Progression of Experimental Blast Furnace in Hasaki R&D Center
Progression of Experimental Blast Furnace in Hasaki R&D Center
Abstract
The experimental blast furnace in Hasaki R&D Center (Kamisu City in Ibaraki Prefec-
ture), constructed as a melting furnace in 1982, carried out a total of 50 test operations over
27 years up to 2008. This article reviews the history of the technological development and
knowledge obtained from the experimental blast furnace.
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Fig. 1 Transitions of iron and crude steel production and experimental blast furnaces
furnace with a furnace volume of 1.3 m3 in 1982 at the same time as furnace). After 1996, the furnace was equipped with measuring de-
the termination of the operation of Tokyo University’s one-ton/day vices such as a sampling device and the like, and the furnace height
furnace. At this time when the domestic crude steel production ex- was extended and an additional material hopper was installed on the
ceeded 100 million tons a year, overtaking the US, the Japanese furnace top. Thus, as a blast furnace simulator, the test operations
steel industry was suffering from the sharp rise of the crude oil continued for the evaluation of raw material quality, etc., and in
price, and was forced to change its energy source. Then, the follow- 2008, after the completion of fourteen test operations as an experi-
ing R&D was conducted: development of coke rate reduction tech- mental blast furnace, it terminated its service after a total of fifty test
nology, the shift from heavy oil injection to pulverized coal injec- operations during the past twenty-seven years. Currently, there are
tion, and development of new processes as substitutes for the blast only two experimental blast furnaces in operation: one from the
furnace method. In the early period, the furnace was mainly used for COURSE50 Project in Japan, 4) and the other in LKAB (Luos-
studies on the maximum amount of pulverized coal injection, and savaara-Kiirunavaara Aktiebolag), a mining company in Sweden.
the feasibility of producing ferroalloys with the blast furnace proc In this article, the history of the experimental blast furnace of the
ess to cope with the electric furnace process. By hot-connecting the Nippon Steel Hasaki R&D Center (hereinafter referred to as Hasaki)
melting furnace and the shaft-type reducing furnace (8 t/d, furnace from 1982 to 2008 (Table 1), and the information obtained there-
volume 1.3 m3) constructed adjacently in 1984, and by separating from are reviewed.
the function of iron ore reduction by a gas reductant and the func-
tion of melting the reduced iron, R&D was promoted for a new 2. Test Operations of the Experimental Furnace as
ironmaking process, the SC Process (Sumitomo/Shaft-Cupola), tar- Melting Furnace
geting the alleviation of raw material quality specifications, drastic 2.1 Pulverized coal injection and combined injection, and fer-
energy saving, and cost reduction. 12) Furthermore, by using the roalloy production development period
melting furnace independently, test operations were conducted to After the oil crisis in the 1970s, as a substitute for the heavy oil
develop new ironmaking process technologies such as oxygen blast injection that was started in the 1960s, the study on pulverized coal
furnace and scrap melting, and a total of thirty-six test operations injection was started in the early 1980s. An actual size model of the
using the furnace for melting were conducted until 1988. lower part of the Kokura No. 1 Blast Furnace with a 48 degree-
After 1989, with the construction of a ceramic heat-exchange- fanned section (after the third repair and improvement, furnace vol-
type hot stove and with the alteration of lance-type blasting to ume 750 m3) was constructed in the Amagasaki R&D Center in
tuyere-type blasting, the furnace was used as an experimental blast 1972 (transferred to Hasaki in 1978, furnace volume expanded to 44
furnace (Sumitomo/Small Test Blast Furnace: STBF) for the devel- m3). Based on the information obtained from the actual size tuyere
opment of the combined blasting of high-rate pulverized coal and combustion experiment conducted on the model, 13) study on the
powder ore (hereinafter referred to as ultra-combined blasting for maximum amount of pulverized coal injection using the melting
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Table 1 Chronology of the experimental blast furnace
Campaign
Schedule Operation subject Equipment transition
No.
SC Evaluation of coke properties and maximum amount of
1982/3-11 1982 Melting Furnace (MF) established (10 t/d, 2.2 m3, 3 mH).
