Fatigue of Materials
Fatigue of Materials
Written by a leading researcher in the field, this revised and updated second edition
of a highly successful book provides an authoritative, comprehensive and unified
treatment of the mechanics and micromechanisms of fatigue in metals, nonmetals
and composites.
The author discusses the principles of cyclic deformation, crack initiation and
crack growth by fatigue, covering both microscopic and continuum aspects. The
book begins with discussions of cyclic deformation and fatigue crack initiation in
monocrystalline and polycrystalline ductile alloys as well as in brittle, semi-
crystalline and noncrystalline solids. Total-life and damage-tolerant approaches are
then introduced in metals, nonmetals and composites along with such advanced
topics as multiaxial fatigue, contact fatigue, variable amplitude fatigue, creep-
fatigue, and environmentally assisted fatigue. Emphasis is placed upon scientific
concepts and mechanisms and the basic concepts are extended to many practical
cases wherever possible. The book includes an extensive bibliography and a problem
set for each chapter, together with worked-out example problems and case studies.
The book will be an important reference for students, practicing engineers and
researchers studying fracture and fatigue in materials science and engineering,
mechanical, civil, nuclear and aerospace engineering, and biomechanics.
Fatigue of Materials
SECOND EDITION
S. SURESH
Massachusetts Institute of Technology
CAMBRIDGE
UNIVERSITY PRESS
CAMBRIDGE UNIVERSITY PRESS
Cambridge, New York, Melbourne, Madrid, Cape Town, Singapore, Sao Paulo
Published in the United States of America by Cambridge University Press, New York
www.cambridge.org
Information on this title: www.cambridge.org/9780521570466
© Subra Suresh 1998
A catalogue record for this publication is available from the British Library
vn
viii Contents
Appendix 609
References 614
Author index 659
Subject index 669
Preface to the second edition
The first edition of this book was written primarily as a research monograph
for the Solid State Science Series of Cambridge University Press. Since its first
publication, however, the book has found wide readership among students and
practicing engineers as well as researchers. In view of this audience base which
evolved to be much broader than what the book was originally intended for, it
was felt that now would be an appropriate time for the preparation of an updated
and revised second edition which includes newer material, example problems, case
studies and exercises. In order to have the greatestflexibilityin the incorporation of
these new items in the book, it was also decided to publish the second edition as a
'stand-alone' book of Cambridge University Press, rather than as a research mono-
graph of the Solid State Science Series.
In writing the second edition, I have adhered to the objectives which are stated in
the preface to the first edition. In order to structure the expanded scope coherently,
the book is organized in the following manner. The introduction to the subject of
fatigue, the overall scope of the book and background information on some of the
necessary fundamentals are provided in the first chapter. The book is then divided
into four parts. Cyclic deformation and fatigue crack nucleation in ductile, brittle
and semi-crystalline or noncrystalline solids are given extensive coverage in Part
One. This is followed by discussions of stress-based and strain-based approaches
to fatigue in Part Two. Principles of fracture mechanics and the characteristics of
fatigue crack growth in ductile, brittle and semi-crystalline or noncrystalline solids
are then taken up in separate chapters in Part Three. Part Four comprises advanced
topics where, in addition to separate chapters on crack growth retardation under
constant and variable amplitude fatigue, small cracks, and environmental interac-
tions, a new chapter on contact fatigue is included. In each chapter, updated material
and references, as well as case studies and worked-out and practice problems are
included.
Since the publication of the first edition, numerous students, research colleagues
and engineers from many countries have provided valuable feedback, constructive
criticisms and suggestions. The first edition was translated into the Chinese language
in 1993 under the sponsorship of the Chinese Academy of Sciences. Z. G. Wang and
his colleagues of the State Key Laboratory for Fracture and Fatigue in Shenyang
deserve special thanks for diligently going over the entire manuscript of the first
edition and offering many helpful suggestions. Every attempt has been made to
respond to these comments in the second edition, while trying to adhere to the
main objectives of writing this book. The first edition as well as drafts of the second
xvii
xviii Preface to the second edition
edition were also used by the author as text material for subjects taught for graduate
students at the Massachusetts Institute of Technology, Harvard University and
Brown University.
I am thankful to many individuals who supplied me with information and original
micrographs for the second edition. They include H. Azimi, U. Essmann, W.
Milligan, T. Nakamura, A. Pineau, R.O. Ritchie and D.F. Socie. A number of
colleagues, especially J. Dominguez, T.C. Lindley, F.A. McClintock, T. Nicholas
and L. Pruitt, kindly read drafts of some chapters and offered helpful suggestions.
During the preparation of this second edition, I have had the good fortune to
interact extensively with four colleagues, A.E. Giannakopoulos, L.P. Kubin, H.
Mughrabi and C.F. Shih, who read many sections of the book, and provided helpful
criticisms, suggestions on key references, solutions to some practice problems and
advice on improvement of presentation. I am most grateful to them for their scho-
larly feedback and strong interest in this book.
I wish to thank S. Capelin of the Cambridge University Press for his strong and
continued support of this book project and for giving me considerable flexibility in
the preparation of the manuscript, and to M. Patterson for her efficient copy-editing
of the manuscript. K. Greene, D. LaBonte, G. LaBonte, C.-T. Lin and L. Ward
deserve special mention for their cheerful help with the preparation of figures and
references.
My research work on fatigue has been supported over the years by the U.S.
Department of Energy, Office of Naval Research, Air Force Office of Scientific
Research, and National Science Foundation. This support is gratefully acknowl-
edged. I thank the Department of Materials Science and Engineering at the
Massachusetts Institute of Technology for giving me the flexibility and the time
for the preparation of this second edition through the award of the R.P. Simmons
Endowed Professorship. In addition, I thank the Swedish Research Council for
Engineering Sciences for awarding me the Swedish National Chair in Mechanical
Engineering for the period 1996-98 at the Royal Institute of Technology (Kungl
Tekniska Hogskolan, KTH), Stockholm, where a significant portion of the new
material for the second edition was written. I thank the colleagues in the
Departments of Solid Mechanics and Materials Science and Engineering at KTH
for their hospitality during my stay in Stockholm.
