Polyethylene Plastics Pipe and Fittings Materials: Standard Specification For
Polyethylene Plastics Pipe and Fittings Materials: Standard Specification For
Designation: D3350 − 21
1 2
This specification is under the jurisdiction of ASTM Committee D20 on For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Plastics and is the direct responsibility of Subcommittee D20.15 on Thermoplastic contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Materials. Standards volume information, refer to the standard’s Document Summary page on
Current edition approved July 1, 2021. Published July 2021. Originally approved the ASTM website.
3
in 1974. Last previous edition approved in 2014 as D3350 – 14. DOI: 10.1520/ The last approved version of this historical standard is referenced on
D3350-21. www.astm.org.
3. Flexural D790 Unspecified <138 138- 276- 552- 758- >1103 Specify
modulus, MPa (psi) (<20 000) <276 <552 <758 <1103 (>160 000) Value
(20 000 to (40 000 to (80 000 to (110 000 to
<40 000) 80 000) 110 000) <160 000)
4. Tensile strength D638 Unspecified <15 15-<18 18-<21 21-<24 24-<28 >28 Specify
at yield, MPa (psi) (<2200) (2200- (2600- (3000- (3500- (>4000) Value
<2600) <3000) <3500) <4000)
5. Slow Crack
Growth Resistance
I. ESCR D1693 Unspecified
a. Test condition A B C C ... ... ... Specify
(100% Igepal.)D Value
b. Test duration, h 48 24 192 600
c. Failure, max, % Unspecified 50 50 20 20
II. PENT (hours) F1473
Molded plaque, Unspecified ... ... ... 10 30 100 500 Specify
80°C, 2.4 MPa Value
Notch depth, Unspecified
F1473, Table 1
6. Hydrostatic Strength
Classification
I. Hydrostatic design D2837 NPRE 5.52 6.89 8.62 11.03 ... ...
basis, MPa (psi), (23°C) (800) (1000) (1250) (1600)
II. Minimum required ISO 12162 ... ... ... ... ... 8 10
strength, MPa (psi), (20°C) (1160) (1450)
A
Compliance with physical properties in accordance with Section 8 is required including requirements for cell classification, color, and ultraviolet (UV) stabilizer, thermal
stability, brittleness temperature, density, tensile strength at yield, and elongation at break.
B
Refer to 10.1.4.1.
C
Refer to 10.1.4.2.
D
There are environmental concerns regarding the disposal of Nonylphenoxy poly(ethyleneoxy) ethanol (CAS 68412-54-4) for example, Igepal CO-630. Users are advised
to consult their supplier or local environmental office and follow the guidelines provided for the proper disposal of this chemical.
E
NPR = Not Pressure Rated.
D2837 Test Method for Obtaining Hydrostatic Design Basis F2263 Test Method for Evaluating the Oxidative Resistance
for Thermoplastic Pipe Materials or Pressure Design Basis of Polyethylene (PE) Pipe to Chlorinated Water
for Thermoplastic Pipe Products 2.2 ISO Standard:
D2839 Practice for Use of a Melt Index Strand for Deter- ISO 12162 Thermoplastic Materials for Pipes and Fittings
mining Density of Polyethylene for Pressure Applications—Classification and
D3035 Specification for Polyethylene (PE) Plastic Pipe (DR- Designation—Overall Service (Design) Coefficient
PR) Based on Controlled Outside Diameter
D3892 Practice for Packaging/Packing of Plastics 3. Terminology
D4218 Test Method for Determination of Carbon Black 3.1 Definitions:
Content in Polyethylene Compounds by the Muffle- 3.1.1 Terms as described in Terminology D883 shall apply
Furnace Technique in this specification.
D4703 Practice for Compression Molding Thermoplastic 3.1.2 polyethylene plastics, n—as defined by this
Materials into Test Specimens, Plaques, or Sheets specification, plastics or resins prepared by the polymerization
D4883 Test Method for Density of Polyethylene by the of no less than 85 % ethylene and no less than 95 % of total
Ultrasound Technique olefins with additional compounding ingredients.
D4976 Specification for Polyethylene Plastics Molding and
Extrusion Materials 3.2 Definitions of Terms Specific to This Standard:
D5033 Guide for Development of ASTM Standards Relating 3.2.1 base materials, n—PE material without non-black or
to Recycling and Use of Recycled Plastics (Withdrawn black pigment, supplied to industry, that is either a PE
2007)3 compound classified by this Standard or a component of a PE
F1473 Test Method for Notch Tensile Test to Measure the compound classified by this standard.
