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Calibration Ceftificate
Certificate no.                 9.8-26999
Task no.:                       t22-32816
Task:                           Calibration
Page:                           lof4
Enclosures:                     1 C¡lculation of Discharge Coefficient according to ISO 5L67-4.
CUSTOMER EQUIPMENT DATA:
    type:
Meter                  Venturi tube
Size:                  6INCH/ASME1500/DN150
       lYear:
Serial no,             220048-D01-t | 2022
   no.:
TAG.                   ÐC(-FE-105
Manufacturer:                   EUROMISURE
CUSTOMER:                       EUROMISURE S.a.s. - A division of the WIKA Group
                                Via Giuseppe Borghisani 4,
                                26035 Pieve San Giacomo (CR), Italy
                          Att.: Leonardo Guarneri
                           PO: PO00017873-3
TEST METHOD/MEDIUM:             Volume flow of natural gas with a static pressure of 30 bar g.
SCOPE OF TEST:                  Calibration at the flows 413, 652, 897, LL42, L46B and 1631   ¡r/h   with 3
                                repetitions.
FOUNDATION:                     FORCE No. 60.10.4.02 Calibration   with 24INCH HPCL no. C03-002.
DATE OF CALIBRATION:            16-11-2022
TRACEABILITY:                   The laboratory is traceable to the harmonized European cubic meter for
                                naturalgas; EuReGa.
                                Working standards used, and calibration setup are given on page 4.
REMARKS:                        Technical evaluation: No Remarks.
ISSUE DATE:                     30-11-2022
SIGNATORIES
                                                                                                  \\\-_
                                                                       Flemming
                                Task   manager                         Signatory
Excel book Venturi tubes HPCL24 version 2.1.
FORCE Technology, Navervej 1, 6600 Vejen, phone: +45 43 25 00 00.
Danish, Designated institute (DI) for gas measurement.
Extracts from the certificate may only be reproduced with a written permission from FORCE Technology.
Cedificate no               9.8-26999
Task no.:
Page:
                            122-32816
                            2of     4
                                                                                                                  FORCE
                                                       Results
Meter data:
Meter type:                 Venturi tube                               Serial no.   / Year:          220048-D011     I   ZO2Z
Size:                       6rNCH/ASME1s00/DN1s0                       TAG. no.:                     )cc(-FE-105
CALIBRATION RESULTS
                                          Upstream pressure tapping                  Average of
              Average of                                 Average of     Measured      Measured         Standard    Absolute     Tempe-
 True flow      True flow   xUcmc       "Reynoldsno.   "Reynolds no       dP             dP           unceftainÇ   Pressure     rature
   m3/h           m3/h        o/o                                         mbar             mbar         mbar          bara        "c
  414,82                     0,17        2,00E+06                        118,99                         0,297        30,916      19,25
  4t4,72                     0,t7        2,00E+06                        118,99                         0,297        30,916      t9,25
   414,69       4r4,744      0,17        2,00E+06       2,000E+06        119,05        1   19,0 14      0,297        30,914      19,25
    645,3                    0,I7        3,11E+06                        286,22                         0,317        30,915      19,30
    645,4                    0,L7        3,11E+06                        285,88                         0,328        30,915      19,27
    645,4        645,35      0,r7        3,11E+06       3,111E+06        286,22       286,106           0,325        30,919      19,30
   891,4                     0,L7        4,29E+06                        551,46                         0,4t6        30,946      L9,72
   891,9                     0,t7        4,29E+06                        551,15                         0,401        30,943      t9,87
   89t,7         891,66      0,L7        4,298+06       4,289E+06        551,01       551,206           0,400        30,940      19,66
   1150,9                    0,t7        5,55E+06                        936,97                         0,624        30,969      19,57
   1151,6                    0,t7        5,55E+06                        938,60                         0,526        30,965      t9,46
   1151,9        1151,48     0,t7        5,55E+06       5,552E+06        938,53       938,034           0,563        30,974      19,54
   1446,7                    0,t7        6,978+06                        1529,00                        1,000        31,006      L9,71
   L446,6                    0,r7        6,978+06                        1528,80                        1,000        31,003      t9,73
   1446,9        1446,73     0,L7        6,97E+06       6,974E+06        1529,85      1529,2t4          1,000        31,000      19,7t
   1595,8                    0,I7        7,708+06                        1887,33                        1,000        31,0r7      19,65
   1595,6                    0,17        7,70E+06                        1886,56                        1,000        31,023      19,67
   1594,3        t595,24     0,I7        7,69E+06       7,695E+06         t882,62     1885,503          1,000        3t,02L      19,70
Note x        The calibration and measurement capability Ucmc includes all significant contributions except the
              meter's contributions, It is the calibration facility's expanded uncertainty excluding contributions
              from the calibrated Venturi tube, See also Measurement UnceftainÇ on page 4.
