Schematic Diagram of Junction Box . · B-2
C. Warranty · C-1
D. Spare Parts Listings · D-1
E. Accessories · E-1

INDEX Index-1

iii Dri-Lab-R2-1/99
. _~~_ Vacuum/Atmospheres

LIST OF FIGURES

Figures

1-1 Dri-Lab Assembly and Connections · 1-2


2-1 Installing Gloves On Glove Box · 2-3
2-2 Leak Testing Dri-Lab Without Detector . · 2-5
3-1 Establishing An Inert Atmosphere · 3-1
3-2 Procedure For Passing Materials Into
Dri-Lab . · 3-4
3-3 Procedure For Passing Materials Out Of
Dri-Lab . · 3-5
4-1 Antechamber Door Assembly . · 4-4
B-2 Schematic Diagram Of JULction Box · B-2

LIST OF TABLES

Table

4-1 Troubleshooting Dri-Lab · 4-3


D-1 Spare Parts List (HE-series) . · D-1
D-2 Spare Parts List (DL-series) . · D-2
D-3 Spare Parts List (GBX-series) · D-3

iv Dri-Lab- R2-1/99
c_ _ _ _ _ _ Vacuum/Atmospheres

INTRODUCTION

This manual provides information necessary to install,


operate, and maintain Vacuum/Atmospheres GBX-, HE- and
DLX- series Dri-Lab boxes.

Additional information relative to any Vacuum/Atmospheres


Company (VAC) system may be obtained from:

Vacuum/Atmospheres Company
P. O. Box 1043
4652 West Rosecrans Avenue
Hawthorne, CA 90250-6896
Telephone: (310) 644-0255
FAX: (310) 970-0980
http://www.vac-atm.com
email:tfitz@vac-atm.com

v Dri-Lab-R2-9/98
VAC _ _ __ Vacuum/Atmospheres

Section 1
OVERVIEW
APPLICATION
The VAC HE-series (or GBX and DLX-series*) Dri-Lab provides a
working area of inert atmosphere nearly free of moisture, oxy-
gen, and if desired, nitrogen. Any material that is sensitive
to moisture, oxygen, or nitrogen may be worked with freely. The
Dri-Lab is designed for use of argon gas as the principal inert
gas, and also may use helium, nitrogen, or any combination of
these gases.

FUNCTIONAL DESCRIPTION
The HE-series Dri-Lab consists of an hermetically sealed glove
box, a side-mounted antechamber, and a full-view window (Figure
1-1). The glove box and antechamber share an entry/exit airlock
door, used for passing materials in and out without disturbing
the glove box atmosphere. All materials are passed in and out
of the glove box on a sliding tray (located on the bottom
of the antechamber). The IS-in. I.D. antechamber, with one
interior and one exterior door, permits large objects to be
passed into and out of the glove box.

Two 9-in. glove ports and butyl rubber gloves, mounted in the
full-view window, provide easy access to all areas of the glove
box. An assortment of gas, water, and electrical connections
are also provided in the rear of the glove box wall. (Refer to
Appendix A for Dri-Lab specifications.)

*For simplicity, this manual will address the HE- rather than
the GBX- and DLX-series Dri-Lab. Both models are essentially
the same. The HE-series has removable end panels and a skylight;
the DLX-series does not. The HE-series is available in aluminum
or stainless steel; the GBX- and DLX-series are available only
in stainless steel. GBX-series has removable end panel~ and no
skylight.

R3~9/99
1-1 Dri-Lab-08/8S
c ._ _ _. ____ ._ _ _ _ _.... _.......... _ _ _ _ _Vacuum/Atmospheres

.. __ - - _ . _ - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - ,
..

FIGURE '1-'1

DRI- LAB ASSEMBLY AND CONNECTIONS

~)

.@

A. SKYLIGHT LEXAN PANEL (HE SERIES ONLY).

B . ANTECHAMBER OUTSIDE DOOR ASSEMBLY.

C.COMPO~ GAUGE.
o p
D. EVACUATION VALVE AND CONNECTION TO IACWM

PUMP.

E . ANTECHAMBER REFILL VALVE.

\ G. ANTECHAMBER INSIDE DOOR ASSEMBLY


\
I
H. GLOVE PORT
\~ @
K. FRONT LEXAN WINDOW,
\
\ L . AUXILIARY FEED THROGGH FORTS.

M. ELECTRICAL CONNECT/ON JUNCTION BOX,

V
\ ~r@ ~@@ (@ V


N. FD. THRU PORT FOR OPTIONAL H'rGROMETER.

O. FD. THRU PORT FOR OPT/ONAL PRESSURE RELIEF.


• P. FD. THRU. PaR7S FOR OPTIONAL PURIFICATION SYSTEM
BACK VIEW
• HE & DLX Only

Rl-12/98 1-2 Dri-Lab-08/85


_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ Vacuum/Atmospheres

Section 2
INSTALLATION

GENERAL
Before starting the installation, read all instructions com-
pletely. Instructions are standard and some may not apply to
custom systems.
A. Remove components from crate. Do not use junction box or
glove ports to lift Dri-Lab.
B. Remove all packing, tape, and shipping blocks or bands.
C. Place Dri-Lab stand in .desired location.
D Place Dri-Lab on stand.
1) Align side opposite antechamber flush with stand end.
2) Align back side flush with stand back (single-sided Dri-
Lab). Align front and back symmetrically on stand width
(double-sided Dri-Lab).

CUSTOMER-FURNISHED ITEMS
Before installation is possible, the customer must furnish the
following items:
A. Vacuum pump, 3 to 5 cfm.
B. 3/B-in. copper or stainless steel tubing for inert gas.
C. utilities, as noted.

UTILITY REQUIREMENTS

Electrical
A. Skylight: 115 V, 5 A.
B. Glove Box Junction-Box: 115 V, 15 A (see Appendix B for
system schematic diagrams).
C. Vacuum Pump: 115/230 V or as required by size and rating of
vacuum pump.