1st-5th PCI
6-12th 1982/12-1983/10 Ferroalloy production
1984 Shaft Furnace (SF) established (8 t/d, 1.3 m3, 3 mH).
13-15th 1984/4-1984/7 Development of SC method Reduction ore hot conveyor, Hot cyclone, and Sampling
sonde were installed.
16-17th 1984/9-1984/11 Ferroalloy production
18-22th 1985/2-1985/10 Development of SC method
Development of oxygen blasting and ultra combined
23-32th 1985/12-1987/10 1987 Hot stove established.
blasting for furnace
1988 Furnace height extension (SL: TY+3.0 mH→3.5 mH)
33-36th 1988/3-1988/12 Development packed bed type scrap melting process
2nd tuyere installation in shaft (TY+0.6 m, 1.2 m)
STBF 1989 Tuyere/Browpipe and hot blast control valve system
1989/5-1991/4 Development of ultra combined blasting for furnace
1st-7th 1990 Furnace height extension (SL: TY+3.5 mH→5.0 mH, 3 m3)
1995 Installation of measurement systems
8th 1996/3/11-3/17 Large amount of PC injection and low slag rate tests (dripping and cohesive zone samplers, liquid level detector,
stock level detector)
HBI charging, reduced iron and ore powder injection
9th 1997/4/14-4/18
tests
Evaluation of effect slag rate and low slag sinter
10th 1997/10/27-10/31
properties on permeability
11th 2000/3/25-3/29 Evaluation of effect of high Al2O3 slag on the operation. 1999 Ground flare stack was installed.
12th 2001/1/29-2/2 Wasted plastic powder injection test
2003 Furnace height extension (SL: TY+5.0 mH→6.0 mH, 4.0 m3)
13th 2003/11/7-11/13 Evaluation of sinter reducibility and coke reactivity
Vertical prove was installed.
14th 2008/11/16-11/21 Evaluation of effect of mixed charge on permeability 2007 Hopper for mixed charging was installed.
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Fig. 6 Distributions of coke properties and gasification degree in melt- Fig. 7 Comparison of operation results of oxygen injection and calcula-
ing furnace tion results
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Table 2 Results on all scrap operations of the experiment blast furnace
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Fig. 12 Vertical stress, variation of stock level with drainage and state of hearth (eleventh test operation)
in the slag phase and floats on the hot metal phase, and it was con- ing lower basicity in the dripping zone has good wettability with
firmed that the state of the deadman coke agrees with the assump- coke.
tion of the abovementioned mechanical balance. Figure 14 shows an example of the results of the in-furnace
After the test operation, the furnace was cooled by nitrogen for sample analysis by the dissection survey and the measurement dur-
two weeks, maintaining the designated stock level, and a dissection ing the operation. The carburization of the hot metal dripping from
survey was conducted. From the top of the furnace, a sample was the upper part of the dripping zone progresses (Fig. 14 (e)), and from
taken at each coke bed and ore bed at predetermined positions in the right after the hot metal/molten slag separation, the slag starts to as-
radial direction. Figure 13 shows an example of the in-furnace bed similate with ash and the basicity decreases. The slag FeO right be-
structure. It was confirmed that the slag formed at above 1 400°C in fore dripping is about 1.0%, which drops to the tapped molten slag
the middle of the cohesive zone has larger angles of contact with level in the upper part of the dripping zone. From the data, the slag
coke, and has not got wet as compared with the slag formed in the physical property can be estimated. In addition, since the analysis
upper cohesive zone right before separation of the molten slag from result of the in-furnace content obtained in the dissection survey and
the hot metal. However, it was confirmed that the molten slag hav- that of the sample taken by the sampling devices during operation
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agree with each other in general, the in-furnace state under any test group that controls the hot stove operation in the instrument pulpit,
conditions can be directly grasped by the sampling device and the the charging group that conducts manual operation in the instrument
dissection survey result. pulpit, mounting work of the material hoppers with a hoist, and the
The one test blast furnace operation continued for about five blending work of raw materials, the powder injection group that
days, and was conducted by about fifteen shift operators on a three- controls the powder material transportation quantity such as pulver-
shift basis. Each shift consisted of the following groups: the blasting ized coal powder and charging to powder material hoppers, the in-
strumentation group that handles various sampling devices, the tap-
ping group that operates the compressed-air-driven tap hole opening
machine, conducts tapping operation using the oxygen opening
method and tap-hole-closing operation by a hydraulic mud gun and
the handling of the molten slag/hot metal ladle, the utility group that
controls the working conditions of equipment and controls the sup-
ply of utilities, and an overall operation control supervisor and as-
sistant operation control supervisor.
