Azadbakht 2018
Azadbakht 2018
PII: S0360-5442(18)31998-4
DOI: 10.1016/j.energy.2018.10.017
Please cite this article as: Mohsen Azadbakht, Mohammad Vahedi Torshizi, Fatemeh Noshad,
Arash Rokhbin, Application of artificial neural network method for prediction of osmotic
pretreatment based on the energy and exergy analyses in microwave drying of orange slices,
Energy (2018), doi: 10.1016/j.energy.2018.10.017
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Abstract
In the present study, artificial neural network (ANN) method was applied for predicting osmotic
pretreatment based on the energy and exergy analyses in microwave drying of orange slices. For
this purpose, the oranges were cut into slices with a thickness of 4 mm and treated with salt (NaCl)
and distilled water solution (7% by weight) for 30, 60, and 90 min as osmosis pre-treatment. Then,
they were dried in three replicates using a microwave dryer and at three powers of 90, 360, and
900 W. The statistical analysis results showed that the osmosis time is significant for the energy
efficiency and exergy efficiency and specific exergy loss at 1% level. The highest energy and
exergy efficiency was observed at 900 W and in the osmosis time of 90 min. The highest energy
and exergy efficiency was observed at 42.1% and 31.08%, respectively. The maximum exergy loss
was seen at 360 W and osmosis time of 60 min. The osmosis time did not affect the specific energy
loss. The microwave power was statistically significant for all the parameters (energy and exergy)
such that with increasing the microwave power, the energy and exergy efficiency increased, while
the specific exergy and energy loss decreased. Overall, with increasing osmosis time and
microwave power, the energy and exergy levels of the microwave dryer increased. The maximum
coefficient of determination (R2) in a network containing 6 neurons in the hidden layer was 0.999
for energy efficiency, R2 = 0.871 for specific energy loss, R2 = 0.999 for specific exergy loss, and
R2 = 0.972 for exergy efficiency. This amount was seen in a network containing 4 neurons in the
hidden layer.
Keywords: microwave dryer, energy, exergy, osmosis, orange, pre-treatment
1. Introduction
Drying is one of the oldest methods for preserving agricultural and food products. One of the main
goals of drying agricultural products is moving the water in solids to the surface of the product to
a certain extent. Drying is performed in order to reduce the amount of microbial activity in the
product and minimize the amount of chemical interactions in order to minimize the damage
imposed on agricultural products[1][2]. Drying also increases the life of the product and, by
reducing the weight and volume of products, facilitates the packaging, transporting, and storage of
the products, leading to reduced costs. In addition to the above-mentioned cases, drying can control
the market of different products so that the desired product can be used in sensitive situations [3].
In practice, drying is a process that requires a high energy consumption due to the latent heat of
water evaporation. In this regard, 10% of the total energy consumption in the food industry is
related to drying food. Therefore, the drying of agricultural products reflects energy efficiency in
the production of food products and it is very important in industrial uses [4]. Microwave drying
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is one of the important drying methods. Because of the better focus of energy on the product, the
removal of moisture is faster and, compared to other meth
compared to other drying methods [5,6].
