Heseries 2993658665
Heseries 2993658665
TECHNICAL MANUAL
GBX, HE & DLX SERIES
DRI-LAB-R1-10/98
Contents
List of Figures iv
List of Tables iv
INTRODUCTION v
1• OVERVIEW • • 1-1
Application • 1-1
Functional Description 1 -1
2. INSTALLATION. · 2-1
General · 2-1
Customer-Furnished Items · 2-1
utility Requirements . · 2-1
Electrical · 2-1
Vacuum Line · 2-2
Gas Supply o 2-2
Installing the Gloves • 2-2
Leak Testing · 2-2
Leak In Gloves · 2-5
Oxygen and Moisture Testing · 2-6
Electric Lightbulb Test · 2-6
Welding Chamber Test · 2-6
Titanium Tetrachloride Test · 2-7
Diethylzinc Test · 2-7
3. OPERATIONS · 3-1
General · 3-1
Establishing An Inert Atmosphere . · 3-1
Antechamber . · 3-2
Evacuate/Refill Procedure • 3-2
Glove Box · 3-2
Passing Materials In/Out of Dri-Lab · 3-3
ii Dri-Lab-08/85
_ _ _ Vacuum/Atmospheres
Contents (Cont'd)
APPENDIXES
A. Specifications and Dimensions · A-1
B. Special Schematics or Diagrams . · B-1
Schematic Diagram of Junction Box . · B-2
C. Warranty · C-1
D. Spare Parts Listings · D-1
E. Accessories · E-1
INDEX Index-1
iii Dri-Lab-R2-1/99
. _~~_ Vacuum/Atmospheres
LIST OF FIGURES
Figures
LIST OF TABLES
Table
iv Dri-Lab- R2-1/99
c_ _ _ _ _ _ Vacuum/Atmospheres
INTRODUCTION
Vacuum/Atmospheres Company
P. O. Box 1043
4652 West Rosecrans Avenue
Hawthorne, CA 90250-6896
Telephone: (310) 644-0255
FAX: (310) 970-0980
http://www.vac-atm.com
email:tfitz@vac-atm.com
v Dri-Lab-R2-9/98
VAC _ _ __ Vacuum/Atmospheres
Section 1
OVERVIEW
APPLICATION
The VAC HE-series (or GBX and DLX-series*) Dri-Lab provides a
working area of inert atmosphere nearly free of moisture, oxy-
gen, and if desired, nitrogen. Any material that is sensitive
to moisture, oxygen, or nitrogen may be worked with freely. The
Dri-Lab is designed for use of argon gas as the principal inert
gas, and also may use helium, nitrogen, or any combination of
these gases.
FUNCTIONAL DESCRIPTION
The HE-series Dri-Lab consists of an hermetically sealed glove
box, a side-mounted antechamber, and a full-view window (Figure
1-1). The glove box and antechamber share an entry/exit airlock
door, used for passing materials in and out without disturbing
the glove box atmosphere. All materials are passed in and out
of the glove box on a sliding tray (located on the bottom
of the antechamber). The IS-in. I.D. antechamber, with one
interior and one exterior door, permits large objects to be
passed into and out of the glove box.
Two 9-in. glove ports and butyl rubber gloves, mounted in the
full-view window, provide easy access to all areas of the glove
box. An assortment of gas, water, and electrical connections
are also provided in the rear of the glove box wall. (Refer to
Appendix A for Dri-Lab specifications.)
*For simplicity, this manual will address the HE- rather than
the GBX- and DLX-series Dri-Lab. Both models are essentially
the same. The HE-series has removable end panels and a skylight;
the DLX-series does not. The HE-series is available in aluminum
or stainless steel; the GBX- and DLX-series are available only
in stainless steel. GBX-series has removable end panel~ and no
skylight.
R3~9/99
1-1 Dri-Lab-08/8S
c ._ _ _. ____ ._ _ _ _ _.... _.......... _ _ _ _ _Vacuum/Atmospheres
.. __ - - _ . _ - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - ,
..
FIGURE '1-'1
~)
.@
C.COMPO~ GAUGE.
o p
D. EVACUATION VALVE AND CONNECTION TO IACWM
PUMP.
V
\ ~r@ ~@@ (@ V
•
•
N. FD. THRU PORT FOR OPTIONAL H'rGROMETER.
Section 2
INSTALLATION
GENERAL
Before starting the installation, read all instructions com-
pletely. Instructions are standard and some may not apply to
custom systems.