3.2 Ultra-combined blasting development period
In the first to the seventh test operations during the period from
1989 to 1991, from the viewpoints of extending the coke oven fur-
nace life, direct use of ore powder, the blast furnace productivity en-
hancement, and the hot metal composition control, the ultra-com-
bined blasting technology in which large amounts of pulverized
coal, ore powder, and slag formers are simultaneously injected in
through the blast furnace tuyeres was developed. 23, 24) Its concept is
shown in Fig. 15.
In 1988, a new coke packed-bed-type combustion furnace (1.5
m long × 1.0 m deep × 2.35 m high with one 65 mm in diameter
tuyere) was built adjacent to the experimental blast furnace across
the hot stove. After fully grasping the combustion state within the
raceway and its periphery based on the detailed study using the fur-
nace, a continuous six-day operation was conducted in the experi-
mental blast furnace under the conditions of 300 kg/t + 100 kg/t and
200 kg/t + 200kg/t of the pulverized coal rate and ore powder rate.
The reducing agent rate was maintained at 600 kg/t, and no slag
FeO increase and no insufficiency in the reduction of the ore powder
were recognized. In the total of eight tests using only one tuyere
conducted during the same period at the Wakayama No. 3 Blast Fur-
nace (after the third repair and improvement, furnace volume 2 150
Fig. 13 Dissection of experimental blast furnace (thirteenth test opera-
tion) m3) and the Wakayama No. 5 Blast Furnace (after the third repair
Fig. 14 Vertical distribution of sample analysis results by dissection and sampling sonde (eleventh test operation)
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rate. 25) In the softening and melting test conducted prior to the ex-
perimental blast furnace operation, 26) the high permeability of HBI
at high temperature was confirmed, and upon application of HBI to
the blast furnace, not only improvements in the productivity and the
reduction in the reducing agent rate, but also a great contribution to
the improvement in permeability were expected.
In the test blast furnace operation, to supply HBI, two methods
were used: charging lump HBI from the furnace top and the injec-
tion of the powder reduced iron (PRI) through the tuyeres. The test
operations were conducted for six cases: the four cases of the HBI
mixing ratio of 0, 25, 50 and 100%, one case of PRI (powder re-
duced iron) injection of 200 kg/t, and one case of powder ore injec-
tion (ore injection: OI) of 200 kg/t for comparison purposes. To
Fig. 15 Concept of ultra combined blasting for blast furnace
compare and verify the improvements in permeability and produc-
and improvement, furnace volume 2 700 m3), in the test under the tivity, all blasting conditions were fixed.
condition of 200 kg/t + 200 kg/t of the pulverized coal rate and ore Throughout the test operation, the furnace condition remained
powder rate, from the fiber scope observation, 24) melting of the ore stable. According to Fig. 16 wherein the representative operation
powder was observed and it was confirmed that the ore powder in- data are prepared, the 5.5% production rate improving effect and the
jection was functioning sufficiently within the raceway. In addition, 4.3% reducing agent reduction effect were obtained per HBI 100 kg/
although the effect of decreasing [Si] by FeO was not as remarkable t, and above HBI 50%, a significant decrease in the resistance to the
as that of a commercial blast furnace test, 14) hot metal chemical in-furnace permeability (permeability resistance) was confirmed. In
compositions almost equal to those of the commercial blast furnace the case of PRI, no changes were observed in the production rate
were obtained. Additionally, to prevent the piping abrasion, a plug- and the reducing agent rate. However, in the case of OI, as the pro-
type pneumatic conveyor powder transportation technology was es- duction rate deteriorated, accompanied by the worsening in the re-
tablished. ducing agent rate, it was concluded that, for the improvement of
After the extension of the furnace height in 1990, a stock level blast furnace productivity using HBI, top furnace charging is more
change test was conducted under identical operation specifications. advantageous than the injection through tuyeres.
