Instrumented Impact Testing of Metallic Materials: Standard Test Method For
Instrumented Impact Testing of Metallic Materials: Standard Test Method For
for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: E2298 − 18
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7.2.5 Calibration shall be performed if the instrumented 7.3.1 Displacement is normally determined by converting a
striker has undergone dismantling or repair, unless it can be strain gage voltage-time measurement to a force-time measure-
shown that removal of the striker from the test machine, and ment. The force-time relationship is proportional to the accel-
subsequent reattachment to the machine, does not affect the eration as a function of time. Given an assumed rigid striker of
calibration. Calibration shall also be performed under the mass m, the initial impact velocity v0, the time t following the
circumstances described below. beginning of the deformation at t0, and expressing the velocity
7.2.6 Requirements on Instrumented Absorbed Energy—For as a function of time by v(t), the specimen bending displace-
each test in which the entire force signal has been recorded ment s(t) is calculated by double numerical integration as
(that is, until the force returns to the baseline), the difference follows:
between absorbed energy given by the dial or optical encoder, t
or both, KV and the instrumented absorbed energy Wt shall be 1
within 15 % or 1 J, whichever is larger. If this requirement is v~t! 5 v0 2
m * F ~ t ! dt (1)
not met but the difference does not exceed 25 % or 2 J, t0
whichever is larger, force values shall be adjusted until KV = t
Wt within 0.01 J (3). If the difference exceeds 25 % or 2 J,
whichever is larger, the test shall be discarded and the user
s~t! 5 * v ~ t ! dt (2)
shall check and if necessary repeat the calibration of the t0
instrumented striker. If recording of the entire force signal is 7.3.2 The initial impact velocity needed to perform the
not possible (for example due to the specimen being ejected above integrations may be calculated from:
from the machine without being fully broken), the user shall
demonstrate conformance to the requirements above by testing v 0 5 =2gh0 (3)
at least five Charpy specimens of any equivalent material. where:
NOTE 1—Specimens with certified values of maximum force (Fm) can g = the local acceleration due to gravity, and
be tested to verify the accuracy of the force values measured by the h0 = the falling height of the striker.
instrumented striker. Dynamic impact force verification specimens are
available6 with certified Fm values of 24.06 kN and 33.00 kN. These 7.3.2.1 Alternatively, the velocity signal registered when the
values have been established at room temperature through an interlabo- pendulum passes through its lowest position and strikes the
ratory study (4) involving six international laboratories, see also 13.1.3. specimen can be optically measured directly to determine v0.
The same verification specimens can also be used for indirect verification 7.3.3 Displacement can also be determined by non-
of the impact machine in accordance with Test Methods E23.
contacting measurement of the displacement of the striker
7.3 Displacement Determination: relative to the anvil using optical, inductive, or capacitive
methods. The signal transfer characteristics of the displace-
ment measurement system must correspond to that of the force
6
The sole source of supply of the specimens known to the committee at this time measuring system in order to make the two recordings syn-
is NIST. If interested, email charpy@boulder.nist.gov. If you are aware of
alternative suppliers, please provide this information to ASTM International
chronous. The displacement measuring system shall be de-
Headquarters. Your comments will receive careful consideration at a meeting of the signed for nominal values of up to 30 mm. Linearity errors in
responsible technical committee,1 which you may attend. the measuring system shall yield measured values to within
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E2298 − 18
+2 % in the range 1–30 mm. Measurements between zero and 10.3 Characteristic Values of Displacement—The forces
1 mm may not be sufficiently accurate to determine the defined in 10.2 have corresponding displacements which are
displacement. In such cases, it is recommended that the given the same subscripts as the forces. In addition, a displace-
displacement of the specimen be determined from time mea- ment corresponding to the end of the force-displacement curve,
surement and the striker impact velocity as indicated in Eq 1 st, is defined.
and 2. 10.3.1 The displacement at the onset of general yielding of
7.4 Recording Apparatus: the ligament is sgy.
7.4.1 The minimum data acquisition requirement is a 10-bit 10.3.2 The displacement at maximum force is sm.
analog-digital converter with a minimum sampling rate of 1000 10.3.3 The displacement at the initiation of unstable crack
data points per millisecond. However, 12-bit or more is propagation is sbf.