2-1 Dri-Lab-OB/B5
c _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres

Vacuum Line
Use 1-in. O.D. vacuum hose from evacuation valve on the ante-
chamber to the vacuum pump (user supplied).

Gas Supply
If your Dri-Lab was not purchased with a VAC pressure control
system, the gas supply should be regulated at 20 psi and con-
nected to a main shutoff valve (user supplied) at a Dri-Lab
feedthrough. VAC recommends customer use as pure a gas as eco-
nomically or conveniently practical.

INSTALLING THE GLOVES


A. Fold glove cuff inside out approximately 2 in. (Figure 2-1).
B. Place glove into glove port/glove box and stretch cuff onto
glove port flange. The bead in the cuff should be
positioned in the inner groove closest to the glove box.
C. Adjust glove so that thumb is pointed in the correct
direction (up for ambidextrous, horizontal for formed L/R
gloves).
D. Stretch a-ring over glove and into the outer groove. Make
sure there are no wrinkles, especially under the a-ring.
E. Cover O-ring with black-plastic electrical tape (user
supplied). Without wrinkling the glove, install the stain-
less steel clamp over the outer a-ring.

LEAK TESTING

I I
Note
Prior to leak testing, if panels were
removed to install equipment inside Dri-
Lab, reinstall panel acorn nuts at 26 to
28 in.-lb.

2-2 Dri-Lab-08/85
. - - - - - - -....... - . - - - - -_ _ _Vacuum/Atmospheres

FIGURE 2-1

INSTALLING GLOVES ON GLOVE BOX

A. GLOV~ PORT RING.

B. GUJV{.
c. o - /~/NG.
D. I~L~CK /JLASTIC 7AP~.

CA) E. CLAMP.

I
/

-~
\
8
'----

®
/
/

2-3 Dri-Lab-OS/85
VA C~ _ _~ _____~_~_ _ ~ _ ~______ VaclJum/Atmospheres

WARNING I
Do not use halogen leak detection equip-
ment for leak testing. Halogens are
harmful to certain materials used in the
construction of VAC equipment (i.e.,
copper and rubber). VAC will not assume
responsibility for systems tested by
methods other than defined in this
manual.

TEST ONE
VAC recommends using helium leak detection equipment. If no leak
detector ~s available, the follow~ng test procedures are recom-
mended (keep Dri-Lab and room temperature constant throughout
testing) :
A. Connect a source of gas to one of the connections in the
back of the Dri-Lab (see Figure 2-2).
B. Close antechamber outside door; close evacuation and refill
valves.
C. Open inside antechamber door.
D. Slowly pressurize Dri-Lab. The gloves will be forced out.
E. Stop pressurizing when gloves are almost horizontal. (Let
gloves break slightly from horizontal.)
F. Place a stool or chair with a ruler taped on its back to
within 1/4 in. of glove finger tip. Note reference point
and wait approximately 1 hr.
o If system leaks, gloves will fall more than 1/8 in.
Locate and seal leaks. Repeat test until gloves remain
steady for several hours.
a Relieve pressure on gloves after testing.
o Replace plugs removed for leak testing with teflon-
taped brass plugs (user supplied).

2-4 Ori-Lab-R2-9/99
c____ _ _ _ Vacuu m/Atmospheres

TEST TWO

If a water manometer is available, connect it directly to Dri-


Lab via any fittings in back and use manometer as a pressure
indicator. (CAUTION: Box pressure should not exceed lO-in.
water column.)
a Set pressure to 4-in. of water column.
a If system leaks, pressure will fall more than liS-in.
Locate and seal leaks. Repeat test untill gloves
remain steady for several hours.
o Relieve pressure on gloves after testing.
o Replace plugs removed for leak testing with teflontaped
brass plugs (user supplied).

TEST THREE

If this glove box equipped with Pressure Control of any model.


Do the following:
A. Set the high side of Pressure Control unit to + 5
inches water column. And set the low pressure side
to + 1 inch water column.
B. By using the foot switch and depressing on the right
side of it the gas valve will energize and the pressure
will rise in the glove box.
C. Set the pressure at + 4 inches water column with all
gloves fully extended outside.
D. After the pressure stabilized, monitor it for any drop.
E. If the pressure drops at any rate then we have a leak.
If not then the system is ok.

NOTE: If the glove box has a Dri-Train or any accessories such


as: CS-40, Cold Well, or Mini AIC, make sure that the
pressure is equal in all the internal of the glove box
including all accessories. That means leave CS-40 door
open, Cold Well lid off, and AIC inside door open.

2-4A Dri-Lab Rl-6/99


- - - - -_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres

FIGURE 2 - 2
LEAK TESTING DRI-LAB WITHOUT DETECTOR

Leak in Gloves
Gloves are vulnerable to leaks, especially in the fingertips. To
check for leaks:
A. Stretch rubber to detect small holes.
B. Check for cracks near glove port.
C. Inflate glove, twist wrist, force into pail of water, and
look for source of bubbles.

INotel
Replace gloves at the first sign of
deterioration. VAC recommends wearing
protective gloves over Dri-Lab gloves if
working processes include handling sharp,
hot, or corrosive materials.

2-5 Dri-Lab-08/85
c _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres

OXYGEN AND MOISTURE TESTING

WARNING I
VAC does not assume responsibility for
accidents resulting from mishandling of
materials used in the following tests.

VAC manufactures instruments that automatically and continuously


monitor Dri-Lab atmosphere for oxygen and/or moisture. In the
absence of more precise instrumentation, the following tests
provide a general idea of the condition of the D~i-Lab

atmosphere. Note that the ppm levels stated in these tests are
estimates only.

Electric Lightbulb Test


A. File an opening or flame torch a hole through a glass 25 W
lightbulb. Do not break filament.
B. Screw bulb into a socket and pass it into the Dri-Lab. Plug
into AC outlet in Dri-Lab junction box.
o If the filament burns out after 6 hr, the oxygen and
moisture content is higher than 5 ppm.
o If the filament burns for days (or even weeks), the
level is between 1 and 5 ppm.