As a result, by changing the stock level from 3.5 m to 5.0 m, de- In addition, the effect of using HBI in the experimental blast fur-
crease in unburnt char trapped in the furnace top was confirmed, and nace was analyzed from the viewpoint of kinetics by using the blast
the furnace top temperature dropped by 100–150°C, the gas utiliza- furnace mathematical models. 27) As shown in Fig. 17, the analysis
tion efficiency increased by 5–6%, and the reducing agent rate de- clarified that the productivity improvement, the reduction of the re-
creased by about 100 kg/t. Further, according to the dissection sur- ducing agent rate, and the decrease in gas utilization efficiency due
vey, in the case of a stock level of 3.5 m, the cohesive layer was to the increase in the HBI charge ratio are thoroughly elucidated.
found in the upper part of the furnace. Therefore, a thermal reserve And additionally, based on the results of this test operation and the
zone was not formed. kinetics analysis, the effect of the employment of HBI in the com-
3.3 Blast furnace raw material evaluation technology develop- mercial blast furnace was estimated. Later on, demonstration tests
ment period up to HBI 100 kg/t were conducted in the Wakayama No. 5 Blast
3.3.1 High pulverized coal rate, low slag rate test Furnace (after the third repair and improvement, furnace volume
In the eighth test operation conducted in March 1996, under the 2 700 m3), and the effects of the productivity improvement and the
ordinary blast furnace raw material condition, namely a sintered ore reducing agent rate reduction were confirmed as predicted by the
ratio of 75% and a lump ore ratio of 25%, the change in the raw ma- theoretical analysis. 28)
terial properties in the furnace due to the difference between the 3.3.3 Evaluation of low slag sintered ore
high pulverized coal rate operation (PCR > 200 kg/t, equal to or The tenth test operation was conducted in October 1997, six
higher than the one in the commercial blast furnace operation) and months after the ninth test operation. The test operation was con-
the entire coke operation was studied. However, as stated earlier, as ducted for quantitative analysis of the effects of the high tempera-
the blast air temperature of the experimental blast furnace is lower ture character, reducibility, and the slag rate of the low SiO2 sintered
than that of the commercial blast furnace, to simulate the tuyere ore on the blast furnace permeability. 29) Table 3 shows the test con-
front combustion condition of the commercial blast furnace, the de- ditions. The test operations were conducted for five cases of four
gree of oxygen enrichment was increased to fit the oxygen excess different types of sintered ore and one case in which the material
coefficient. As a result of the test operation, in the high pulverized property and the blast furnace slag rate were changed by adjusting
coal rate operation, the soot generated at the furnace top increased, the amount of the flux materials. The blasting condition, charged O/
and an increase in the strength of the coke at the furnace bottom C, and the target slag compositions are fixed.
considered to be the effect of the unburnt char generated in the fur- As a result of the test, in Fig. 18, the effects of the blast furnace
nace was observed. In addition, it was confirmed that these phenom- slag rate and the high temperature permeability resistance index of
ena become more remarkable in the low slag rate operation where the sintered ore (KS) 26) measured by the softening and melting test
the sintered ore ratio is lowered to 25%. on the blast furnace permeability resistance index (KR) 30) are
3.3.2 Evaluation of reduced iron shown. Focusing on Case 1 in Table 3 as the basis of the compari-
The ninth test operation was conducted in April 1997 to quanti- son, in Case 2, with the low SiO2 of the sintered ore, KS decreases
tatively grasp the effects of hot briquette iron (HBI) on the blast fur- and the blast furnace slag rate decreases along with the decrease of
nace productivity improvement and reduction of the reducing agent SiO2. In Case 3, the decrease in the blast furnace slag rate is covered
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Fig. 16 Relative production rate, reducing agent rate and permeability through the reduced iron melting tests using experimental blast furnace
Case No. 1 2 3 4 5
Sinter Sample A B B C D
SiO2 (%) 5.01 3.89 3.89 4.63 4.60
CaO (%) 9.99 9.09 9.09 9.44 9.86
MgO (%) 1.09 1.11 1.11 1.19 0.94
Al2O3 (%) 2.09 1.87 1.87 1.95 1.84
FeO (%) 7.47 5.88 5.88 6.93 5.86
RI (%) 64.6 68.0 68.0 68.1 66.9
KS × 105 1 500 648 648 1 085 1 195