Using microwave waves can reduce drying time by up to 50% or more, while it depends on the
type of product and the drying conditions in different methods. In the microwave drying, the
product is exposed to high-intensity electromagnetic waves. These high-frequency waves select
polar molecules (dipoles) and ions and coordinate them with a fast orientation of the electrical
field. In this orientation process, an adequate amount of heat is produced throughout the product
so that bipolar molecules such as water and salt are vibrated while microwave waves are passing
through inside the product and its biological tissue; as a result of these vibrated molecules, a high
heat content is generated [7]. The drying temperature and microwave power are two important
factors in microwave drying of agricultural products. These two factors significantly affect the
drying parameters such as drying time, drying curve, drying rate, drying efficiency, and final
product quality [8]. The effect of microwave power on drying of products has been examined by
many researchers. For example, Sharifian et al. (2015) evaluated the energy and mass transfer in
a microwave dryer on figs and found that the drying rate increases with increasing microwave
power, and the mass transfer increases when power increases [9]. In addition, Dadal et al. (2010)
examined the effect of the power levels and sample mass on drying okra with microwave. By
increasing microwave power, the drying time of okra was significantly reduced [10]. Darvishi et
al. (2014) analyzed the energy and exergy of white mulberries in the process of drying with a
microwave dryer and reported that the specific energy loss increases with increasing microwave
power. Additionally, energy efficiency was reduced by decreasing the moisture content and
microwave power. The best energy and exergy for white mulberry was observed at 100 W
microwave power [11]. Darvishi et al. (2016) conducted energy and exergy analysis, modeled
Kiwi slices with a microwave dryer, and reported that the energy and exergy efficiency increases
with increasing microwave power and decreasing the thickness of kiwi slices. Additionally, this
parameter decreased by reducing the moisture content of slices [12]. Moreover, nowadays,
improving the quality of agricultural products during the drying is of the highest importance. One
technique commonly used in this regard is pre-treatment [13], which can be applied to preserve
foods and improve the appearance of dried products [14].
According to the literature, osmosis pre-treatment is an easy, controllable, and good method for
fruit drying. It is also an economical and cost-effective method to remove part of the water from
plant and animal products by dipping it into solution [15]. In addition, the use of this method results
in a reduction in the drying time and improves the apparent quality of the samples after drying
[16].
The use of pretreatment in the drying of products was also reported in the following studies: Al-
Harahsheh et al. (2009) examined tomato drying in a microwave dryer with osmosis pretreatment
and reported that by increasing the dryer power and content of salt concentration, the rate of dryer
increased [17]. In addition, Azoubel et al. (2009) examined the effect of osmosis pre-treatment on
drying kinetics and quality of cashew apple and concluded that osmosis of cashew apples had a
higher rate of drying compared to non-pretreated fruits [18]. Moreover, the artificial neural
network (ANN) modeling is widely used in many fields. This method is of high efficiency in
solving the complex and non-linear equations in dryers [19]. Nikbakht et al. (2014) used the ANN
to predict the exergy and drying energy of pomegranate in a thin-layer dryer with microwave [20].
Aghbashlo et al. (2012) used an ANN to predict the performance of the spray dryer for oil and fish
[21]. Azadbakht et al also examined the exergy and energy of the fluid bed dryer using an ANN
for potato drying [22].
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The objective of this research is the energy and exergy performance analyses of microwave dryers
for drying orange slices under pre-treatment of osmosis in order to reduce the energy consumption
in the microwave dryer and increase the energy and exergy efficiency of the microwave with new
processes. For this purpose, the ANN was applied to verify the accuracy of the numbers obtained.
Additionally, the sensitivity coefficient test was applied to relate the energy and exergy factors to
microwave and pre-treatment.
2. Materials and methods
2.1. Sample preparation
Freshly harvested oranges (Tamson variety) were purchased from a local store in Gorgan city in
Iran and were kept at 10℃ in the laboratory. At the beginning of each experiment, the oranges
were washed and the slices were cut in a circular in a thickness of 4 mm and they were weighted.
Then, samples were pretreated by placing them in an osmosis solution (7 wt.%) containing 1000
gr of distilled water and 70 g salt (NaCl) for 30, 60, and 90 min. Drying process was performed in
a microwave dryer with 1.2, 4.8, and 12 W/g specific power density in the BioSystem Mechanics
Department of Gorgan University of Agricultural Sciences and Natural Resources (Fig. 1).
2.2. Experiment method
Slices were pretreated and placed in containers and dried at three powers of 90, 360, and 900 W.
The weight of oranges was measured using a 0.01 mg precision scale. The weight of each sample
was measured and recorded at a time interval of 1 min to reach a constant moisture. For each
treatment, the experiments were repeated in triplicate. Environmental conditions for testing were
conducted at a temperature of 20℃ and a relative humidity of 71%. First, the oranges were equal
to the slices of the same size, then the sample was placed inside the oven and the weight of the
sample was measured according to the standards. Then, using Eq. 1, the moisture content was
calculated [23].
