MATERIAL TEST CERTIFICATE

AS PER STD EN 10204 TYPE 3.1

Customer : TechnipFMC TC No. : EC1650 Date : 13.06.2023

Invoice No.: WIF/EX/23-24/ Date :
P.O. No.: 4500705714 Line Item: 00010 PO Date : 02.06.2023 Spec. Ref.: M25070 Rev. : F (Date:16.07.2021)

Die No. Description Part No. Condition Forging Qty Material Melting Practice
Drg. No. PSL Level Ratio Sr.No. Mill
BODY FORGING, ULT PLUG
1299 3257105 Rev K Forged, 30.47 : 1 970 Nos. AISI 4140 BF-EOF-LRF-VD-CCM
VALVE 1 ULT150 F/3 IN
Normalized,
UNION ENDS AISI 4140
Quenched &
- JSW STEEL
Tempered,
Heat Code: NSN DU500001271 Rev B Shot Blasted

CHEMICAL COMPOSITION ( % )
Heat No :- C Mn Si S P Cr Mo V Ni Grain Size
F12396 0.40 0.91 0.19 0.008 0.015 1.05 0.23 0.003 0.03 7
Specn. Min. 0.38 0.75 0.15 - - 0.80 0.15 - - 6
Max. 0.43 1.00 0.35 0.025 0.025 1.10 0.25 0.30 1.00 -
HEAT TREATMENT
Procedure :- Q00025 Rev S

Heat Treatment Furnace :- Continous Type Furnace (CHTF) Temperature Monitoring Method:- Side Thermocouples in the Working Zone ( Method A)

HT Load No. of N :- AF-979 HT Batch No. of Q&T:- AF-985 Qty :- 970 Nos.
Test Piece Heat Treatment :- Along with job QTC location:- Sacrificial QTC Size- Actual Part
Hot Working Normalising Time Hardening Time Quench Quench Bath Temp. 1st Temper Time
Ratio Temp. Hrs. Temp. Hrs. Media Start End Temp. Hrs.
QTC 30.47 : 1 900⁰C 3 Hrs 20 Min 870⁰C 3 Hrs 20 Min OIL 36°C 50°C 545°C 5 Hrs (Air Cool)
Forging 30.47 : 1 900⁰C 3 Hrs 20 Min 870⁰C 3 Hrs 20 Min OIL 36°C 50°C 545°C 5 Hrs (Air Cool)
Specn. Min. 870⁰C 840⁰C --- --- 540⁰C
Max. 925⁰C 900⁰C --- 80⁰C 700⁰C
MECHANICAL PROPERTIES
QTC Test Specimen QTC Test UTS YS Elg RA Charpy Impact
Specimen Orientation Hardness Temp. 0.2 % Offset Test ( Charpy ) J
Location after H.T. ⁰C PSI PSI % % Temp. Requirement 1 2 3 Average

Refer annexure for testing details

Test Piece Orientation:- Longitudinal & Transverse Charpy 'V' notch
Test Piece Size :- 8.75 mm Dia, 35 mm Gauge Length 10 mm X 10 mm X 55 mm LG
Remarks : All the jobs have been visually examined and are free from bursts, laps, seams, cracks, porosity.
All the jobs have been 100% checked for MPI test and found satisfactory.

Enclosures: 1) Steel Mill TC 2) Hardness report 3) Dimensional Report 4) Testing Annexure

Note :- We hereby guarantee no weld repairs performed.
. We hereby certify that the above figures are correct as contained in the records of the company
For Heat Treatment batch traceability point, "AF-985" stamped near to Heat code.
Furnace calibration done as per AMS 2750G and meets the requirements.
Forging Method - Closed Die Forging

Ajay Joshi (HEAD-MQC, HT & NDT)

Authorised Signatory

F-MQC-10 / Rev. 00 / 01-Apr-2016

Works & Registered Office Tel : +91-02137-679819

Gat No. 163, Hissa No.1, Pune-Nagar Road, Fax : +91-02137-679820
Sanaswadi, Tal. Shirur, Pune- 412208 (INDIA) customerservice@westernindiaforgings.com
www.westernindiaforgings.com CIN : U28910PN1981PTC024155
 HARDNESS TEST REPORT

