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IJARSCT
International Journal of Advanced Research in Science, Communication and Technology (IJARSCT)
International Open-Access, Double-Blind, Peer-Reviewed, Refereed, Multidisciplinary Online Journal
Impact Factor: 7.53 Volume 4, Issue 1, August 2024
Abstract: Solid perfume based on beeswax is a unique and natural fragrance product that provides a long-
lasting scent while being gentle on the skin. This type of perfume is made from a combination of natural
ingredients, including beeswax, carrier oils, and essential oils. The beeswax acts as a natural emulsifier,
which helps to blend the other ingredients and create a solid, compact texture. The carrier oils and
essential oils provide the fragrance, which is released slowly and subtly throughout the day. Solid perfume
based on beeswax is an excellent alternative to traditional liquid perfumes, as it is more portable, easy to
apply, and environmentally friendly. It is also a perfect choice for those with sensitive skin, it contains no
alcohol or synthetic ingredients that can irritate the skin. To ensure the success of the presented collection,
several quality factors have been established, which will be the same for all four perfumes in the collection,
as well as the evaluation indexes of these factors. Quality factors have been classified as sensory, with
factors such as the applicability of the product to the skin, and physicochemical, establishing the melting
point and stability of the product.mm/second, melting point 90°C and pH value 4.
Keywords: Product development, formulated products, personal care, perfumery, solid perfumes, quality
factors, formulation, process synthesis.
I. INTRODUCTION
Solid perfumes have been gaining popularity in recent years as a more sustainable and eco-friendly alternative to
traditional liquid perfumes. Unlike liquid perfumes, which are often packaged in plastic or glass bottles and contain
high amounts of synthetic fragrances, solid perfumes use natural waxes and carrier oils as a base, and are typically
scented with essential oils or herbal extracts. This project aims to develop a beeswax and almond carrier oil-based solid
perfume that is scented with rose oil. The goal is to create a natural and sustainable solid perfume that provides a
delightful floral fragrance, while also offering therapeutic benefits through the use of essential oils1. The formulation of
the solid perfume will be based on a blend of natural ingredients, including beeswax and almond carrier oil. Beeswax is
a natural wax produced by honey bees, and has unique emollient and protective properties, making it an excellent
natural alternative to synthetic waxes and petroleum- based ingredients commonly found in cosmetics. Almond carrier
oil, on the other hand, is a light, non-greasy oil that is easily absorbed by the skin, providing nourishing and
moisturizing properties. The fragrance of the solid perfume will be provided by rose oil, a natural essential oil extracted
from rose petals. Rose oil has a delicate and pleasant floral fragrance, and is known for its calming and relaxing
properties2. We will be using a variety of essential oils to create our unique fragrance. Essential oils are concentrated
plant extracts that are derived from flowers, leaves, and other parts of plants. They have a wide range of therapeutic
benefits and can be used to create beautiful and complex fragrances.
Here are the essential oils we will be using in solid perfume3:
1. Lavender essential oil - known for its calming and soothing properties.
2. Rose essential oil a romantic and uplifting scent.
3. Ylang-ylang essential oil - a sweet and floral fragrance.
4. Cedarwood essential oil - a woody and grounding scent.
5. Bergamot essential oil - a citrusy and refreshing fragrance.
Together, these essential oils will create a beautiful and balanced fragrance that will be perfect for creating beeswax
solid perfume, we will need a few additional ingredients. In addition to the essential oils mentioned earlier, we will be
using carrier oils to help dilute the essential oils and create a smooth and spreadable texture.
Here are the carrier oils we will be using4:
1. Sweet almond oil - a light and nourishing oil that is easily absorbed by the skin.
2. Jojoba oil a versatile and moisturizing oil that is similar in composition to our skin's natural oils.
3. Coconut oil - a soothing and hydrating oil that is solid at room temperature, making it ideal for a solid perfume.
This project will involve selecting appropriate ingredients, formulating the perfume, testing and evaluating the product,
and designing eco-friendly packaging. The final product will be a natural and sustainable alternative to traditional liquid
perfumes, offering a delightful floral fragrance with therapeutic benefits.