𝑊 ‒ 𝑊e
𝑀𝐶 = (1)
𝑊
2.3. Energy analysis
Energy used in the drying and heating process is important for production processes in the
industrial and household sectors. However, the price of this energy is extremely expensive;
therefore, there is a strong incentive to invent processes that will use energy efficiently.
Currently, widely used drying and heating processes are complicated and inefficient and are
generally damaging to the environment. Thus, it is required to have a simplified lower-cost
approach replicable in a wide range of situations [24].
The mass and energy survival in the microwave dryers’ chamber is shown in Fig. 2. The general
relation of mass moisture survival is calculated using Eq. (2) [12].
According to Eq. 3, the initial mass of the sample is equal to the amount of water vapor removed
and the rate of dried sample mass.
𝑚𝑜 = 𝑚𝑒𝑤 + 𝑚𝑝 (3)
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The latent heat of the orange samples is calculated using Eq. 7 [26].
𝜆𝐾
= 1 + 23exp ( ‒ 40𝑀𝑡) (7)
𝜆𝑤𝑓
The latent heat of free water evaporation was calculated according to Broker et al. using Eq. 8
[27].
The thermal capacity is a function of the moisture content and can be calculated through Eq. 9
[28].
𝑀𝑡
𝐶𝑃 = 840 + 3350 × ( ) (9)
1 + 𝑀𝑡
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With the onset of the energy crisis, energy and exergy (the maximum useful work that comes
from a certain amount of available energy or from the flow of materials) analyses are among the
leading thermodynamic research works. In the exergy analysis, the main purpose is to determine
the location and amount of irreversible production during the various processes of the
thermodynamic cycle and the factors affecting the production of this irreversibility. In this way,
in addition to evaluating the performance of various components of the thermodynamic cycle,
methods to increase cycle efficiency are also identified [30].
The amount of exergy transmitted due to evaporation in the drying chamber was calculated using
Eq. 14 [31]
𝑇0
𝑒𝑥'𝑒𝑥𝑎𝑝 = (1 ‒ ) × 𝑚𝑤𝑣𝜆𝑤𝑝 (14)
𝑇𝑝
Exergy efficiency for each dryer system – as the exergy rate used in drying the product to the
exergy of drying source supplied to the system – is calculated by Eq. 17 [32]
𝑒𝑥𝑒𝑟𝑔𝑦 𝑎𝑏𝑠𝑜𝑟𝑝𝑡𝑖𝑜𝑛
𝜂𝑒𝑛 = × 100 (17)
𝑃𝑖𝑛 × 𝑡
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In this research, the source of temperature and pressure in the environment was 20℃ and 101.3
MPa, respectively.
𝐸𝑋𝑖𝑛 ‒ 𝐸𝑋𝑎𝑏𝑠
𝐸𝑋𝑙𝑜𝑠𝑠 = (18)
𝑚𝑤
2.4. Mass Transfer Parameters
2.4.1Drying Kinetics
The change of moisture in orange slice during the drying process was expressed as the moisture ratio defined
as[33]:
𝑀𝑡 ‒ 𝑀𝑒
𝑀𝑅 = ( )
𝑀0 ‒ 𝑀
𝑒
(19)
∞ 𝐷
6 1 2 2 𝑒𝑚
𝑀𝑅 = 2 ∑
𝜋 𝑛 = 0𝑛
2
exp ( ‒ 𝑛 𝜋
𝑟
2
𝑡)
(20)
Simplifying Eq. 20 by taking the first term of the series solution gives [12]:
6 𝐷
2 𝑒𝑚
𝑀𝑅 = 2
exp ( ‒ 𝜋 2 𝑡) (21)
𝜋 𝑟
Effective diffusivity is also typically calculated using the slope of Eq. (22); when a natural logarithm of MR
versus time was plotted, a straight line was obtained with a slope of:
𝐷
2 𝑒𝑚
𝜋 2
(22)
𝑟
𝑉𝑝
ℎ𝑚 =‒ ln (𝑀𝑅) (23)
𝐴𝑝 × 𝑡
For a symmetrically heated sphere, V/A is equal to the radius [35], hence for a given orange slice, Eq. (24) can
be simplified to:
𝑟
ℎ𝑚 =‒ ln (𝑀𝑅) (24)
𝑡
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Table 3: ANOVA results of energy efficiency, specific lost energy lost, specific lost exergy and
exergy efficiency, effective moisture diffusivity and mass transfer coefficient under different
powers and osmoses
Specific exergy
Parameter
Energy efficiency Specific energy loss loss Exergy efficiency
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8
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9
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applied for drying. Furthermore, according to the results, at 900 watts, the highest effective
moisture diffusivity was observed. In this power, the energy consumed and specific energy loss
was at best. According to the results obtained for the effective moisture diffusivity, it can be stated
that the best power and osmotic time were 900 watts and 90 min, respectively. The obtained results
are consistent with those of Darvishi et al. (2017) on SOYBEAN drying in a microwave dryer
[27].
