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DRY PRACTICAL 3.docx-1-2

The document outlines a laboratory procedure for determining the value of X in a dibasic acid through titration with sodium hydroxide. It includes specific instructions for measuring volumes, calculating molarity, and writing chemical equations. Additionally, it describes tests on solid M, including observations and inferences based on reactions with water and sodium hydroxide.

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0% found this document useful (0 votes)
2K views2 pages

DRY PRACTICAL 3.docx-1-2

The document outlines a laboratory procedure for determining the value of X in a dibasic acid through titration with sodium hydroxide. It includes specific instructions for measuring volumes, calculating molarity, and writing chemical equations. Additionally, it describes tests on solid M, including observations and inferences based on reactions with water and sodium hydroxide.

Uploaded by

savai.joe321
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Name………………………………………………………. Date…………………………….

QUESTION 1
You are provided with the following:
● Solution A: containing 2.95g dibasic acid, H2X in 250 cm3 of solution.
● Solution B: containing 4g of sodium hydroxide in 500 cm3 of solution.

You are required to determine the value of X in the formula of the acid A.

Procedure
Fill the burette with solution A. Using pipette and pipette filler, place 25cm3 of solution B in a conical flask.
Add two drops of phenolphthalein indicator and titrate with solution A. Fill the table below. Repeat the titration
two more times and record the results

Titration I II III

Final burette reading (cm3) 40.3 20.8

Initial burette reading (cm3) 0.0 20.7

Volume of solution A used (cm3) 20.7 20.8

a. Determine the average volume of solution A used (1mk)


……………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………
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b. Determine the molarity of sodium hydroxide solution (3mk)
……………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………
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c. Calculate the number of moles of sodium hydroxide in the 25cm3 used (3 mks)
……………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………
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d. Write the equation of the reaction between acid A (dibasic Acid) and sodium hydroxide. (1mk)
……………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………
e. Determine:

1
i. The number of moles of acid A in the average volume used. (3 mks)
……………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………
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ii. The molarity of acid A (3mks)
……………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………
iii. The molar mass of the acid A. (2mks)
……………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………
f. Determine the mass of X in one mole of the acid. (H= 1.0) (3mk)
……………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………
……………………………………………………………………………………………………………………

QUESTION 1
You are provided with solids M, N and P. Carry out the following tests and write your observations and
interferences in the spaces provided.

TESTS ON SOLID M

Procedure Observation Inference

a. Place all of solid M in a solid dissolves to form a


boiling tube. Add 10cm3 of colourless solution.
distilled water and shake
thoroughly. Label the
resulting mixture M.

b. To about 2 cm3 of M in white precipitate formed


a test tube, add 2M dissolves in excess
sodium hydroxide
solution drop wise until
in excess.

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