Finally, I express my deepest gratitude to my wife Mary and our daughters Nina
and Meera for all their patience and support during the time I spent writing this
book. Without their care, affection and tolerance, this project could not have been
completed.
S. Suresh
Preface to the first edition
The topics addressed in this book are developed to the extent that the presentation
is sufficiently self-explanatory. The scope of the book is spelled out in Chapter 1.
Some background information on the relevant topics is also provided in the first
chapter to set the scene for later developments. This book could serve as a state-of-
the-art reference guide to researchers interested in the fatigue behavior of materials
and as a text for a graduate course on fatigue. Sections of the book could also be
used for an introductory course on fatigue for practicing engineers. Senior under-
graduate and graduate students taking courses on mechanical behavior of materials
or fracture mechanics may find this monograph useful as a supplement to their
textbooks.
xix
xx Preface to the first edition
I express my profound gratitude to my wife Mary for her support, devotion and
patience throughout this project. The company of our little daughters Nina and
Meera provided joyful breaks from long hours of concentrated work.
Finally, I wish to dedicate this book to my mother Lakshmi on the occasion of her
sixtieth birthday. Her countless sacrifices for the sake of my education are gratefully
acknowledged.
S. Suresh
CHAPTER 1
The word fatigue originated from the Latin expression fatigare which
means 'to tire'. Although commonly associated with physical and mental weariness
in people, the word fatigue has also become a widely accepted terminology in engi-
neering vocabulary for the damage and failure of materials under cyclic loads. A
descriptive definition of fatigue is found in the report entitled General Principles for
Fatigue Testing of Metals which was published in 1964 by the International
Organization for Standardization in Geneva. In this report, fatigue is defined as a
term which 'applies to changes in properties which can occur in a metallic material
due to the repeated application of stresses or strains, although usually this term
applies specially to those changes which lead to cracking or failure'. This description
is also generally valid for the fatigue of nonmetallic materials.
Fatigue failures occur in many different forms. Mere fluctuations in externally
applied stresses or strains result in mechanical fatigue. Cyclic loads acting in associa-
tion with high temperatures cause creep-fatigue; when the temperature of the cycli-
cally loaded component also fluctuates, thermomechanical fatigue (i.e. a combination
of thermal and mechanical fatigue) is induced. Recurring loads imposed in the pre-
sence of a chemically aggressive or embrittling environment give rise to corrosion
fatigue. The repeated application of loads in conjunction with sliding and rolling
contact between materials produces sliding contact fatigue and rolling contact fati-
gue, respectively, while fretting fatigue occurs as a result of pulsating stresses along
with oscillatory relative motion and frictional sliding between surfaces. The majority
of failures in machinery and structural components can be attributed to one of the
above fatigue processes. Such failures generally take place under the influence of
cyclic loads whose peak values are considerably smaller than the 'safe' loads esti-
mated on the basis of static fracture analyses.f
Failing to recognize this fact was the primary cause of catastrophic accidents involving the first com-
mercial jet aircraft, the Comet. A case study of the Comet aircraft failures is provided in Section 1.1.1.
Introduction and overview
first half of the nineteenth century. Since that time, scores of scientists and engineers
have made pioneering contributions to the understanding of fatigue in a wide variety
of metallic and nonmetallic, brittle and ductile, monolithic and composite, and natural
and synthetic materials. It is not feasible to present, in a few pages, a comprehensive
survey of the historical development of these contributions to fatigue. Nevertheless, in
an attempt to highlight the salient topics of fatigue and to set the scene for the scope of
this book, an overview of major advances and of key areas in fatigue is given in this
section. The chapters to follow provide detailed discussions of various fatigue phe-
nomena along with the relevant historical backgrounds wherever appropriate.
The expression fatigue has been in use for a very long time. In the days of long
distance travel aboard sailing vessels, the straining of masts due to the frequent
hoisting of sails was referred to as fatigue. The first study of metal fatigue is believed
to have been conducted around 1829 by the German mining engineer W.A.J. Albert
(see Albert, 1838). He performed repeated load proof tests on mine-hoist chains
made of iron. One end of the chain was loaded while the chain was supported on
a 360-cm (12-ft) disc. The chain links were repeatedly subjected to bending, at a rate
of 10 bends per minute up to 100 000 bends, by a crank coupling which oscillated the
disc through an arc.
Interest in the study of fatigue began to expand with the increasing use of ferrous
structures, particularly bridges in railway systems. The first detailed research effort
into metal fatigue was initiated in 1842 following the railway accident near Versailles
in France which resulted in the loss of human lives (The Times of London, May 11,
1842; for a comprehensive description of this accident, see Smith, 1990). The cause of
this accident was traced to fatigue failure originating in the locomotive front axle. As
early as 1843, W.J.M. Rankine, a British railway engineer who later became famous
for his contributions to mechanical engineering, recognized the distinctive character-
istics of fatigue fractures and noted the dangers of stress concentrations in machine
components. The Institution of Mechanical Engineers in Britain also began to
explore the so-called 'crystallization theory' of fatigue. It was postulated that the
weakening of materials leading to eventual failure by fatigue was caused by the
crystallization of the underlying micro structure. In 1849, the British Government
commissioned E.A. Hodgkinson to study the fatigue of wrought and cast iron used
in railway bridges. The report of this commission (Hodgkinson, 1849) described
alternating bending experiments on beams whose midpoints were repeatedly
deflected by a rotating cam. In this time period, research on fatigue fracture was
also documented in the work of Braithwaite (1854) who employed the term fatigue
exclusively to denote the cracking of metals under repeated loading. (Braithwaite
(1854), however, credits one Mr. Field for coining this term. Poncelet (1839) is also
generally given credit for introducing the term fatigue in connection with metal
failure, although it had been used earlier in the context of other phenomena.)