Overall, this project represents an exciting opportunity to explore the potential of natural ingredients in creating
sustainable and eco-friendly cosmetics, while also providing a delightful fragrance experience.
Consumer behavior: The research will also explore consumer behavior and preferences related to solid perfumes,
including their attitudes towards eco-friendly products, their purchasing habits, and their satisfaction with the quality
and performance of different types of solid perfume products. This will help to identify opportunities for innovation and
improvement in the solid perfume industry, as well as areas where further research is needed to meet consumer demand.
The heating process changes the physical properties of beeswax. Shrinkage of heated beeswax occurs by 10% upon
cooling. When the beeswax is heated at the temperature of 30-35°C, it attains the properties of plastics. Beeswax is
insoluble in water and soluble in organic solvents, such as ether, acetone, xylol, benzene, chloroform, and
tetrachloromethane. In order to completely dissolve the beeswax, the temperature must be increased beyond its melting
point. The edible coating made up of beeswax, coconut oil, and sunflower oil has been used on strawberries and apricot
fruits. This coating showed a positive effect on the moisture loss, appearance, texture, and firmness. The coconut oil
containing monolauric acid showed antifungal effect on the coated fruit samples (Irina, 2012). The edible coating of
hydroxypropyl methylcellulose, beeswax, and antifungal components, such as sodium methyl paraben, sodium
benzoate, and sodium ethyl paraben has been studied on cherry tomatoes. It was found that the coating of
hydroxypropyl methyl cellulose-beeswax containing sdium benzoate (2%) showed a decreased rate of change in the
weight or moisture loss, firmness, and respiration5.
2) Carrier oils.
What are carrier oils?
Carrier oils and essential oils are made from plants. Carrier oils are used to dilute essential oils and "carry" them to your
skin. That's because essential oils are potent and can cause irritation when applied directly to your skin.
Copyright to IJARSCT DOI: 10.48175/IJARSCT-19352 411
www.ijarsct.co.in
ISSN (Online) 2581-9429
IJARSCT
International Journal of Advanced Research in Science, Communication and Technology (IJARSCT)
International Open-Access, Double-Blind, Peer-Reviewed, Refereed, Multidisciplinary Online Journal
Impact Factor: 7.53 Volume 4, Issue 1, August 2024
Most carrier oils are unscented or lightly scented and don't interfere with an essential oil's therapeutic properties. They
may be used alone or with other oils to nourish your skin6.
Fi
gure No-2 Almond oil7
Combining with other carrier oils. Almond oil can help lighten heavier carrier oils, helping them absorb more easily
Bath oil. Almond oil is a great choice as a carrier oil for essential oil-based bath oils. This helps to increase
moisturizing properties while maximizing the benefits of the essential oils. Skin moisturizers. Because it is easily
absorbed and moisturizing, almond oil can make a great carrier oil for natural essential oil-based lotions, lotion bars,
balms or moisturizing scrubs. Topical application. Because it has a subtle scent and doesn't leave a greasy residue,
almond oil is a great choice as a carrier oil for basic topical essential oil application, for example - massage oils.
3) Essential Oil
An essential oil is a concentrated hydrophobic liquid containing volatile (easily evaporated at normal temperatures)
chemical compounds from plants. Essential oils are also known as volatile oils, ethereal oils, aetheroleum, or simply as
the oil of the plant from which they were extracted, such as oil of clove. An essential oil is essential in the sense that it
contains the essence of the plant's fragrance the characteristic fragrance of the plant from which it is derived8. The term
"essential" used here does not mean indispensable or usable by the human body, as with the terms essential amino acid
or essential fatty acid, which are so called because they are nutritionally required by a living organism9.
Essential oils are generally extracted by distillation, often by using steam. Other processes include expression, solvent
extraction, sfumatura, absolute oil extraction, resin tapping, wax embedding, and cold pressing. They are used in
perfumes, cosmetics, soaps, air fresheners and other products, for flavoring food and drink, and for adding scents to
incense and household cleaning products. essential oils are often used for aromatherapy, a form of alternative medicine
in which healing effects are ascribed to aromatic compounds. Aromatherapy may be useful to induce relaxation, but
there is not sufficient evidence that essential oils can effectively treat any condition. Improper use of essential oils may
cause harm including allergic reactions, inflammation and skin irritation. Children may be particularly susceptible to
the toxic effects of improper use. Essential oils can be poisonous if ingested or absorbed through the skin10.
