Report
Report
a r t i c l e i n f o a b s t r a c t
Article history: Early-age cracking due to plastic shrinkage is often attributed to reducing the durability of concrete
Received 1 October 2015 structures. The objective of this paper is to evaluate the potential use of chopped basalt fibres in pre-
Received in revised form venting these cracks. Testing was undertaken to measure the magnitude of shrinkage strain that de-
15 July 2016
velops in unrestrained specimens, and the severity of cracking that occurs when shrinkage is restrained.
Accepted 1 October 2016
Available online 4 October 2016
Results indicate basalt fibres are effective in preventing cracks by reducing the magnitude of free
shrinkage, and by restricting the growth of cracks if they do occur. The latter mechanism is more
prominent when the w/c ratio is decreased.
Keywords:
Basalt fibre
© 2016 Published by Elsevier Ltd.
Minibars
Basalt fibre reinforced concrete
Durability
Plastic shrinkage cracking
http://dx.doi.org/10.1016/j.cemconcomp.2016.10.004
0958-9465/© 2016 Published by Elsevier Ltd.
J. Branston et al. / Cement and Concrete Composites 74 (2016) 182e190 183
regards to mitigating cracking at later ages, and in-turn, minimizing measurement of strain when the specimens are unrestrained (free
long-term maintenance costs. shrinkage), and the measurement of crack severity in specimens
It has been well established that the addition of short, randomly that are restrained from shrinking with a rectangular restraint
distributed fibres to concrete is an effective method in mitigating element. The primary importance of this study lies in the fact there
plastic shrinkage cracking. The fibres are effective in this regard for is minimal literature addressing the usefulness of basalt fibres for
two reasons: first, they reduce the overall shrinkage strains and early-age crack control in concrete. Secondly, the work provides
lower the possibility of tensile stresses exceeding tensile strength, some insight on test methods for measuring free and restrained
and second, the fibres are able to restrict their development if they plastic shrinkage, for which there seems to be a lack of any one
do occur [14]. According to Naaman et al. [15], the addition of any generally accepted test method.
fibre with a diameter smaller than 40 mm, an aspect ratio above
200, in volume fractions of 0.2%e0.4%, should effectively eliminate 2. Experimental procedure
plastic shrinkage cracking in concrete. Hence, it is unsurprising
such a wide variety of fibres have been shown to be beneficial in 2.1. Environmental chamber
this regard, including: steel, glass, various synthetic fibres (poly-
propylene, polyethylene, polyvinyl, and carbon), and various nat- All testing was completed in an environmental chamber that
ural fibres (sisal, coconut, flax, and cellulose) [15e20]. However, the operated at a temperature of 48 C (±2 C) and relative humidity of
mechanisms by which different fibres reduce plastic shrinkage 15% (±3%). This was achieved by connecting a heater fan to a
strain, and the resultant cracking, is not as thoroughly studied. This temperature and humidity controller capable of reading tempera-
is an important consideration in order to understand the circum- ture accurate to ±1.5 C and relative humidity to ±2%. These con-
stances in which the use of a particular type of fibre is most ditions resulted in an evaporation rate of approximately 0.75 kg/
effective. m2/h. The environmental chamber is depicted in Fig. 1.