A. Wohler conducted systematic investigations of fatigue failure during the period
1852-1869 in Berlin, where he established an experiment station. He observed that
1.1 Historical background and overview
the strength of steel railway axles subjected to cyclic loads was appreciably lower
than their static strength. Wohler's studies involving bending, torsion and axial
loading included fatigue tests on full-scale railway axles for the Prussian Railway
Service and on a variety of structural components used in small machines. His work
(e.g., Wohler, 1860) also led to the characterization of fatigue behavior in terms of
stress amplitude-life (S-N) curves and to the concept of fatigue 'endurance limit'.
The rotating bending machine widely used today for cyclically stressing metals is
conceptually the same as the one designed by Wohler. Although his rotating bending
apparatus had a maximum speed of only 72 revolutions per minute, one of his
fatigue test specimens was subjected to 132 250000 stress cycles without producing
fracture.
Another well known fatigue researcher of this era was W. Fairbairn who per-
formed tests on riveted wrought iron girders for the British Board of Trade; in
some cases, as many as 3100000 load cycles were applied. On the basis of his
experiments, Fairbairn (1864) concluded that the wrought iron girders subjected
to cyclic stresses with a maximum of only one-third of the ultimate strength
would fail. In 1874, the German engineer H. Gerber began developing methods
for fatigue design; his contribution included the development of methods for fatigue
life calculations for different mean levels of cyclic stresses. Similar problems were
also addressed by Goodman (1899).
The notion that the elastic limit of metals in reversed loading can be different from
that observed in monotonic deformation was popularized by Bauschinger (1886).
His work essentially identified the occurrence of cyclic softening and cyclic strain
hardening. Bauschinger also confirmed many of the results reported earlier by
Wohler. By the end of the nineteenth century, some eighty papers on fatigue had
been published in such diverse application areas as railway rolling stock axles,
crankshafts, chains, wire ropes, and marine propeller shafts (see, for example, the
survey by Mann, 1958).
Interpretations of fatigue mechanisms based on the old crystallization theory were
laid to rest by the pioneering work of Ewing & Rosenhain (1900) and Ewing &
Humfrey (1903). These researchers investigated the fatigue of Swedish iron and
published optical micrographs of cyclic damage on the specimen surface. It was
convincingly shown that slip bands developed in many grains of the polycrystalline
material. These slip bands broadened with the progression of fatigue deformation
and led to the formation of cracks; catastrophic failure of the specimen was insti-
gated by the growth of a single dominant flaw. They showed that the slip bands
intersecting the polished surface caused slip steps in the form of elevations and
depressions which we now commonly refer to as 'extrusions' and 'intrusions', respec-
tively. (The micromechanisms of fatigue damage and crack nucleation in metals
form the topics of discussion in Chapters 2-4 of this book.)
In 1910, O.H. Basquin proposed empirical laws to characterize the S-N curves of
metals. He showed that a log-log plot of the stress versus the number of fatigue
Introduction and overview
cycles resulted in a linear relationship over a large range of stress. Significant con-
tributions to the early understanding of cyclic hardening and softening in metals
were also made by Bairstow (1910). Using multiple-step cyclic tests and hysteresis
loop measurements, Bairstow presented results on the hysteresis of deformation and
on its relation to fatigue failure. In France, Boudouard (1911) conducted fatigue
experiments on steel bars which were subjected to vibrations by means of an electro-
magnetic apparatus similar to the one designed earlier by Guillet (1910). The effect
of heat treatments on the fatigue resistance of steels was the subject of Boudouard's
study. Other notable contributions of this time period included those of Smith
(1910), Bach (1913), Haigh (1915), Moore & Seeley (1915), Smith & Wedgwood
(1915), Ludwik (1919), Gough & Hanson (1923), Jenkin (1923), Masing (1926)
and Soderberg (1939). In 1926, a book entitled The Fatigue of Metals was published
by H.J. Gough in the United Kingdom. A year later, a book bearing the same title
was published by H.F. Moore and J.B. Kommers in the United States. By the 1920s
and 1930s, fatigue had evolved as a major field for scientific research. Investigations
in this time period also focused on corrosion fatigue of metals (Haigh, 1917;
McAdam, 1926; Gough, 1933), damage accumulation models for fatigue failure
(Palmgren, 1924; Miner, 1945), notch effects on monotonic and cyclic deformation
(e.g., Neuber, 1946), variable amplitude fatigue (Langer, 1937), and statistical the-
ories of the strength of materials (Weibull, 1939). A prolific researcher of this period
was Thum (e.g., Thum, 1939) who, along with many German colleagues, reported
experimental results on such topics as fatigue limits, stress concentration effects,
surface hardening, corrosion fatigue and residual stresses in numerous publications.
Gassner (1941) was another prominent German researcher whose studies of variable
amplitude fatigue found applications in the German aircraft industry. (A compre-
hensive survey of the contributions of German engineers and scientists to the field of
fatigue, particularly during the period 1920-1945, can be found in Schutz, 1996.)
Chapters 7 and 8 discuss the key features of these developments in the context of
total-life approaches.
The occurrence df fretting was first documented by Eden, Rose and Cunningham
(1911) who reported the formation of oxide debris between the steel grips and the
fatigue specimen that was contacted by the grips. Tomlinson (1927) performed the
first systematic experiments on fretting fatigue by inducing repeated small amplitude
rotational movement between two contacting surfaces, and introduced the term 'fret-
ting corrosion' to denote the oxidation due to this repeated contact. The deleterious
effects of fretting damage on the fatigue properties of metals, as reflected in the for-
mation of pits on the fretted surface and in the marked reduction in fatigue strength,
were reported by Warlow-Davies (1941) and McDowell (1953). Discussions of fatigue
failures arising from fretting as well as sliding and rolling are considered in Chapter 13.
