Techniques For Measuring Stress-Strain Relations at High Strain Rates
Techniques For Measuring Stress-Strain Relations at High Strain Rates
by Frank E. Hauser
ABSTRACT---Thequalitative dependence of the mechanical                      suits have been valuable to check proposed rate-
behavior of some materials on strain rate is now well                       determining plastic-deformation mechanisms. T h e
known. But the quantitative relation between stress,
strain and strain rate has been established for only a few                  necessity of knowing the effect of rate on the be-
materials and for only a limited range. This relation,                      havior of materials is not only necessary to scientific
the so-called constitutive equation, must be known before                   endeavors, b u t also to practical engineering con-
plasticity or plastic-wave-propagation theory can be used                   siderations when designing members which are sub-
to predict the stress or strain distribution in parts sub-                  jected to impacts. Thus, under the combined
jected to impact stresses above the yield strength.
   In this paper, a brief review of some of the experi-                     pressure of scientific as well as practical investiga-
mental techniques for measuring the stress, strain,                         tions of the rate effect, m a n y schemes have been
strain-rate relationship is given, and some of the difficul-                devised to measure the stress, strain and strain
ties and shortcomings pointed out. Ordinary creep or                        rate over wide ranges of strain rate.
tensile tests can be used at plastic-strain rates from 10 -8
to about 10-1/sec. Special quasi-static tests, in which                        J. NI. Krafft I and H. Kolsky ~have given excellent
the stress- and strain-measuring devices as well as the                     reviews of some of the earlier schemes of measuring
specimen geometry and support have been optimized,                          high strain rates. I n prior publications on strain-
are capable of giving accm'ate results to strain rates of                   rate effects by the author, 3-5 the emphasis has been
about i02/sec. At higher strain rates, it is shown that
                                                                            on the material properties, and the experimental
wave-propagation effects must be included in the design
and analysis of the experiments. Special testing machines                   techniques for measuring these properties were not
for measuring stress, strain and strain-rate relation-                      included. I n this paper, after a brief section on the
ships in compression~ tension and shear at strain rates up                  derivation of pertinent equations, the experimental
to 105/sec are described, and some of the results pre-                      techniques used b y the author will be explained and
sented. With this type of testing machine, the analysis
of the data requires certain assumptions whose validity                     typical results presented.
depends upon proper design of the equipment. A                                 I n a simple tension test, such as Fig. l(a), the
critical evaluation of the accuracy of these types of                       load and the initial specimen area are k n o w n and,
tests is presented.                                                         thus, the engineering stress readily defined. Also,
                                                                            the initial gage length and change in length as a
Introduction                                                                function of time can be measured, and the engineer-
The mechanical behavior of most materials is known                          ing strain and strain rate calculated. Then, if one
to be influenced greatly by the testing temperature                         assumes uniform strain distribution t h r o u g h o u t the
and, to a somewhat lesser degree, b y the rate of de-                       gage section, the true stress and strain can be cal-
formation. The m a n y studies of the temperature                           culated. B u t if localized deformation such as a
effect have helped not only the engineer in design-                         Lfiders' band or necking occurs, the local stress and
ing structures at temperature extremes, but also the                        strain can only be obtained b y measuring the
scientist in the understanding of the basic plastic-                        elongation in the small region where these strains
deformation mechanisms. Only more recently                                  can again be assumed to be uniform. Similarly, if
have accurate studies of the rate effect over wide                          the rate of loading is increased greatly, at a n y in-
ranges of strain rate become possible, and these re-                        stant of time the load reading at the load cell m a y be
                                                                            different from the load carried b y the specimen.
Frank E. Hauser is Associate Pzwfessor of Mechanical Engineering and        The strain distribution within the gage length m a y
Research Engineer for the Inorganic Materials Research Division of the      also v a r y considerably due to the finite rate of
Lawrence Radiation Laboratory, University of California, Berkeley, Calif.