Welding Chamber Test


A. Pass a portable welder and clean sample of stainless steel
into Dri-Lab.
B. Weld a bead on the clean sample of stainless steel.
o If bead is clean and silver, moisture and oxygen content
is between 1 and 2 ppm.
o If bead appears blue-black, a considerable amount of
oxygen and moisture is present.

2-6 Dri-Lab-08/85
_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres

Titanium Tetrachloride Test


A. Pass a bottle of titanium tetrachloride into Dri-Lab.
B. Open the bottle inside the glove box, but be prepared to
close the bottle immediately if you see smoke. For best
results, hold a black-gloved hand behind the bottle: the
white smoke will be better seen against the black back-
ground.
o If smoke is observed, moisture exists at a relatively
high level.
o If no smoke is observed, the dew point is less than
-60 o C (10 ppm).

Diethylzinc Test

Materials used in the following test are


pyrophoric when mixed -- use extreme
caution in handling.

A. Pass a bottle of diethylzinc, a bottle of heptane, and an


empty bottle with cap into Dri-Lab.
B. Mix a small amount of each material together in the empty
bottle, but be prepared to cover the bottle immediately if
smoke is seen. For best results, hold a gloved hand behind
the bottle: the white smoke will be better seen against the
black background.
a If there is less than 5 ppm of oxygen within the Dri-
Lab, the mixture will not emit smoke.
o If smoke is seen, a relatively high amount of oxygen
exists. Cap bottle immediately.

2-7 Dri-Lab-08/85
_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres

Section 3
OPERATIONS

GENERAL
The instructions that follow are for basic operation of the Dri-
Lab without a Dri-Train automatic recirculating system. Opera-
ting instructions for the combined Dri-Lab/Dri-Train are found in
the Dri-Train manual.

ESTABLISHING AN INERT ATMOSPHERE


A good purge is required to establish an inert atmosphere. The
purge described herein requires 200 to 250 ft 3 of gas for a
25-ft 3 box (this equals about 10 volume changes). For best
results, use as pure a gas as is available.
A. Install purge inlet and exhaust valves (user furnished) on
two ports in back of the Dri-Lab (Figure 3-1).
B. Connect gas supply to Dri-Lab inlet purqe valve.

FIGURE 3-1
ESTABLISHING AN INERT ATMOSPHERE

/
HE- LAB

ANTECHAMBER

GAS ~

PURGE
INLET ~ REFILL

~ PURGE EXHAUST TO VACUUM


PUMP ~
~ = CUSTOMER FURNISHED

3-1 Dri-Lab-08/85
_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres

C. Close antechamber inside door, refill valve, and evacuation


valve.
D. Open purge exhaust valve.
E. Open purge inlet valve and begin gas flow. Keep the Dri-
Lab pressure positive. The gloves must be extended to
almost horizontal, but not ballooned.
F. When purge is completed, close purge inlet valve and then
the purge outlet valve before the gloves drop. Leave a
positive pressure in the Dri-Lab.

ANTECHAMBER

Evacuate/Refill Procedure
Any time the antechamber is exposed to atmosphere, the following
procedure must be used before opening the inside antechamber door
to the glove box:
A. Both antechamber doors must be closed.
B. Refill valve must be closed.
C. Open evacuation valve and evacuate to 50 microns (minimum).
E. Close evacuation valve.
F. Open refill valve.

Since the antechamber refills from the glove box, additional gas
will be required to make up for the decrease in pressure in the
glove box. Add gas via the glove box inlet valve to make up for
this decrease in pressure.

GLOVE BOX
Be aware of the following items when using the Dri-Lab glove box:
• Watch the gloves during antechamber evacuation. If the
gloves are drawn into the glove box, check the inside ante-
chamber door and/or refill valve; either one may be open.
Close the door and refill valve to the antechamber.
• Keep the antechamber doors and valves tightly closed when
not in use.

3-2 Dri-Lab-08/85
c ._ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres

• Never attempt to force the antechamber doors open.


• When opening the antechamber doors, back door off firmly
against the bar before raising.
• Do not allow the glove box pressure to go negative. Refill
gas into the glove box at a rate that maintains the same
volume of gas as before the antechamber was filled.

PASSING MATERIALS IN/OUT OF DRI-LAB


Passing materials into and out of the Dri-Lab are explained in
Figures 3-2 and 3-3, respectively.

3-3 Dri-Lab-08/85
_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres

FIGUR'E 3-2

PROCEDURE FOR PASSING MATERIALS INTO DRI- LAB

STEP I - ARTICLE OUTSIDE A/C.


- INSIDE DOOR CLOSED.
- OUTSIDE DOOR OPENED,
- A IC IS CONTAMINATED.
(
- DRI - LAB i-IAS INERT ATMOSP-IERt,

STEP 2 - ARTICLE IS IN Ale


\.J l) C
- BOTi-I DOORS ARE CLOSED. \J l) 0
Co
\J C
- AIC IS PARTlA~LY EVACUATED. 0
-
)

- DRI - LAB i-IAS INERT ATMOSFi-IEF£,


0 u
c
)
MI
c

STEP 3 - ARTICLE IS IN A Ie. o 0 //


- A/C IS COMPLETELY EVACUATED.
o c
- DRI-LAB i-IAS INERT ATMOSPi-iERE, G
' • .1 (.... n ' - - - - - ' - - n / /

" 0
o u ///
(I C CI 0
/
STEP 4 - ARTICLE IS IN Ale
- BOTH DOORS STILL CLOSED
'---0-0--:::0=--=0---:0'---=0--' /
- Alc IS BACKFILLED WlTI-I ATMOSPHERE
n 0 0 0 0
FROM DRI - LAB. o -0 0 0 (1 0 0 '
- DR/-LAB ¥ Alc HAVE INERT ATMOSPHERE O, 0 n "(,J
.i C' 0 0 () 0., 0 /
o 0 0 0 0 aU /
oo 0 °0 0 '-
) 0
nCO,
0 0
Go~
0 ~c"
0
,u,,',
,.' 'j

STEP 5 - OUTSIDE ODOR CLOSED,


-INSDE DOOR OPENED.
- ARTICLE MOVED INTO DRI - LAB, o
° °00 0 0 0 °
0

o (10<)° 0 °
C)_ ') ° () 0
°°
~
\)" ,-, - 0
~
1
" 0- 0 ,0
NDTE!3: c ou C,O, c"nu
:) :) ~ '-' I:) "\,, ,-,' 0 ('

=
~) " )
1-0 VALVE OPEN.
) (») I)') "j 1

2- VALVE CLOSE.
3 - KEEP Alc DOORS CLOSED UNLESS IN USE.