A. Remove components from crate. Do not use junction box or
glove ports to lift Dri-Lab.
B. Remove all packing, tape, and shipping blocks or bands.
C. Place Dri-Lab stand in .desired location.
D Place Dri-Lab on stand.
1) Align side opposite antechamber flush with stand end.
2) Align back side flush with stand back (single-sided Dri-
Lab). Align front and back symmetrically on stand width
(double-sided Dri-Lab).
CUSTOMER-FURNISHED ITEMS
Before installation is possible, the customer must furnish the
following items:
A. Vacuum pump, 3 to 5 cfm.
B. 3/B-in. copper or stainless steel tubing for inert gas.
C. utilities, as noted.
UTILITY REQUIREMENTS
Electrical
A. Skylight: 115 V, 5 A.
B. Glove Box Junction-Box: 115 V, 15 A (see Appendix B for
system schematic diagrams).
C. Vacuum Pump: 115/230 V or as required by size and rating of
vacuum pump.
2-1 Dri-Lab-OB/B5
c _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres
Vacuum Line
Use 1-in. O.D. vacuum hose from evacuation valve on the ante-
chamber to the vacuum pump (user supplied).
Gas Supply
If your Dri-Lab was not purchased with a VAC pressure control
system, the gas supply should be regulated at 20 psi and con-
nected to a main shutoff valve (user supplied) at a Dri-Lab
feedthrough. VAC recommends customer use as pure a gas as eco-
nomically or conveniently practical.
LEAK TESTING
I I
Note
Prior to leak testing, if panels were
removed to install equipment inside Dri-
Lab, reinstall panel acorn nuts at 26 to
28 in.-lb.
2-2 Dri-Lab-08/85
. - - - - - - -....... - . - - - - -_ _ _Vacuum/Atmospheres
FIGURE 2-1
B. GUJV{.
c. o - /~/NG.
D. I~L~CK /JLASTIC 7AP~.
CA) E. CLAMP.
I
/
-~
\
8
'----
®
/
/
2-3 Dri-Lab-OS/85
VA C~ _ _~ _____~_~_ _ ~ _ ~______ VaclJum/Atmospheres
WARNING I
Do not use halogen leak detection equip-
ment for leak testing. Halogens are
harmful to certain materials used in the
construction of VAC equipment (i.e.,
copper and rubber). VAC will not assume
responsibility for systems tested by
methods other than defined in this
manual.
TEST ONE
VAC recommends using helium leak detection equipment. If no leak
detector ~s available, the follow~ng test procedures are recom-
mended (keep Dri-Lab and room temperature constant throughout
testing) :
A. Connect a source of gas to one of the connections in the
back of the Dri-Lab (see Figure 2-2).
B. Close antechamber outside door; close evacuation and refill
valves.
C. Open inside antechamber door.
D. Slowly pressurize Dri-Lab. The gloves will be forced out.
E. Stop pressurizing when gloves are almost horizontal. (Let
gloves break slightly from horizontal.)
F. Place a stool or chair with a ruler taped on its back to
within 1/4 in. of glove finger tip. Note reference point
and wait approximately 1 hr.
o If system leaks, gloves will fall more than 1/8 in.
Locate and seal leaks. Repeat test until gloves remain
steady for several hours.
a Relieve pressure on gloves after testing.
o Replace plugs removed for leak testing with teflon-
taped brass plugs (user supplied).
2-4 Ori-Lab-R2-9/99
c____ _ _ _ Vacuu m/Atmospheres
TEST TWO
TEST THREE
FIGURE 2 - 2
LEAK TESTING DRI-LAB WITHOUT DETECTOR
Leak in Gloves
Gloves are vulnerable to leaks, especially in the fingertips. To
check for leaks:
A. Stretch rubber to detect small holes.
B. Check for cracks near glove port.
C. Inflate glove, twist wrist, force into pail of water, and
look for source of bubbles.
INotel
Replace gloves at the first sign of
deterioration. VAC recommends wearing
protective gloves over Dri-Lab gloves if
working processes include handling sharp,
hot, or corrosive materials.
2-5 Dri-Lab-08/85
c _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres
WARNING I
VAC does not assume responsibility for
accidents resulting from mishandling of
materials used in the following tests.
atmosphere. Note that the ppm levels stated in these tests are
estimates only.
