cp501405 Rev7
cp501405 Rev7
Amundsenweg 13
4462 GP Goes
The Netherlands
430-GC
Pre-installation Requirements
The information provided here will help you identify and prepare a suitable installation site
for your 430-GC. This instrument is a stand-alone version that is equipped with a display,
keypad, detector and/or GSV/LSV.
The Bruker 430-GC has been designed to operate reliably under carefully controlled
environmental conditions. It is your responsibility to provide a suitable location, power
source, and operating environment. Operating or maintaining a system in conditions outside
of the power and operating environment limits described below could cause failures of many
types. The repair of such failures is specifically excluded from the Warranty and Service
contract conditions.
All phases of the installation site preparation must conform to local safety,
electrical, and building codes. These codes take precedence over any
recommendations in these instructions, and compliance to them is the
responsibility of the customer.
© 2012 Bruker Chemical Analysis B.V. Printed in the Netherlands CP501405 Rev:7 January 2012
Bruker Chemical Analysis B.V.
Table of Contents
POWER REQUIREMENTS............................................................................................................................... 4
INSPECTION .................................................................................................................................................. 12
SPARE PARTS............................................................................................................................................... 13
PREVENTIVE MAINTENANCE...................................................................................................................... 13
Tables
Requirements
Principal installation area is in compliance with all relevant safety regulations
Entrance to the lab is at least 91.5 cm (36 in.) wide
Sufficient bench space is available for all components
Bench can support system weight
Specified electrical supply and power outlets installed
Lab temperature maintained between10 and 40 °C (50 and 104 °F)
Relative humidity maintained between 5 and 95% RH
Laboratory is free of excessive particulate matter
System bench is free from vibrations
Exhaust system is suitable
Carrier gas, regulator, and gas lines are installed.
Detector gas, regulator, and gas lines are installed.
Appropriate gas filters are on site
If the GC will be connected to the company network, the required materials are on site
The shipping cartons were examined for damage and if damaged, the conditions were
reported
If Bruker is performing the installation, the system operator is available during the
installation
After preparing your site, contact the Customer Service office in your region to schedule installation. Keep
this checklist available, and review it with your Bruker Representative.
Before arranging for delivery of the 430-GC to your facility, please make sure that all
passages to the site of installation are least 91.5 cm (36 in.) wide. Allow additional room for
maneuvering the shipping container around corners and/or through doors.
Table 1 identifies the space and weight requirements of the 430-GC components. The GC
is intended to sit on a workbench that is wide enough and deep enough to accommodate
these components, and sturdy enough to support their combined weight. Allow at least 5
cm (2 in.) of space at the sides and rear of the GC to permit free air circulation. For optimum
column oven cooldown performance, 15 cm (6 in.) is required at the rear of the instrument.
Power Requirements
A separate circuit is required for each 430-GC. The mating socket must have adequate
amperage capacity and a reliable ground.
Note: 120V and 101V GCs are designed for single phase User only.
All voltages of the 430-GC are supplied with a standard molded power cord with an
IEC60320 “Hot” connector. This connector plugs into the receptacle on the rear of the GC
as shown below. This power cord can be replaced to suit local power requirements.
Ground (green/yellow)
Line 2
(blue)
Line 1 (brown)
Ground
(green/yellow)
Use of a 430-GC near the low limit of the permissible line voltage will increase the time
required for thermal zones to reach their final setpoint temperature, and may adversely
reduce the maximum usable ramp rate for programmable thermal zones.
Care must be taken to ensure that sources of radio frequency interference (RFI) and
electromagnetic interference (EMI) are not placed on the same power line, or share the
same ground plane, since this can degrade the performance of the GC. Equipment such as
motors, solenoids, fluorescent light fixtures, and radio communication transmitters should
be isolated from the instrument and connecting cables as much as possible.
Operating Environment
You are responsible for providing an acceptable operating environment. Attention paid to
the operating environment will ensure the continued peak performance of your 430-GC.
The 430-GC is intended for indoor use and certified to an altitude of 2000 meter. Protect
your GC from corrosive chemicals or gases and from direct venting of air conditioners,
heaters, furnaces or fans.
