Chapter Four: Mix Design
Chapter Four: Mix Design
Chapter Four
Mix Design
Introduction
Bituminous mixes are used in the surface layer of road and airfield pavements. The mix is composed
usually of aggregate and asphalt cements. Some types of bituminous mixes are also used in base coarse.
There are several methods to design the Asphalt Mix, the common methods are Marshall Stability,
Hveem Stabilometer and Supper Pave tests.
1. Resistance to permanent deformation: The mix should not be displaced when subjected to traffic
loads. The resistance to permanent deformation is more important at high temperatures.
2. Fatigue resistance: the mix should not crack when subjected to repeated loads over a period of time.
3. Resistance to low temperature cracking: This mix property is important in cold regions.
4. Durability: the mix should contain sufficient asphalt cement to ensure an adequate film thickness around
the aggregate particles. The compacted mix should not have very high air voids, which accelerates the aging
process.
5. Resistance to moisture-induced damage.
6. Skid resistance.
7. Workability: the mix must be capable of being placed and compacted with reasonable effort.
8. Low noise and good drainage properties: If the mix is to be used for the surface (wearing) layer of
the pavement structure.
In Marshall Mix Design method, the resistance to plastic deformation of a compacted cylindrical specimen
of bituminous mixture is measured when the specimen is loaded diametrically at a deformation rate of 50
mm per minute.
The Marshall stability of the mix is defined as the maximum load carried by the specimen at a standard test
temperature of 60C. The flow value is the deformation that the test specimen undergoes during loading up
to the maximum load. Flow is measured in 0.25 mm units. In this test, an attempt is made to obtain optimum
binder content for the type of aggregate mix used and the expected traffic intensity.
                                                                                                   Page 1
Highway Materials
Objective
1. To prepare standard specimens of asphalt concrete for measurement of stability and flow in the
     Marshall apparatus.
2. To determine density, percentage air voids, and percentage of aggregate voids filled with binder.
3. To find the optimum binder content in the mix.
Apparatus
1. Specimen mold 101.6 mm diameter and 76.2 mm height with extension collar and base plate
2. Specimen extractor
3. Compaction hammer 4.536 kg weight, 457.2 mm drop
4. Specimen mold holder
5. Breaking head
6. Ring dynamometer assembly
7. Flow meter
8. Oven or hot plate
9. Mixing bowls
10. Water bath
11. Water tank balance
12. Thermometers                                        Marshall Sample               Water tank balance
13. Miscellaneous apparatus
Materials:
1. Coarse Aggregate
2. Fine Aggregate
3. Filler
4. Bitumen
Preparation of Material
1.   The aggregate, graded according to Iraqi Specification road mix (see Table 1 and Figure 1), is dried at
     105-110 oC and sufficient amount is weighed (about 1200 g) to give a height of 63.5 + 1.3 mm when
     compacted in the mould.
                                                                                                    Page 2
Highway Materials
2. The required quantity of bitumen is weighed out and heated to a temperature which will give a
    viscosity of 170 + 20 mm 2/s.
3. The aggregate is heated in the oven to a temperature not higher than 28⁰ C above the binder
    temperature.
Preparation of specimens:
1. The compaction mould assembly and rammer are cleaned and kept pre-heated to a
    temperature of 100C to 145C.
2. The heated aggregates and bitumen are thoroughly mixed at a temperature of 154 – 160Co.
3. Place the mixture in a preheated Marshall mould with a collar and base. Place filter paper on
    top and bottom of the sample.
4. Place the mould in a Marshall Compaction pedestal and compact the materials with a
    specified number of blows by the rammer on either side at temperature of 138 to 149Co.
5. After compaction, invert the mould. With the collar on the bottom, remove the base and
    extract the sample by pushing it out by the extractor.
6. Allow the sample to cool. Obtain the sample’s mass in air and submerged to measure density
    of specimen.
7. Preferably, five specimens are required with two specimens having bitumen content above
    and two below the expected optimum content.
8. Specimens are heated to 60±1 Co, either in a water bath for 30 – 40 min or in an oven for 2
    hours.
                                                                                                 Page 3
Highway Materials
Testing of specimens:
   1. Remove the specimen from the water bath and place in the lower segment of the breaking head
       on the specimen and place the complete assembly in position on the testing machine.
   2. Place the flow meter over one of the post and adjust it to read zero.
   3. Apply the load at a rate of 50 mm/min until the maximum load reading is obtained.
                                                                                             Page 4
Highway Materials
    4. Record the maximum load reading in Newton and obtain the flow as recorded on the flow meter
        in units of 0.25 mm.