2-6 Dri-Lab-08/85
_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres
Diethylzinc Test
2-7 Dri-Lab-08/85
_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres
Section 3
OPERATIONS
GENERAL
The instructions that follow are for basic operation of the Dri-
Lab without a Dri-Train automatic recirculating system. Opera-
ting instructions for the combined Dri-Lab/Dri-Train are found in
the Dri-Train manual.
FIGURE 3-1
ESTABLISHING AN INERT ATMOSPHERE
/
HE- LAB
ANTECHAMBER
GAS ~
PURGE
INLET ~ REFILL
3-1 Dri-Lab-08/85
_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres
ANTECHAMBER
Evacuate/Refill Procedure
Any time the antechamber is exposed to atmosphere, the following
procedure must be used before opening the inside antechamber door
to the glove box:
A. Both antechamber doors must be closed.
B. Refill valve must be closed.
C. Open evacuation valve and evacuate to 50 microns (minimum).
E. Close evacuation valve.
F. Open refill valve.
Since the antechamber refills from the glove box, additional gas
will be required to make up for the decrease in pressure in the
glove box. Add gas via the glove box inlet valve to make up for
this decrease in pressure.
GLOVE BOX
Be aware of the following items when using the Dri-Lab glove box:
• Watch the gloves during antechamber evacuation. If the
gloves are drawn into the glove box, check the inside ante-
chamber door and/or refill valve; either one may be open.
Close the door and refill valve to the antechamber.
• Keep the antechamber doors and valves tightly closed when
not in use.
3-2 Dri-Lab-08/85
c ._ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres
3-3 Dri-Lab-08/85
_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres
FIGUR'E 3-2
" 0
o u ///
(I C CI 0
/
STEP 4 - ARTICLE IS IN Ale
- BOTH DOORS STILL CLOSED
'---0-0--:::0=--=0---:0'---=0--' /
- Alc IS BACKFILLED WlTI-I ATMOSPHERE
n 0 0 0 0
FROM DRI - LAB. o -0 0 0 (1 0 0 '
- DR/-LAB ¥ Alc HAVE INERT ATMOSPHERE O, 0 n "(,J
.i C' 0 0 () 0., 0 /
o 0 0 0 0 aU /
oo 0 °0 0 '-
) 0
nCO,
0 0
Go~
0 ~c"
0
,u,,',
,.' 'j
o (10<)° 0 °
C)_ ') ° () 0
°°
~
\)" ,-, - 0
~
1
" 0- 0 ,0
NDTE!3: c ou C,O, c"nu
:) :) ~ '-' I:) "\,, ,-,' 0 ('
=
~) " )
1-0 VALVE OPEN.
) (») I)') "j 1
2- VALVE CLOSE.
3 - KEEP Alc DOORS CLOSED UNLESS IN USE.
3-4 Dri-Lab-08/85
._ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres
FIGURE 3 - 3
PROCEDURE FOR PASSING MATERIALS OUT OF DRI- LAB
o 0 0 (' c'
o 0 (;
o o-().~ c.
o l· U
o 0 u 0
c (; C 0 u-,
00 0 l i lv c
o c c
/
,J
NOTES:
/- 0 VALVE OPEN.
2 _~ VALVE CLOSE.
3 _ KEEP A C DOORS CLOSE UNLESS IN USE.
3-5 Dri-Lab-08/85
_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres
Section 4
MAINTENANCE AND TROUBLESHOOTING
GENERAL
Maintenance of the HE-series Dri-Lab is uncomplicated due to
relative simplicity of the unit's design and component selection.
However, standard safe practices should always be observed during
maintenance.
Periodic Maintenance
Visual inspection of Dri-Lab O-rings, gloves, and vacuum system
should be performed to ensure tightness of glove box and proper
operation of the vacuum system. (See also Section 2-5, Leak
Test. )
Lexan Panels
Clean panel with a clean cloth and either soap and water or a
commercial glass cleaner.
4-1 Dri-Lab-08/85
c _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ Vacuum/Atmospheres
Dri-Lab
Use mild soap and water to clean the outside painted surfaces.
Dry the unit with compressed air. At recommended 3-mo intervals,
all valves, fittings, lines, tubing, and connections should be
inspected for general mechanical and electrical integrity.
Antechamber
Check the sealing a-rings periodically and replace when worn or
damaged. Clean antechamber doors periodically with a mild
solvent, and coat the sealing surfaces with a light coat of
vacuum grease. If required, adjust antechamber door tension as
follows:
A. Close door and loosen jam nut at door clamp (Figure 4-1).
Loosen nut 2.
