Lecture 5 – Evaporation (Part 2)
Dr. Hanee Farzana Hizaddin
KIL3007 Separation Processes 2
www.um.edu.my
Learning Outcomes
 Calculations for multiple effect evaporators
                                                2
Motivation
In evaporation of solutions in a single-effect evaporator, a
major cost is the cost of the steam used to evaporate the
water.
A single-effect evaporator is wasteful of steam costs, since
the latent heat of the vapor leaving the evaporator is usually
not used.
However, to reduce this cost, multiple-effect evaporators are
used which recover the latent heat of the vapor leaving and
reuse it.
                                                                 3
                              Vi                         Va                          V3
             F                                      T
                                                    Yi
                      I
                                                                  v,       Is
                                                                                              v2   ,   Tsz
                 Ps                         S TsI
                                              ,
                                                                       ,
                                                                                T2
                               L1   ,
                                        x
                                        ,                Le   ,   2                  L3 X3,
In the first effect raw steam is used as the heating medium to this first effect, which is boiling at
temperature T1 and pressure P1.
The vapor removed from the first effect is used as the heating medium, condensing in the second effect
and vaporizing water at temperature T2 and pressure P2 in this effect.
To transfer heat from the condensing vapor to the boiling liquid in this second effect, the boiling
temperature T2 must be less than the condensing temperature. This means that the pressure P2 in the
second effect is lower than P1 in the first effect.
In a similar manner, vapor from the second effect is condensed in heating the third effect.
Hence, pressure P3 is less than P2 .
If the first effect is operating at 1 atm abs pressure, the second and third effects will be under vacuum.
                                                                                                             4
In the first effect, raw dilute feed is added, and it is partly concentrated.
Then this partly concentrated liquid flows to the second evaporator in series, where it is
further concentrated.
This liquid from the second effect flows to the third effect for final concentration.
When a multiple-effect evaporator is at steady-state operation, the flow rates and rate of
evaporation in each effect are constant.
The pressures, temperatures, and internal flow rates are automatically kept constant by
the steady-state operation of the process itself.
To change the concentration in the final effect, the feed rate to the first effect must be
changed.
The overall material balance made over the whole system and over each evaporator itself
must be satisfied.
If the final solution is too concentrated, the feed rate is increased, and vice versa.
Then the final solution will reach a new steady state at the desired concentration.
                                                                                             5
Comparison between Forward Feed vs. Backward/Reverse Feed
                                          https://www.yasa.ltd/post/multiple-
                                          effect-evaporator-forward-feed-
                                          backward-feed-parallel-feed-for-
                                          multi-effect-evaporation
                                                                                6
Temperature Drops and Capacity of Multiple-Effect Evaporators
                 constant
                                                                7
                      /Va
ATa   =
          EAT
                10.   +   /on + Vs
                                     8
9
Calculations for Multiple-Effect Evaporators
In doing calculations for a multiple-effect evaporator system, the values to
be obtained are usually the area of the heating surface in each effect, the kg
of steam per hour to be supplied, and the amount of vapor leaving each
effect, especially the last effect.
The given or known values are usually as follows:
 »   1. steam pressure to first effect,
 »   2. final pressure in vapor space of the last effect,
 »   3. feed conditions and flow to first effect
 »   4. the final concentration in the liquid leaving the last effect
 »   5. physical properties such as enthalpies and/or heat capacities of the liquid and vapors, and
 »   6. the overall heat-transfer coefficients in each effect.                                  &           10%
Usually, the areas of each effect are assumed equal.             by finding but later   we   have to reconfirm
                                                                                                                  aug   area
The calculations are done using material balances, heat balances, and the
capacity equations =            for each effect.
A convenient way to solve these equations is by trial and error.
                                                                                                                               10
Step-by-Step Calculation Methods for Triple-Effect Evaporators
                                                                 11
                          area          value       are
    see     if    each
    close        to   each        other     .
    so    kind        average      ,
                                       if       less than
                                                          then
M                             % difference
                             10
                             acceptable .
                                                                 12
13
Example 1: Evaporation of Sugar Solution in a Triple-Effect Evaporator
  A triple-effect forward-feed evaporator is being used to evaporate a sugar
  solution containing 10 wt.% solids to a concentrated solution of 50%. The boiling-
  point rise of the solutions (independent of pressure) can be estimated from
  BPR°C = 1.78 + 6.22 2 ,where is wt. fraction of sugar in solution. Saturated
  steam at 205.5 kPa [121.1°C saturation temperature] is being used. The pressure
  in the vapor space of the third effect is 13.4 kPa. The feed rate is 22 680 kg/h at
  26.7°C. The heat capacity of the liquid solutions is cP = 4.19       2.35 kJ/kg· K.
  The heat of solution is considered to be negligible. The coefficients of heat
  transfer have been estimated as U1=3123, U2=1987, and U3=1136 W/m2.K. If each
  effect has the same surface area, calculate the area, the steam rate used, and
                                Az             A,       Az
  the steam economy.                                =        =
     S
                        Vi   +   v2   +   Ve
  steam   economy
                    =
                                                                                        14
Solution
           15
              F       +        b                =
                                                            $         +           vi       +    vz   +   vz   +   43
                       F       =            V
                                                    ,
                                                        +       Ve       +       Vz    +   43
                                            V,                  vz
         22688                 =                        +                +       Vz    +
                                                                                           13
              Fxz              =
                                       L3Xz
     (22680)               (0 10)  .
                                                    =
                                                            13 (0 50)    .
                           13          =
                                                4536kg/h
         Assume                V,           =
                                                    V2       =
                                                                    V.
         22680             =
                                       Vi       +       V2      +    V3      +    4536
         22680             =           3V , + 4536
         Vz
Vz                V=                   6048                 kgth
     =        =            =
     effect       1        :
                                       FXF              =
                                                             L, X
     effect       2        :           L , X1           :
                                                                12   X
                                                                             2
     effect
                           :
                  3                    LeXc                 =
                                                                    13 X
16
17
                                                                                                         T
        these          all                                               letak   15 C
                                                                                  %
                                                                   nak
                are            just   estimates   ,
                                                      bolen   je
                                                                                        it   must    add              tak   boleh   lebih
Kalar   increase      AT        AT2    and   AT3       Kena        decrease                                  to
                                                                                                                  S
                           ,                                                                        up
                                                                                                                                            18
(difference   between   steam   temp and        AT )
                                                   ,
                                Cactual   boiling point)
                                                           19
datum              °
              :
                  0 C
temperature
                        BPR
                              20
BPR
BPR
      21
22
23
24
25
26
27
                                                     different   values   of V
                                                                             .
bila              semva       we    get   to   see
       solve              ,
                  atas        was    just      an   assumption .
       >   davi
                                                                                 28
29
Reflections
Multiple effect evaporator – arrangement vs calculations
Reflect on the calculation method for multiple effect
evaporator
                                                           30