PDF#08-0247: QM=Indexed(I); d=Guinier(114.
6mm); I=Densitometer
Sulfur, syn
S Yellow
Radiation=CuKa1 Lambda=1.5405 Filter=
Calibration= 2T=11.498-69.346 I/Ic(RIR)=
Ref: de Wolff, P., Technisch Physische Dienst, Delft, The Netherlands.
ICDD Grant-in-Aid
Orthorhombic - Powder Diffraction, Fddd (70) Z=128 mp=112.8$DE
CELL: 10.45 x 12.84 x 24.46 <90.0 x 90.0 x 90.0> P.S=oF128 ($GA) (S)
Density(c)=2.076 Density(m)=2.070 Mwt=32.06 Vol=3281.99 F(30)=29.7(0.023,44/0)
Ref: Ibid.
Strong Lines: 3.85/X 3.21/6 3.44/4 3.33/3 3.11/3 3.08/2 2.84/2 5.76/1 2.62/1 2.42/1
NOTE: Validated by calculated pattern 24-733.
Other data 21-1066.
To replace 1-478.
2-Theta d(�) I(v) h k l Theta 1/(2d) 2pi/d n^2
11.498 7.6900 3.0 1 1 1 5.749 0.0650 0.8171
15.370 5.7600 9.0 1 1 3 7.685 0.0868 1.0908
15.588 5.6800 4.0 0 2 2 7.794 0.0880 1.1062
18.469 4.8000 2.0 2 0 2 9.234 0.1042 1.3090
21.187 4.1900 2.0 1 1 5 10.593 0.1193 1.4996
21.873 4.0600 11.0 2 2 0 10.937 0.1232 1.5476
22.723 3.9100 12.0 1 3 1 11.362 0.1279 1.6070
23.082 3.8500 100.0 2 2 2 11.541 0.1299 1.6320
24.921 3.5700 9.0 1 3 3 12.460 0.1401 1.7600
25.879 3.4400 45.0 0 2 6 12.939 0.1453 1.8265
26.346 3.3800 5.0 2 2 4 13.173 0.1479 1.8589
26.749 3.3300 29.0 3 1 1 13.375 0.1502 1.8868
27.769 3.2100 72.0 0 4 0 13.884 0.1558 1.9574
28.680 3.1100 31.0 3 1 3 14.340 0.1608 2.0203
28.966 3.0800 22.0 1 3 5 14.483 0.1623 2.0400
29.159 3.0600 3.0 0 0 8 14.580 0.1634 2.0533
31.452 2.8420 24.0 0 4 4 15.726 0.1759 2.2108
33.305 2.6880 3.0 3 3 1 16.652 0.1860 2.3375
33.497 2.6730 3.0 2 4 2 16.748 0.1871 2.3506
34.182 2.6210 21.0 1 3 7 17.091 0.1908 2.3972
34.276 2.6140 6.0 4 0 0 17.138 0.1913 2.4037
34.896 2.5690 12.0 3 3 3 17.448 0.1946 2.4458
35.876 2.5010 12.0 2 4 4 17.938 0.1999 2.5123
37.057 2.4240 22.0 3 1 7 18.528 0.2063 2.5921
37.376 2.4040 3.0 4 0 4 18.688 0.2080 2.6136
37.850 2.3750 6.0 4 2 2 18.925 0.2105 2.6456
37.999 2.3660 7.0 3 3 5 19.000 0.2113 2.6556
39.347 2.2880 10.0 0 2 10 19.674 0.2185 2.7461
40.700 2.2150 3.0 2 0 10 20.350 0.2257 2.8367
42.070 2.1460 7.0 1 1 11 21.035 0.2330 2.9279
42.780 2.1120 18.0 3 1 9 21.390 0.2367 2.9750
43.080 2.0980 4.0 2 2 10 21.540 0.2383 2.9948
43.983 2.0570 4.0 5 1 1 21.991 0.2431 3.0545
44.346 2.0410 4.0 2 4 8 22.173 0.2450 3.0785
45.233 2.0030 4.0 3 5 3 22.617 0.2496 3.1369
45.594 1.9880 8.0 4 0 8 22.797 0.2515 3.1606
46.358 1.9570 4.0 2 6 2 23.179 0.2555 3.2106
47.149 1.9260 4.0 4 4 4 23.574 0.2596 3.2623
47.834 1.9000 16.0 5 1 5 23.917 0.2632 3.3069
49.041 1.8560 4.0 3 1 11 24.521 0.2694 3.3853
49.554 1.8380 4.0 1 5 9 24.777 0.2720 3.4185
49.989 1.8230 8.0 2 4 10 24.995 0.2743 3.4466
51.252 1.7810 26.0 2 6 6 25.626 0.2807 3.5279
52.100 1.7540 18.0 5 3 5 26.050 0.2851 3.5822
53.044 1.7250 18.0 6 0 2 26.522 0.2899 3.6424
53.955 1.6980 18.0 1 3 13 26.977 0.2945 3.7003
55.114 1.6650 5.0 6 2 2 27.557 0.3003 3.7737
55.367 1.6580 5.0 2 0 14 27.683 0.3016 3.7896
55.768 1.6470 14.0 3 5 9 27.884 0.3036 3.8149
56.705 1.6220 14.0 6 2 4 28.353 0.3083 3.8737
57.283 1.6070 14.0 4 0 12 28.642 0.3111 3.9099
57.518 1.6010 5.0 6 0 6 28.759 0.3123 3.9245
57.754 1.5950 10.0 4 6 4 28.877 0.3135 3.9393
59.052 1.5630 5.0 4 4 10 29.526 0.3199 4.0200
59.938 1.5420 5.0 3 7 5 29.969 0.3243 4.0747
60.414 1.5310 5.0 0 0 16 30.207 0.3266 4.1040
61.119 1.5150 5.0 3 5 11 30.560 0.3300 4.1473
61.615 1.5040 5.0 1 7 9 30.807 0.3324 4.1777
62.258 1.4900 5.0 2 8 4 31.129 0.3356 4.2169
62.963 1.4750 5.0 6 2 8 31.482 0.3390 4.2598
63.637 1.4610 5.0 7 1 3 31.818 0.3422 4.3006
64.727 1.4390 11.0 4 4 12 32.363 0.3475 4.3664
65.494 1.4240 11.0 0 8 8 32.747 0.3511 4.4123
65.753 1.4190 5.0 7 1 5 32.877 0.3524 4.4279
67.251 1.3910 6.0 3 5 13 33.625 0.3595 4.5170
68.881 1.3620 6.0 5 7 3 34.441 0.3671 4.6132
69.346 1.3540 11.0 7 3 5 34.673 0.3693 4.6405