B. Open door and rotate door clockwise (increase tension) or
counterclockwise (decrease tension).
C. Close door to fully closed position - firm pressure should
be required to close door.
D. Tighten nut 2 and then jam nut.
4-2 Dri-Lab-08/85
~~ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _v~umwmoo~~
Accessories
For maintenance of purchased accessories, refer to accessory
instruction sheets in Appendix E.
TROUBLESHOOTING
Failures in operating the Dri-Lab may occur in one or more of the
following areas: a) glove box, b) vacuum system, or c) ante-
chamber. Check these areas first. Table 4-1 provides additional
information in locating and correcting problems.
~ e
'~
I!
G')
c:
~
.+::0-
I :x:J
.+::0-
m
~
I
...L
M - DOOR BOSS
N - SHOULDER BOLT.
o- DOOR STOP.
P- HEX.HD.BOlT.
F
Q - TORQUE ADJUSTER.
R - pm HD.SCREW.
S - DOOR BAR SPRING
~
T- HEX.HD.BOlT. o
c
S? N c
"j' U - HEX.HD.BOLT. s::
S- V - LOCK WASHER. ~
O" s::
I
;0
Z - FLAT WASHER. o
(/)
0.1 '1J
I I
co fTl
;:0
~ fTl
(/)
1.0
Detailed Instruction For
Antechamber Door Adjustment
D<x>r Tension
Tools required:
! !NOTE! !
! !NOTE! !
Use a clamp on the end of the door bar (E) at the door
boss close to the window. This will keep the door bar
from flying up and back to the door stop, because of
the balance weight (D) and no door for counter balance.
D)To replace door clamp (F), install jam nut (K) until
it is fully seated against the door clamp shoulder.
E)Open the door clamp (F) fully then slowly turn CW
until you have engaged the threads in the door bar
(E). Now close the door clamp slowly to pick up the
door screw (G) while turning the door clamp CWo Let
the door handle move freely while turning. Turn the
door handle until it is as close to the door bar (E)
as possible. Now return the handle to the original
position and tighten jam nut (K) against door bar.
F)Refill antechamber and go to Tension Adjustment on
page one.
Table 4-1
Troubleshooting Dri-Lab
4-5 Dri-Lab-08/85
VAC _ _ __ ._ _ _ _ _ Vacuum/Atmospheres
Section 5
REPLACEMENT POLICY
SPARE PARTS
VAC spare part numbers are listed in Tables 0-1 and D-2
of Appendix o. To order spare or replacement parts,
contact Vacuum/Atmospheres Company direct.
ACCESSORIES
APPENDIXES
Appendix A
GLOVE BOX
Construction:
(GBX-series) Modular structure with elastomer-gasketed
end panels and full-view front window for
ease of removal and replacment. All
interior corners are 3/8-in. minimum
radius; no seams, cracks, or crevices.
Additional box modules may be added at any
time. Aluminum antechamber may be moved
to either end.
Material:
(GBX-series) 12-guage, Type 304 stainless steel inside
and textured paint outside.
Appendix A (cont'd)
Lighting:
(GBX-series) One 30 W, external flourescent tube in a
separate housing on top of full-view
front panel. (Optional)
Electrical
Outlets:
(GBX-series) Typically one duplex, 115 V, 15 A outlets.
Appendix A (Cont'd)
Feedthrough
Ports:
(GBX-series) Four 1/4-in. FPT couplings.
One 1/2-in. FPT coupling for hygrometer
probe.
Two 1/4-in. FPT couplings for oxygen
sample lines.
Test &
Certification: No detectable leaks at +8-in. water column
helium and sniffed with a helium mass
spectrometer with a calibrated sensitivity
-8 .
of 3 x 10 std. cclsec (the sniff probe
sensitivity is less than 1 x 10
-5 std.
ccl sec).
ANTECHAMBER
Material:
(GBX-series) 1/8-in., Type 5052-H32 aluminum, textured
paint on outside only.
Appendix A (Cont'd)
Vacuum
3
Capability: One micron (1 x 10- torr).
Test &
Certification: No detectable leaks at full vacuum with
helium mass spectrometer calibrated at
3 x 10- 8 std. cc/sec.