The notion that plastic strains are responsible for cyclic damage was established by
Coffin (1954) and Manson (1954). Working independently on problems associated
with fatigue due to thermal and high stress amplitude loading, Coffin and Manson
1.1 Historical background and overview
spacing between adjacent striations with the rate of fatigue crack growth, first pub-
lished by Forsyth & Ryder (1960), became central to the development of various
theories for fatigue crack growth (Chapters 10 and 12) and to the analysis of fatigue
failures in engineering structures. Studies in this area by many researchers have
provided valuable information on substructural and microstructural changes respon-
sible for the cyclic hardening and softening characteristics of materials (Chapters 2
and 3) and on the role of such mechanisms in influencing the nucleation (Chapters 4-
6) and growth (Chapters 10-12) of fatigue cracks.
With the application of fracture mechanics concepts to fatigue failure, increasingly
more attention was paid to the mechanisms of subcritical crack growth. Conceptual
and quantitative models were developed to rationalize the experimentally observed
fatigue crack growth resistance of engineering materials (e.g., Laird & Smith, 1962;
McClintock, 1963; Weertman, 1966; Laird, 1967; Rice, 1967; Neumann, 1969;
Pelloux, 1969). Concomitant with this research, there was expanding interest in
understanding the processes by which the stress intensity factor range could be
altered by the very history of crack advance. An important contribution in this
direction came from the experimental results of Elber (1970, 1971) who showed
that fatigue cracks could remain closed even when subjected to cyclic tensile loads.
This result also implied that the rate of fatigue crack growth might no longer be
determined by the nominal value of stress intensity factor range, AK, but rather by
an effective value of AK which accounted for the details of fracture surface contact
in the wake of the advancing fatigue crack tip. Elber's work focused on the influence
of prior plastic deformation on crack closure during fatigue fracture. Although
Elber's conclusion about the role of crack closure in influencing fatigue crack growth
has since remained controversial, it also became evident from the studies of a num-
ber of researchers in the 1970s and early 1980s that Elber's arguments of premature
contact between the crack faces (based on the effects of prior crack tip plasticity)
represented just one mechanism associated with the phenomenon of fatigue crack
closure. From a survey of published information and on the basis of new results
obtained from their own investigations, Ritchie, Suresh & Moss (1980), Suresh,
Zamiski & Ritchie (1981), and Suresh & Ritchie (1984a) categorized the basic fea-
tures and implications of various types of crack closure and coined the expression
'plasticity-induced crack closure' for Elber's mechanism of crack face contact due to
prior plastic deformation. Further contributions to crack closure may arise from
fracture surface oxidation, viscous environments trapped within the crack walls and
stress-induced phase transformations. In addition, periodic deflections in the path of
a fatigue crack can cause reductions in the effective driving force for fatigue fracture
(Suresh, 1983a, 1985a) by partially 'shielding' the crack tip from applied stresses. A
discussion of the historical development of these concepts is presented in Chapter 14.
A significant outcome of the investigations of different types of crack shielding
processes is the realization that the rate of fatigue crack growth is not only affected
by the instantaneous value of imposed AK, but also by prior loading history and
1.1 Historical background and overview
crack size. As the mechanics of fatigue fracture become dependent on the geome-
trical conditions, the similitude concept implicit in the nominal use of fracture
mechanics, namely the notion that cracked components of different dimensions
exhibit the same amount of crack growth when subjected to the same value of
AK, is no longer applicable. This breakdown of the similitude concept is further
accentuated by the experimental observations that small fatigue flaws (typically
smaller than several millimeters in length and amenable to be characterized in
terms of linear elastic fracture mechanics) often exhibit growth rates which are
significantly faster than those of longer flaws (typically tens of millimeters in length),
when subjected to identical values of far-field AK. Furthermore, fatigue flaws of
dimensions comparable to or smaller than the characteristic microstructural size
scale often exhibit rates of crack growth which diminish with an increase in crack
length. Such crack growth cannot be satisfactorily analyzed in terms of available
theories of fracture mechanics. This so-called 'short crack problem', apparently first
identified by Pearson (1975), most severely affects the development of design meth-
odology for large structural components on the basis of experimental data gathered
from smaller-sized laboratory test specimens. It is, therefore, not surprising to note
that a significant fraction of research effort since the late 1970s has been devoted to
the study of crack closure phenomena and crack size effects on the progression of
fatigue fracture. Associated with this research effort are attempts to develop char-
acterization methodology for the propagation of fatigue flaws in the presence of
large-scale plastic deformation and in the vicinity of stress concentrations (see
Chapters 4, 7, 8 and 15).
Although fatigue failure under fixed amplitudes of cyclic stresses generally forms
the basis for fundamental studies, service conditions in engineering applications
invariably involve the exposure of structural components to variable amplitude
spectrum loads, corrosive environments, low or elevated temperatures and multiaxial
stress states. The development of reliable life prediction models which are capable of
handling such complex service conditions is one of the toughest challenges in fatigue
research. Although major advances have been made in these areas, the application of
fatigue concepts to practical situations often involves semi-empirical approaches.
Available models for fatigue involving conditions of multiaxial stress conditions,
complex load spectra and detrimental environments are discussed in Chapters 3, 7,
8, 10 and 16.