Fig. 17 Calculated results of experimental blast furnace operation RDI (%) 41.7 42.8 42.8 45.3 44.2
TI (%) 76.9 81.3 81.3 75.1 67.2
Fluxes (kg/t-HM) 33.5 13.3 74.1 5.5 19.3
by the blast furnace flux materials. The figure shows that the effect Slag rate (kg/t-HM) 302 258 302 271 271
of KS on the blast furnace permeability is significant, and the effect Ore/Coke (-) 3.64 3.58 3.60 3.59 3.61
of the blast furnace slag rate is considerably small as compared with
that of KS. Further, under these test conditions, there were no effects
of RI and RDI of the sintered ore on the permeability. er, in the case of the Kashima No. 2 Blast Furnace, the blast furnace
Based on the result of this test operation, to grasp the effect of slag rate changed with the change of KS. However, despite that, in
KS on the permeability in the commercial blast furnace, the soften- both blast furnaces, since the behavior of the change of the values
ing and melting test result was formulated and was incorporated into calculated by the model into which the KS evaluation model was in-
the blast furnace mathematical models, and the commercial blast corporated without taking into consideration the influence of the
furnace permeability based on this model 27) was evaluated. The cal- blast furnace slag agrees with the behavior of the change of the ac-
culation results agree very well with respect to not only the static tual values, it was concluded that, even in the commercial blast fur-
pressure distribution on the experimental furnace wall when high/ naces, similarly to the result of the test blast furnace operation, the
low SiO2 sintered ore is used, but also, as Fig. 19 shows, very well effect of the blast furnace slag rate is small compared with that of
with respect to the actual KR values obtained from the Kokura No. 2 KS.
Blast Furnace (after the second repair and improvement, furnace 3.3.4 Evaluation of high Al2O3 slag
volume 1 850 m3) and the Kashima No. 2 Blast Furnace (after the The eleventh test operation was conducted in March 2000. The
third repair and improvement, furnace volume 4 800 m3). In the case objectives of the test operation were to lower SiO2 of the sintered
of the Kokura No. 2 Blast Furnace, during the period of the subject ore aimed at blast furnace permeability improvement, and to clarify
operations, the blast furnace slag rate was almost constant. Howev- the in-furnace phenomena focusing on the permeability in the lower
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Table 4 Results of experimental blast furnace operation
part of the furnace and the slag drainage characteristics on the fur-
nace working floor, to cope with the rise of the slag Al2O3 concen-
tration coming from the blast furnace slag reducing movement pro-
moted from the viewpoints of reducing the amount of slag disposal
and the environmental protection. 31) The test operations were con-
ducted, under the condition of fixed per tap slag output, for five cases Fig. 20 Effect of the slag content on drainage rate
wherein two types of sintered ore were used and the slag Al2O3, slag
MgO, and the CaO/SiO2 levels were differentiated by the addition to the effect of the wettability via the slag static hold-up, and the ef-
of flux materials. Table 4 shows the results. fects of the slag viscosity and the crystallization temperature are
Figure 20 shows the effect of the slag contents on the slag drain- small. Furthermore, as Fig. 22 shows, the permeability resistance
age rate on the 1 500°C corrected base, eliminating the influence of index of the cohesive zone (KRM) is confirmed to depend on the sin-
temperature. Along with the rise of slag Al2O3, the slag viscosity rises tered ore KS. Namely, even in the high Al2O3 sintered ore, the rise
and the slag drainage rate lowers, and as MgO rises, the slag viscos- of the KS value is suppressed by increasing MgO, and the permea-
ity lowers and the drainage rate rises. On the other hand, no effect of bility of the cohesive zone is maintained thereby.
the slag crystallization temperature on the slag drainage rate was 3.3.5 Evaluation of material quality
observed. Namely, the slag drainage phenomenon is a fluidity-domi- In the twelfth test operation in January 2001, waste plastic pow-
nant phenomenon, and since the high MgO slag content in the high der was injected through the tuyere. However, since a sturdy hang-
Al2O3 content slag, despite raising the crystallization temperature, ing was built right after the start of the injection of the waste plas-
lowers the slag viscosity, high MgO was found to be effective in en- tics, the test operation was terminated.