The binder content is determined with Marshall Stability, flow, void content, voids filled with binder and
density requirements for the mix being investigated.
Steps of Design
                                                                                                  Page 5
Highway Materials
                                                                                                      Page 6
Highway Materials
4. Low permeability
5. High stability
6. Difficult to compact
Dense-Graded Aggregate
Densest aggregate gradations give greatest durability and minimize air voids in bituminous materials.
According to the Iraqi specification (SCRB, 2007, R9), the asphalt concrete mixtures for base course
(type I), binder course (type II) and surface course (type IIIA or IIIB) shall be composed basically of
coarse aggregate, fine aggregate, mineral filler (if needed), and asphalt cement.
                                                                                                 Page 7
Highway Materials
The Iraqi SCRB (2009, R9) stated that contractor will be allowed the tolerances from the approved job-
mix formula shown in Table 2.
Blending of Aggregates
1. Numerical method
2. Trial and error
3. Basic formula
4. Graphical
                                                                                              Page 8
Highway Materials
Apparatus
1. A set of sieves.
2. Laboratory oven
3. Riffle box
4. Balance
Procedure
1. Place the aggregate under test in a heap. Divide it into four parts by quartering (passing vertical sections
   the two being at right angles to each other). This can also be done using a Riffle box. Divide it further
   into parts so as to obtain finally about 1.5 Kg of the aggregate sample.
2. Dry the aggregate in the oven at approximately 105 co for about 4 hours.
3. Clean and dry the set of sieves as desired. Find the weights of ovary sieves (empty) individually.
4. Place the sieves one above the other in a manner that the max. Aperture size will be at the top and the
   minimum aperture size will be at the bottom which will be just above the pan.
6. Shake the sieves (preferably by mechanical source) for a period not less than 2 minutes and not
   exceeding 7 minutes.
7. Remove the sieves from the shaker and find the weights of every sieve (containing aggregate particles)
   individually.
8. Enter all the above readings in the observation chart, and calculate the cumulative percentage passing
   for every sieve separately.
9. Plot a graph in a semi log paper. The aperture size will be plotted in the x axis which will be in
   logarithmic scale while the corresponding passing percentage will be plotted on the Y axis in ordinary
   scale. Draw the gradation curve.
10. Repeat the whole above procedure for the second and subsequent aggregate samples and plot the
    corresponding gradation curves.
                                                                                                      Page 9
Highway Materials
Blending of Aggregate
                                                                                                    Page 10
Highway Materials
                                                                                             Page 11
Highway Materials
         Percentage of                                                                 Design of
                           22% of     45% of     25 % of       8% of   Cumulative
                                                                                         spec.
         each fraction       A          B           C           D       grading
                                                                                        grading
              19.0            22        45          25           8       100.0            100
              13.2           18.7       45          25           8       96.7              90
               6.7           6.6       40.5         25           8       80.1              78
              4.75             0       31.5         25           8       64.5              61
              2.38             0       11.25      23.75          8       43.0              45
              1.18             0        4.5        17.5          8       30.0              30
              0.600            0         0         12.5          8       20.5              22
              0.300            0         0         7.5          7.6      15.1              16
              0.150            0         0         2.5          6.4       8.9              12
              0.075            0         0          0            4        4.0               6
Trial and error procedure: Vary the proportion of materials until the required aggregate gradation is
achieved.
A trial percentage of each aggregate source is assumed and is multiplied by the percentage passing each
sieve. These gradations are added to get the composite percentage passing each sieve for the blend. The
gradation of the blend is compared to the specification range to determine if the blend is acceptable. With
Where:
Pi = blend material passing sieve size i.
A, B, C, … = Percent of aggregates A, B, C, passing sieve i.
a, b, c, … = decimal fractions by weight of aggregates A, B, and C used in the blend, where the total is
1.00.