The majority of fatigue research reported in the open literature pertains to metallic
materials. There has, however, been a surge in interest aimed at nonmetallic materials
and composites which offer the potential for mechanical, thermal and environmental
performance hitherto unobtainable in conventional metals. This growing interest has
also generated a corresponding increase in research into the fatigue behavior of
advanced ceramics (e.g., Suresh, 1990a,b; Roebben et ah, 1996), polymers (e.g.,
Hertzberg & Manson, 1980; Hertzberg, 1995), and their composites. While the exis-
tence of cyclic slip has traditionally been considered a necessary condition for the
Introduction and overview
There are several basic requirements for the optimum performance of a passenger jet aircraft. Firstly, it
must travel as fast as possible for optimizing such factors as fuel efficiency, number of flights per unit
time period, and return on capital expenses. Secondly, it must fly below the speed of sound in order to
avoid a precipitous rise in the specific energy consumption, which is related to the ratio of thrust to
weight or to the ratio of drag to lift. Thirdly, the colder the air through which the aircraft flies, the
greater the efficiency of the jet engine. Fourthly, an aircraft should notflyat an altitude higher than what
is necessary because flying through rarefied atmosphere requires oversized wings. For passenger jet
aircraft, the first two requirements suggest a maximum cruising speed typically in the neighborhood
of 90% of the speed of sound or Mach 0.9, and the last two requirements suggest an optimum altitude of
10000-12000 m (Tennekes, 1996).
1.1 Historical background and overview
and thunderstorms are rare so that meteorological conditions do not impede flight
schedules during cruising. The colder outside air at such altitudes also enhances the
efficiency of the jet engines as the difference between the intake temperature and the
combustion temperature is raised.
A particularly important issue for high altitude flights was the design of the cabin
wherein the temperature and pressure had to be at near-ground levels for the comfort of
the passengers and the crew. The aircraft fuselage would have to be repeatedly stressed
from no pressure differential between the inside and the outside whilst on the ground to a
large pressure difference between the inside passenger cabin and the rarefied atmosphere
outside during cruising. The fuselage, therefore, had to be capable of withstanding high
stresses arising from cabin pressurization during such high altitude flights in thin air. It
would turn out that the fatigue stress cycles induced on the metal skin of the fuselage by
the repeated pressurization and depressurization of the cabin during each flight
contributed to the catastrophic fracture in several Comet airplanes (e.g., Dempster, 1959;
Petroski, 1996).
On the first anniversary of commercial jet aircraft operation, May 2, 1953, a de
Havilland Comet airplane disintegrated in mid-air soon after take-off from the airport in
Calcutta, India. The crash occurred during a heavy tropical thunderstorm. The official
organization investigating the crash concluded that the accident was the result of some
form of structural fracture, possibly arising from higher forces imposed on the airframe
by the stormy weather, or from the overcompensation by the cockpit crew in trying to
control the plane in response to such forces. Consequently, the design of the aircraft
structure was not viewed as a cause for concern.
On January 10, 1954, another Comet aircraft exploded at an altitude of 8230 m
(27 000 ft) in the vicinity of Elba Island in the Mediterranean Sea, after taking off from
Rome in good weather. Once again, no flaws in design were identified, and the aircraft
was placed back in service only weeks after this second crash.
The third accident took place soon afterwards on April 8, 1954, when a Comet
exploded in mid-air upon departure from Rome, after a brief stopover during a flight
between London and Cairo. The wreckage from the crash fell in deep sea water and could
not be recovered. This led investigators from the Royal Aircraft Establishment (RAE),
Farnborough, England, to renew efforts to recover pieces from the second crash over
Elba. Evidence began to emerge indicating that the tail section was intact from the Elba
crash, and that the pressurized cabin section had torn apart before fire broke out.
In order to probe into the origin of cabin explosion, RAE engineers retired a Comet
airplane from service and subjected its cabin to alternate pressurization and
depressurization, to about 57kPa (8.25 psi) over atmospheric pressure, by repeatedly
pumping water into it and then removing it. During such simulated cabin pressurization,
the wings of the aircraft were also stressed by hydraulic jacks to mimic wing loading
during typical flight conditions. After about 3000 pressurization cycles, a fatigue crack
originating in a corner of a cabin window advanced until the metal skin was pierced
through. Figure 1.1 schematically shows the location of cracks in a failed Comet airplane.
The Comet, being the first commercial jetliner, was designed and built at a time when
the role of fatigue in deteriorating the mechanical integrity of airframe components was
not appreciated, and when subcritical fatigue crack growth had not evolved into a topic
10 Introduction and overview
frame 26
peeling off failure
direction of propagation
of main cracks
signs of fatigue
in skin at this corner
reinforcing
plates
Fig. 1.1. Schematic diagram illustrating the location of fatigue cracks in a failed Comet
airplane. (After Petroski, 1996.)
of extensive research. It was assumed that the possibility of one fatigue cycle per flight,
due to cabin pressurization upon take-off and depressurization during landing, would not
be significant enough to advance any flaws in the fuselage to catastrophic proportions.
The cabin walls were designed to contain a pressure of 138 kPa (20psi), two and a half
times the service requirements. As an added demonstration of safety, the passenger cabin
of each Comet was pressurized once to 114 kPa (16.5 psi) in a proof test, before the plane
was placed in service. The investigative report of the Court of Inquiry into the Comet
failures noted that the de Havilland designers believed '... that a cabin (which) would
1.2 Different approaches to fatigue 11
survive undamaged a test to double its working pressure ... would not fail in service under
the action of fatigue...'. This notion was proven erroneous, at a significant cost to de
Havilland and to the British commerical aircraft industry.
The RAE tests revealed that the cabin failures in the first three Comet accidents were
due to fatigue cracking which was aided by stress elevation at the rivet holes located near
the window openings of the passenger cabin. In subsequent designs of the new Comet 4
models, which facilitated trans-Atlantic commercial jet travel for the first time, the
window sections were replaced with a new reinforced panel which had much greater
resistance to fatigue failure.
No aircraft has contributed more to safety in the jet age than the Comet. The lessons it
taught the world of aeronautics live in every jet airliner flying today.
