IMZRYa
IMZRYa
ZIRCONIA OXYGEN
ANALYZER CONVERTER
TYPE: ZRY
OXYGEN ANALYZER
Vol% O2
INZ-TN1ZRYa-E
PREFACE
We are grateful for your purchase of Fuji Electric’s Zirconia Oxygen Analyzer Converter (ZRY).
• First read this instruction manual carefully until an adequate understanding is acquired, and then
proceed to installation, operation and maintenance of the analyzer converter. Wrong handling may
cause an accident or injury.
• The specifications of this analyzer converter will be changed without prior notice for further prod-
uct improvement.
• Modification of this analyzer converter is strictly prohibited unless a written approval is obtained
from the manufacturer. Fuji Electric will not bear any responsibility for a trouble caused by such
a modification.
• This instruction manual shall be stored by the person who actually uses the analyzer converter.
• After reading the manual, be sure to store it at a place easier to access.
• This instruction manual should be delivered to the end user without fail.
i
CAUTION ON SAFETY
First of all, read this “Caution on safety” carefully, and then use the analyzer in the correct way.
• The cautionary descriptions listed here contain important information about safety, so they should always be
observed. Those safety precautions are ranked 2 levels; DANGER and CAUTION.
• Even an undesirable action described in “ CAUTION ” may lead to a grave result depending on situation.
Be sure to observe DANGER and CAUTION because they are both important for ensuring safety.
Caution on piping
ii
Caution on wiring
• The unit must be earthed as specified. Otherwise, it may cause elec-
tric shocks, malfunction, etc.
• Be sure to use a power supply of correct rating. Connection of power
CAUTION supply of incorrect rating may cause fire.
• Wiring work must be performed with the main power set to OFF to
prevent electric shocks.
• Use wiring materials that match the rating of the unit. Use of wiring
materials out of rating may cause fire.
Caution on use
• During operation, avoid opening the casing and touching the internal
parts. Otherwise, you may suffer a burn or shock hazard.
• Avoid touching the detector with bare hand during operation. Other-
CAUTION wise, you may suffer a burn because the detector may have reached a
high temperature (about 800°C).
• During operation, avoid removing and placing the detector on or near
a combustible material. Otherwise, fire may occur.
Others
iii
CONTENTS
PREFACE ................................................................................................................................................ i
CAUTION ON SAFETY ....................................................................................................................... ii
CONTENTS .......................................................................................................................................... iv
1. GENERAL DESCRIPTION ........................................................................................................... 1
1.1 Direct insertion type zirconia oxygen analyzer ................................................................................... 1
1.2 Confirmation of delivered components ............................................................................................... 1
1.3 Confirmation of type of delivered components................................................................................... 1
3. INSTALLATION ............................................................................................................................ 3
3.1 Location for installation ...................................................................................................................... 3
3.2 Installation ........................................................................................................................................... 3
8. CALIBRATION ............................................................................................................................ 10
8.1 Preparation ........................................................................................................................................ 10
8.2 Manual calibration ............................................................................................................................ 10
iv
1. GENERAL DESCRIPTION
This instruction manual describes the installation, operation and maintenance of the single-channel type
converter, so read through it before using the converter. For the sensor, flow guide tube used with the con-
verter, refer to relevant instruction manuals.
CAUTION
Power voltage for the converter must conform to that for the detector (ZFK2 or 5)
to be connected. Don’t use any power voltage different from the power specifica-
tions of the detector.
Because it may result in damage to the sensor.
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2. NAME AND FUNCTION OF EACH PART
OXYGEN ANALYZER
Vol% O2
FUSE AC250V
3.15A T 500mA T
HEATER POWER
OXYGEN ANALYZER
Vol% O2
FUSE AC250V
1 2 3 4 5 6 7 8 9 10 11 12 13 14 3.15A T 500mA T
+ - + - + - N L
T.C Zr.SIG A.OUT ALARM HEATER FG POWER HEATER POWER
2 3 4 5
}
ZERO key
SPAN key Refer to each operation procedure flow in chapter 6 to
CAL key 10.