                                                                                                   Page 12
Highway Materials
1. Aggregate Gradation
 Sieve size      (19-9) mm           (9-4) mm        (4-0) mm        Filler    Desired blend          Mid Specification
   (mm)            P = 31              P = 46          P = 16        P=7         gradation                 Limits
    19.1                31             46              16              7               100                   100
    12.7                23             46              16              7               92                     95
    9.5                 11             46              16              7               80                     80
    4.75                0              27              16              7               50                     50
    2.36                0              17              12              7               36                     36
   0.300                0                0              6              7               13                     12
   0.075                0                0              0              6                6                     6
Second Trial:
The proportion of each aggregate size is as follows:
A = 31, B = 53, C = 9, D = 7
                                                                                                                   Page 13
Highway Materials
Third Trial:
The proportion of each aggregate size is as follows:
A = 39, B = 39, C = 15, D = 7
                                      Table 4-8: Blend gradation Results
 Sieve size      (19-9) mm      (9-4) mm       (4-0) mm     Filler     Desired blend     Mid Specification
   (mm)            P = 39         P = 39         P = 15     P=7          gradation            Limits
    19.1              39               39          15         7                100                100
    12.7              28               39          15         7                89                 95
    9.5               14               39          15         7                75                 80
    4.75              0                23          15         7                45                 50
    2.36              0                15          11         7                33                 36
   0.300              0                0           5          7                12                 12
   0.075              0                0           0          6                 6                  6
The first trial is the best proportion for blending aggregate, the proportion of each aggregate size is as
follows:
A = 31, B = 46, C = 16, D = 7
3. Determine the specific gravity of the aggregate combination and asphalt cement:
% Blending of Aggregates 31 46 16 7
                                                                                                        Page 14
Highway Materials
                                                                100
Sp. Gr. of total Aggregate =
                                 %Agg. 1    %Agg. 2   %Agg. 3   %Agg. 4   %Agg. 5 %filler Cement
                                  Spgr. 1 + Spgr. 2 + Spgr. 3 + Spgr. 4 + Spgr. 5 + Spgr + Spgr
                           100
Gsb = 31            46        16             7     = 2.615
               +           +           +
       2.606       2.626       2.618       2.580
                                                                                              Page 15
Highway Materials
   % A.C by
                Wt. in air   Wt.in Water      Wt. SSD           Vol. Cc =   Bulk-Gmb Sp.Gr.        Unit Weight
   weight of
                   A              C              B               (B-C)          A/(B-C)            = ρw ∗ Gmb
     mix
     3.5          1220            731             1244            513              2.378              2.378
      4           1223            734             1245            511              2.393              2.393
     4.5          1227            739             1251            512              2.396              2.396
      5           1228            739             1250            511              2.403              2.403
     5.5          1229            738             1250            512              2.400              2.400
          Effect Specific Gravity for Asphalt Mix Design (Loose HMA (Not Compacted))
                 Wt. of                                 Wt. of Wt. of        Wt. of
        %                    Wt. of      Wt. of
                 sample                               sample + bowl         sample     Volume       Gmm=
      Asphalt                bowl in    sample in
                 + bowl                                bowl in  in          in water   C= A-B        A/C
      Content                  air       air (A)
                  in air                                water  water           (B)
        3.5      2785.6      1565        1220.6        4481.7 3745.5         736.2         484.4     2.520
         4       2798.9      1565        1233.9        4486.3 3745.5         740.8         493.1     2.502
        4.5       2783       1565         1218          4473       3745.5      727.5       490.5     2.483
         5       2775.2      1565        1210.2        4464.8      3745.5      719.3       490.9     2.465
        5.5      2761.9      1565        1196.9        4453.2      3745.5      707.7       489.2     2.447
                                                                                                             Page 16
Highway Materials
      100 − 3.5
Gse = 100 3.5 = 2.659                    %AC = 3.5%
          −
      2.52 1.03
      100 − 4.0
Gse = 100 4.0 = 2.66                     %AC = 4%
     2.502 − 1.03
      100 − 4.5
Gse = 100 4.5 = 2.659                     %AC = 4.5%
          −
     2.483 1.03
         100 − 5.0
Gse =              = 2.66                %AC = 5%
         100 5.0
             −
        2.465 1.03
         100 − 5.5
Gse =              = 2.659                %AC = 5.5%
         100 − 5.5
        2.447 1.03
          100
Gmm = 96.5 3.5 = 2.520                    %AC = 3.5%
      2.66 + 1.03
         100
Gmm = 96     4 = 2.502                    %AC = 4%
           +
      2.66 1.03
         100
Gmm = 95.5 4.5 = 2.483                    %AC = 4.5%
           +
      2.66 1.03
         100
Gmm = 95     5 = 2.465                    %AC = 5%
           +
      2.66 1.03
         100
Gmm =            = 2.447                  %AC = 5.5%
      94.5 + 5.5
      2.66 1.03
                                                                    Page 17
Highway Materials
7. Calculate the percentage of voids, and percent voids filled with Bitumen in each
   specimen:
   Asphalt concrete primarily consists of three different components or phases: aggregate,
   asphalt binder, and air, see the figure 4.