D.D. Dempster, 1959, in The Tale of the Comet
crack initiation
and early growth low-cycle
fatigue test
specimen
fatigue crack
growth test
specimen
plastic
zone
Fig. 1.2. Schematic diagram illustrating the various stages of fatigue in an engineering
component and the approaches used to estimate the fatigue life. (After Coffin, 1979.)
crack growth life (see Chapters 7, 8, 10 and 14-16). This intrinsically conservative
approach to fatigue has been widely used in fatigue-critical applications where cat-
astrophic failures will result in the loss of human lives; examples include the aero-
space and nuclear industries.
to the predicted life for the entire population of the same component) is considered to be
utilized. The individual component is retired from service when there is a specific reason
or cause for removal from service, such as the existence of aflawof a certain (maximum)
allowable or detectable size. This system replaced classical low-cycle fatigue approaches
where an entire population of components of a certain type were retired, regardless of the
condition, when a pre-determined time or number of cycles was expended.
Analyses of crack growth and damage tolerance were carried out to identify which, if
any, components were candidates for RFC. Subsequently, a list of components and
combinations of inspection sizes and intervals were identified.! The F100 engine, for
which the RFC program has initially been implemented, is currently in service in the
twin-engine F-15 military aircraft built by the McDonnell Douglas Corporation and in
the single-engine F-16 fighter aircraft built by the General Dynamics Corporation. There
are over 3200 such engines in the operational inventory of the US Air Force. A total of
twenty-three components used in such parts as fan, compressor and low pressure turbine
rotors are being managed under this philosophy. The F100 engine overhaul manuals have
been revised such that the RFC procedure replaces the classical time to retirement
guidelines.
There were several developments for damage tolerance analysis and maintenance
which evolved from the RFC program. One such development is the refinement of a
nondestructive inspection method, based on eddy current monitoring, which is now
commonly used under the RFC program management. Another outcome of this program
is a cryogenic spin pit test for some titanium alloy discs. In this procedure, the component
is spun at a low temperature where the fracture resistance drops. If the disc does not burst
during the spin and safe operation is guaranteed above a certain 'inspection' size, the disc
is placed back in service until the next inspection. It was also demonstrated that if cracks
below the inspection size were to be present, the cryogenic spin pit test would not further
extend these cracks or cause the damage zone dimensions at the crack tip to be altered.
Whereas RFC was implemented on an F100 engine which was already designed and built,
improvements to damage-tolerant design were implemented by another effort termed the
ENgine Structural Integrity Program (ENSIP). Under ENSIP (Nicholas, Laflen, &
VanStone, 1986; Cowles, 1988), all critical structural components in an engine had to be
designed such that they could be inspected and, based on the inspection flaw size, could
be flown safely until the next inspection. Thus, all components became, by definition,
Candidates for RFC. Since the inception of such damage tolerance procedures in the
design Stage, failure incidents due to low-cycle fatigue have been essentially eliminated
from the US Air Force jet engine inventory.
The economic implications of such changes in failure control philosophy are also
substantial. Initial estimates by the US Air Force reveal that, over the time period 1986-
2005, the (life cycle) cost savings realized from the implementation of the RFC
methodology to the F100 engines alone will amount to nearly $1 billion. Additional
savings, amounting to as much as $655 million, are projected over this time period as a
consequence of reductions in labor and fuel costs arising from the extension of maintenance
intervals for the upgraded F100 core engines.
All of the components which were analyzed did not meet the criteria for RFC; the ones which failed the
criteria are still being retired after their design life, predicated upon low-cycle fatigue estimates, is
expended.
1.3 The need for a mechanistic basis 17
(1) The size scale over which permanent damage occurs at the tip of a fatigue
crack is generally comparable to the characteristic micro structural dimen-
sion of the material, even if the component dimensions and the crack size are
orders of magnitude larger than the scale of the microstructure.
(2) The total life and fracture mechanics approaches provide methods for char-
acterizing the resistance of the material to crack initiation and growth under
cyclic loads. However, these concepts alone cannot offer a quantitative
description of the intrinsic resistance of the material to fatigue. This infor-
mation can be obtained only if there exists a thorough understanding of the
' The 1985 crash of a Japan Airlines Boeing 747 due to a catastrophic fatigue failure of the rear pressure
bulkhead and the resulting loss of 520 human lives is a case in point. A failure analysis of this accident is
presented in Chapter 10.
18 Introduction and overview
coordinate system shown in Fig. 1.3, the stress components at a point are contained
in the matrix
(1.1)
°yy
°zz,
yz
where i,j = 1, 2, 3, and ay is the ith component of the force per unit area on a plane
whose outward normal points toward the positive Xj direction; X\ = x, x2 = y, and
x3 = z. Each infinitesimal volume element in the body must be in mechanical equili-
brium. Since there can be no net torque on the element, o^ = a^. Similarly, no net
force can act on the element, so that
i = 1,2,3, (1.2)
dx2
where bt is the ith component of the body force per unit volume. In the absence of
body forces, Eq. 1.2 can be expressed as
— = 0, (1.3)
where summation over j is implied. Equations 1.2 and 1.3 are known as the equili-
brium equations.
Under the influence of applied forces, let ut be the components of displacement at
a point in the body. The components of infinitesimal strain are defined as
(1.4)
2
When i ^j in this equation, the shear strains are obtained. However, it is impor-
tant to note that, for / ^y, Eq. 1.4 provides only one-half of the shear strains that are
commonly denned in engineering where y^ = 2eiJ. In Eq. 1.4, six components of
small strain, e^, have been expressed in terms of three components of the displace-
20 Introduction and overview
ment. This implies that the strains must be interrelated. For the strain components in
the x\-x2 plane,
du\ du2 1 /3wi du2
dXi dx2 2 \dx2 dxi
From Eqs. 1.5, one finds that
for deformation on the xx-x2 plane. Equation 1.6 is one of the so-called compatibility
equations.