ESC key
-2-
3. INSTALLATION
CAUTION
• Install the analyzer safely and securely so that it will not fall.
(3) No direct influence of radiation from heating furnace or the like (converter).
(5) No electric machinery nearby, which may cause noise trouble (such as motor, transformer) or produce
electromagnetic and electrostatic induction.
(6) Ambient temperature within -10 to +50 and ambient humidity less than 90%RH (converter).
3.2 Installation
3.2.1 Panel mounting
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4. WIRING AND PIPING
CAUTIONS
• Wiring work must be carried out with all power supplies turned off.
Otherwise, you may suffer electric shock.
OXYGEN ANALYZER
Vol% O2
FUSE AC250V
3.15A T 500mA T
HEATER POWER
1 2 3 4 5 6 7 8 9 10 11 12 13 14
N L
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4.3 Wiring and piping diagram
With flow guide tube
Red
Calibra-
AC power supply
tion gas White
inlet
1R/min Blue
Yellow
Black
White
2-core
exclusive cable
Standard gas
Manual operated Pressure reducing
Flow rater O2/N2 (ZBM)
valve for zero gas valve for standard
0.2 to 2R/min gas
Pressure reducing valve
Instrumentation air
Manual operated or standard gas (ZBM)
valve for span gas
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5. PREPARATION FOR OPERATION
6.1 Starting
After correct wiring and piping has been completed, turn the converter power ON, and measuring opera-
tion will start.
Note : 15 minutes is required for warming-up after power ON.
Caution before starting operation
Furnace operation should be started after 15 minutes. or more of warmup time has elapsed.
When a sensor is to be installed in a furnace during operation, take care to blow out harmful
gas from the furnace and then install the fully warmed up sensor quickly.
6.2 Shutdown
(1) When a process (furnace etc.) is to be shutdown for a short time (about one week)
The sensor should be operated continuously to avoid possible deterioration of platinum electrodes
and destruction of its element by repeating power ON-OFF operation in a wet condition (depending
on the condition in furnace and/or ambient conditions)
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6.3 Key operation flow diagram (outline)
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6.4 Check on alarm data
When a fault (error) warning output appears at the converter alarm contact output terminals (No. 7 and No.
8), the alarm data can be checked by the following operation.
Measurement
display
Alarm data display
ESC ESC
Keep key on for 3 sec. Keep key on for 3 sec.
After checking the alarm data, press the CAL key and the alarm of zero/span calibration error will be
cleared.
Alarm data
The 3rd digit ; 50°C (or more) higher than the detector control temperature
Temperature error
; 50°C (or less) lower than the detector control temperature
The 2nd digit ; Difference of more than 5%O2 between zero calibration gas
Zero calibration error concentration and zero calibration set value
Blank ; Normal
The 1st digit ; Difference of more than 5%O2 between span calibration gas
Span calibration error concentration and span calibration set value
Blank ; Normal
Conditions of converter alarm contact output (between No.7 and No.8 terminals)
-8-
7. SETTING OF CALIBRATION GAS CONCENTRATION
While setting zero/span calibration concentration, press the ZERO key once, then the number of the digit
increases by one digit, and press the SPAN key, then the number of the digit decreases by one digit. Setting
digit is moved to the right by one by pressing the ENT key. However, if the ENT is pressed while setting the
3rd digit, calibration concentration setting will be ended.
Note) Pressing the ESC key allows the setting to be canceled midway.
Operation How to set the span calibration gas concentration to 21.0% O2.
Order
(It is generally set to 20.9% O2 before shipment).
Key operation Description Displayed message
SPAN + ESC Press the SPAN key and ESC key simulta-
neously, then the lamp begins to blink (the
number in the 1st digit blinks).
ENT , ZERO Press the ENT key to blink the 2nd digit. Press
the ZERO key to change “0” to “1”.
ENT , ZERO Press the ENT key to blink the 3rd digit. Press
the ZERO key (increase) to change “9” to “0”.
Press the ENT key, then the display set to 21.0
ENT returns to measurement display status.