3-4 Dri-Lab-08/85
._ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres

FIGURE 3 - 3
PROCEDURE FOR PASSING MATERIALS OUT OF DRI- LAB

o 0 0 (' c'
o 0 (;
o o-().~ c.
o l· U
o 0 u 0
c (; C 0 u-,
00 0 l i lv c
o c c
/

STEP I - ARTICLE INSIDE DRI-L-AE.


- INSIDE DOOR CLOSED.
- OUTSIDE DOOR OPENED
- Alc IS CONTAMJ'I, ...TED. -,
- DRI-LAB :'1AS IlVERT An;/J~~Ft-IERE ··18
STEP 2 - ARTICLE INSIDE DRI-LAB.
- BOTH ODORS ARE CLOSED.
- AIC IS PARTIALLY EVACUATED.
'.1
- DRI-LAB HAS INERT ATMO::PHEFiE ) ,

STEP 3 - ARTlCLL INSIDE DRI-LAB.


- A/C IS COMPLETELY EVACUAF--:J.
- DRI-LAB HAS INERT ATMOSPHEPE

STEP 4 - ARTICLE INSIDE DRI-LAB


- BOTH DOORS STILL CLOSED.
- ATMOSPHERE FROM uRI-LAE BACKFILLS A/C. (' r

- DR/-LAB ¥ AIC HAVE fNERT ATMJSFr-£RE.


I '.
STEP 5 - INS/DE DOOR OPENED
- ARTICLE MOVED INTO Ale.
~"
. , ')
- DRf-LAB ~J. ,L /e H,J,VE I:'VERT ATiv1J:"'~?HERE

STEP 6 - INSIDE ODOR CLOSED.


- OUTSIDE DOOR OPENED.
- ARTICLE IS MOVED OUTSIDE A/e.
( )

,J

NOTES:
/- 0 VALVE OPEN.
2 _~ VALVE CLOSE.
3 _ KEEP A C DOORS CLOSE UNLESS IN USE.

3-5 Dri-Lab-08/85
_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres

Section 4
MAINTENANCE AND TROUBLESHOOTING

GENERAL
Maintenance of the HE-series Dri-Lab is uncomplicated due to
relative simplicity of the unit's design and component selection.
However, standard safe practices should always be observed during
maintenance.

Periodic Maintenance
Visual inspection of Dri-Lab O-rings, gloves, and vacuum system
should be performed to ensure tightness of glove box and proper
operation of the vacuum system. (See also Section 2-5, Leak
Test. )

Safety Glass Panels (Optional)


Refer to Safety Glass Windows in Appendix E for installation
instructions and replacement procedures.

Lexan Panels
Clean panel with a clean cloth and either soap and water or a
commercial glass cleaner.

Do not use abrasives such as steel wool,


stiff paper towels, or abrasive clean-
sers to clean panels.

To replace window or metal panels:


A. Remove 7/16-in. acorn nuts at frame and panel.
B. Clean gasket, panel, and box and apply a light coat of
vacuum grease to gasket. Replace worn or damaged gaskets.
C. Replace panel and frame over the gasket onto the box studs,
andcinstall acorn nuts at 26 to 28 in.-lb torque.
D. Leak check all joints.

4-1 Dri-Lab-08/85
c _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ Vacuum/Atmospheres

Dri-Lab
Use mild soap and water to clean the outside painted surfaces.
Dry the unit with compressed air. At recommended 3-mo intervals,
all valves, fittings, lines, tubing, and connections should be
inspected for general mechanical and electrical integrity.

Antechamber
Check the sealing a-rings periodically and replace when worn or
damaged. Clean antechamber doors periodically with a mild
solvent, and coat the sealing surfaces with a light coat of
vacuum grease. If required, adjust antechamber door tension as
follows:
A. Close door and loosen jam nut at door clamp (Figure 4-1).
Loosen nut 2.
B. Open door and rotate door clockwise (increase tension) or
counterclockwise (decrease tension).
C. Close door to fully closed position - firm pressure should
be required to close door.
D. Tighten nut 2 and then jam nut.

Replacing Old Gloves


Gloves should be replaced at the first sign of deterioration. To
replace old gloves with a minimum of Dri-Lab contamination:
A. Seal glove port with internal glove port cover (optional
equipment).
B. Remove glove by reversing the procedure for installing
gloves as outlined in Section 2-4.
C. Install new glove as outlined in Section 2-4.
D. Before installing clamp, purge glove as follows:
1) Increase and maintain positive pressure in glove box at
approximately 4-in. water column.
2) Loosen glove port cover to allow glove to fill with
inert gas from glove box.
3) Once glove is pressurized, tighten glove port cover
again.

4-2 Dri-Lab-08/85
~~ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _v~umwmoo~~

4) Roll glove slowly toward box, starting at fingers,


intermittently releasing glove around glove port to
allow pressure to release. Continue until glove has
been rolled up to glove port.
5) Repeat steps 1 to 4 approximately two or three times
before removing glove port cover and placing it back in
the glove box.
E. Install clamp over O-ring.
F. Remove inte~nal glove port cover and check for leaks.

Accessories
For maintenance of purchased accessories, refer to accessory
instruction sheets in Appendix E.

TROUBLESHOOTING
Failures in operating the Dri-Lab may occur in one or more of the
following areas: a) glove box, b) vacuum system, or c) ante-
chamber. Check these areas first. Table 4-1 provides additional
information in locating and correcting problems.