recommended. A minimum storage capacity of 8000 data 10.3.4 The displacement at the end (arrest) of unstable crack
points is required. propagation is sa (generally, sa is approximately equal to sbf
7.4.2 The instrumented absorbed energy shall be compared due to the steep drop in the force-displacement curve between
with the absorbed energy shown by the machine dial or optical Fbf and Fa).
encoder, or both. For requirements on the comparison between 10.3.5 The displacement at the end of the force-
KV and Wt, refer to 7.2.6. displacement curve is st. This point is defined as the displace-
ment at which the force has decreased to the pre-test baseline
8. Test Specimens value.
8.1 The CVN specimens shall be in accordance with Test 10.4 Characteristic Values of Partial Instumented Absorbed
Methods E23. The MCVN specimens shall be in accordance Energy:
with Test Method E2248. 10.4.1 Given the force definitions in 10.1, the force-
displacement curve may be partitioned and corresponding
9. Procedure
partial instrumented absorbed energies may be determined. The
9.1 Specimen Testing—The test is performed using the same values of the partial instrumented absorbed energies are given
procedure as the CVN or MCVN impact test according to Test the same subscript as the force at the end of the appropriate part
Methods E23 or E2248, respectively. In addition, the voltage- of the force-displacement curve.
time curve is measured and evaluated to give the force- 10.4.2 The area under the complete force-displacement
displacement curve. The force-displacement curve is evaluated curve up to st is the instrumented absorbed energy with the
with respect to the characteristic phases of the deformation and abbreviation Wt.
fracture stages. 10.4.3 The partial instrumented absorbed energy up to
9.2 Data Acquisition—The high speed acquisition system maximum force is Wm.
(the portion of the system which is capable of storing the 10.4.4 The partial instrumented absorbed energy up to the
dynamic response signal) shall be triggered such that baseline force at the initiation of unstable crack propagation is Wbf.
data before loading and after fracture (or release of the 10.4.5 The partial instrumented absorbed energy up to the
specimen from the anvils) is retained in computer memory. force at the arrest of unstable crack propagation is Wa (on
account of the steep drop in the force-displacement curve
10. Characteristics of the Force-Displacement Curve between Fbf and Fa, it is generally the case that Wbf is
10.1 Type of Force-Displacement Curve—Representative approximately equal to Wa).
force-displacement curves and their characteristic force values
11. Evaluation of the Force-Displacement Curve
are illustrated in Fig. 2.
11.1 The force-displacement curve is determined by double
10.2 Characteristic Values of Force:
numerical integration of the force-time curve.
10.2.1 The general yield force Fgy is the force at the
transition point from the initial linear elastic part, discarding 11.2 Representative force-displacement curves of various
the inertia peaks (normally one, unless the specimen was not types are given in Fig. 2. These can be grouped as the
fully in contact with the anvils), to the curved increasing part following types:
of the force-displacement curve. It serves, to a first Type A Lower shelf (brittle fracture)
approximation, as an indication of yielding across the entire Type B Ductile-to-Brittle Transition Region (mixed mode
fracture)
ligament. Type C Upper shelf (ductile fracture)
10.2.2 The maximum force Fm corresponds to the maximum
NOTE 2—The type of force-displacement curve may be determined by
value of the curve fitted through the oscillations of the comparison with the examples shown in Fig. 2.
force-displacement curve following the onset of yield of the
entire ligament. 11.2.1 With force-displacement curves of type A, typically
10.2.3 The force at the initiation of unstable crack propaga- only unstable (brittle) crack propagation occurs. For type B,
tion Fbf is the force at the beginning of the steep drop in the various amounts of stable and unstable crack propagation can
force-displacement curve. It characterizes the beginning of occur. For type C, only stable (ductile) crack propagation
unstable crack propagation. occurs.