Only one study, completed by the Florida Department of
Transportation (FDOT), could be found in regards to the usefulness 2.2. Free shrinkage testing
of basalt fibres on early-age cracking due to shrinkage. The study
concluded that stiff fibres, including basalt, steel, and glass, should The test setup for the free (unrestrained) shrinkage testing was
not be used for early-age crack control due to drying shrinkage, developed based on similar methods used by other researchers
since it was evident their stiffness initiated cracking sooner, and the [23,24]. Concrete specimens were 500 mm in length and 80 mm by
cracks were wider [21]. The conclusions were based on the results 80 mm in cross-section. The interior of the forms were lined with a
of the ASTM C1581 [22] test method, in which a steel ring is used as thick polypropylene sheet (vapour barrier) that was lightly coated
a restraint element. In that case, the poor performance of the stiff with Teflon spray. A Teflon plate was placed at one end of the form
fibres may be due to the relatively lower ability of the fibres to bend with a 9.5 mm diameter bolt threaded into it that extended 30 mm
and align with the circumference of the cracks that develop due to into the form. The Teflon plate was loose fitting so that it could
the circumferential shrinkage stress induced by the ring, in com- move with minimal resistance. As shrinkage occurred, the plate
parison with the other more flexible fibres used (e.g. poly- was moved by the bond between the bolt and the concrete. The
propylene). The results in that study may not be a good displacement of the plate was measured with a 5 mm linear vari-
representation of the effectiveness of basalt fibres in structures able differential transformer (LVDT) that was accurate to 5 mm. A
with more typical rectangular geometry, where there is greater 25 mm thick piece of foam was placed behind the Teflon plate so
probability of the fibres bridging cracks in a more favorable that movement due to thermal expansion was also possible. The
orientation. The test method has previously been criticized for forms were placed in the environmental chamber and data was
producing an unrealistic stress field in regards to repair overlays collected for 4 h. Free shrinkage test results reported in this study
[14]. are the mean values calculated based on three specimens per fibre
The purpose of the experimental work reported in this paper is dosage. The setup is illustrated in Fig. 2.
to evaluate the influence of three different types of basalt fibre on
the plastic shrinkage of concrete. The basalt fibres used in this study 2.3. Restrained shrinkage testing
are: bundle dispersion fibres (BD), filament dispersion fibres (FD)
and minibars (MB). The influence of the fibres is quantified by the The test setup for restrained shrinkage testing closely followed
the method proposed by Banthia and Gupta [14], with two excep- reported in this study are the mean values calculated based on
tions: the length of the restraint element (Fig. 3a) was increased three specimens per fibre dosage.
from 300 mm to 500 mm to match that of the free shrinkage
testing, and the thickness of the mortar overlay was reduced from 2.4. Materials and specimen preparation
60 mm to 35 mm to represent a typical concrete cover for the
application of the results directly to a rehabilitation project in the All mixes were made with general use limestone (GUL) Portland
field. The restraint elements had an average 28 day compressive cement conforming to CSA A3001 [25], and regular drinking water.
strength of approximately 60 MPa. The mortar overlay was placed Fine aggregate was local river sand with a fineness modulus of 2.7,
over the restraint element and then the form was placed in the and the coarse aggregate was well-graded with a maximum size of
environmental chamber. The form was carefully removed after 1.5 h 19 mm. The cement had a Blaine fineness of 488 m2/kg, and con-
in order to increase the exposed surface area of the concrete, and sisted of 9.5% limestone (94% CaCO3 in limestone). The chemical
in-turn, the severity of the cracking. Fig. 3b depicts the develop- composition of the cement can be found in Table 1.
ment of cracks after removing the specimen from the environ- The cement fineness and chemical composition have a direct
mental chamber after a total of 4 h. The cracks were measured influence on shrinkage, and are further discussed in section 3.2.
using a 240 magnification digital microscope. The total area of all Mortar was generally used in this study to increase the magnitude
cracks on the surface for each specimen was measured, and the of shrinkage strain and in-turn, cracking severity, so that the in-
largest crack width was recorded. Restrained shrinkage test results fluence of the fibre could be more readily measured. Table 2 shows
Table 1
Portland cement type GUL chemical composition (%).
Loss on ignition SiO2 Fe2O3 Al2O3 CaO Free CaO MgO SO3 K2O Na2O TiO2
4.8 18.2 2.76 4.5 62.3 1.5 3.1 3.47 0.45 0.22 0.21
Table 2
Mass proportions of concrete mixes used.
the proportions (by mass) of each type of mix used in this work, Table 3
along with a description indicating the purpose of the mix. Fibre dosages and test matrix.
Cement to sand proportions of 1:2 (M1 and M2) and 1:1 (M4 Designation Fibre type Length (mm) Dosage
and M5) were selected in an attempt to produce results comparable Volume (%) kg/m3
to other researchers using different fibres [17,20,24,26]. A w/c ratio
PM No fibre 0 0
of 0.5 was selected as a control to produce a mix with a high flow.