Rl-1/99 4-3 Dri-Lab-08/85


§
A - A/C FlANGE.
n
',,~
B - O-RING.
e - DOOR.
n- BAlANCE WEIGHT.
E- DOOR BAR.
F- CLAMP.
G - STUD.
H - NUT 1
J - NUT 2
B K - JAM NUT.
L - DOOR BOSS

~ e
'~

I!
G')
c:

~
.+::0-
I :x:J
.+::0-
m
~
I
...L

M - DOOR BOSS
N - SHOULDER BOLT.
o- DOOR STOP.
P- HEX.HD.BOlT.
F
Q - TORQUE ADJUSTER.
R - pm HD.SCREW.
S - DOOR BAR SPRING
~
T- HEX.HD.BOlT. o
c
S? N c
"j' U - HEX.HD.BOLT. s::
S- V - LOCK WASHER. ~
O" s::
I
;0
Z - FLAT WASHER. o
(/)
0.1 '1J
I I
co fTl
;:0
~ fTl
(/)
1.0
Detailed Instruction For
Antechamber Door Adjustment

D<x>r Tension

Tools required:

9/16 inch open/end/box wrench, 1 each.


1-1/2 inch thin open/end wrench, if adjusting Clamp.
(Bonney 1-1/2 inch open/end thin wrench #1248, 1 each)
3/4 inch open/end/box wrench, if adjusting Spring, 1 each.

! !NOTE! !

Before adjusting the door make sure that the opposing


door is closed, to avoid accidental contamination of
glove box atmosphere. If adjusting inside door,
evacuate and refill Antechamber using your standard
pump down time.

1 .)Tension Door Adjustment:


A)Close door and loosen nut 2 (J) close to the
door clamp (F). Never loosen nut 1 (H) (Figure 4-1).
B)Release door clamp (F), until door will turn.
C)Turn door (C) (clockwise CW to increase tension),
(counterclockwise CCW to decrease tension).
D)Close door clamp (F) fully. Firm pressure should
be required to close door. This may require several
movements of the door (C) to increase or decrease
the tension required to close the door.
E)Close door clamp (F) fully then tighten nut 2 (J).

2.)Adjustinq L Replacing Door Clamp:


A)Close door, evacuate antechamber to 10 inches Hg.
B)Loosen nut 2 (J) and jam nut (K).
C)Release door clamp (F). Turn CCW allowing the door
clamp handle to move freely.

Rl-l/99 4-4-A Dri-Lab-08/91


Detai1ed Instruction For
Antechamber Door Adjustment

! !NOTE! !
Use a clamp on the end of the door bar (E) at the door
boss close to the window. This will keep the door bar
from flying up and back to the door stop, because of
the balance weight (D) and no door for counter balance.

D)To replace door clamp (F), install jam nut (K) until
it is fully seated against the door clamp shoulder.
E)Open the door clamp (F) fully then slowly turn CW
until you have engaged the threads in the door bar
(E). Now close the door clamp slowly to pick up the
door screw (G) while turning the door clamp CWo Let
the door handle move freely while turning. Turn the
door handle until it is as close to the door bar (E)
as possible. Now return the handle to the original
position and tighten jam nut (K) against door bar.
F)Refill antechamber and go to Tension Adjustment on
page one.

3. ) Adjustinq Counter Ba1ance Spring (Dri-Labs 1989 and Newer)


A)Open door clamp (F). Do not raise door bar (E).
B)Place your 3/4 inch open end wrench on flats of
the door boss spring holder located at the door
hinge point. (Note the present location of the
screw holding the end of the spring for a
reference point).
C)Holding the 3/4 inch open end wrench with one
hand, use your other hand, with the 9/16" box end
wrench loosen the 9/16 inch bolt by turning it CCW.
D)Now you are ready to adjust the Counter Balance
Spring. You turn the door boss spring holder with
the 3/4 inch open end wrench so that the door bar
(E) will stay balance and horizontal with the floor
of the Dri-Lab. Tighten the 9/16 inch bolt before
releasing pressure on the 3/4 inch wrench for each
adjustment.
Dri-Lab-08/91
Rl-l/99 4-4-B
~~I:: __________________________________________________________vacuum/AtmosPheres

Table 4-1
Troubleshooting Dri-Lab

Problem Test Solutions

I. Glove box does not _ Check leak test _ New gloves.


hold pressure or procedures for _ Tighten loose con-
unable to establish glove box. nections into
low oxygen levels _ Visually inspect glove box.
(bad atmosphe-re). gloves for holes or _ Clean or replace
damage; inspect purge exhaust
purge exhaust valve. valve.

II. Pressure decreases • Dirty/damaged • Clean or replace


in glove box when inside door O-ring. valves/O-ring.
evacuating anti- • Defective anti-
chamber. chamber refill
valve - can be
or eliminated from
problem by plugging
Oxygen levels hole inside Dri-Lab.
increased when
opening outside anti-
chamber door.

III. Atmosphere deterior-


ates inside glove box
_ Dirty/damaged out-
side door O-ring.
• Clean or replace
O-ring.
when inside ante-
chamber door is opened
and outside door is
_ Insufficient tension
on outside door
clamp.
- Increase tension
of outside door
clamp.
closed.

IV. Excessive pressure


inside glove box. -• Inspect purge inlet
valve.
Inspect purge exhaust
_ Clean or replace
purge inlet
valve.
valve for blockage. _ Clean or replace
purge exhaust
valve.

4-5 Dri-Lab-08/85
VAC _ _ __ ._ _ _ _ _ Vacuum/Atmospheres

Section 5

PARTS AND ACCESSORIES

REPLACEMENT POLICY

Vacuum/Atmospheres Company warrants all parts in the


HE, DLX and GBX series Dri-Labs. All parts or assemblies
ins taIled. in these Dri-Labs, whether or not they are
built by VAC, are warranted under the Warranty in
Appendix C.