Measurement diaplay
To cancel the setting, press the ESC key.
Operation How to set the zero calibration gas concentration to 1.00% O2.
Order
(It is generally set to 1.01% O2 before shipment).
Key operation Description Displayed message
ZERO + ESC Press the ZERO key and ESC key simulta-
neously, then the lamp begins to blink (the
number in the 1st digit blinks).
ENT , ENT , Press the ENT key twice to blink 3rd digit.
SPAN Press the SPAN key (decrease) to change “1” to
“0”.
ENT Press the ENT key, then the display that is set
to 1.00 returns to measurement display status.
Measurement diaplay
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8. CALIBRATION
In order to maintain good accuracy, proper calibration using calibration gas is necessary.
Perform manual operation (Refer to 8.2).
8.1 Preparation
• Wiring/piping check
Wiring and piping work should be made correctly referring to Item. 4.3. The main plug of standard gas
should be left open. Since high pressure is present at piping connections, use blind-nut type joints and
take special care with regard to air-tightness. Calibration gas flow should be 1 to 1.5r/min.
• Setting of calibration gas concentration
Referring to Chapter 7 “Setting of calibration gas concentration”, set the oxygen concentration in standard
gas cylinder to be used.
Measurement diaplay
SPAN Press SPAN , then the message at right ap-
pears. All of 3 digits blink.
Measurement diaplay
ZERO Press ZERO , then the message at right
appears. All of 3 digits blink.
(All of 3 digits blink)
ENT When display is stabilized, press ENT key and
zero calibration is completed.
Measurement diaplay
Close the stop valve.
To cancel span calibration, press the ESC key.
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9. RANGE SELECTION
Operation panel
J1 : 0 to 10%range
J2 : 0 to 5%range
J3 : 0 to 25%range
Set before delivery
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10. ADJUSTMENT
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10.2 Temperature input adjustment
Description
• This is used to adjust zero/span adjustment of the thermocouple.
In general, do not perform the above operation because it is based on the factory adjustment mode.
ENT + ESC Hold down the ENT key and ESC key simulta-
neously for more than 5 seconds, then the decimal
point in the 1st digit begins to blink.
ZERO Press the ZERO key, 2nd digit blinks in 700 display.
After confirming that voltage is applied to the termi-
ENT nals, press the ENT key, and then zero adjustment can
be performed.
SPAN Press the SPAN key, 3rd digit blinks in 800 display.
After confirming that voltage is applied to the termi-
ENT nals, press the ENT key, and then span adjustment
can be performed.
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10.3 Current output adjustment
Description
• This adjustment should be made when
required accuracy can not be obtained after
calibration.
This is adjusted prior to delivery, so no Ammeter
250Ω
further adjustment is required for normal
operation.
• Adjust current by connecting an ammeter
and a load resistor of 250Ω to external
terminals 5(+) and 6( ).
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10.4 Setting of detector control temperature
Description
• Setting of control temperature is required according to types of the detector to be connected.
Type of detector and control temperature
ZFK2 (general use type) .... Set to 800°C
ZFK5 (corrosion-proof type) ... Set to 750°C
In general, do not perform the above operation because it is based on the factory adjustment mode.
When the detector needs to be replaced with another type, it becomes necessary to change the set value.
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10.5 Selection of alarm contact output
Description
• Select the converter alarm contact output.
• Select the contact output from the 5th digit of the converter code symbols.
The 5th digit of code symbol:
B.... Normal Open contact is selected.
C.... Normal Close contact is selected.
For details of alarm contact output, refer to Item 6.4 Check on alarm data (Page 8).
In general, do not perform the above operation because it is based on the factory adjustment mode.
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11. MAINTENANCE AND CHECK
11.1 Check
In order to keep the instrumentation operating in good condition, perform the following periodical mainte-
nance and check.
Perform maintenance and check once every year or 2, or at time of furnace check.
Check items Measures
Zero, span calibration Calibrate once every week (Refer to Chapter 8 “Calibration”)
Deterioration of packings If deteriorated, replace with new ones.