10.2.4 The force at the end (arrest) of unstable crack 11.3 A condition for further evaluation of the force-
propagation is Fa. displacement curve is the occurrence of a well defined general
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E2298 − 18
yield force Fgy. It should be noted that force oscillations are values allows an approximate value of the proportion of ductile
observed on the pre-maximum force test record which arise fracture surface (SFA) to be calculated. Several researchers
from force interaction between the striker and the specimen. have reported good correlation for pressure vessel materials
These oscillations are usually damped out by plasticity before using one or more of the equations given below (1, 5):
maximum force.
11.4 Determination of the Characteristic Values of Force:
SFA 5 1 2F F bf 2 F a
Fm G
3 100 (4)
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E2298 − 18
accordance with Practice E691 in eight laboratories, each one V-notch specimens with square cross section (4.83 × 4.83
obtaining from five to six test results for each test parameter mm2) of A533B C1.1 (tested at room temperature and 150 °C)
(Table 2). See ASTM Research Report No. E28–1040.7 and of two reference materials produced by the National
13.1.3 Another interlaboratory study (2) of characteristic Institute of Standards and Technology, Boulder CO (low
instrumented impact forces and instrumented absorbed ener- energy and high energy). The ILS was conducted in accordance
gies was conducted using Charpy V-notch specimens (see Test with Practice E691 in six laboratories, each one obtaining up to
Methods E23) of two reference materials produced by the six test results for each test parameter (Table 5). See ASTM
National Institute of Standards and Technology, Boulder CO Research Report No. E28–1038.10
(low energy and high energy). The ILS was conducted in 13.1.7 Another interlaboratory study (8, 9) of characteristic
accordance with Practice E691 in six laboratories with eight instrumented impact forces, displacements and instrumented
different test machines providing ten test results for each test absorbed energies was conducted using miniaturized Charpy
parameter (Table 3). See ASTM Research Report No. V-notch specimens with rectangular cross section (3 × 4 mm2)
E28–1035.8 of A533B Cl.1. The ILS was conducted in accordance with
13.1.4 A third interlaboratory study (7) of characteristic Practice E691 in thirteen laboratories with fourteen test
instrumented impact forces and instrumented absorbed ener- machines, each one obtaining up to five test results for each test
gies was conducted using Charpy V-notch specimens (see Test parameter (Table 6). See ASTM Research Report No.
Methods E23) of one reference material produced by the E28–1037.11
Institute for Reference Materials and Measurements, Geel 13.2 Bias—This Test Method has no bias because charac-
Belgium (ERM high energy). The ILS was conducted in teristic instrumented impact forces, displacements and instru-
accordance with Practice E691 in nine laboratories, each mented absorbed energies are defined only in terms of this Test
providing two test results for each test parameter (Table 4). See Method. Furthermore, since there is no accepted reference
ASTM Research Report No. E28–1036.9 material, method, or laboratory suitable for determining the
13.1.5 MCVN Specimens—Results from two interlaboratory bias for the procedure in this Test Method, no statement on bias
studies are used to establish the precision of this Test Method is being made.
for MCVN specimens.
13.1.6 An interlaboratory study (6) of characteristic instru- 14. Keywords
mented impact forces, displacements and instrumented ab- 14.1 impact test; instrumented impact testing; miniaturized
sorbed energies was conducted using miniaturized Charpy Charpy test; notched specimens; pendulum machine; shear
fracture appearance
7
Supporting data have been filed at ASTM International Headquarters and may
be obtained by requesting Research Report RR:E28-1040.
8 10
Supporting data have been filed at ASTM International Headquarters and may Supporting data have been filed at ASTM International Headquarters and may
be obtained by requesting Research Report RR:E28-1035. be obtained by requesting Research Report RR:E28-1038.
9 11
Supporting data have been filed at ASTM International Headquarters and may Supporting data have been filed at ASTM International Headquarters and may
be obtained by requesting Research Report RR:E28-1036. be obtained by requesting Research Report RR:E28-1037.