Table 6 shows the best network between input data and the data simulated by the network for each
of the neurons in the hidden layer. Smaller epochs suggest that the number of neurons in the layer
successfully learned by the neural network compared to other neurons.
As shown in Table 6, the best network for energy efficiency at training step (Run = 1, Epoch = 21)
in the 6-neuron state in the hidden layer reaches a constant value after about 21 generations of
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error. In addition, the best network for the specific energy loss in training (Run = 1, Epoch = 13)
in 8-neuron state in the hidden layer reaches a constant value after about 19 generations of errors.
For exergy efficiency of training value (Run = 1, Epoch = 14), in the 6-neuron state in the hidden
layer and for the specific exergy loss (Run = 1, Epoch = 17), an appropriate overlap was obtained
between the mean square error of the input numbers and the numbers simulated by the network.
To examine the effect of input parameters and identify the most influential factor, the sensitivity
analysis test was performed on the considered networks. As shown in Fig. 10, the osmosis time in
an ANN with 6 neurons in the hidden layer was considered as the most effective factor in
predicting energy efficiency. In addition, in this network, microwave power in hidden layers with
8 neurons had the highest sensitivity.
The results of the sensitivity analysis for the specific energy loss are shown in Fig. 11. Based on
this figure, the highest sensitivity was obtained for the microwave power and the osmosis time in
the hidden layers with 4 neurons. In fact, in the specific energy loss, with increasing the number
of neurons in hidden layers, the sensitivity of input parameters to output data decreased.
For the exergy efficiency, the sensitivity analysis is shown in Fig. 12. Based on this figure, the
highest sensitivity for the microwave power was obtained in the hidden layers with 4 neurons
while the maximum sensitivity coefficient for the osmosis time was obtained in hidden layers
with 4 neurons. Based on the sensitivity analysis for energy efficiency, the sensitivity of
microwave power is reduced with increasing the number of neurons in the hidden layers, while
the sensitivity of osmosis time increases with increasing the number of neurons in the hidden
layers.
Fig. 13 illustrates the sensitivity coefficient for the specific exergy loss. As can be seen, the
highest sensitivity for the microwave power was calculated in hidden layers with 6 neurons while
the highest sensitivity for osmosis time was calculated in the hidden layers with 4 neurons.
Additionally, in all three neuron numbers of 4, 6, and 8, the microwave power sensitivity
coefficient for the specific exergy loss was higher than that of osmosis time.