Rose oil
Rose oil is a fragrant essential oil that is extracted from the petals of various species of roses, most commonly Rosa
damascena and Rosa centifolia. It is a highly prized and valuable oil in the perfume industry due to its complex and rich
floral scent, as well as its therapeutic properties.
Copyright to IJARSCT DOI: 10.48175/IJARSCT-19352 412
www.ijarsct.co.in
ISSN (Online) 2581-9429
IJARSCT
International Journal of Advanced Research in Science, Communication and Technology (IJARSCT)
International Open-Access, Double-Blind, Peer-Reviewed, Refereed, Multidisciplinary Online Journal
Impact Factor: 7.53 Volume 4, Issue 1, August 2024
B) Method of Preparation12
Sr Ingredients Quantity
1 Bees wax 10 gm
2 Carrier oil 30 gm
3 Essential oil or etheral oil. 20 drops
4 Oil soluble color qs.
Table No 01. Formula
The Process of Making Solid Perfume, beeswax were melted at 90°C. Rose oil as fragrance was mixed with Almond oil
and then added to wax compound. After that, Rose oil was added gradually. The mixture was stirred until homogeneous
for 30 minutes then cooled and allowed to harden at room temperature. The composition of solid perfume is shown in
i) Melt together the wax with the jojoba or sweet almond oil. You can either microwave the ingredients for a few
seconds in a microwave-safe container or else you can heat the mixture over a double-boiler.
ii) Once this mixture has liquefied, remove it from heat. Stir in the essential oils. You can use a toothpick, straw or even
a spoon. Expect your perfume to coat the stirrer, so either use something disposable or else something you can wash
(i.e., don't use a wooden spoon, unless you want it to smell pretty forever).
iii) Pour the liquid into your final container. Set the lid on top of the container, but leave it ajar. This will help prevent
condensation inside your container while minimizing the chance of microbial contamination of the product.
iv) Apply the perfume by rubbing a finger on the product to liquefy it, then rub your finger on the area you want to be
scented.
V. EVALUATION
Assessment of prepared perfume Organoleptic assessment Done for color, odor, appearance, pearlescence, roughness,
texture grade, etc.
A) Chemical assessment
Saponification value It is defined as the number of milligrams of KOH required to hydrolyze Igram of wax. It is
expressed as mg KOH/g.
SAPONIFICATION VALUE = 56.1 × (B-S) × N × W……………………………………………………………….1
Where; B = volume in ml of the standard hydrochloric acid required for the blank,
S = volume in ml of standard hydrochloric acid required for the wax,
N = normality of standard hydrochloric acid, and
M = mass in gms of the wax taken for the test.
Acid value it is defined as the number of milligrams of KOH required to neutralize Igram of the wax. It is expressed as
mg KOH/g.
ACID VALUE=56.1xVxNxW..................................................................................................2
Where; V = volume in ml of standard potassium hydroxide solution used
N= normality of standard potassium hydroxide solution,
M=mass in grams of the wax taken for the test.
Ester value It is defined as the difference between the acid value and saponification value.
Ester Value = Saponification Value - Acid Value.................................................................3
Ester to acid ratio It is defined as the number obtained by dividing the ester value by the acid value (Sahu et al., 2016).
B) Physical assessment
1) Determination of homogeneity- The formulations were tested for homogeneity by by touch and visual appearance.
2) Determination of spreadability - Spreadability may be expressed by area extent to which the topical application
spreads when applied to the parts of the skin that is affected. Sample of known weight was applied on a known area and
spreadability factor was determined.
3) Determination of solubility- The solubility of the formulation was checked in different mediums.
4) Determination of absorption -The amount of formulation absorbed in a given area was observed.
5) Determination of the type of smear - It was determined by applying the solid perfume on the skin surface of a
human volunteer. After applying solid perfume, the type of smear or film formed on the skin was checked
6) Determination of Emolliency - Slipperiness, emolliency and amount of residue left after the applying fixed amounts
of cream was checked.