SPARE PARTS

VAC spare part numbers are listed in Tables 0-1 and D-2
of Appendix o. To order spare or replacement parts,
contact Vacuum/Atmospheres Company direct.

ACCESSORIES

Refer to Appendix E for instructions on those accessories


provided with Dri-Lab.

Rl-9/99 5-1 Ori-Lab-08/85


~~I:: _______________________________________________________vacuum/AtmosPheres

APPENDIXES
Appendix A

Specifications And Dimensions

Specifications and dimensions are as outlined below. These


details are standard and some may not apply to custom systems.

GLOVE BOX

Construction:
(GBX-series) Modular structure with elastomer-gasketed
end panels and full-view front window for
ease of removal and replacment. All
interior corners are 3/8-in. minimum
radius; no seams, cracks, or crevices.
Additional box modules may be added at any
time. Aluminum antechamber may be moved
to either end.

(HE-series) Modular structure with elastomer-gasketed


end panels and full-view front window for
ease of removal and replacement.
Additional box modules may be added at any
time. Antechamber may be moved to either
end.

(DLX-series) One-piece structure with elastomer-


gasketed front window for ease of removal
and replacement. All interior corners are
1/2-in. minimum radius; no seams, cracks, or
crevices.

Material:
(GBX-series) 12-guage, Type 304 stainless steel inside
and textured paint outside.

(HE-series) 3/16-in. Type 6061 brushed aluminum inside


and textured paint outside, or II-gauge,
Type 304 stainless steel.

R2-10/98 A-l Dri-Lab-08/85


~C _________ _ _ _ Vacuu m/Atmospheres

Appendix A (cont'd)

Specifications And Dimensions

(DLX-series) 12-gauge, Type 304 stainless steel inside


and textured paint outside.

Window: Scratch and chemically resistant, optically


clear, 1/4-in. Lexan with high-impact
resistance; or safety glass.

Ports/Gloves: One pair of 9-in. glove ports, 18-in. on


center. No. 8B3032 butyl rubber gloves
(optional) 15- or 30- mm thick, ambi-
dextrous or formed left and right hands.

Lighting:
(GBX-series) One 30 W, external flourescent tube in a
separate housing on top of full-view
front panel. (Optional)

(HE-series) Skylight panel, 26-1/2-in. long x 14-1/2-in.


wide. Two 20 W, external flourescent tubes
in a separate housing on top of the glove
box (optional). Light produces 60 foot-
candles on glove box floor. Separate AC
cord is provided.

(DLX-series) One 30 W, external flourescent tube in a


separate housing on tip of full-view front
panel (optional).

Electrical
Outlets:
(GBX-series) Typically one duplex, 115 V, 15 A outlets.

(HE-DLX-series) Typically two duplex, 115 V, 15 A outlets.

R2-10/98 A-2 Dri-Lab-08/85


~c _____________.____________ Vacuum/Atmospheres

Appendix A (Cont'd)

Specifications And Dimensions

Feedthrough
Ports:
(GBX-series) Four 1/4-in. FPT couplings.
One 1/2-in. FPT coupling for hygrometer
probe.
Two 1/4-in. FPT couplings for oxygen
sample lines.

(HE-DLX-series) Four 1/2-in. FPT couplings.


Two 1-1/2-in. circulation ports.
One 1-in. FPT coupling for bubblers
One 1/2-in. FPT coupling for hygrometer
probe.
One 1/4-in. FPT coupling.

Test &
Certification: No detectable leaks at +8-in. water column
helium and sniffed with a helium mass
spectrometer with a calibrated sensitivity
-8 .
of 3 x 10 std. cclsec (the sniff probe
sensitivity is less than 1 x 10
-5 std.
ccl sec).

ANTECHAMBER

Construction: High-vacuum design, O-ring sealed doors


and valves. TIG-welded structure.

Material:
(GBX-series) 1/8-in., Type 5052-H32 aluminum, textured
paint on outside only.

(HE-series) 1/8-in., Type 6061 aluminum or 12-gauge,


Type 304 stainless steel, textured paint
on outside only.

R2-10/98 A-3 Dri-Lab-08/85


~C _ _ _ __ _ _ _ Vacuum/Atmospheres

Appendix A (Cont'd)

Specifications And Dimensions

(DLX-series) 12-gauge, Type 304 stainless steel,


textured paint on outside only.

Vacuum
3
Capability: One micron (1 x 10- torr).

Size: is-in. diameter x 24-in long.

Doors: Single, center-clamped, a-ring sealed,


counterbalanced vertical action.

Gauge: 2-1/2-in. compound Bourdon tube, dial-type.

Tray: 23-in long x 12-in. wide extending ii-in


beyond each end, mounted on ball bearing
slide.

Connections: i-in evacuation valve, 1/4-in. refill valve.

Test &
Certification: No detectable leaks at full vacuum with
helium mass spectrometer calibrated at
3 x 10- 8 std. cc/sec.

STAND (Optinal)

Construction: Table top stand with removable legs, or


tubular frame for bolting on Dri-Lab.

Material: Mild steel.

R2-10/98 A-4 Dri-Lab-08/8S


VAl:: Vacuum/Atmospheres

Appendix B
Special Schematics or Diagrams

B-1 Dri-Lab-08/85
VAt: · - - - - - - - - -_ _---Vacuum/Atmospheres

FIGURE B- 2
SCHEMATIC DIAGRAM OF JUNCTION BOX

BLACK
BLACK

NICKEL PLATED
SCREWS

WHITE
WHITE

B-2 Dri-Lab-08/85
VACUUM/ATMOSPHERES
4652 West Rosecrans Avenue
P.O. Box 1043
Hawthorne, CA 90250-6896
(310) 644-0255
FAX: (310) 970-0980

IMPORTANT
SERVICE BUlLEllN

READ CAREFULLY

Dear Customer:

Vacuum/ Atmospheres Company wishes to continue to provide you with the very best service possible.
Recent changes in environmental laws now require some changes in ollr "returned goods" pOlicies.