                                                                            stress and strain propagation. T o obtain useful
Paper was presented at 1965 S E S A Spring Meeting held in Denver, Colo.,
on M a y 5-7.                                                               data at high strain rates, the load cell must be small
                                                                   //JJ
                                                                     JH~"Jz.~
                                                                          /,'Fz.z
                                                                             /,"I///L'//////
                                                                                ,.z.z,-p,,..~,.J--                      I~"~
                                                                   /       '         ,,                         Input bar
Specime
                                                                   ~1/11/I/111/I//I
                                 Lood
                                  cell " ~     I
                                   '//////I/////////
                                                                                                               OutputbarL
                                                                                                                                                         a~ff\[
                                                                                                                                                    COMPRESSION
At the i n t e r f a c e , Ram
~BF = O~
Combine to get-
                                       @                               |
                                           I        |                   J
                                                                              -                                      Effect of Plastic:Deformation
                                                                                                                     on Wave Propagation
                                                 ~=ld~               c I = c2 = Cs = 2 0 0 , 0 0 0 in/sec.
                                                                     Hence transit time = 5/.zsecs.                       T h e use of eq (3) in the previous section implied
     Let A,= A3= 2A2;                      ~='P2 = &                                                                 the assumption t h a t d z / d e = E and t h a t E is a
     Then (I)'-'-'~)             ~tt = 4'/5 o~ and ~rr = - I/3 ~r~                                                   constant for a given material. This a s s u m p t i o n is
     so                          a~ : z/3 o~,   a-c: 4/3 ai                                                          valid for crystalline solids where the stretching of
              |174               ~t'= z/3 % and ~ ' = I/3 %                                                          the atomic bonds is nearly linear and r a t e inde-
     so                          o~ = 8/9 o-1 ,                a-|         I % o~                                    pendent. T h e a s s u m p t i o n of constant E for poly-
                                                                                                                     mers would certainly not be a good one because the
                                                                                                                     complex molecular bonding causes a nonlinear a n d
,%                                                                                                                   rate-sensitive stress-strain relation. Similarly, if
                             i                                                             r                         the stress at a n y point in a m e t a l exceeds the yield
          l---2,u secs. rise time 20                                   30                40     t # secs.            strength, plastic d e f o r m a t i o n occurs, and d z / d e is no
+l 0 I0
                                                         5g.
                                                                                                                     longer constant. T o m a k e use of a unique static
                                                                                                                     stress-strain relation in order to determine ( d z /
                       DUMMY
                                     LAND
                                    CAMERAS
                                            I--"-]
                                                                    U
                      IUMMY
                        I GAGES I                   ___
                                                                                                    (
                                               SR-4 STRAIN          LSR-4 STRAIN
                    OUT-PUT BAR~                (TRANSMI
                                                   WAVE)TTED(IN-POTWAVE)
                                                  GAGE                  GAGE
                                 i                     r
                                                               ou,pu,
AREA =~ c la gove. at t[
9 -o7 at I
                   +~atO
                                          O~t ~    O~t" ~c,o gove. at t,                          Level of O~i
                       /
                                                                                              /
                                                                                          /
                   /                                           \               /1"                 \
                                                                          /
                                                                                                       \
               /                                                        //(T    t' at B
           /                                                                                                        Fig. 6--Graphical solution
       /                                                           i                                                to eqs (7) and (8)
       I~ 2 d L / c l -~ ~zz "       tl     d~                     -c
                                                                   _L     2/ct (,~output_do)~
gages are subjected to high accelerations b y the                              uniformly within the specimen. T h e elastic rods at
passing stress waves. (The particle velocity in the                            the ends of the specimen constrain the lateral plastic
bar m a y go from zero to a b o u t 100 ft/sec in 3 ~sec.)                     deformation somewhat due to friction, but, with a
Because of the high harmonic content of a sharply                              good surface finish on the rods and a light film of
rising square wave, the electronic signal amplifiers                           lubricant, the final shape of the deformed compres-
must have a wide band pass, or the filtering action of                         sion specimens shows little barreling below 15-per-
t h e circuits will remove some of ~he information re-                         cent strain. This lateral constraint nevertheless
quired for analysis. For o p t i m u m results, a band                         limits the m i n i m u m thickness of the specimen.
pass of 10 mc or greater is desirable. T h e amplified                             The mathematical analysis for obtaining the
input and o u t p u t signals are displayed on single-                         stress, strain and strain-rate data has been pre-
sweep oscilloscopes and recorded by means of a                                 sented previously 3 b u t is included here in a more
camera m o u n t e d on the scope. The over-all experi-                        complete form.