Resistance to Slow Crack Growth of Polyethylene Pipes 3.2.2 PE compounds, n—has the same meaning as PE
and Resins plastics materials, compounds, and plastics.
S 5 3 PL/2 bd2
10.1.9.1 Specimens—Press small pieces of the pipe into
films 0.127 6 0.013 mm (0.0050 6 0.0005 in.) thick. Cut at
where: least three disks 6.35 6 0.13 mm (0.250 6 0.005 in.) in
S = stress in the outer fiber at 2 % strain, diameter from the film.
P = load corresponding to 2 % strain, N (lbf), 10.1.9.2 Procedure—Place the disk of film in a small
L = test span = 50 mm (2 in.), aluminum cup used in the DSC in a stretched condition, as
d = specimen depth = 3.2 mm (1⁄8 in.), and shown in Fig. 1(a). Place a small piece of indium (melting
b = specimen width = 12.7 mm (1⁄2 in.). point 156.6°C) or anisic acid (melting point 183.0°C) for a
The secant modulus at 2 % strain is the ratio of stress to temperature reference standard contained in a similar cup (see
strain or S/0.02. Fig. 1(b)) in the reference position. Use an oxidized copper
10.1.6 Tensile Strength at Yield—The tensile strength at
yield and elongation at break shall be determined in accordance
with Test Method D638. The speed of testing shall be 500 4
Instruments are available from TA Instruments, Perkin-Elmer, and others.
reference disk for black, filled, or dark brown test specimens 10.1.10 Carbon Black Content—Test Method D1603 or Test
and an aluminum disk for natural or light pigmented polymers. Method D4218 shall be used. Make duplicate determinations
Place the specimen and reference standard cups in the instru- from a sample of the material in the form of powder, granules,
ment which is preset at approximately 150°C. The bottoms of or pellets.
the cups shall be pressed and rubbed securely against the flat 10.1.11 Oxidative Resistance Test—Test specimens shall
surface so as to ensure that thermal contact is made. Allow 5 consist of extruded 4-in. DR11 IPS pipe meeting the dimen-
min for the cups to reach thermal equilibrium. Begin the sional requirements of Specification D3035. All specimens
programmed heating at approximately 150°C at a heating rate shall be from the same lot of pipe. Test a minimum of five (5)
of 10.0°C/min in static air. Test at least three film specimens specimens in accordance with Test Method F2263 at one of the
from each sample and use the average value for the induction temperature and stress combinations of Table 2.
temperature.
NOTE 15—If a selected temperature/stress condition results in prema-
NOTE 14—Since the indium standard may change with use, it should ture failures, testing may be conducted at a lower stress as shown in Table
not be used more than 30 times without confirming that no significant 2.
change in melting point has occurred. This check can be made by
comparison with a fresh piece of indium. 10.1.11.1 Calculation—Calculate the log average test time
10.1.9.3 Results—The temperature change (ΔT) or heat using all failures and non-failures. All specimens shall have
absorption rate (J/s) in the specimen plotted against tempera- been tested at the same nominal test stress. Data from not less
ture shall produce a line with a clear rise in slope. The than five specimens are required for compound classification.
induction temperature (degradation onset) is the intersection of 10.1.11.2 Significance—Testing is only required to be per-
the extended base line and a line tangent to the leading slope of formed on representative pipe samples for the original valida-
the exothermic decomposition peak (see Fig. 2). tion of a particular compound.
11. Inspection at the lowest rate to the point of delivery, unless otherwise
11.1 Inspection of the material shall be made as agreed upon specified in the contract or order.
between the purchaser and the manufacturer as part of the 13.2 Marking—Unless otherwise agreed upon between the
purchase contract. seller and the purchaser, shipping containers shall be marked
with the name of the material, identification in accordance with
12. Retest and Rejection
this specification, the lot or batch number and quantity con-
12.1 If any failure occurs, and when specified by the tained therein, as defined by the contract or order under which
manufacturer, the material shall be retested to establish con- shipment is made, and the name of the manufacturer.
formity in accordance with the agreement between the pur-
chaser and the manufacturer. 13.3 All packing, packaging, and marking provisions of
Practice D3892 shall apply to this specification.
13. Packaging and Marking
13.1 Packaging—The material shall be packaged in stan- 14. Keywords
dard commercial containers, so constructed as to ensure 14.1 cell classification system; pipe and fittings material;
acceptance by common or other carriers for safe transportation polyethylene; recycled
Committee D20 has identified the location of selected changes to this standard since the last issue
(D3350 – 14) that may impact the use of this standard. (July 1, 2021)
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