Temperature/Humidity
The optimal operating temperature range for the GC is between 10 to 40 °C (50 to 104 F).
The acceptable storage temperature is between -20 to 65 °C (-4 to 149 F).
Hot air vented from the GC column oven may contribute to room heating and to the resulting
air conditioning load. Ducting the GC column oven air out of the lab should reduce this
heating effect.
The relative humidity (RH) of the operating environment must be between 5 and 95%, with
no condensation. Operating the GC at very low humidity will result in the accumulation and
discharge of static electricity which shortens the life of electronic components. Operating
the system at high humidity will produce condensation and result in short circuits.
Particulate Matter
Vibration
Ensure that laboratory benches are free from vibrations, e.g., those caused by equipment in
adjoining locations.
Exhaust System
It is your responsibility to provide an adequate exhaust system. Consult local regulations for
the proper method of exhausting the fumes from your system.
Gas Requirements
H2 40 psig / 2.8 bar/ 280 kPa 100 psig / 6.5 bar/ 650 kPa 99.999
TCD Makeup Gas: He, N2, Ar 80 psig / 5.5 bar/ 550 kPa 150 psig / 10 bar/ 1000 kPa 99.999
Makeup Gas: H2 40 psig / 2.8 bar/ 280 kPa 100 psig / 6.5 bar/ 650 kPa 99.999
He, N2, Ar 80 psig / 5.5 bar/ 550 kPa 150 psig / 10 bar/ 1000 kPa 99.999
H2 40 psig / 2.8 bar/ 280 kPa 100 psig / 6.5 bar/ 650 kPa 99.999
FID Detector Gas: H2 40 psig / 2.8 bar/ 280 kPa 100 psig / 6.5 bar/ 650 kPa 99.999
Air 60 psig / 4.1 bar/ 410 kPa 100 psig / 6.5 bar/ 650 kPa 0 grade
Makeup Gas: He, N2 80 psig / 5.5 bar/ 550 kPa 150 psig / 10 bar/ 1000 kPa 99.999
* High pressure applications requires inlet pressure between 80-160 psig / 5.5 – 10 Bar
Obtain gases for chromatographic use from a supplier who is aware of your
requirements. An analysis of selected impurities is used to determine the purity
rating for a given gas. If your supplier does not establish purity based on an
analysis of appropriate chromatographic contaminants, a purity rating of 99.999%
may not be suitable for GC use. A quality supplier of gas and the regular use of
filters will minimize system contamination problems.
Detector
Carrier Gas Oxygen Filter Moisture Filter Column
TCD
Makeup Gas: He, N2, Ar
Reference
H2 Channel
TCD
Moisture filter: BRF0101
Oxygen filter : BRF0102
Make-Up Gas
(if necessary)
Detector
Carrier Gas Oxygen Filter Moisture Filter Column
FID
Detector Gas: H2
Air Make-Up
Gas
Makeup Gas: He, N2 Hydrogen Charcoal Filter
Moisture filter: BRF0101 FID
Oxygen filter : BRF0102 Air Charcoal Filter
Charcoal filter: BRF0103
Detector
Carrier Gas Oxygen Filter Moisture Filter Column
FID
Detector Gas: H2 Make-Up Gas Charcoal Filter
Air
Makeup Gas: He, N2 Hydrogen Charcoal Filter
Observe safe laboratory practice in the transportation, storage, and usage of gas cylinders
under high pressure.
Never move a cylinder with a regulator installed. Make sure safety cap is in place over
valve when transporting cylinder.
Always chain or strap cylinders in the laboratory and in storage.
Always use cylinder condition labels to show whether tank is FULL, IN USE, or EMPTY.
Always leave at least 100 psig (6.9 bar) residual gas in a depleted cylinder. Always
store in empty tank storage area with tank valve closed. Empty cylinders should be
clearly marked as such and dated.
Do not expose cylinders to temperatures above 125 °F (50 °C).
Regulator Installation
Carrier gases must have a two-stage regulator having a 0–100 psig (6.9 bar) low-pressure
stage. The inlet pressure for He is normally 80 psig (5.5 bar).