Daily and O-rings
check Check for loose cable Retighten or replace the packing.
ground
Check the remain pressure Check the amount using primary pressure.
in the calibration gas
cylinder
Clogging or corrosion of Remove the flow guide tube from the furnace wall, remove the
Peri- flow guide tubes detector and wash the flow guide tube with water.
odical Clogging or corrosion of Remove the ejector from the furnace wall, disassemble the
check ejector type sampling prove prove and wash it with water.
Clogging of air outlet of Remove the ejector from the furnace wall and clean the air
ejectors outlet located in the heat insulation layer of the furnace wall.
Specification
For circuit ø5.2 × 20mm 0.5A JIS C 6575 MF51 250V 0.5A
For heater ø5.2 × 20mm 3A JIS C 6575 MF51 250V 3.15A
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11.3 Troubleshooting
Symptoms Probable causes Checking methods Remedy
No display Converter fuse blown Check the fuse and supply voltage specifica- Replace fuse
out tion. Check power supply
voltage
Indication Filter and/or flow Visual check of filter and flow guide tube for Clean or replace filter
does not guide tube clogged contamination or clogging. Tighten pipe connec-
change or Check for loosen and gas leaks at piping tions
slow re- connections and mounting place of detector.
sponse Sensor element Change over between zero and span gas and Replace sensor element
deterioration check if 5 minutes or longer is needed for
90% response.
Decrease in flow Check response to process gas after shutting Increase process gas
velocity of exhaust gas down calibration gas. flow into the flow
Move the direction (mounting position) of guide tube
“arrow” of the flow guide slightly.
Indication Loose flange and its Check for gas leaks in detector and mount- Tighten mounting
too high or surroundings ing part of flow guide tube flange. screws
too low Replace O-ring
Deteriorated Check for leaks from the outside. Seal
O-rings
Senor malfunction Check for gas leaks at calibration gas inlet. Tighten connectors
Check sensor element voltage (mV) for
higher or lower than other sensor when Replace sensor element
flowing zero gas
Break of wiring Ohmic check of wiring Replace
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12. APPENDIX
12.1 Specification
(1) General
• Measured gas : Oxygen contained in non-combustible gas
• Measuring method : Direct inserting type zirconia system
• Measuring range : 0 to 5%, 1 to 10% and 1 to 25% (selected by setting pin)
• Oxygen concentration : 4 to 20mA DC (allowable load resistance 500Ω max.)
output signal Input-output isolation, linear characteristic versus oxygen concentration
• Alarm contact output : • Contact specifications; 1 point, 1a, 250V AC, 2A
• Contact function; Fault (error)
Alarm contact Close/Open is as specified.
• Self-diagnosis function : Detector temperature error, zero calibration error, span calibration error
• Repeatability : ±1% FS
• Linearity : ±2% FS
• Response speed : Within 7 sec for 90% response (from calibration gas inlet)
• Power supply : 100/115, 200/220 or 230V AC 50/60Hz
• Power consumption : 15VA + 50VA in normal operation
15VA + 200VA at startup
• Warmup-time : 15 minutes approx.
• Cable : Maximum length between sensor and converter 100m (To be ordered separately)
(2) Oxygen detector (type ZFK2, 5)
• Measuring instrument : General use ZFK2
For corrosive gas ZFK5
• Measured gas temperature : -20 to 600°C for flow guide tube type (for general use, corrosive gas)
• Measured gas pressure : -3 to +3kPa {-300 to +300mmH2O}
• Flow guide tube : Without blow-down nozzle
Flange : JIS-5K 65A FF
Insertion length (according to specification) : 0.3, 0.5, 0.75, 1.0m
• Ambient temperature : -20 to 60°C (for cable section)
125°C or less at the sensor flange surface with power ON
• Structure : Dust/rain-proof structure (IEC standard IP55)
• Filter : Alumina (filtration accuracy 50µ) and quartz paper
• Material of gas-contacting : General use detector : Zirconia, SUS316, SUS304, platinum
parts For corrosive gas detector : Zirconia, titanium, platinum, SUS316 (flow guide tube)
• Detector mounting : Horizontal ±45°, surrounding air should be clean.
