MATERIAL TEST CERTIFICATE

AS PER STD EN 10204 TYPE 3.1

Customer : TechnipFMC TC No. : EC0176 Date : 22.05.2022

Invoice No.:WIF/EX/22-23/ Date :
P.O. No.: 4500620576 Line Item: 0020 PO Date : 13.12.2021 Spec. Ref.: M25070 Rev. : F (Date:16.07.2021)

Die No. Description Part No. Condition Forging Qty Material Melting Practice
Drg. No. 502 PSL Level Ratio Sr.No. Mill
BODY FORGING, ULT PLUG F/
1299 VALVE 1 ULT150 F/3 IN 3257105 Rev K NQT/SB 24.25 88 Nos. AISI 4140 BF-EOF-LRF-VD-CCM
UNION ENDS AISI 4140
- JSW STEEL LIMITED
Heat Code: LPC DU500001271 Rev B
CHEMICAL COMPOSITION ( % )
Heat No :- C Mn Si S P Cr Mo V Ni Grain Size
C63775 0.41 0.90 0.25 0.008 0.011 1.02 0.22 0.005 0.22 7
Specn. Min. 0.38 0.75 0.15 - - 0.80 0.15 - - 6
Max. 0.43 1.00 0.35 0.025 0.025 1.10 0.25 0.30 1.00 -
HEAT TREATMENT
Procedure :- Q00025 Rev S

Heat Treatment Furnace :- Continous Type Furnace (CHTF) Temperature Monitoring Method:- Side Thermocouples in the Working Zone ( Method A)

HT Load No. of N :- CW-851 HT Batch No. of Q&T:- CW-853 Qty :- 88 Nos.

Test Piece Heat Treatment :- Along with job QTC location:- Sacrificial QTC Size- Actual Part
Hot Working Normalising Time Hardening Time Quench Quench Bath Temp. 1st Temper Time
Ratio Temp. Hrs. Temp. Hrs. Media Start End Temp. Hrs.
QTC 24.25 900⁰C 2.40 870⁰C 2.40 OIL 26°C 44°C 610°C 4 (Air Cool)
Forging 24.25 900⁰C 2.40 870⁰C 2.40 OIL 26°C 44°C 610°C 4 (Air Cool)
Specn. Min. 870⁰C 840⁰C --- --- 540⁰C
Max. 925⁰C 900⁰C --- 80⁰C 700⁰C
MECHANICAL PROPERTIES
QTC Test Specimen QTC Test UTS YS Elg RA Charpy Impact
Specimen Orientation Hardness Temp. 0.2 % Offset Test ( Charpy ) J
Location after H.T. ⁰C PSI PSI % % Temp. Requirement 1 2 3 Average

Refer annexure for testing details

Test Piece Orientation:- Longitudinal & Transverse Charpy 'V' notch
Test Piece Size :- 8.75 mm Dia, 35 mm Gauge Length 10 mm X 10 mm X 55 mm LG
Remarks : All the jobs have been visually examined and are free from bursts, laps, seams, cracks, porosity.
All the jobs have been 100% checked for MPI test and found satisfactory.

Enclosures: 1) Steel Mill TC 2) Hardness report 3) Dimensional Report 4) Testing Annexure

Note :- We hereby guarantee no weld repairs performed.
. We hereby certify that the above figures are correct as contained in the records of the company
For Heat Treatment batch traceability point, "CW-853" stamped near to Heat code.
Furnace calibration done as per AMS 2750F and meets the requirements.

Mr. Ajay Joshi (HEAD-MQC, HT & NDT)

Authorised Signatory

F-MQC-10 / Rev. 00 / 01-Apr-2016

Works & Registered Office Tel : +91-02137-679819

Gat No. 163, Hissa No.1, Pune-Nagar Road, Fax : +91-02137-679820
Sanaswadi, Tal. Shirur, Pune- 412208 (INDIA) customerservice@westernindiaforgings.com
www.westernindiaforgings.com CIN : U28910PN1981PTC024155
 HARDNESS TEST REPORT

Customer:- TechnipFMC TC No: EC0176

P.O. No.:- 4500620576 Line Item: 0020 PO Date : 13.12.2021 Date : 22.05.2022
BODY FORGING, ULT PLUG VALVE 1 ULT150 F/3
Item : IN UNION ENDS AISI 4140 Material : AISI 4140