A state of plane stress or plane strain is characterized by the conditions
9( )/3JC 3 = 0 and a 13 = a23 = 0, with xx and x2 taken as independent variables.
For plane stress, the stress-strain relationships (to be discussed in the next subsec-
tion) are used along with the additional condition that <r33 = 0. Similarly, for plane
strain, the stress-strain relationships are applied with e33 = 0. An anti-plane state is
characterized by the conditions that on = G22 = a 33 = a 12 = 0.
Standard procedures of coordinate transformation (see, for example, Malvern,
1969) are used to derive the equilibrium and compatibility equations and strain-
displacement relationships for the cylindrical coordinate system from the results
discussed above for the cartesian reference system, Eqs. 1.3 and 1.6. These results
for the cylindrical coordinate reference are presented in Section 9.3.2.
The equilibrium conditions are fulfilled automatically if the stresses are expressed
in terms of the so-called Airy stress function x, which is defined by the relationships
where Cijki are the elastic constants which, for isotropic material response, are
Cijki = k&ijhi + G(8ik8ji + 8u8jk). (1.10)
1.4 Continuum mechanics 21
X is known as the Lame constant and G is the shear modulus. 8{j is the Kronecker
delta with the property that 8tj = 0 for / / y and that 8tj — 1 for / =j. The isotropic
elastic constants defined by Young's modulus E and Poisson's ratio v are related to
G and k by the expressions
Young's modulus E is the ratio of the axial stress to the axial strain, whereas
Poisson's ratio v represents the ratio of transverse contraction to (axial) elongation
in simple tension. The strains can be related to the stresses in terms of the elastic
constants,
[ K + >L
1
r M
fe ( + <T33)],
[ K + ) ]
When the volume element shown in Fig. 1.3 deforms reversibly by an infinitesimal
strain increment de^, the stresses do work on the element by the amount
Aw = (Jijdtij = Cijkl€kid€ij. (1.13)
73 =
The coefficients Ix, I2 and 73 are independent of the orientation of the coordinate
system chosen to describe the stress components. These coefficients are termed stress
22 Introduction and overview
invariants because the principal stresses are physical quantities at the point in the
solid under consideration. Any combination of these stress invariants also results in
an entity which is an invariant.
The normal mean stress or the hydrostatic stress, aH, is defined as
These deviatoric stress components, unlike the hydrostatic stress, bring about a
change of shape in the body and influence the plastic deformation. Analogous to
the stress invariants 71? I2 and 73, a new set of scalar invariants, / 1? J2 and J$, based on
the principal components of the deviatoric stress tensor, s\, s2 and s$, can be defined:
Jx = ou - Ix = 0,
J2 = 2S(JSiJ =
2^1 +
^2 ^ S
^ '
J
2 = 3 isijsjkSki) = S\ ^2^3 • (1-20)
(2) A hardening rule, which prescribes the work hardening of the material and
the change in yield condition with the progression of plastic deformation.
(3) A flow rule, which relates the increments of plastic deformation or the
components of plastic rate-of-deformation to the stress components.
Plastic deformation is determined by a yield condition which is a function/(cr^) of
the current stress state. In most cases, the associative flow rule is used which assumes
that the plastic strain increments are proportional to a function/(o^-) which depends
on the current plastic state of the material. All rate-independent plasticity theories
postulate that the material response is elastic for fiery) < 0- Elastic unloading occurs
from a plastic state when fiery) = 0 and (df /'dcry)dcry < 0, where day is the stress
increment. Plastic deformation occurs when fiery) = 0 and idf/der^doy > 0. If the
material deformation is isotropic, the yield function is an isotropic function of stress
such that/((jzy) = / ( / ! , 72, 73) =/(o r i, er2, a3)- Since the deformation of metallic mate-
rials is insensitive to moderate levels of hydrostatic stress <JH, the yield function
depends only on the deviatoric stress Sy. If the yield response of the material is the
same in tension and compression, i.e. if the material does not exhibit the Bauschinger
effect (Chapter 3),f(Sy) =f(—Sy). T h e n / is an even function of/ 3 .
The von Mises and Tresca yield conditions are the most widely used flow criteria
for metals. The von Mises condition states that
f = j2-k2= \sySij - k2 = 0, (1.21)
(b)
Fig. 1.4. (a) The yield surface drawn in three-dimensional principal stress space. The von Mises
and Tresca conditions for yield are represented by the right circular cylinder and the inscribed
hexagonal prism, respectively, (b) von Mises ellipse and Tresca hexagon for a state of biaxial
stress.
denotes the condition <j\ = a2 = cr^.'f The surfaces of the von Mises cylinder or the
Tresca hexagonal prism are perpendicular to the deviatoric plane or IT plane (such as
the plane ABCDEF in Fig. \A(a)), which describes the condition ox + <J2 + <r3 = 0.
In a biaxial stress state represented by the principal stress coordinates ox and cr2, the
von Mises yield condition is represented by an ellipse and the Tresca condition is
shown by the inscribed hexagon, Fig. 1.4(6). Since net work has to be expended on
the body during plastic deformation, the rate of energy dissipation is nonnegative,
such that
> 0. (1.24)
Geometrically, this condition implies that the yield surface must be convex. Thus the
yield condition requires the stress point to be on the yield surface and to be directed
outward from the surface. At a smooth point on the yield surface, Eq. 1.24 implies
that the incremental plastic strain vector de?- must be normal to the yield surface, and
that the vector denoting the incremental change in stress day must have an acute
angle with the strain vector. At a corner on the Tresca yield surface, this criterion
must be applied separately to the two surfaces intersecting the corner.