hancing the slag drainage rate. The thirteenth test operation was conducted in November 2003
As Fig. 21 shows, a positive correlation is recognized between with the objectives of evaluating the quality of the high-reducibility
the calculated static hold-up in the dripping zone and the permeabil- sintered ore and inspecting the effectiveness of the high-reactivity
ity resistance index in the dripping zone (KRL). The pressure drop in coke under the joint use state with the high-reducibility sintered
the dripping zone of the experimental blast furnace rises with the in- ore. 32) In the experimental blast furnace, the reducing agent rate was
crease of the slag Al2O3, slag CaO/SiO2, which is mainly attributed 700–800 kg/t, higher than that of the commercial blast furnace due
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Table 5 Test cases of the experimental blast furnace
Coke (CRI)
Coke A (25.6) Coke B (42.2)
Sinter A (65.3) Case 1 -
Sinter (RI) Sinter B (72.3) Case 2 Case 3
Sinter B-fine (86*) Case 4 Case 5
*
Apparent RI
achieved.
As shown in Table 5, the test operations were conducted for the
four cases wherein the combination of each of the two types of coke
and each of the two types of sintered ore arranged as below was
Fig. 22 Effect of sinter high temperature property KS on permeable changed. Two types of coke were produced by changing the coal
resistance index of cohesive zone KRM of experimental blast blending ratio so that the coke reactivity index (CRI) of the coke is
furnace
differentiated by 10%. The two types of sintered ore have different
levels of reducibility index (JIS-RI). One case in which the apparent
to: the large per ton hot metal heat diffusion from the furnace be- JIS-RI of the high-reducibility sintered ore is further improved by
cause of the restricted furnace volume, higher furnace top gas tem- grain-refining was additionally arranged.
perature because of the restricted furnace height and the restricted In the case where the coke reactivity is fixed and the sintered ore
blast air temperature. Therefore, upon evaluating the sintered ore reducibility is changed, in addition to the rise of the hot metal form-
quality and the coke quality, various countermeasures were taken to ing rate, increase of the top gas utilization and improvement in the
conduct the operation under the in-furnace reducing condition as reducing agent rate by the enhanced JIS-RI, the improvement in
closely as possible to the actual blast furnace operation conditions. permeability was confirmed. In the case where the sintered ore re-
As for the modifications of the equipment, aiming at heat loss ducibility is fixed and the coke reactivity is changed, improvement
improvement, the furnace height was extended, and the stock level in the top gas utilization efficiency and lowering of the top gas tem-
was set at the height of 6.0 m from the tuyere level, heightened from perature by the use of high-reactivity coke were confirmed, while
the past 4.5 m level. By the extension of the furnace height, the fur- the amount of solution loss carbon decreased. As shown in Fig. 23,
nace volume was expanded to 4.0 m3 from the past 3.0 m3. Further- according to the measurement by the vertical probe at the same
more, as new sensors to grasp the in-furnace state of the reaction time, with the high-reactivity coke, the thermal reserve zone tem-
further, a rigid-type vertical probe that follows the descent of the perature dropped to 920°C from 980°C, and the improvement in re-
burden was installed, and the gas sampling devices that enable si- action efficiency was confirmed. Simultaneously, to grasp the in-
multaneous gas-sampling in the height direction were installed on furnace phenomena when the high-reactivity coke is used, evalua-
the furnace wall (Fig. 10). The modifications in the blasting condi- tion of the strength of the in-furnace coke sampled by the sampling
tion are: increase of the bosh-gas volume anticipating improvement device during operation was also conducted.
in the heat loss by the increased production, the rise of the tempera- According to Fig. 24, when the high-reactivity coke was used
ture set in front of the tuyere anticipating increase in the hot gas (Case 3), the amount of solution loss carbon decreased as compared
flow rate, decrease in pulverized coal rate, and the dehumidified with Case 2, and as a result thereof, the degradation of coke was
blasting by the application of nitrogen injection. Additionally, as a considered to be suppressed. However, when KR was maintained at
result of thinning the charged material layer aimed at improving the the same level as that of Case 2, the improvement of the in-furnace
reactivity efficiency, and lowering the targeted hot metal tempera- permeability was not confirmed, which is considered to be attributed
ture, an operation with a reducing agent rate of below 600 kg/t was to the extremely small load in the experimental furnace as compared
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Table 6 Layer structures of test cases
rials of ore and coke which had been previously blended according
to the predetermined weight ratio (Fig. 10).