Pressure inlet must be 30 psig (2 Bar) higher then the Column Head Pressure.
Gas Connections
Helium and other gasses are connected to 1/8" Swagelok fittings on the rear of the
instrument.
*For use on pipe fittings ONLY. Never use Teflon tape on Swagelok fittings.
A 1/16" Stainless Steel tubing is required to connect the carrier gas supply cylinder to the
instrument bulkhead fitting. However, additional tubing may be required to connect the GC
to the required gas supplies.
Gas Lines
Table 5: Stainless Steel Tubing
Use these plastic closures to keep metal tubing interiors clean during storage.
Gas Filters
Carrier gas filters should be installed to further clean high purity gases, reduce detector
noise, and protect the chromatography system from potential contamination. Carrier gas
filters should be installed where the indicator is visible. The following filters are
recommended for GC systems (see Table 2 for filter kit part numbers):
IMPORTANT NOTE: Filters are used to remove small amounts of contaminants from high
purity gases. They are not capable of removing all of the contaminants from low purity
gases. The purity specifications listed in Table 2 are minimum acceptable values.
BRB1110B8P Gas Clean GC/MS filter kit (incl. 1 connecting unit 1/8” and 2 GC/MS filters)
BRB1110B4 Gas Clean GC/MS filter kit (incl. 1 connecting unit 1/4” and 2 GC/MS filters)
BRB1110SK8 Gas Clean GC/MS filter installation kit (incl. CP17976 1 mtr copper tubing, 2 nuts and 2 ferrules 1/8”)
CP736530 Gas Clean filter kit (connecting unit for 4 filters, incl. 4 filters (1/8” tube))
Network Requirements
If you intend to connect your 430-GC to a company network, you will need to provide a
standard network cable with RJ45-style connectors on both sides. In addition, the company
network must allow TCP/IP communications to be routed across it from the 430-GC to the
Workstation.
You or your network administrator must provide any hardware, adapters, cables, and
configuration and setup work required to convert from the company network wiring type to 430-
GC network.
Inspection
When your 430-GC arrives, carefully inspect the exterior of the shipping cartons for
evidence of any damage that might have occurred during shipment. Inspect the cartons for
the following:
Water stains
Cuts, punctures, or deep indentations
Crushed corners or excessively abraded edges
If one or more of the above conditions are evident on any of the shipping cartons, report the
conditions to the carrier at time of receipt.
Systems are shipped either FOB Bruker or FOB Destination. The manner of shipment
determines who has responsibility for filing a claim against the carrier if the system is
damaged in transit. Most systems are shipped FOB Bruker, and in this instance any
damages incurred in shipment are the responsibility of the purchaser and the carrier.
Contact Bruker Service for assistance with claims filing and billing for repairs if necessary. If
the system is shipped FOB Destination, contact Bruker Order Processing who will file a
claim against the carrier. Note, however, that Bruker will not accept liability for damage if
you receive obviously damaged materials but do not make note of the damage on the
receiving documents.
If none of the conditions listed above are evident after inspecting the shipping carton, place
the shipping container on the floor near the installation site. Before proceeding, you should
make sure that the site to be used for installation has the required power and meets the
space requirements described in these instructions.
If a Bruker Representative installs your instrument, the representative will demonstrate the
fundamentals of operating the GC and will review the maintenance procedures.
To take full advantage of this on-site visit, please arrange to have your system operator
available during the installation. The Bruker Representative will run a chromatogram using a
test column and sample. Be sure the conditions are recorded on the chromatogram. Store
the chromatogram for future use in analyzing possible chromatographic problems.
At the time of installation, the Bruker Representative will demonstrate that your system
meets the performance specifications written into your sales contract. Please do not make
plans to analyze samples with the system until after the installation has been completed and
you have accepted the conditions of delivery.
Spare Parts
The 430-GC User Manual provides a list of spare parts for normal operation.
Preventive Maintenance
Please note that it is essential that you perform regular preventive maintenance on your GC.
By performing this maintenance, you will increase the life of the system, increase system
uptime, and enjoy optimum system performance. Please refer to the Maintenance section of
the 430-GC User Manual for details.