Customer:- TechnipFMC TC No: EC1650

P.O. No.:- 4500705714 Line Item: 00010 PO Date : 02.06.2023 Date : 13.06.2023
BODY FORGING, ULT PLUG VALVE 1
Item : Material : AISI 4140
ULT150 F/3 IN UNION ENDS AISI 4140
Part No.: 3257105 Rev K Heat No. : F12396
Drawing No.: DU500001271 Rev B Ambient Temp : 29°C
Die No.: 1299 Hardness Range:- 277 - 331 HBW
Qty.: 970 Nos. Test Method : Brinell Hardness Test
Vendor Sr.No.: - Equipment Used: Brinell Hardness Tester
HT Load No.: N: AF-979 QT: AF-985 Sr No.09/2021-036 | 2017/09
Reference Standard: ASTM E10 Machine Make: SAROJ | FSA
Load Applied: 3000 Kgs Calibration Agency: MTMS | MME
Cert. No.: MATRIX/CAL/2022-23/12/4205 |
Type of Penetrator: Dia 10 mm Carbide Ball
MME/CAL/63/23-24
Std Block Details: SH-2349/23 (Hardness value - 304.0 HBW) Calibrated On: 09.12.2022 | 10.02.2023
Entity Performing Test: WIF Sanaswadi Calibration Due On: 08.12.2023 | 09.08.2023
Hardness
Q03006 Rev. AC / Q03009 Rev. X Date of Test :- 04 & 05.05.2023
Procedure :-
Precise Measuring Method of HBW Impression : Type B : Hand-Held Microscope with fixed measuring lines.

Qty. Hardness in HBW

970 Nos. 285-321 HBW

Test Performed By Reviewed By Approved By :

Atul Jedhe Satish Gadgil (Sr.Manager HT) Ajay Joshi (HEAD-MQC, HT & NDT)

F-HT-10 / Rev. 00 / 01-Apr-2016

 Mechanical Test Annexure
Die No.: 1299 Material Grade: AISI 4140

Heat No.: F12396 HT Lot No. : AF-985

Heat Code: NSN TC No. : EC1650

TENSILE TEST

QTC Test QTC Hardness after UTS YS Elg RA

Specimen Test Temp. NABL Lab Sample
Specimen H.T. 0.2 % Offset
Orientation (⁰C) Report No. No.
Location HBW KSI KSI % %

0.5" below
L 321, 321 Ambient B-23-629-P 1 148.39 127.53 17.66 60.58
HT Surface

277 - 331 Spec. Min. 120.00 100.00 16.00 35.00

IMPACT TEST

QTC Test
Specimen Requirement Test Temp. NABL Lab Sample
Specimen 1 2 3 Average
Orientation (⁰C) Report No. No.
Location
Avg. - 42 J Min
58 50 64 57.33
Single - 32 J Min
LE - 0.51 mm Min -29°C B-23-630-P 0.96 0.88 1.00 0.95

%Shear - Report 50 40 55 48.33

L
Avg. - 27 J Min
50 44 34 42.67
Single - 20 J Min

LE - Report -40°C B-23-631-P 0.75 0.68 0.54 0.66

%Shear - Report 40 35 25 33.33

0.5" below
Avg. - 28 J Min 1
HT Surface 34 36 44 38.00
Single - 18.7 J Min

LE - Report -29°C B-23-632-P 0.52 0.54 0.60 0.55

%Shear - Report 25 30 35 30.00

T
Avg. - 20 J Min
26 34 28 29.33
Single - 14 J Min

LE - Report -40°C B-23-633-P 0.37 0.46 0.39 0.41

%Shear - Report 20 25 20 21.67

Ajay Joshi (HEAD-MQC, HT & NDT)

Authorised Signatory
 CERTIFICATE OF COMPLIANCE
Customer : TechnipFMC TC No.: EC1650
Date: 13.06.2023
Die No. : 1299 Heat Code : NSN
PO No : 4500705714 Line Item No : 00010
Offer Qty. : 970 Nos.
Part No/ Rev : 3257105 Rev K Drg No / Rev : DU500001271 Rev B
BODY FORGING, ULT PLUG VALVE
Part Name : Serial No. : -
1 ULT150 F/3 IN UNION ENDS AISI
4140

I. Material
A. Material Type : AISI 4140
B. Material Spec/ Rev. : As per Spec no : M25070 Rev No. F (Date:16.07.2021)
C. Material Test Report No : Mill Heat No : F12396

II. Dimensional
A. AQL : AS PER QUALITY PLAN B. Sample Size : 8 Nos.

III. Secondary Process : Heat Treatment

A. Process Name : Normalised
Heat Lot No. : AF-979 Process Spec : Q00025 Rev S

B. Process Name : QT
Heat Lot No. : AF-985 Process Spec : Q00025 Rev S

IV. NDE
A. Process Name : MPI

Certificate No : NA Process Spec : NA

B. Process Name : UT
Certificate No : NA Process Spec : NA

This is certified that subjected material is manufactured from material mentioned above &
verified by us as per written sample size & found conforming to requirements.
For Heat Treatment batch traceability point, "AF-985" stamped near to Heat code.
Sign with Stamp

Ajay Joshi (HEAD-MQC, HT & NDT)