BD-25-0.05 Bundle dispersion 25 0.05 1.3
For that reason, the mix would generally not be used in practical BD-25-0.1 0.1 2.6
applications. However, it is useful for laboratory testing since it BD-25-0.3 0.3 7.8
results in high shrinkage strain and promotes cracking, which FD-25-0.05 Filament dispersion 25 0.05 1.3
makes the effect of the fibres easier to measure. The purpose of FD-25-0.1 0.1 2.6
FD-25-0.3 0.3 7.8
reducing the w/c ratio was for insight on the benefit of the fibres in FD-12-0.05 Filament dispersion 12 0.05 1.3
a more realistic setting, where it is almost certain their effect on FD-12-0.1 0.1 2.6
workability will need to be accounted for with the use of super- FD-12-0.3 0.3 7.8
plasticizer. Consequently, the effect of superplasticizer in this MB-43-0.3 Minibar 43 0.5 6.2
MB-43-1.0 1.0 20
context should also be studied. Superplasticizer dosages in Table 2
listed as ‘varied’ refers to the increasing dosages required to pro-
duce an equivalent flow for increasing fibre dosages. It is well un-
derstood that fibres have an adverse effect on the flow (or mix time reached 3 min. Water (and plasticizer mixed in with the
workability) of concrete, and thus, greater quantities of super- water as necessary) was then added and the mix continued for
plasticizer were required as fibre dosages increased (further another 2 min. In all cases, the fibres dispersed without any
explained in section 3.1). Likewise, the effect of the fibres in a noticeable balling or clumping. The flow of the mortar mixes was
concrete mix with coarse aggregate (M3) is also considered as measured as per ASTM C1437 [27].
additional way of producing data more representative of actual
application. 3. Results and discussion
Three types of basalt fibre were evaluated: filament dispersion
(FD), bundle dispersion (BD) and minibars (MB). Filament disper- 3.1. Mortar flow
sion fibres disperse into individual filaments during mixing,
whereas bundle dispersion fibres have a coating (sizing) that keeps The effect of the 25 mm filament dispersion fibres on the flow of
the filaments together as a bundle. Minibars are an epoxy based the control mix M1, and the reduced w/c ratio max M2, is shown in
polymer reinforced with basalt filaments; essentially a scaled down Table 4, since they had the greatest effect of all fibres tested. In this
version of basalt fibre reinforced polymer rebar. These differences table, Di is the initial diameter of the mortar, and Df is the diameter
are depicted in Fig. 4. of the mortar after dropping the plate 25 times within 15 s.
The filament and bundle dispersion fibres consist of filaments Results for other types of fibre followed the same trend, and
16 mm in diameter, and the minibars are constructed with filaments thus, are not shown in this table. However, it should be noted that
17 mm in diameter. A summary of the fibre dosages used in this the order from greatest to least in terms of their effect on the flow
study is shown in Table 3. Designations are labelled according to was: FD-25, FD-12, BD-25, and MB-43. In cases where the mortar
fibre type, fibre length, and dosage. For example, the designation spilled off the plate before being dropped 25 times, the flow could
BD-25-0.1 indicates basalt bundle dispersion fibres of 25 mm not be accurately calculated. The effect of the fibres is evident by
length at a dosage of 0.1% by volume. the decreasing value of Di with increasing fibre dosages in M1. The
Cement and aggregate was mixed dry for 1 min. Next, fibres number of drops required to cause the mortar to spill increased
were slowly added by hand, and the dry mix continued until total from 17 without fibre, to 22 when a fibre dosage of 0.05% was used.
Fig. 7. Comparison between reduced w/c ratio mix (M2) and concrete mix (M3).