mental arrangement is shown in Fig. 5.                                             I n Fig. 4 (a), on impact of the ram, a compressive
                                                                               stress ~ propagates down the input bar and is
Analysis of the Measurements                                                   partially reflected on reaching the specimen. This
                                                                               reflected stress ~, due to the impedance m i s m a t c h
   As was shown in Fig. 3, reflections and transient
                                                                               at the interface I, propagates back toward the r a m
stress waves arise even in a completely elastic
                                                                               past the input gage. The input gage then records
specimen. These transients can be accounted for
                                                                                ( ~ - ~). At interface I, t h a t p a r t of the input
b y the use of eqs (4) and (5). B u t if plastic de-
                                                                               stress which the specimen can support is trans-
formation takes place in the specimen, the transient
                                                                               mitted as at. As the specimen strain-hardens, a
stress waves will differ from those predicted b y the
                                                                               higher stress can be supported and at increases while
elastic analysis, and it is this difference t h a t con-
                                                                                ar decreases as a function of time. T h e t r a n s m i t t e d
tains the information as to the plastic behavior of
                                                                               stress at, in turn, is partially reflected at interface I I
the specimen. Since the input and o u t p u t rods re-
                                                                               as ~1 and the stress ~t 1 is t r a n s m i t t e d into the out-
main in the elastic state at all times, the stress and
                                                                               p u t bar and recorded at the o u t p u t gage. T h e
particle velocity can be determined for sections I
                                                                               reflected part of at at interface I I is reflected back
and I I in Fig. 4 at all times. These sections are
                                                                               and forth within the specimen and soon reaches the
c o m m o n to the bars and the specimen and, so, the
                                                                               equilibrium distribution (see a2 in Fig. 3).
stress and particle velocity at each end of the gage
                                                                                   Considering the equilibrium of forces at I and I I ,
section is known. I f the specimen is small enough
                                                                               we have
so t h a t the transit time for the elastic wave is short,
equilibrium t h r o u g h o u t the specimen is rapidly                                            ~FI ~   (~i -   ~r)A1 = ~tA2
established, and plastic deformation takes place                                                  ~FII --~ (~t -- ~rl)A~ = ~tIA1
v, r 280 ft./see.
                                                  20,000
    Fig. 7--Transient elastic-
    stress distribution in a
                                         Stress,
    stepped bar                          o'-, psi I 0 , 0 0 0
                                                                                                                     I                       IfI    \\   I
                                                                           ,oo                                                       /,,-.
                                                                        TimeH secs.                                        ', \
                                                -I 0,000
     ~4
     z
     -  2
20
          15
     n
     0
     .J
          IO
     z
     t~
400 I A u g u s t 1 9 6 6
                                                                                                           thick section. F r o m t h a t time on, there is appre-
                                                                      .././         :+ ~ ' - 1 5 9         ciable deviation of the observed record from the
 I0,000                                                                                                    predicted wave shape. Therefore, the one-dimen-
                                                             7+ ~ 158                                      sional elastic analysis used is n o t very accurate
                                                                                                           when one a t t e m p t s to predict stress waves in thick
                     141-~4~_~L_
                              7 7"--                                                I                      sections 9
n
                    ,40,--~1
                         ~/-~+/I'~J         '+"~147
                                                                                                               T h e experimental results of a plastically deform-
                                                                                                           ing compression specimen are shown in Fig. 8.
(~ I 0 0 0                                                                                                 T h e 0.4-in.-long, a/4-in.-diam tubular a l u m i n u m
(D                                          150
DJ
(13
                                                                                                           specimen was held between two hardened alu-
r~                                                                                                         m i n u m tubes of the same cross section. T h e experi-
Ld
D_                                                        GAGE                  APPLIED                    mental arrangement and analysis are as shown in
                                                TEST     LENGTH                  STRESS
I,I                                              NO.      (1 {IN)               0"-A {PSI)                 Fig. 6. The resulting stresses, strains and strain
<
rr
                                                 140             0.2             19,500                    rates at three points are indicated. Although the
                                                 14 I            O. I            19,000
z     I00                                        142             0.4             15,000                    example shown in Fig. 8 shows poor alignment and
                                                 147             0.4            37, 000
                                                 148             0.1            36~000
                                                                                                           large oscillations, the over-all strain measured on
t--
ffl                                              150             0.8            36,000                     the specimen after the experiment was within
                                                 15 I             1.6           37,000
tJA                                              157             0.4            48,000                     5 percent of the total strain predicted in the anal-
(.9
                                                 [58             0.2            49,000                     ysis.