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E2298 − 18
TABLE 3 Results from ILS on CVN specimens (2)
Repeatability Reproducibility
Energy Repeatability Reproducibility
Parameter Average Standard Standard
Level Limit Limit
Deviation Deviation
Fgy, kN Low 29.85 0.68 4.19 1.89 11.73
High 19.42 0.40 1.09 1.12 3.06
Fm, kN Low 31.90 0.65 3.85 1.82 10.79
High 23.50 0.16 1.96 0.44 5.49
Wt, J Low 18.63 0.63 1.23 1.76 3.45
High 108.39 2.55 4.13 7.13 11.55
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REFERENCES
(1) Nanstad, R. K., and Sokolov, M. A., “Charpy Impact Test Results on Bury St. Edmunds, Suffolk, IP32 6BW UK, 1996.
Five Materials and NIST Verification Specimens Using Instrumented (6) Manahan, M. P., Sr., Martin F. J., and Stonesifer, R. B., “Results of the
2-mm and 8-mm Strikers,” Pendulum Impact Machines; Procedures ASTM Instrumented/Miniaturized Round Robin Test Program,” Pen-
and Specimens for Verification, ASTM STP 1248, T. A. Siewert, and dulum Impact Testing: A Century of Progress, ASTM STP 1380, T. A.
A. K. Schmieder, eds., ASTM, 1995, pp. 111-139. Siewert and M. P. Manahan, Sr., Eds., American Society for Testing
(2) McCowan, C. N., Splett, J. D., and Lucon, E., “Dynamic Force and Materials, West Conshohocken, PA, 1999.
Measurement: Instrumented Charpy Impact Testing,” NISTIR 6652, (7) International Atomic Energy Agency, Final Report of Coordinated
January 2008 . Research Project 8 (CRP-8), “Master Curve Approach to Monitor
(3) Lucon, E., Chaouadi, R., and van Walle, E., “Different Approaches for
Fracture Toughness of Reactor Pressure Vessels in Nuclear Power
the Verification of Force Values Measured with Instrumented Charpy
Plants,” in preparation.
Strikers,” Pendulum Impact Machines: Procedures and Specimens,
ASTM STP 1476, T. A. Siewert, M. P. Manahan, Sr., and C. N. (8) Lucon, E., “Round-Robin on Instrumented Impact Testing of Sub Size
McCowan, eds., ASTM, 2006, pp. 95-103. Charpy-V Specimens: Results of Phase 1,” ESIS TC5, Final Report,
(4) McCowan, C. N., Santoyo, R. L., and Splett, J. D., “Certification 2 April 1998 .
Report for SRMs 2112 and 2113,” NIST Special Publication 260-172, (9) Lucon, E., “European Activity on Instrumented Impact Testing of
July 2009. Subsize Charpy V-Notch Specimens (ESIS TC5),” Pendulum Impact
(5) van Walle, E., “Evaluating Material Properties by Dynamic Testing,” Testing: A Century of Progress, ASTM STP 1380, T. A. Siewert, and
ESIS Publication 20, 1996 (European Structural Integrity Society), M. P. Manahan, Sr., Eds., American Society for Testing and Materials,
Mechanical Engineering Publications Limited, Northgate Avenue, West Conshohocken, PA, 1999, pp. 242-252.
SUMMARY OF CHANGES
Committee E28 has identified the location of selected changes to this standard since the last issue (E2298–15)
that may impact the use of this standard.
(1) 3.1 was revised to define absorbed energy, instrumented (5) 4.2, 5.3, 10.4, 10.4.1 to 10.4.5, 11.6, and 12.5 were revised
absorbed energy, and partial instrumented absorbed energy and to use partial instrumented absorbed energy.
add a shear fracture appearance definition. (6) 5.2 was revised to force.
(2) 1.1, 5.1 and 12.3 were revised to use absorbed energy. (7) Note 1 was revised to delete absorbed energy.
(3) 4.1, 5.3, 7.2.2, 7.2.6, 12.2, 13.1.2, 13.1.3, 13.1.4, 13.1.7, (8) 11.7, 11.7.1 and Section 14 were revised to use shear
and 13.2 were revised to use instrumented absorbed energy. fracture appearance, SFA.
(4) 7.4.2 was simplified and to use instrumented absorbed
energy.
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