both the flow and shrinkage of the mortar are strongly influenced benefit of reducing shrinkage strain. Superplasticizer is a key
by the frictional effects of the fibres. Consequently, adding super- component in concrete mixes with a low w/c ratio (e.g. high-
plasticizer to the mix so that it is workable seems to negate the strength concrete). Thus, the addition of fibres in these types of
188 J. Branston et al. / Cement and Concrete Composites 74 (2016) 182e190
mixes will only be useful if they are effective in bridging shrinkage aggregate was reduced for mix M4, which in-turn increased the
cracks to restrict their growth. unit volume of cement and water. Since plastic shrinkage is largely
The FDOT [21] found that the addition of fibres (including influenced by the pore pressure of evaporating water, this resulted
basalt) at low dosages (<0.5%) generally did not have a significant in greater shrinkage strain and more cracking. In-turn, the effect of
effect on the workability of concrete; though it should be noted that the different fibres could be more easily distinguished. Fig. 9 shows
marginal decreases in the workability were found with stiffer fi- the typical appearance of fibre reinforced specimens with varying
bres. Boghossian and Wegner [17] studied the effect of flax, poly- fibre dosages versus an unreinforced specimen after 4 h. Addi-
propylene, and glass fibres on free shrinkage and found that glass tionally, the influence of the fibres on the total crack area and
fibres, having a higher elastic modulus than the other fibres, were largest crack width are shown in Figs. 10 and 11, respectively.
the only type of fibres to consistently reduce the free shrinkage Again, the 25 mm filament dispersion fibres had the greatest
strain. This may suggest that the use of relatively high-modulus effect. In this case, they produced the greatest reduction of the
fibres like basalt comes with a trade-off: they are more effective crack area and the crack width. The results from the free shrinkage
in decreasing the free shrinkage strain, but probably have a more testing correlated well with both measured parameters: total crack
adverse effect on workability than low-modulus fibres (e.g. poly- area and largest crack width. In other words, the magnitude of
propylene). Wongtanakitcharoen and Naaman [24] expressed the shrinkage strain was very indicative of the crack severity. However,
idea that assuming everything else being the same, fibres with a it is clear that the benefit of the fibres is not just because of their
higher elastic modulus should produce greater frictional resistance, ability to reduce free shrinkage strain. The fibres are effective, at
and therefore, lead to a greater reduction in free shrinkage strain. least partly, due to their ability to bridge cracks and restrict growth,
However, in their study with carbon, polypropylene, and PVA fi- as shown in Fig. 12.
bres, the results did not support that idea. That is likely due to the Further evidence of their ability to restrict crack growth is
fact that the condition of ‘everything else being the same’ was not provided in Fig. 13, in which it can be found that the 25 mm fila-
met, since the range of elastic modulus considered was the result of ment dispersion fibres are also effective in reducing the crack area
using different materials. Results presented in this paper would in the low w/c ratio mix M5. Free shrinkage testing revealed that
suggest it could be possible to predict the reduction fibres have on the fibres did not have a significant effect on the reduction in strain
free shrinkage strain by measuring their effect on the flow, for when superplasticizer was used to produce an equivalent flow to
which related literature suggests the fibre elastic modulus is likely that of the unreinforced control specimen. Therefore, their effec-
to be a major influencing factor. Although this could perhaps be of tiveness in this case must be attributed to their ability to restrict the
interest for future research, the ability of the fibres to prevent growth of cracks.
shrinkage cracking is most important. The performance of 12 mm filament dispersion fibres was very
similar to that of the 25 mm filament dispersion fibres. It is likely
3.3. Restrained shrinkage testing the greater bond strength, due to their increased length, makes
them more effective in restricting crack growth. Banthia and Gupta
Preliminary testing showed that at the lowest dosage (0.05% by [16] reported similar findings in their study on polypropylene fi-
volume), 25 mm filament dispersion fibres completely eliminated bres. In the case of bundle dispersion fibres and minibars, the fibres
shrinkage cracking in the control mix M1. Thus, the amount of fine were not observed bridging the cracks. This makes sense, since
Fig. 10. Effect of fibres on total crack area on specimen surface in M4.
J. Branston et al. / Cement and Concrete Composites 74 (2016) 182e190 189
Fig. 12. Crack development without fibre (a) and with fibre (b).