CK                                               159             0.1            48,000
>                                                                                                              B y performing a series of experiments using dif-
 I                                                                                                         ferent gage length and impact velocities, the con-
                                                                                             g             stitutive equation curves for the material at a par-
                                        ,UASI-STATIC                                o      I%              ticular temperature can be constructed, as shown in
                                          T E STS                                   []     2%
                                                                                    A      4%              Fig. 9. This particular stress, strain and strain-
                                                                                    ~7     8%              rate relation has been used b y R a j n a k and Hauser 4
                                                                                    +      16 %
                                   E=AVERAGE STRAIN                                                        to predict the final shape of a long t u b u l a r cylinder
                                        AT T = 295r
                                                                                                           impacted at one end and free at the other. T h e
         I                                  I                I                                             final " t r u m p e t " shape of the tube was calculated
               10,000       15,000       2.0,000        25,000                50,000         35,000
                        ~7~mE.-AVERAGE STRESS IN PSI
                                                                                                           using the m e t h o d of characteristics to solve the
                                                                                                           governing plastic-wave-propagation equations. Un-
        Fig. 9--Effect of stress on strain rate in work-hardened                                           fortunately, even with the simple b o u n d a r y con-
        a l u m i n u m at c onstant strain, showing sampling of                                           ditions in t h a t problem, the solution necessitated
        experimental records
                                                                                                           the lengthy use of a computer, b u t the final predicted
                                                                                                           strain distribution agreed very closely to the meas-
        where c2 is the wave velocity in the specimen and a                                                ured distribution.
        is the gage length. F o r very short specimens, the                                                    I n Fig. 9, it can be seen t h a t almost identical re-
        lower time-limit correction for XH becomes negligi-                                                sults are obtained for long specimens impacted at
        ble.                                                                                               high velocities (such as No. 150) or short specimens
           The average strain in the specimen of gage length                                               at low velocities (No. 140). At the same strain and
        a will then be                                                                                     strain rate, the measured flow stresses are equal,
                XI - XII                                                                                   indicating the negligible effect t h a t the difference in
        ~avg
                    a                                                                                      ratio of end-constrained volume to total volume
                                                                                                           produces.
                             lIs
                            pC~          (r -- ~ ) d t - f a                        ~tIdt1           (7)       As an example of a more strain-rate-sensitive
                                                                              /c2                          material, the stress, strain and strain-rate relation
        and the average strain rate                                                                        for a t y p e 304 stainless steel are shown in Fig. 10.
                                                                                                           Here, the static tests are also included showing the
                        9          d~      (~i    -     ~)        -      ~                           (8)
                        ~vg = ~It =                     pca                                                effect of changing the strain rates by seven orders
        Figure 6 shows the procedure for the graphical                                                     of magnitude. T h e m a x i m u m strain rate attained
        solution of eqs (7) and (8).                                                                       in these tests was limited b y the m a x i m u m velocity
                                                                                                           of the impact r a m (1000 in./sec). T h e titanium
                                                                                                           input and o u t p u t bars used in this test have a yield
         Examples of Results                                                                               strength of 150 ksi, and this strength would impose
            Figure 7 illustrates the use of eqs (4) and (5) to                                             a new upper stress limit if a higher-velocity-impact
         predict the transient stress at station 1 in the                                                  source were available.
         elastic bar with a single change in cross section. I n                                                The final example shows the experimental records
         the measured record, the rise time is a b o u t 10 #sec,                                          obtained when testing a brittle material. Gabbro
         and the oscillations on the first step are due to lat-                                            rock, which normally crumbles at a compressive
         eral vibrations excited b y the lateral Poisson's ex-                                             stress of a b o u t 30 ksi, withstood over 65 ksi for
         pansion. I n the fourth step on the stress curve,                                                 a b o u t 3 #sec when loaded rapidly, as shown in Fig.