4. Conclusion
Microwave power plays an important role in determining the characteristic of orange drying. An
increase in the power of the microwave increases the energy and exergy efficiency drying,
leading to the reduced drying time. Osmosis pre-treatment has no significant effect on energy
and exergy loss, and power plays a more important role in these two factors. In addition, osmosis
pre-treatment increases the absorption of heat in orange, leading to an increase in the energy and
exergy efficiency during drying. Also, increasing the osmosis time and microwave power had a
significant effect on the amount of energy and exergy. Based on the results obtained, osmosis
time had more effect on the energy efficiency than the exergy efficiency.According to the results
obtained for the effective moisture diffusivity and mass transfer coefficient, the best power and
osmotic time were 900 W and 90 min. Based on the results obtained from the ANN, the highest
R2 value for energy efficiency, specific energy loss, and exergy efficiency is seen in the ANN
with 6 neurons while for the specific exergy loss, the highest R2 is seen in the network with 4
neurons in the hidden layers. Data obtained from the network and the initial data obtained from
the experiment overlap for the energy efficiency, the specific exergy loss, and the exergy
efficiency in a network with 6 neurons in the hidden layer. Meanwhile, for the specific exergy
loss, the data in a network with 4 neurons in the hidden layer overlap. With this number of
neurons in the hidden layer, the fastest type of learning was seen in the ANN. Based on the
results obtained, the sensitivity coefficient shows the highest sensitivity to osmosis neural
network with 4 neurons in the hidden layers. However, this value for the exergy efficiency was
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obtained in the hidden layer with 8 neurons. The maximum microwave power sensitivity
coefficient for the energy efficiency and specific exergy loss was obtained in a network with 6
neurons in the hidden layer while for exergy efficiency and specific energy loss, it was obtained
in a network with 4 neurons in the hidden layer. Given the results obtained for R2, RMSE, and
Epoch, it can be stated that the ANN designed in this work has the ability to predict the energy
efficiency, specific energy loss, exergy efficiency, and specific exergy loss at an acceptable level
for orange.
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Figures caption:
Nomenclature
Cp Heat capacity (J/kg K)
Dem Effective moisture diffusivity (m2/s)
E Energy,(J)
Eloss Specific energy loss (J/kg water)
Eabs Exergy absorbed (J)
Ein Exergy input (J)
Eref Exergy reflected (J)
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Figures:
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50 aA
45 90W 360W 900W
40 aAB
35 bA
30 aB
bB
25
bC cA
20
15 cA cA
10
5
0
30min 60min 90min
Osmotic time(min)
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7 B
6
5
4
3
2 C
1
0
90 Microwave Power(W)
360 900
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25
aA
20 aAB
15
aA
bB bA
10 aB
cA
cA aB
5
0
30 60 90
Osmotic time(min)
Fig. 7. Effect of osmotic pre-treatment and microwave power on specific exergy loss
The similar capital letters represent non-significance in the same power while the similar small
letters represent the non-significance in the same osmosis time.
Osmotic Time(min)
30 60 90
Effective moisture diffusivity
0.0006 Aa
0.0005
0.0004 aB
0.0003 aB
bA bA bA
0.0002 bB cB
0.0001 cC
0
90 360 900
Microwave power(W)
Fig. 8. Effect of osmotic pre-treatment and microwave power on effective moisture diffusivity
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Osmotic Time(min)
mass transfer coefficient (m/s) 30 60 90
0.035
Aa
0.03
0.025 bA
aB
aB