Part No.: 3257105 Rev K Heat No. : C63775

Drawing No.: DU500001271 Rev B Ambient Temp : 25°C
Die No.: 1299 Hardness Range:- 277 - 331 HBW
Qty.: 88 Nos. Test Method : Brinell Hardness Test
Vendor Sr.No.: - Equipment Used: Brinell Hardness Tester
HT Load No.: N: CW-851 QT: CW-853 Sr No.2017/09 & 09/2021-036
Reference Standard: ASTM E10 Machine Make: FSA & SAROJ
Load Applied: 3000 Kgs Calibration Agency: MM Engineers & MTMS
Cert. No.: MME/CAL/260/21-22 (FSA)
Type of Penetrator: Dia 10 mm Carbide Ball
Cert. No.: MATRIX/CAL/2021-2022/12/2040 (SAROJ)
Std Block Details: SH-249 (Hardness value - 287.4 HBW) Calibrated On: 14.08.2021(FSA) & 10.12.2021(SAROJ)
Entity Performing Test: WIF Sanaswadi Calibrated Due On:13.02.2022(FSA) & 09.12.2022(SAROJ)
Hardness
Q03006 Rev. AC / Q03009 Rev. X Date of Test :- 07.01.2022
Procedure :-
Precise Measuring Method of HBW Impression : Type B : Hand-Held Microscope with fixed measuring lines.

Qty. Hardness in HBW

88 Nos. 285-321 HBW

Test Performed By Reviewed By Approved By :

Atul Jedhe Satish Gadgil (Sr.Manager HT) Mr. Ajay Joshi (HEAD-MQC, HT & NDT)

F-HT-10 / Rev. 00 / 01-Apr-2016

 Mechanical Test Annexure
Die No.: 1299 Material Grade: AISI 4140

Heat No.: C63775 HT Lot No. : CW-853

Heat Code: LPC TC No. : EC0176

TENSILE TEST

QTC Test QTC Hardness after UTS YS Elg RA

Specimen Test Temp. NABL Lab Sample
Specimen H.T. 0.2 % Offset
Orientation (⁰C) Report No. No.
Location HBW KSI KSI % %

0.5" below HT
L 302, 311 Ambient J-22-848-P 1 155.65 137.081 20.06 61.81
Surface

277 - 331 Spec. Min. 120.00 100.00 16.00 35.00

IMPACT TEST

QTC Test
Specimen Requirement Test Temp. NABL Lab Sample
Specimen 1 2 3 Average
Orientation (⁰C) Report No. No.
Location
Avg. - 42 J Min
60 66 62 62.67
Single - 32 J Min
LE - 0.51 mm Min -29°C 0.77 0.83 0.79 0.80
%Shear - Report 50 55 55 53.33
L
Avg. - 27 J Min
48 58 60 55.33
Single - 20 J Min
LE - Report -40°C 0.63 0.75 0.77 0.72

%Shear - Report 40 50 50 46.67

0.5" below
Avg. - 28 J Min J-22-848-P 1
HT Surface 28 28 32 29.33
Single - 18.7 J Min
-29°C
LE - Report 0.38 0.39 0.43 0.40

%Shear - Report 20 20 20 20.00

T
Avg. - 20 J Min
24 20 24 22.67
Single - 14 J Min
LE - Report -40°C 0.34 0.30 0.35 0.33

%Shear - Report 15 10 15 13.33

Mr. Ajay Joshi (HEAD-MQC, HT & NDT)

Authorised Signatory
 Certificate of Compliance

Customer : TechnipFMC TC No.: EC0176

Date: 22.05.2022
Die No. : 1299 Heat Code : LPC
PO No : 4500620576 Line Item No : 0020
Offer Qty. : 88 Nos.
Part No/ Rev : 3257105 Rev K Drg No / Rev : DU500001271 Rev B
BODY FORGING, ULT PLUG VALVE
Part Name : Serial No. : -
1 ULT150 F/3 IN UNION ENDS AISI
4140

I. Material
A. Material Type : AISI 4140
B. Material Spec/ Rev. : As per Spec no : M25070 Rev No. F (Date:16.07.2021)
C. Material Test Report No : Mill Heat No : C63775

II. Dimensional
A. AQL : AS PER QUALITY PLAN B. Sample Size : 13 Nos.

III. Secondary Process : Heat Treatment

A. Process Name : Normalised
Heat Lot No. : CW-851 Process Spec : Q00025 Rev S

B. Process Name : QT
Heat Lot No. : CW-853 Process Spec : Q00025 Rev S

IV. NDE
A. Process Name : MPI

Certificate No : NA Process Spec : NA

B. Process Name : UT
Certificate No : NA Process Spec : NA

This is certified that subjected material is manufactured from material mentioned above &
verified by us as per written sample size & found conforming to requirements.
For Heat Treatment batch traceability point, "CW-853" stamped near to Heat code.
Sign with Stamp

Mr. Ajay Joshi (HEAD-MQC, HT & NDT)