Note "        Reynolds no. are non-accredited services. Density are calculated according to AGA 8 Third Edition April20t7
              Viscosity are calculated according to Viscosity Measurements and Predictions for Natural Gas, P. Schley,
              M. Jaeschke, C Küchenmeister and E. Vogel.
Cetificate no,:        9.8-26999
Task no.:              L22-328r6
Page:                  3of4
GALTBRATTON RESULTS, CONTTNUED
                                      Differential Pressure curve
          2000
          1800
          1600
          1400
     (o
    -o
     E
     o-
    E
    so    1200
     qJ
     b0
     t!
     o
          1000
            800
            600
            400
            200
              0
             1,5E+06    2,5E+06    3,5E+06    4,5E+06      5,5E+06   6,5E+06   7,5E+06   8,5E+06
                                                Reynolds no.
    Certificate no.:     9.8-26999
    Task no.:            122-328L6
                         4of4
                                                                                                    H
                                                                                                    t:l   FORCE
    Page:
                                                                                                    EÉI I@M@
    CALIBRATION EQUIPMENT
    Calibration facility no. C03-002.
    Working standards: Turbine meters and rotary meter.
    Traceability: EuReGa, The European Harmonized cubic meter for natural gas
    Calibration and measurement capability Ucmc is 0,t7o/o.
               Standards used duri             the calibration
            WS used              FORCE        Id.          Flow ra
i
               X                    WS1                  650   - 4000   m3/h
                                    WS2                  650   - 4000   m3/h
                                    WSs                  650   - 4000   mg
                                    WS4                  650   - 4000   ma h
               X                    Wss                  120   - 1000 ms I h
                                    WS6                        8 - 400 m3/h
                                    WS7
    Other
               used                                           FORCE No.
               X                         re
               X            Pressure gauges           PT}C(
               X            dP Pressure               PDTrc(
               X            dP Pressure qauqe         A80241                       0-500 mbar
                               Pressure               480242                       500-1000 mbar
                            dP Pressure gauge         A80243                       0-100 mbar
                            dP Pressure               A20072                       0-2500 mbar
                            Micromanometer            A00027                       0-50 mbar
               X            Multimeter                AOOOBB
    ROOM TEMPERATURE AND BAROMETRIC PRESSURE
    Room temperature were within the interval [20,9"C ; 20,9oC]
    Barometric pressure were within the interual [1002,5mbar            ; 1002,6mbar]
    CALIBRATION SETUP
    Up-stream                                                                      Down-stream
    Spool 6STD-L2-ID 142,6 mm length 4027 mm                                       Adapter 390 mm
    Adapter 390 mm                                                                 Spool 6STD-L2-ID L44,3 mm lenght 2023 mm
    Temperature measurement 700 mm down-stream meter,
    Pressure measurement at upstream pressure tapping.
    GAS MIXTURE
                                   Name                   Col¡¡rqqltion
                                                                  molo/o       I
    rCH4                       Methane                             98,36       )
    c2H6                       Ethane
    C3HB
    n-C4H10                    n-Butane
    i-c4H10                    i-Butane
    n-C5H12             !
                               n-Pentane
    i-csH12                    i-Pentane
    :cdl                       Hexane
     coz                       Carbon dioxide                      0!914       ,
    N2                         Ni!¡99en                            0,724
                                                                   100,0
    M EASU REM ENT UNCERTAINTY
    The coverage factor k is 2 in all calculations of expanded uncertainty.
    The reported expanded uncertainty of measurement is stated as the standard uncertainty of measurement
    multiplied by the coverage factor k such that the coverage probability corresponds to approximately 95 o/o.