7) Determination of Physical appearance-The physical appearance of solid perfume was inspected visually against a
dark background.
8) After feel-The nature of the skin texture on the applied area was assessed after the application of the formulation.
9) Ease of Removal - The ease of removal of the cream applied was determined by washing the applied part with tap
water.
Melting point from solid perfume products generally ranged above 70°C. Solid perfume with the highest melting point
was the formulation with the lowest bees wax concentration by value 10%. The increased of melting point proportional
with the increased of product hardness¹9. This corresponded to the decreased of rheological properties along with
increased bees wax concentration. It caused a decrease in the solid perfume products' melting point at high bees wax
concentration.
Acid Number and Saponification Number of Bees wax Characterization of acid number and saponification number of
Bees wax raw material was carried out to determine the quality of the material compared with the SNI 3748:2009
quality standard. Characterization of acid number and saponification number the presence of excess free fatty acids in
Bees wax products were undesirable because it indicated low quality product due to moist and unclean storage.20The
saponification number indicates the amount of fatty acids.21
Copyright to IJARSCT DOI: 10.48175/IJARSCT-19352 416
www.ijarsct.co.in
ISSN (Online) 2581-9429
IJARSCT
International Journal of Advanced Research in Science, Communication and Technology (IJARSCT)
International Open-Access, Double-Blind, Peer-Reviewed, Refereed, Multidisciplinary Online Journal
Impact Factor: 7.53 Volume 4, Issue 1, August 2024
Standard Test-1
As per result we observed that there is no growth of microbes as compare with standard
Homogeneity Test
a) b)
c) d)
Physical evaluation, disclosed the details as mentioned in Table No 3, regarding the physical properties of the
formulation, which are essential for its applicability and stability aspect. The formulation was found to be homogenous,
witheven spreadibility, absorbability, uniform and consistent in nature.wetness, An emollient is a liquid or cream which
you put on your skin to make it softer Physical Appearance of formulation is uniform. After applied the formulation
Feel The skin was smooth and soft while performing we observed there was no microbial growth on medium microbial
colonies are not observed.
7) Packaging22
The packaging of Beeswax-based solid perfume is an essential aspect of the product's sustainability and eco-
friendliness. As a natural and sustainable alternative to traditional liquid perfumes, it is crucial to design packaging that
aligns with the product's ethos.
Here are some ideas for eco-friendly packaging options for Beeswax-based solid perfume:
1. Metal tins: Metal tins are a popular choice for solid perfumes as they are reusable, recyclable, and lightweight. They
also offer a sleek and minimalist look, which can be customized with labels or designs.
2. Glass jars: Glass jars are another eco-friendly option for solid perfumes. They are recyclable, reusable, and can be
airtight, which helps preserve the fragrance. They also have an elegant look that can be customized with labels or
etching.
3. Bamboo containers: Bamboo is a sustainable and eco-friendly material that can be used to make containers for solid
perfumes. It is a renewable resource that grows quickly, and its production has a lower carbon footprint than other
materials. Bamboo containers also offer a unique and natural look that can be customized with labels or engraving.
4. Recyclable paper packaging: Paper packaging is an eco-friendly option for solid perfumes. It is recyclable,
biodegradable, and compostable. It can also be printed with eco-friendly ink, and the design can be customized to
match the brand's ethos.
5. Upcycled containers: Upcycling containers can be an innovative way to create unique and eco- friendly packaging
for Beeswax-based solid perfume. Containers like tea tins, vintage compacts, and small glass bottles can be repurposed
to create unique packaging that aligns with the product's sustainable ethos.
Copyright to IJARSCT DOI: 10.48175/IJARSCT-19352 418
www.ijarsct.co.in
ISSN (Online) 2581-9429
IJARSCT
International Journal of Advanced Research in Science, Communication and Technology (IJARSCT)
International Open-Access, Double-Blind, Peer-Reviewed, Refereed, Multidisciplinary Online Journal
Impact Factor: 7.53 Volume 4, Issue 1, August 2024
VII. CONCLUSION
In conclusion, the development of a herbal solid perfume is a project that requires careful consideration of various
factors, including the selection of appropriate ingredients, formulation, production process, and packaging. The aim of
this project was to create a natural and sustainable solid perfume that is free from synthetic fragrances, while also
providing therapeutic benefits through the use of herbal ingredients.