STAND (Optinal)
Appendix B
Special Schematics or Diagrams
B-1 Dri-Lab-08/85
VAt: · - - - - - - - - -_ _---Vacuum/Atmospheres
FIGURE B- 2
SCHEMATIC DIAGRAM OF JUNCTION BOX
BLACK
BLACK
NICKEL PLATED
SCREWS
WHITE
WHITE
B-2 Dri-Lab-08/85
VACUUM/ATMOSPHERES
4652 West Rosecrans Avenue
P.O. Box 1043
Hawthorne, CA 90250-6896
(310) 644-0255
FAX: (310) 970-0980
IMPORTANT
SERVICE BUlLEllN
READ CAREFULLY
Dear Customer:
Vacuum/ Atmospheres Company wishes to continue to provide you with the very best service possible.
Recent changes in environmental laws now require some changes in ollr "returned goods" pOlicies.
Before any item may be returned for repair or replacement, a Returned Goods Authorization Number
(RGA) must be obtained from the VAC Sales Department. Be prepared to provide information about the
chemicals which the item to be returned has been exposed. VAC Sales may be reached at:
The RGA Number must be shown on the packing slip accompanying the item and be marked on the
outside of the shipping container. Items without a RGA Number will not be accepted for repair or
replacement.
Ma.terial Safety Data Sheets (MSDS) for each chemical to which the returned item has been exposed,
must accompany the item being returned.
Any item being returned must be cleaned for safe handling before being shipped to VAC.
Documentation showing that all contamination has been removed must be provided. Vacuum
Pumps must be drained of all pump oil before being returned. Items that have not been cleaned and
made safe for handling WILL NOT BE ACCEPlED for repair or replacement.
If you have any questions, please call or fax VAC at the numbers listed above.
OVER
ROTRON BLOWERS
This document outlines the requirements for returning ROTRON blowers to Vacuum Atmospheres
Company (VAC). These requirements are applicable to all ROTRON blowers that have been put into
service or use.
The following guidelines and procedures for disassembly and decontamination of ROTRON blowers must
be completed before a Return Material Authorization (RGA) number can be issued.
Disassembly Procedure
It is recommended that the following guidelines and procedures be reviewed and approved by your
company Health & Safety Officer or other company official. These considerations should include a review
of material safety sheets (MSDS') of all materials the ROTRON blower has been exposed to before it is
disassembled and before a decontamination plan is detennined.
Tools Required
Steps
1. Remove the two end cap retainer screws using the 3/8 socket and the 3/8 open end wrench
2. Using the mallet to remove the end caps, strike the end caps outwards at the point where the retainer
screws were located. You must work on one side at a time, back and forth on the retainer point.
3. After removing both end caps, use the 5/32 Allen wrench on the center screw turning it (CAW) to
loosen the impeller from the shaft.
4. There are three #2 Phillips screws on one end. Remove the screws and the small retainer cap. Next,
remove the four large Phillips screws using the impact screwdriver.
5. Pull the case apart. Do not use a screwdriver to pry the case halves apart, you will damage them.
Now all ROTRAN blower parts are accessible.
Decontamination
Decontaminate all ROTRON blower parts with the appropriate solvents or other methods prescribed by
your company official.
Shipping
7. Do not reassemble the ROTRON blower after decontamination. After you receive an RGA number
from VAC, ship the ROTRON blower to V AC in its disassembled state.
Appendix C
Warranty
C-1 Dri-Lab-08/85
~~ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _~_ _ _ _ _v~umwm~~e~
Appendix D
Spare Part Listings
D-1 Dri-Lab-08/85
Appendix D (Cont'd)
D-2 Dri-Lab-08/85
Appendix D (Cont'd)
D-3 Dri-Lab-9/98
VAl:: _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres
Index
Index-1 Dri-Lab-08/85
VAC ._ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _---:---:_ _ _ _ Vacuum/Atmospheres
Index (Cont'd)
Index -2 Dri-Lab-08/85
VAC _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres
Index (Contrd)
Replacing
gloves (see Gloves)
panels, 4-1
windows, 4-1
Testing
leak, 2-2
moisture; 2-6
oxygen, 2-6
Titanium tetrachloride
test, 2-7
Troubleshooting, 4-1 - 4-5
Tubing, 2-1
Vacuum
line, 2-2
pump, 2-1
Valves
inlet/exhaust, 3-1
(see Evacuation or
Refill)
Warranty, C-1
Index-3 Dri-Lab-08/85
VAC _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _Vacuum/Atmospheres
Appendix E
Accessories
E-1 Dri-Lab-08/85