Certificate No.:          9.8-26999
Task No.:                 122-328t6                                                                     FORCE
Enclosure:                1                                                                               TECHNOLOGY
Page:                     IofZ
             Calculation of Discharge Coeffic¡ent accord¡ng to ISO 5L67'4
             The data marked with a x on this enclosure are non-accredited seruices
Meter data
Pipe Inner Diameter:                     142,47 mm                              Diameter Ratio:                         0,4649
Throat Diameter:                          66,24 mm
                                                                                          xDensity at
   True         True          xTrue      Diff.               xlsent.   Pres.      Eksp.    entrance     xDischarge    xAverage
   flow            flow   mass flow    Pressure   Pressure    exp.     Relati    factor     cylinder    coefficient      of
                   Qu           rh       AP          P1         K         T         €          p            cd           cd
    Qu
   m3/h         m3/s           kg/s     mbar       mbar                                     kg/m3
  4t4,82       0,1 1523       2,5442   118,99      30916     1,3268    0,9962    0,9977     22,079        0,9967
  414,72       0,1 1520       2,5436   118,99      30916     1,3268    0,9962    0,9977     22,090        0,9965
  4t4,68       0,11519        2,5432   119,05      30914     1,3268    0,9961    0,9977     22,078        0,9961       0,9964
  645,3        0,t793         3,957    286,22      30915     1,3268    0,9907    0,9944     22,074        1,0029
  645,4        0,1793         3,958    285,88      3091s     t,3268    0,9908    0,9944     22,078        1,0036
  645,4        0,t793         3,958    286,22      30919     1,3268    0,9907    0,9944     22,078        1,0031       1,0032
  89t,4         0,2476        5,462    551,46      30946     t,3267 0,9822       0,9892     22,059        1,0029
  891,9         0,2477        5,461    551,15      30943     t,3266 0,9822       0,9892     22,042        1,0033
  89t,7         0,2477        5,464    551,01      30940     1,3267    0,9822    0,9892     22,060        1,0037       1,0033
  1150,9       0,31971        7,0622   936,97      30969     r,3267    0,9697    0,9817     22,089        1,0018
  1151,6       0,31990        7,0688   938,60      30965     1,3268    0,9697    0,9816     22,097        t,0017
  1151,9       0,31996        7,0699   938,53      30974     1,3268    0,9697    0,9816     22,096        1,0019       1,0018
  t446,7       0,40186        8,8830   1529,00     31006     1,3267    0,9507    0,9700     22,t04        0,9979
  1446,6       0,40183        8,8806   1528,80     31003     t,3267    0,9507    0,9700     22,100        0,9978
  L446,9       0,40192        8,8827   1529,85     31000     I,3267    0,9507    0,9700     22,t}t        0,9977       0,9978
  1595,8       0,44327        9,8011   1887,33     31017     1,3268    0,9392    0,9629     22,tlr        0,9982
  1595,6       0,44323        9,8014   1886,56     31023     1,3268    0,9392    0,9630     22,tL4        0,9983
  1594,3       0,44287        9,7918   1882,62     31021     t,3267    0,9393    0,9630     22,110        0,9984       0,9993
                                                              Average of all Discharge    coefficients:   1,0001
Certificate No          9.8-26999
Task No.:
Enclosure:
                         122-328t6
                         1
                                                                               FORCE
Page:                   2ofZ
             Calculation of Discharge Coefficient according to ISO 5L67-4, cont¡nued
The following formulas are not covered by DANAK accreditation no. 9
         r Isentrop exponent       (Cplq,)
         r Pressure relation
         p Density
         e Ekspansions factor
         p Diameter ratio
        Cd Discharge coeffic¡ent
        Co Isobaric heat capacity
        q   Isochoric heat capacity
          d Throat diameter
          D Pipe inner diameter
         rh Mass flow rate
         P1 Upstream pressure
         P2 Throat pressure
        AP Differential pressure
        Qv Volume flow rate
                                                           +xJt-g*
                                      C¿     = rhx
                                                     exnxdzx 2xLPxp
                                        rcxtzl* 7_ß4     1_T(rc-t)lrc
                               t
                                         rc_I 1_ß4x.r¿ltc L_t
                                                         tit= pxQ.
                                                          P2 P1-LP
                                                     T
                                                          P.     P"
End of ceftificate.