• Outline dimensions : (L × max. dia.) 210 × 100mm (sensor)
• Mass : Sensor, approx. 1.6kg
Flow guide tube of 1m (general use type), approx. 5kg
• Finish color : Silver and SUS metalic color
(3) Oxygen converter (type ZRY)
• Display : 3-digit LED
• Calibration method : Manual calibration with calibration key
• Calibration gas : • Setting range for zero gas; 0.01 to 9.99% O2
span gas; 10.0 to 29.9% O2
• Recommended concentration of calibration gas :
zero gas; 0.25 to 2.0% O2
span gas; 20.6 to 21.0% O2 (air)
• Structure : Dust/rain-proof structure (IEC standard IP65)
Use a block cap of G1/2 for useless wiring port.
To prevent water leak, use cable gland for other wiring ports.
to prevent water leak.
• Mounting method : Mounting on panel surface
• Finish color : Munsell 6PB35/10.5, Silver
• Outline dimensions (H × W × D) : 230 × 220 × 95mm
• Mass : Approx. 4.5kg
• Ambient temperature : -10 to 50°C
• Ambient humidity : 90%RH or less
• Power source : 90 to 230V AC 50/60Hz
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12.2 Designation of type (PILC code table)
(1) Type of converter 1 2 3 4 5 6 7 8 9 10 11 12
ZRY 1 1 1 - 1 RE 0 Description
Alarm contact output, measurement output
B “Close” at alarm, 4 to 20mA DC
C “Open” at alarm, 4 to 20mA DC
Option
Y Without selector cock
D With selector cock
Thermocouple specification
R Thermocouple R
Specification
0 Standard
ZFK R 4- - Description
Application
2 General use
5 For corrosive gas (refuse incinerator)
Calibration gas inlet
1 Polyproprene joint for ø6 tube
2 Brass joint for ø1/4 in. tube
Power supply
1 100/115V AC 50/60Hz
3 200/220V AC 50/60Hz
5 230V AC 50/60Hz (CE-marking approved)
Flow guide tube
Flange material Type Length
0Y0 None
5A3 SUS304 General use 300mm
5A5 SUS304 General use 500mm
5A7 SUS304 General use 750mm
5A1 SUS304 General use 1000mm
5B3 SUS316 For corrosive gas 300mm
5B5 SUS316 For corrosive gas 500mm
5B7 SUS316 For corrosive gas 750mm
5B1 SUS316 For corrosive gas 1000mm
ZZZ Others
NOTE) As for the flange dimension, JIS 5K-65A FF is standard.
Protection cover
Y Without
A With
Reference air inlet
Y None
A Rc 1/8
B NPT 1/8
None-standard spec.
Z Other none-standard items
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(3) Type of exclusive cable connecting converter to sensor
1 2 3 4 5 6 7 8 9 Digit
Z R Z 1 Description
Specification
P For ZRY
Type
R For thermocouple R
Termination
0 Without
1 One end (sensor ZFK side)
2 Both ends
1 2 3 4 5 6 7 8 9 10 11 12 13 Digits
ZFK R 4 - 0 Y0 YY Description
Application
2 General use
5 For corrosive gas (refer to incinerater)
Calibration gas inlet
1 Polyproprene joint for ø6 tube
2 Brass joint for ø1/4 in. tube
Power supply
1 100/115V AC 50/60Hz
3 200/220V AC 50/60Hz
5 230V AC 50/60Hz (CE-marking approved)
-21-
12.3 Outline diagram (unit:mm)
2-
ø 9
20
72 195
220
Selector cock
312
14 230
3.2 95
5
ø1
Cable gland
For ø23.5/ø15.8 tube
39
5-G1/2
40 40 40 40
Connection diagram
1 2 3 4 5 6 7 8 9 10 11 12 13 14
N L
Thermo- Zirconia Analog Alarm Detector Power
couple signal output contact heater supply
signal output power
signal supply
-22-