Fig. 13. Effect of FD-25 on crack area in low w/c ratio mix M5.
cracks are more likely to develop where fibres are not present. The agreement of results would only be possible in the unlikely case
filament dispersion fibres cover a much greater area, and therefore, that cracks in fibre reinforced specimens in this work began
there is a higher probability they will bridge a developing crack. growing at a faster rate than the unreinforced specimens in the
Restrained shrinkage testing was not undertaken with the three weeks following testing.
concrete mix M3, since the size of the aggregate used relative to the
thickness of the overlay was prohibitive. However, it would be 4. Conclusions
reasonable to assume that basalt fibres would have a similar benefit
in concrete mixes and this could be of interest to future research. The results presented in this paper suggest basalt fibres are
The results of the restrained shrinkage testing in this paper would effective in mitigating the detrimental effects of plastic shrinkage
seem to disagree entirely with those of the FDOT [21], which not by reducing the magnitude of the shrinkage strain, and by
only found basalt fibres were ineffective, but detrimental. In that restricting the growth of cracks if they do occur. As the w/c ratio
case, crack measurements were taken after 12 and 28 days of decreases, it is the latter mechanism that becomes more promi-
curing, and so the results are not directly comparable. However, nent. However, related literature suggests that high-modulus fibres
190 J. Branston et al. / Cement and Concrete Composites 74 (2016) 182e190
like basalt have a more severe impact to workability than low- structures, Constr. Build. Mater. 96 (2015) 37e46.
[2] P. Iyer, S. Kenno, S. Das, Mechanical properties of fiber-reinforced concrete
modulus fibres. Therefore, the application of basalt fibres for
made with basalt filament fibers, J. Mater. Civ. Eng. (2015) 04015015.
early-age crack control is likely best suited for general-use concrete, [3] C. Jiang, K. Fan, F. Wu, D. Chen, Experimental study on the mechanical
where the w/c ratio is often high enough that the fibres will not properties and microstructure of chopped basalt fibre reinforced concrete,
require additional measures (and cost) to restore workability. Mater. Des. 58 (2014) 187e193.
[4] ACI Committee 544, 544.1R-96: Report on Fiber Reinforced Concrete (Reap-
Moreover, they will be more efficient in this scenario due to the proved 2009), Technical Documents, 1996.
ability to simultaneously reduce the shrinkage strain and restrict [5] J.J. Lee, J. Song, H. Kim, Chemical stability of basalt fiber in alkaline solution,
crack growth. An example of such a mix can be found in a previous Fibers Polym. 15 (11) (2014) 2329e2334.
[6] F. Rabinovich, V. Zueva, L. Makeeva, Stability of basalt fibers in a medium of
study, in which it was shown the addition of basalt filament hydrating cement, Glass Ceram. 58 (11e12) (2001) 431e434.
dispersion fibres did not have a significant effect on the workability [7] ACI Committee 224, 224.1R-07: Causes, Evaluation, and Repair of Cracks in
of regular-strength concrete (30e35 MPa compressive strength) Concrete Structures, Technical Documents, 2007.
[8] H.M. Aktan, G. Fu, W. Dekelbab, U. Attanayaka, Investigate Causes & Develop
with a w/c ratio of 0.5 until a dosage of approximately 0.46% by Methods to Minimize Early-age Deck Cracking on Michigan Bridge Decks,
volume [2]. 2003.
The filament dispersion fibres were most beneficial, likely due to [9] K. Folliard, C. Smith, G. Sellers, M. Brown, J. Breen, Evaluation of Alternative
Materials to Control Drying-shrinkage Cracking in Concrete Bridge Decks,
two reasons: an increased surface area resulting in greater fric- 2003.
tional restraint, and a greater probability of bridging cracks because [10] M.S. Linford, L.D. Reaveley, A Study of the I-15 Reconstruction Project to
of the increased number of uniformly spaced filaments. Moreover, Investigate Variables Affecting Bridge Deck Cracking, 2004.
[11] M.A. Saadeghvaziri, R. Hadidi, Cause and Control of Transverse Cracking in
filament dispersion fibres 25 mm in length were more effective
Concrete Bridge Decks, 2002.
than fibres 12 mm in length, although the difference was minor and [12] Transportation Research Board, Control of Cracking in Concrete, Policy Anal-
may be a result of the inherent variability in both test methods ysis, 2006.
applied. Using the filament dispersion fibres, shrinkage cracks were [13] ACI Committee 446, 446.1R-91: Fracture Mechanics of Concrete: Concepts,
Models, and Determination of Material Properties (Reapproved 1999), Tech-
completely eliminated at a dosage of 0.1% by volume in all cases in nical Documents, 1991.
this study. However, in practical applications, shrinkage cracking [14] N. Banthia, R. Gupta, Test method for evaluation of plastic shrinkage cracking
could likely be eliminated at even lower fibre dosages, since the in fiber-reinforced cementitious materials, Exp. Tech. 31 (6) (2007) 44e48.