Table 6 shows the layer structure for each test case. The conven-
tional layer structure of ore and coke charging is taken as the basis
for comparison, and the following three cases of mixed layer ar-
rangement were prepared: Case 1: half of the entire charging materi-
als in terms of weight are mixed (partly mixed condition); Case 2:
the coke of the mixed layer of Case 1 is grain-refined (partly refined-
Fig. 25 Effect of JIS-RI and CRI on reducing agent rate coke mixed condition); and Case 3: fully mixed case of Case 1
(completely mixed condition).
with that of a commercial blast furnace. Figure 26 shows the result of each case of the test operation
Figure 25 shows the effects of the sintered ore JIS-RI and the with respect to the reducing agent rate, top gas utilization efficiency,
coke CRI on the reducing agent rate. With a fixed CRI, along with and the in-furnace pressure drop. Together with the order of increase
the rise of JIS-RI, the top gas utilization rises and the reducing agent in the mixing ratio, or the charging layer structure change from the
rate is lowered. When JIS-RI is fixed, since the abovementioned conventional layer arrangement to the partial mixing and the com-
trend is remarkable when the high-reactivity coke is used, it was plete mixing arrangement, the top gas utilization is improved and
confirmed that the operation-improving effect of the high-reactivity the reducing agent rate is enhanced. From the result of the measure-
coke works effectively under the joint use with the high-reducibility ment by the vertical probe, as compared with the base case of the
sintered ore. Further, JIS-RI of the grain-refined high-reducibility conventional layer structure, in Case 3 of complete mixing, the ther-
sintered ore is equivalent to 86%. However, its effect on the gas uti- mal reserve zone temperature and the top gas temperature are lower,
lization efficiency and the reducing agent rate was small. The rise of and improvement in the top gas utilization was confirmed. Further-
the top gas temperature is considered to offset the reducibility im- more, in the result of the dissection survey of the experimental blast
proving effect by grain-refining. furnace, in the mixed layer of coke and ore, the bedrock-like fu-
3.3.6 Evaluation of the effect of mixed layer sioned ore layer normally observed in the conventional ore/coke
The fourteenth test operation, the last test operation, was con- layer structure was not confirmed. This is considered to be attributed
ducted in November 2008, five years after the implementation of the to the aggregate effect of the mixed coke. In the experimental blast
thirteenth test operation. To realize the high productivity and low re- furnace wherein the load exerted by the burden is smaller than that
ducing agent rate, the effect of the mixed layer of ore and coke of a commercial blast furnace, the lowering of the pressure drop was
(proximate arrangement of ore and carbonaceous material) on reac- not confirmed. In the cases of partial mixing, the pressure drop is
tivity and permeability was evaluated. 33) For the implementation of higher than that of the base case, the phenomenon of which is con-
this test, in addition to the then existing hoppers for coke and ore sidered to be attributed to the decrease in the void fraction of the
use, an additional hopper was installed for charging the mixed mate- packed bed, and the increase in the slag holdup caused by the coex-
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References
1) The Bureau of Mines, The Ministry of Agriculture and Commerce: Ref-
erence document pertaining to iron and steel industry. 1919
2) The Bureau of Mines, The Ministry of Commerce and Industry: Refer-
ence document pertaining to iron and steel industry. 1931