         the first reflection from the free end arrives with the                                           11. T h e dip in the input bar stress at 40 #sec
         much larger amplitudes of oscillations from the                                                   corresponds to the elastic compression of the rock,
                           ///
              I0     QUASI-STATIC
                       TESTS      "                                            tion of m a n y materials in the range f r o m 100/sec
                                                                               to a b o u t 100,000/sec. However, there are certain
                                                                               limitations inherent in the method. As the anal-
                                                                               ysis assumes equilibrium conditions in the sample
   z                                                                           being deformed, and this condition does not exist
   ~-         0.1                                                              during the first few microseconds of the test, the
   w                                                                           d a t a obtained at v e r y low strain values are not
                                                                               reliable. Proper design of the e q u i p m e n t helps,
                                                                               b u t the problem can only be minimized and not
                                                                               eliminated. T h e u p p e r limit of strain r a t e and
                                                                               stress are determined b y the yield strength of the
         0.001                                                                 i n p u t bar. I f plastic deformation takes place in
                                                                               this bar, the analysis as described no longer applies,
                                                                               as the position of the interface between specimen
        0.0001                                                                 and bar can no longer be determined b y the elastic
                          40          50     60         70                80   eq (3). Finally, the operation of the tester and the
                         O~AV.-E AVERAGESTRESS IN (lO3-PSI)
                                                                               interpretation of the records require a thorough
  Fig. 10--Effect of stress on strain rate at constant strain                  understanding of the mechanical and electrical
  for stainless steel, showing sampling of experimental                        systems involved. This, unfortunately, prevents
  record
                                                                               the procedure f r o m becoming a simple routine test.
                                                                               B u t as a research tool, the tester operated b y m a n y
                                                                               different students at the University of California
        80                                                                     has yielded heretofore unavailable high-strain-rate
                                                                               information. These d a t a h a v e been of great help
                                                                               in research on basic deformation and fracture
                                                                               mechanisms.
        6o                                                                                               Acknowledgments
                                                                                   T h e a u t h o r wishes to express his appreciation to
                                                                               the C o n v a i r Division of General D y n a m i c s Corp.
   a. 50
   o                                                                           and to the Inorganic Materials Research Division of
   o
   _o                                                                          the Lawrence R a d i a t i o n L a b o r a t o r y for s u p p o r t and
   z_ 4c                                                    L                  sponsorship of the research. H e also wishes to
                                                                               t h a n k C. A. Winter for help in the design of the
   hJ                                                                          tester and to J. E. D o r n for his continued interest
   (nt- 3 0
   cr
                          f//INPUT BAR                      k~,                and suggestions.
         2O
                                                            .,,\                                              References
                                                                                  1. Krafft, 17. M . , "'Instrumentation for High-Speed Strain Measure-
                                     (~t') BAR
                                   OUTPUT         I
                                                            ~1~                ments," Response of Metals to High Velocity Deformation, 9, Interscience,
                                                                               N e w York (1961).
         jc                                "~     I                               2. Kolsky, H., Stress Waves in Solids, Oxford University Pressl London
                                                                               (1953).
                                                                                  3. Hauser, F. E., Simmons, g. A., and Dorn, J . E., "Strain Rate
         0                   I               d/                     ~-,        Effects in Plastic Wave Propagation," Response of Metals to High Velocity
              0     I0      20       50    40             50       60     70   Deformation, 93, lnterseience, N e w York (1961).
                                 TIME IN p SEC.                                   4. Rajnak, S. L., and Hauser, F . E., "Plastic Wave Propagath~n in
                                                                               Rods," Syrup. Dynamic Behavior of Marls., A S T M Special Publ. No. 336,
                                                                               167 (1962).
  Fig. 11--Experimental record for ~/4-in.-Ionggabro rock                         5. Larsen, T. L., Rajnak, S. L., Haaser, F . E., and Dorn, J. E., "Plastic
  (static yield strength = 30,000 psi)                                         Stress~Strain Rate~Temperature Relations in H.C.P. Ag-Al Under
                                                                               Impact Loading," Jnl. Mech. Phys. Solids, 12, 361 (1964).
                                                                                  6. Chiddister, J. L., and Malvern, L. E., "'Compression-impact Testing
  while the dip at a b o u t 47/~sec in b o t h records corre-                 of A1 at Elevated Temperatures," EXPERIMENTAL MECHANICS, 3 (4), 81
                                                                                (1963).
  sponds to the stepwise crumbling of the material.                                7. Ripperger, E. A., and Yeakley, L. M., "'Measurement of Particle
                                                                               Velocities Associated with Waves Propagating in Bars," 1bid. (2), 47
  Other tests on single crystals of MgO show steps                             (1963).
  on t h e rising p a r t o f the output~ba-r -stress, indicating                 8. Malvern, L. E., and Efron, L., "'Longitudinal Plastic Wave Propaga-
                                                                               tion in Annealed Aluminum Bars," Tech. Rpt. No. 1, N S F Grant G-24898,
  some possible local yielding or cracking before final                        Michigan State Univ. (1964).