[15] A.E. Naaman, T. Wongtanakitcharoen, G. Hauser, Influence of different fibers
environmental conditions and mix proportions used in this study on plastic shrinkage cracking of concrete, ACI Mater. J. 102 (1) (2005).
were designed to exaggerate the effects of shrinkage. From a [16] N. Banthia, R. Gupta, Influence of polypropylene fiber geometry on plastic
manufacturing point of view, the fibre dosage required to eliminate shrinkage cracking in concrete, Cem. Concr. Res. 36 (7) (2006) 1263e1267.
[17] E. Boghossian, L.D. Wegner, Use of flax fibres to reduce plastic shrinkage
cracking could likely be decreased further by reducing the diameter cracking in concrete, Cem. Concr. Compos. 30 (10) (2008) 929e937.
of the filaments. This would increase the number of individual fil- [18] H. Shah, J. Weiss, Quantifying shrinkage cracking in fiber reinforced concrete
aments and the surface area of the fibres, with respect to the using the ring test, Mater. Struct. 39 (9) (2006) 887e899.
[19] P. Soroushian, S. Ravanbakhsh, Control of plastic shrinkage cracking with
quantity of material. specialty cellulose fibers, ACI Mater. J. 95 (4) (1998).
Although this study has concluded that bundle dispersion fibres [20] R.D. Toledo Filho, K. Ghavami, M.A. Sanjua n, G.L. England, Free, restrained and
and minibars are not optimal for controlling plastic shrinkage drying shrinkage of cement mortar composites reinforced with vegetable fi-
bres, Cem. Concr. Compos. 27 (5) (2005) 537e546.
cracking, they were still clearly effective, albeit to a lesser extent
[21] N. Suksawang, A. Mirmiran, D. Yohannes, Use of Fiber Reinforced Concrete for
than the filament dispersion fibres. Therefore, it may be of interest Concrete Pavement Slab Replacement, 2014.
to pursue future research into the use of these fibres as secondary [22] ASTM C1581, Standard Test Method for Determining Age at Cracking and
reinforcement with the intent of minor enhancements to both Induced Tensile Stress Characteristics of Mortar and Concrete under
Restrained Shrinkage, ASTM International, West Conshohocken, PA, 2009.
mechanical behaviour and reductions to plastic shrinkage strains [23] D. Myers, T.H.-K. Kang, C. Ramseyer, Early-age properties of polymer fibre-
and early-age cracking. reinforced concrete, ACI Mater. J. 2 (1) (2008) 9e14.
[24] T. Wongtanakitcharoen, A.E. Naaman, Unrestrained early age shrinkage of
concrete with polypropylene, PVA, and carbon fibers, Mater. Struct. 40 (3)
Acknowledgements (2007) 289e300.
[25] CSA, Cementitious Materials Used in Concrete. Mississauga, Ontario, 2013.
The authors appreciate the financial assistance received from [26] P. Mangat, M. Azari, Plastic shrinkage of steel fibre reinforced concrete, Mater.
Struct. 23 (3) (1990) 186e195.
OCE, NSERC, Connect Canada, and MEDA Limited. The authors also [27] ASTM C1437, Standard Test Method for Flow of Hydraulic Cement Mortar,
appreciate the technical assistance and donation of materials from ASTM International, West Conshohocken, PA, 2013.
MEDA Limited. [28] E.E. Holt, Early Age Autogenous Shrinkage of Concrete, PhD thesis, 2001.
[29] W. Kurdowski, Cement and Concrete Chemistry, Springer, Dordrecht, 2014.
References
[1] C. High, H.M. Seliem, A. El-Safty, S.H. Rizkalla, Use of basalt fibers for concrete