Air can exist in pores on the aggregate surface, pockets within aggregate particles, or voids with
in the asphalt binder or between the binder and aggregate particles. Only the last type of air is
included in the air void content of asphalt concrete mixtures.
                                                                                          Page 18
Highway Materials
Voids in the mineral aggregate (VMA) refers to the space between aggregate particles in an asphalt
concrete mixture VMA is also often used to characterize loose aggregate. Voids in
mineral aggregate (VMA) is composed of asphalt binder and air voids.
Asphalt Absorption:
              Gse − Gsb
Pba = (100)               Gb
              Gsbx Gse
              2.66 − 2.615
Pba = (100)                    x 1.03 = 0.666
              2.615 x 2.66
              0.666
Pbe = 3.5 −         x 96.5 = 2.857                     %AC = 3.5%
               100
            0.666
Pbe = 4 −           x 96 = 3.361                       %AC = 4%
              100
              0.666
Pbe = 4.5 −         x 95.5 = 3.864                     %AC = 4.5%
               100
            0.666
Pbe = 5 −         x 95 = 4.367                         %AC = 5%
             100
                                                                                          Page 19
Highway Materials
            0.666
Pbe = 5.5 − 100 x 94.5 = 4. 871   %AC = 5.5%
                                               Page 20
Highway Materials
                2.378 x 96.5
VMA = 100 −                  = 12.2   %AC = 3.5%
                   2.615
                2.393 x 96
VMA = 100 −                  = 12.1   %AC = 4%
                     2.615
                2.396 x 95.5
VMA = 100 −                  = 12.4   %AC = 4.5%
                   2.615
                2.403 x 95
VMA = 100 −                = 12.7      %AC = 5%
                   2.615
                2.400 x 94.5
VMA = 100 −                  = 13.3    %AC = 5.5%
                   2.615
             2.520 − 2.378
Va = 100 x                 = 5.63     %AC = 3.5%
                 2.520
             2.502 − 2.393
Va = 100 x                 = 4.36     %AC = 4%
                 2.502
             2.483 − 2.396
Va = 100 x                   = 3.5    %AC = 4.5%
                    2.483
             2.465 − 2.403
Va = 100 x                 = 2.52     %AC = 5%
                 2.465
                                                    Page 21
Highway Materials
             2.447 − 2.400
Va = 100 x                 = 1.92    %AC = 5.5%
                 2.447
                                                  Page 22
Highway Materials
               12.2 − 5.63
VFA = 100 x                = 54%                 %AC = 3.5%
                   12.2
               12.1 − 4.36
VFA = 100 x                = 64%                 %AC = 3.5%
                   12.1
               12.4 − 3.5
VFA = 100 x               = 72%                 %AC = 3.5%
                  12.4
               12.7 − 2.52
VFA = 100 x                = 80%                 %AC = 3.5%
                   12.7
               13.3 − 1.92
VFA = 100 x                = 86%                 %AC = 3.5%
                   13.3
                                                               Page 23
Highway Materials
                                              Page 24
Highway Materials
Phase diagram approach to calculate the volumetric properties of HMA paving mixture:
Ma Air Va
                                                                     VMA
                                  Mbe       Asphalt binder    Vbe
                        Mb                                                 Vb
                                  Mba      Absorbed asphalt   Vba
              Mmb                                                                Vmb
                             Ms
                                              Aggregate             Vsb
                                  Mse                                      Vse
                                                                                   Page 25
Highway Materials
                                                  Pmm−Pb
Effective Specific Gravity of Aggreagte: Gse =
                                                  Pmm Pb
                                                  Gmm− Gb
          100 − 5
Gse =              = 2.66
        100     5
             −
        2.465 1.03
                                          Ms
Effective volume of Aggregate: Vse =    G se ρm
                                    Ms
Bulk volume of Aggregate: Vsb = G
                                    sb ρm
        0.025
Pa =          x 100 = 2.5
          1
                                      Va + Vbe
Voids in Mineral aggregate: VMA =                x 100
                                            Vm
          0.025 + 0.102
VMA =                   x 100 = 12.7
                1
                                    Vbe
Voids filled with Asphalt: VFA =            x 100
                                   VMA
         0.102
VFA =          x 100 = 80.31
         0.127
         0.1051
Pbe =           x 100 = 4.37
         2.403
                                                             Mba
AbsorbedAsphalt Content(%Mass of Aggregate): Pba =                 x 100
                                                             Ms
Pb a=
                                                                           Page 27
   Highway Materials
0.0154
2.283     x 100
          =
          0.674
Page 28