Fig. 27 Relationship between reducing agent rate and gas utilization of
3) The Japan Iron and Steel Federation: Handbook for Iron and Steel Sta-
experimental blast furnaces
tistics. 1961–2018
4) The Japan Iron and Steel Federation HP: http://www.jisf.or.jp
5) Tate, M.: Met. Technol. (Jpn.). 399, 36 (1963)
istence of the mixed coke of remarkably decreased grain size due to 6) Tate, M.: Tetsu-to-Hagané. 70 (11), 1501 (1984)
prior solution loss reaction and the relatively sound slit coke in the 7) Nakata, Y. et al.: Tetsu-to-Hagané. 16 (11), 1205 (1930)
dripping zone. 8) Yasumoto, T.: Blast Furnace Ironmaking Method. Sangyotosho, 1954
9) Miyashita, T. et al.: Tetsu-to-Hagané. 57 (11), S351 (1971)
10) Miyashita, T. et al.: Tetsu-to-Hagané. 58 (5), 608 (1972)
4. Conclusion 11) Ando, R. et al.: Nippon Kokan Tech. Rep. 54, 371 (1971)
Much information was obtained from the experimental blast fur- 12) Miyazaki, T. et al.: Tetsu-to-Hagané. 73 (15), 2122 (1987)
nace of Nippon Steel constructed in Hasaki after those in Higashida, 13) Hatano, M. et al.: Tetsu-to-Hagané. 62 (5), 505 (1976)
Tobata, and that of the University of Tokyo which have supported 14) Mizuno, Y. et al.: Tetsu-to-Hagané. 70 (4), S35 (1984)
the development of blast furnace operation technologies, and the in- 15) Kamei, Y. et al.: Tetsu-to-Hagané. 79 (4), 449 (1993)
16) Kamei, Y. et al.: Tetsu-to-Hagané. 79 (4), 456 (1993)
formation obtained continues to be used up to the present day. As 17) Miyazaki, T. et al.: Tetsu-to-Hagané. 72 (4), S120 (1986)
for the problem of dissimilarity which is inevitable in a small-scale 18) Yamaoka, H. et al.: Tetsu-to-Hagané. 77 (12), 2099 (1991)
experimental blast furnace, thanks to the development of equipment 19) Miyazaki, T. et al.: Tetsu-to-Hagané. 73 (4), S129 (1987)
and operation technologies, improvements in the reducing agent rate 20) Kamei, Y. et al.: Tetsu-to-Hagané. 79 (2), 139 (1993)
21) Yamamoto, T. et al.: CAMP-ISIJ. 6 (4), 1012 (1993)
and the gas utilization have been achieved, approaching the com-
22) Ishida, H. et al.: CAMP-ISIJ. 10 (1), 197 (1997)
mercial blast furnace levels as shown in Fig. 27. 23) Yamagata, C.: et al.: CAMP-ISIJ. 4 (1), 143 (1991)
Furthermore, owing to today’s highly accurate mathematical 24) Yamagata, C.: et al.: CAMP-ISIJ. 4 (4), 1020 (1991)
models, the issue of dissimilarity has been considerably comple- 25) Ujisawa, Y. et al.: Tetsu-to-Hagané. 92 (10), 591 (2006)
mented, and the precise estimation of the operation of commercial 26) Mochizuki, K. et al.: Tetsu-to-Hagané. 72 (14), 1855 (1986)
27) Takatani, K. et al.: ISIJ Int. 39 (1), 15 (1999)
blast furnaces based on the quantitative analysis of the operation re- 28) Ujisawa, Y. et al.: CAMP-ISIJ. 22 (1), 282 (2009)
sult obtained from the experimental blast furnace has become possi- 29) Matsukura, Y. et al.: Tetsu-to-Hagané. 87 (5), 350 (2001)
ble. However, there is still room for further study on the effects of 30) Matoba, Y. et al.: Tetsu-to-Hagané. 60 (5), S354 (1974)
the in-furnace load on the difference in the ore-softening and shrink- 31) Sunahara, K. et al.: Tetsu-to-Hagané. 92 (12), 875 (2006)
32) Natsui, T. et al.: Tetsu-to-Hagané. 99 (4), 267 (2013)
ing behaviors of iron ore, and on the permeability. Therefore, the
33) Natsui, T. et al.: CAMP-ISIJ. 25 (2), 958 (2012)
significance of the R&D method using an experimental blast fur-
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NIPPON STEEL TECHNICAL REPORT No. 123 March 2020
Takuya NATSUI Yoshinori MATSUKURA
Senior Researcher Senior Manager
Ironmaking Research Lab. Experimental Blast Furnace Project Div.
Process Research Laboratories Process Research Laboratories
20-1 Shintomi, Futtsu City, Chiba Pref. 293-8511
Kaoru NAKANO
Chief Researcher
Ironmaking Research Lab.
Process Research Laboratories
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