0.02 bA aA aB
cA bB
0.015
0.01
0.005
0
90 360 900
Microwave power(W)
Fig. 9. Effect of osmotic pre-treatment and microwave power on mass transfer coefficient
8 Microwave power
7 Time osmotic
6
5
Sensitivity
4
3
2
1
0
8 6 4
Neuron in hidden layer
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0.4
0.3
0.2
0.1
0
8 6 4
Neuron in hidden layer
12 Microwave power
Time osmotic
10
8
Sensitivity
0
8 6 4
Neuron in hidden layer
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8 Microwave power
7 Time osmotic
6
5
Sensitivity
4
3
2
1
0
8 6 4
Neuron in hidden layer
Formula
Formula Reference
Number
𝑥 ‒𝑥
𝑒 ‒𝑒
Tanh = (25) [36]
𝑥 ‒𝑥
𝑒 +𝑒
∑𝑛 (𝑃𝑖 ‒ 𝑂𝑖)
2
𝑖=1
2 R2 = 1- (26) [37]
(𝑃𝑖 ‒ 𝑂)
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∑𝑛 (𝑃𝑖 ‒ 𝑂𝑖)
2
𝑖=1
1‒ 2
r= (27)
(𝑃𝑖 ‒ 𝑂)
2
(𝑃𝑖 ‒ 𝑂𝑖)
RMSE = ∑𝑛 (28) [32]
𝑖=1 𝑛
∑𝑛 |𝑃𝑖 ‒ 𝑂𝑖|
𝑖=1
MAE = (29) [38]
𝑛
Tables:
Table 4: Regression equations of power (90, 360 and 900 W) for Specific exergy loss
Microwave Power Equating R²
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90 y = 6.1096x0.9259 0.548
360 y = 9.3684x-0.104 0.9379
900 y = 15.882e0.3322x 0.9901
Table 5: Error values in predicting experimental data using optimal artificial neural network
Energy efficiency
Mean squared error 40.7364295 4.010991123 2.988120859
Normalized Mean squared
error 0.387597681 0.022064854 0.119134058
Mean absolute error 4.032143844 1.417448017 1.489954289
Correlation coefficient 0.831286093 0.999303134 0.977049886
Specific energy loss
Mean squared error 4.337581878 0.025695416 0.866819665
Normalized Mean squared
error 39.32863229 0.028049053 0.221324525
Mean absolute error 1.618505148 0.106840226 0.658209612
Correlation coefficient 0.417441698 0.991636439 0.94131972
Exergy efficiency
Mean squared error 2.861528643 2.041341749 5.169678018
Normalized Mean squared
error 0.063233888 0.792429787 0.264937076
Mean absolute error 1.56647252 1.255905643 1.989219103
Correlation coefficient 0.972033224 0.495847176 0.96768871
Specific exergy loss
Mean squared error 29.67488181 0.010963853 29.00512733
Normalized Mean squared
error 0.636353366 0.000271428 0.812034038
Mean absolute error 2.754316991 0.07534787 2.748302448
Correlation coefficient 0.77300422 0.999934906 0.750517268
Table6: Some of the best MLP neural network topologies to predict test values
Energy efficiency
3 neuron in hidden layer 5 neuron in hidden layer 7 neuron in hidden layer
Cross Cross Cross
Training Training Training
Validation Validation Validation
Run # 1 1 1 2 1 3
Epoch # 38 33 21 5 27 6
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Minimum
0.021512597 0.00194432 0.023753914 0.021932085 0.025436747 0.001191989
MSE
Final MSE 0.021512597 0.001970578 0.023753914 0.038460095 0.025436747 0.008555116
Specific energy loss
Run # 1 2 1 3 1
Epoch # 13 4 57 14 19
Minimum
0.029177034 0.004976503 0.041720161 0.001642759 0.026481779
MSE
Final MSE 0.029177034 0.104359341 0.041720161 0.01981361 0.026481779
Exergy efficiency
Run # 1 1 1 1 1 2
Epoch # 35 17 14 7 29 4
Minimum
0.001758156 0.000763416 0.002044987 0.000826504 0.001330489 0.003554999
MSE
Final MSE 0.001758156 0.009132225 0.002044987 0.007230043 0.001330489 0.007237963
Specific exergy loss
Run # 1 1 1 1 1 2
Epoch # 23 23 17 12 47 18
Minimum
0.00788163 2.63784E-05 0.032262786 0.000125721 0.008362538 0.000251749
MSE
Final MSE 0.00788163 2.63813E-05 0.032262786 0.000164817 0.008362538 0.000252867
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An increase in the power increases the energy and exergy efficiency drying.
Osmosis pre-treatment has no significant effect on energy and exergy loss.
Osmosis pre-treatment, leading to an increase in the energy and exergy efficiency.
Increasing the time and power have effect on the amount of energy and exergy.
The ANN designed has the ability to predict the energy and exergy items.