Before any item may be returned for repair or replacement, a Returned Goods Authorization Number
(RGA) must be obtained from the VAC Sales Department. Be prepared to provide information about the
chemicals which the item to be returned has been exposed. VAC Sales may be reached at:

Telephone: (310) 644-0255 (8:00am - 5:00pm PST)

Fax: (310) 970-0980 (24 Hours)

The RGA Number must be shown on the packing slip accompanying the item and be marked on the
outside of the shipping container. Items without a RGA Number will not be accepted for repair or
replacement.

Ma.terial Safety Data Sheets (MSDS) for each chemical to which the returned item has been exposed,
must accompany the item being returned.

Any item being returned must be cleaned for safe handling before being shipped to VAC.
Documentation showing that all contamination has been removed must be provided. Vacuum
Pumps must be drained of all pump oil before being returned. Items that have not been cleaned and
made safe for handling WILL NOT BE ACCEPlED for repair or replacement.

If you have any questions, please call or fax VAC at the numbers listed above.

OVER
ROTRON BLOWERS

This document outlines the requirements for returning ROTRON blowers to Vacuum Atmospheres
Company (VAC). These requirements are applicable to all ROTRON blowers that have been put into
service or use.

The following guidelines and procedures for disassembly and decontamination of ROTRON blowers must
be completed before a Return Material Authorization (RGA) number can be issued.

Disassembly Procedure

It is recommended that the following guidelines and procedures be reviewed and approved by your
company Health & Safety Officer or other company official. These considerations should include a review
of material safety sheets (MSDS') of all materials the ROTRON blower has been exposed to before it is
disassembled and before a decontamination plan is detennined.

Tools Required

1. 5/32 Allen wrench


2. 3/8 socket wrench, 114 drive
3. 3/8 open end wrench
4. Rubber or wooden mallet
5. Appropriate safety equipment and material.
6. #2 Phillips screwdriver
7. #3 Phillips bit and impact type screwdriver

Steps

1. Remove the two end cap retainer screws using the 3/8 socket and the 3/8 open end wrench

2. Using the mallet to remove the end caps, strike the end caps outwards at the point where the retainer
screws were located. You must work on one side at a time, back and forth on the retainer point.

3. After removing both end caps, use the 5/32 Allen wrench on the center screw turning it (CAW) to
loosen the impeller from the shaft.

4. There are three #2 Phillips screws on one end. Remove the screws and the small retainer cap. Next,
remove the four large Phillips screws using the impact screwdriver.

5. Pull the case apart. Do not use a screwdriver to pry the case halves apart, you will damage them.
Now all ROTRAN blower parts are accessible.

Decontamination

Decontaminate all ROTRON blower parts with the appropriate solvents or other methods prescribed by
your company official.

Shipping

7. Do not reassemble the ROTRON blower after decontamination. After you receive an RGA number
from VAC, ship the ROTRON blower to V AC in its disassembled state.

ROTRON.DOC REV-B 1999


~~ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _v~um~~~~~

Appendix C
Warranty

This unit is warranted to be free from defect in factory


material and workmanship for a period of 1 year from
date of purchase, subject to normal wear, and freedom
from undue abuse during handling and operation.

This warranty applies only to new equipment that, after


shipment from the factory, has not been altered or
treated in any manner whatsoever, and does not extend to
trade accessories operated with VAC's own equipment.

VAC warrants that it will repair or furnish, FOB its


factory, a replacement provided a part is found to have
been defective at the time it was received and the
defective part is returned to the factory, charges
prepaid.

This warranty is the only warranty expressed, implied,


or statutory upon which said equipment is sold. All
other damages and warranties, statutory and otherwise,
being hereby expressly waived by purchaser.

Components purchased from other manufacturers and


included in the unit are subject to warranties as
offered by the manufacturer of said components; of these
components, certain expend~ble items are not covered;
others are warranted for 90 days; others are warranted
for 1 year.

C-1 Dri-Lab-08/85
~~ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _~_ _ _ _ _v~umwm~~e~

Appendix D
Spare Part Listings

Table D-1. Spare Parts List (HE-series)

Item Description Part No. Qty.

1 Lexan Front Panel 08651 1


2 1/211 Saf'ety Glass Front Panel 013545 1
3 Front Panel Gasket (all) 08698 1
4 End Panel Gasket (HE-43/553) 08699 1
5 End Panel Gasket (HE-243/453-2) 08700
6 End Panel Gasket (HE-453-6) 08615 1
7 Skylight Gasket (all) 08695 1
8 a-ring Antechamber 1 5" dia. 2633 2
9 a-ring over glove 2631 1
10 a-ring Glove Port (Lexan) 2744 1
11 Gasket Glove Port (glass) 013921 1
12 a-ring Inside Door Boss 2635 1
13 1/4" Antechamber Refill Valve 2534 1
14 1" Antechamber Evacuation Valve 2743 1
15 1-1/2" Circulation Valve 7416 1
16 Gauge, Vacuum/Pressure (antechbr.) 2600-2 1
17 30 mil Butyl Rubber Glove 9-3/4" -
Formed L & R 8B3032-L&R 1 pr
Ambidextrous 8B3032-A 1 pr
18 15 mil Butyl Rubber Glove 9-3/4" -
Formed L & R 8B1532-L&R 1 pr
Ambidextrous 8B1532-A 1 pr
19 Dri-Lab Filter Replacement Cartridge 1 211 2

D-1 Dri-Lab-08/85
Appendix D (Cont'd)

Table D-2. Spare Parts List (DL-series)

Item Description Part No. Qty.