The formulation of the herbal solid perfume was based on beeswax, rose oil, and a blend of essential oils. Beeswax was
chosen as the main ingredient because of its ability to provide a stable and smooth texture, while also offering emollient
and protective properties for the skin. Almond oil was added for its nourishing and moisturizing properties, and its
ability to mimic the skin's natural sebum. The essential oils was carefully selected based on their therapeutic benefits,
such as their ability to promote relaxation, improve mood, and enhance mental clarity.
The production process of the herbal solid perfume involved melting the beeswax and almond oil together in a double
boiler, then adding the essential oils and herbal extracts. The mixture was then poured into a small tin and allowed to
cool and solidify. The final product had a pleasant and natural fragrance, and was easy to apply and absorb into the
skin.
The packaging of the herbal solid perfume was designed to be simple, yet aesthetically pleasing and functional. The
small tin container was convenient and portable, allowing users to carry the solid perfume with them wherever they go.
The packaging was also eco-friendly, using minimal materials and avoiding unnecessary plastic or synthetic
components.
In terms of the evaluation of the herbal solid perfume, several tests were performed to assess its fragrance, texture,
longevity, packaging, and antimicrobial properties. The fragrance of the solid perfume was found to be pleasant and
long-lasting, while the texture was smooth and easy to apply. The packaging was deemed convenient and eco-friendly,
while the antimicrobial properties of the essential oils were found to provide some level of protection against harmful
microorganisms.
Overall, the development of the herbal solid perfume was a successful project that demonstrated the feasibility of
creating a natural and sustainable alternative to traditional liquid perfumes. The use of beeswax and herbal ingredients
provided a stable and effective formulation that was gentle on the in, while also providing therapeutic benefits. The
project also highlighted the importance of considering the environmental impact of product packaging and choosing
eco-friendly options whenever possible.
In conclusion, the herbal solid perfume project represents an exciting opportunity for further research and development
in the area of natural and sustainable cosmetics. With the growing demand for environmentally friendly and health-
conscious products, the herbal solid perfume provides a promising alternative to traditional perfumes that aligns with
these values.
The packaging of Beeswax-based solid perfume should be designed with sustainability in mind. Eco- friendly options
like metal tins, glass jars, bamboo containers, recyclable paper packaging, and upcycled containers can all be used to
create packaging that aligns with the product's natural and sustainable ethos. The packaging should be customizable to
match the brand's ethos and provide a unique and memorable experience for customers.
REFERENCES
[1]. Clark E. and Grande (1975) Study of Odour Variation with Structural Change in Cosmetic Perfume. Florida:
CRC Press.
[2]. Harvard T.H (2021) The Nutrition Source, Chan School of Public Health, Boston.
[3]. Oxford English Dictionary (ordine American English ed.) "essential oil".. Archived from the original on
2014-08-09. Retrieved 2014-07-21.
[4]. FAOStat (2020) Crops of almondwithshell. "2019.https://www.fao.org/faostat/fr/#data/QC.
[5]. S. Ramlah, "Characteristics of Quality and Effect of Polyphenol Addition to Bees wax Based Hand Body
Lotion to Skin," J. Ind. Has. Perkeb.vol. 12, no. 2, pp. 29-39, 2017.
[6]. Burger P., Plainfossé H., Brochet X., Chemat F., Fernandez X. (2019). Extraction of natural fragrance
ingredients: History overview and future trends. Chem. Biodivers.
Copyright to IJARSCT DOI: 10.48175/IJARSCT-19352 419
www.ijarsct.co.in
ISSN (Online) 2581-9429
IJARSCT
International Journal of Advanced Research in Science, Communication and Technology (IJARSCT)
International Open-Access, Double-Blind, Peer-Reviewed, Refereed, Multidisciplinary Online Journal
Impact Factor: 7.53 Volume 4, Issue 1, August 2024