1 Lexan Front Panel (DLX) 08651 1


2 Lexan Front Panel (DL) 013349 1
3 1/2" Safety Glass Front Panel (DLX) 013545 1
4 1/2" Safety Glass Front Panel (DL) 011461-03 1
5 Front Panel Gasket (DLX) 08698 1
6 Front Panel Gasket (DL) 013350 1
7 a-ring Antechamber 15" dia. 2633 2
8 a-ring over gloves 2631 1
9 a-ring Glove Port (Lexan) 2744 1
10 Gasket Glove Port (glass) 013921 1
11 a-ring Inside Door Boss 2639 1
12 1/4" Antechamber Refill Valve 2534
13 1" Antechamber Evacuation Valve 2743 1
14 1-1/2" Circulation Valve 7416 2
15 Gauge, Vacuum/Pressure (antechbr.) 2600 1
16 30 mil Butyl Rubber Glove 9-3/4" -
Formed L & R 8B3032-L&R 1 pr
Ambidextrous 8B3032-A 1 pr
17 15 mil Butyl Rubber Glove 9-3/4" -
Formed L & R 8B1532-L&R 1 pr
Ambidextrous 8B1532-A 1 pr
18 Dri-Lab Filter Replacement Cartridge 1211 2

D-2 Dri-Lab-08/85
Appendix D (Cont'd)

Table D-3. Spare Parts List (GBX-series)

Item Description Part No. Qty.

1 Lexan Front Panel (GBX) 08651 1


2 Front Panel Gasket (GBX) 08698 1
3 O-ring Antechamber 15" dia. 2633 3
4 O-ring Over Gloves 2631 2
5 O-ring Glove Port (Lexan) 2744 1
6 O-ring Inside Door Boss 2639 1
7 1/4" Antechamber Refill Valve 2534 1
8 1" Antechamber Evacuation Valve 2743 1
9 1-1/2" Circulation Valve 7416 2
10 Gauge, Vacuum/Pressure
(antechbr.) 2600-2 1
11 30 mil Butyl Rubcer Gloves
9-3/4" - Formed L & R 8B3032-L&R 1 pr
Ambidextrous 8B3032-A 1 pr
12 15 mil Butyl Rubber Glove
9-3/4" - Formed L & R 8B1532-L&R 1 pr
Ambidextrous 8B1532-A 1 pr
13 Dri-Lab Filter Replacement
Cartridge 1211 2

D-3 Dri-Lab-9/98
VAl:: _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres

Index

Aligning Dri-Lab, 2-1 Compound gage, 1-2


Adjusting gloves, 2-2 Connections
Accessories, 4-4, 5-1, E-1 gas, 1 - 1 - 1 _. 2, 3 - 1
Acorn nuts, 2~2, 4-1 electrical, 1 -1 _. 1 2 1

Antechamber wa ter, 1 1 - 1 -·2 ,


evacuate procedure, 3-2 Contents r ii
door assembly, 4-3 Corrosive materials, 2 5
refill procedure, 3-2 Clamp
specifications, A-3 stainless steel, 2-3
maintenance, 4-2 Cleaners, 4-1
Appendixes, A 1 - E·1 Cleaning (see Maintenance)
Application (Dri-Lab), 1-1
Area (working) r 1-1 A-1 Diethylzinc test, 2-7
Argon gas r 1 1 Dimensions (see Specifications)
Assembly Door
Dri -Lab, 1-2 assembly (see Antechamber)
Atmosphere (see Establishing tension I 4 -·2
Inert Atmosphere)
Auxilliary feedthrough Electric lightbulb test, 2-6
ports f 1-2 Electrical
schematic diagram, B-1
Balance weight, 4-3 utility requirements, 2-1
Bead Establishing inert
glove, 2-2 - 2 3 atmosphere, 3-1 - 3-2
welded, 2-6 Evacuate procedure, 3-2
Blockage Evacuation
valve, 4-·5 valve, 1-2, 2-2, 2-4
Box Exhaust valve, 3-1
studs, 4-1
pressure (see Glove Box) Functional description, 1·1

Index-1 Dri-Lab-08/85
VAC ._ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _---:---:_ _ _ _ Vacuum/Atmospheres

Index (Cont'd)

Gas Leak testing, 2-2


inert, 1 -1, 2-1 Lexan panel
supply F 2 -2, 3-1 maintenance, 4-1
General List of Figures, iv
installation, 2-1 List-of Tables, iv
maintenance: 4-1
operation, 3 1 Maintenance, 4 --1 - 4-4
Gloves Moisture testing, 2-6
installation, 2 2 - 2 3
leaks, 2-5 Operation
replacement, 4-2 antechamber, 3-2
Glove box general, 3-1
description, 1-1 glove box, 3 --2
maintenance (see Maintenance) passing materials, 3-4 - 3-5
operation, 3 2 Overview; 1-1
user information, 3-2 Oxygen testing r 2-6
Glove port, 1-2, 2-1 a-ring
antechamber, 4-3
Halogen leak detection, 2-4 glove box, 2-2 - 2-3
Helium leak detection, 2-4
Hose
vacuum, 2-2 Panels
Lexan, 4-1
Inert atmosphere (see safety glass, 4-1
Establishing Inert Parts, 5-1
Atmosphere) Passing materials in/
Installation, 2 1 - 2-7 out, 3-4 - 3-5
Introduction, v Periodic maintenance, 4-1
In/Out procedures (see Passing
Materials In/Out) Refill procedure, 3-2
Refill valve, 1-2, 3-2
Jam nut, 4-2 - 4--3 Replacement policy, 5-1
Junction box, 1-2, 2-1, 2-6, B-1

Index -2 Dri-Lab-08/85
VAC _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres

Index (Contrd)

Replacing
gloves (see Gloves)
panels, 4-1
windows, 4-1

Schematic diagram, B-1


Skylight, 1-1 - 1-2, 2-1
Sliding tray, 1-1
Spare parts, 5-1
Spare parts listing, D-1 - D~2

Specifications 1 A--1 - A-2

Testing
leak, 2-2
moisture; 2-6
oxygen, 2-6
Titanium tetrachloride
test, 2-7
Troubleshooting, 4-1 - 4-5
Tubing, 2-1

utility requirements, 2-1

Vacuum
line, 2-2
pump, 2-1
Valves
inlet/exhaust, 3-1
(see Evacuation or
Refill)

Warranty, C-1

Index-3 Dri-Lab-08/85
VAC _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres

Appendix E
Accessories

E-1 Dri-Lab-08/85

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