This normality of the plastic strain increment to the yield surface is reflected by the
flow rule,
' This is so because if the stress state characterized by (au <J2, cr3) lies on the yield surface, so does
fa + crH, <r2 + <rH, <T3 + <7H), where <xH is any value of the hydrostatic stress defined in Eq. 1.17.
1.4 Continuum mechanics 25
Given the representation of the flow criterion in terms of the yield surface, it is
important to know how the yield surface changes during plastic deformation. The
theory of perfectly (or ideally) plastic solids assumes that the yield function is unaf-
fected by plastic deformation. If the material exhibits increasing resistance to plastic
deformation with plastic straining, the simplest approach to handle such strain hard-
ening is to invoke the so-called isotropic hardening model. During isotropic hard-
ening, the yield surface expands uniformly, but it has a fixed shape and its center
remains fixed in stress space. The dependence of the size of the yield surface on
deformation can be determined by developing a universal stress-strain relationship
(1.26)
which relates two scalar quantities through the function h: the effective stress ae
(which measures the size of the yield surface) and the effective plastic strain incre-
ment dep. If one uses the von Mises criterion for yield,
(1.27)
The numerical constant on the right hand side of this equation is chosen such that
ae = \an\ in uniaxial loading. The effective plastic strain increment is defined as
(1.28)
where the numerical factor is chosen such that in a state of uniaxial stress crn,
dep = devn = -2de p 2 = -2de p 3 .
An alternative statement of the isotropic hardening rule is obtained from the
argument that the size of the yield surface is a function F only of the total plastic
work, such that
where the integration is carried out over the actual strain path. This condition
provides results equivalent to Eq. 1.26.
The use of isotropic hardening for tension-compression cyclic deformation in
many metallic materials does not rationalize the differences in elastic limit commonly
found between forward and reverse loading. In an attempt to account for this so-
called Bauschinger effect, an alternative hardening rule, known as kinematic hard-
ening, has been proposed. In the classical models of kinematic hardening, the yield
surface does not change its shape and size, but simply translates in stress space in the
direction of its normal. The application of isotropic hardening and various kine-
matic-type hardening rules to cyclic deformation is described in Chapter 3.
The discussions up to this point have focused on the incremental ox flow theories
of plasticity. There is also a different approach, known as the deformation or total
strain theory, which is adopted in plasticity problems mainly in view of its mathe-
matical simplicity. The deformation theory, where the total strain ezy is taken to be a
26 Introduction and overview
Creep response
u u u
r
t t t
F\ F F
1
-11 i t
0
i i t
1 t
Relaxation response
F F F
K t t t
u
1
L
u
u0 fL Tor
u
(a) (b)
Fig. 1.5. Schematic arrangement (top row), creep response (middle row) and relaxation response
(bottom row) of (a) the Maxwell element, (b) the Kelvin-Voigt element, and (c) a standard
linear model. The creep response includes loading and unloading.
The Maxwell element thus characterizes steady creep under a constant load FQ
after an initial glassy response with the displacement Fo/K, in the following manner:
M(f) = ^ +^ . (1.34)
If a displacement u(t) is suddently applied such that u{i) = 0 when / < 0 and
w(/) — u0 when ^ > 0, stress relaxation characterized by the Maxwell solid takes
the form:
F{t) = UQ. (1.35)
The ratio r = rj/JC denotes the relaxation time which is the rate of decay of the force
according to the exponential law in Eq. 1.35 after the sudden imposition of the
28 Introduction and overview
where the retardation time r is the time required for {(F0/JC) — u} to be reduced by a
factor of l/e. Equation 1.36 thus indicates that the equilibrium displacement is
approached only asymptotically.
In the standard linear model shown in Fig. 1.5(c),
ER(u + x¥u) = F + r u F, ER • r F • u(0) = ruF(0), (1.37)
where r F is a constant which denotes the time of relaxation of u under constant F,
and ru is the time of relaxation of F under constant u. With different values of the
spring constants and viscosity, different values of ER, r F and ru result, and thus the
model may be described by a constitutive equation of the form: F -\-f\F = uxu + u2u,
where/j and ut are constants. This equation typically characterizes in a qualitative
way the deformation of a cross-linked polymer.
A generalized Kelvin-Voigt model, which comprises a number of Kelvin-Voigt
elements in series, or a generalized Maxwell model, which comprises a number of
Maxwell elements in parallel, are commonly used to 'fit' the creep response of metals
and polymers with greater degrees of precision (see, for example, Malvern, 1969). An
example of the transient viscoelastic response of polymers subjected to cyclic varia-
tions in applied stress is presented in Chapter 6.
Recall that stj is the component of the deviatoric stress defined in Eq. 1.19, and that
J2 is the second invariant of the deviatoric stress, Eq. 1.20. Further extensions of this
approach, including the assumption of compressibility, have been introduced in the
literature.
Most commonly, tensile tests are carried out at different strain rates and tempera-
tures to characterize the viscoplastic creep response of materials. The results of such
tests are commonly analyzed using empirical approximations of the form:
a = o,(ec)m{tC)\ (1.40)
c c
where a is the uniaxial tensile stress, e is the viscous part of the true strain, e is the
viscous strain rate, m is the strain-rate sensitivity parameter, n is the strain hardening
exponent, and a0 is a material parameter. In steady-state creep, where the strain rate
remains roughly constant, the constitutive response is given by the so-called Norton-
Odqvist law:
4=
3
2
where crQ is the von Mises effective stress, Eq. 1.27, ay is the yield strength, ey is the
yield strain rate and nc is the power-law creep exponent.
Since creep deformation is a thermally activated process, the mechanistic origins
of the evolution of strain rate are tied to an Arrhenius-type equation,
€c = Ae-(Q/RT)^ ( 1 4 2 )
where Q is the activation energy, T is the absolute temperature and R is the universal
gas constant. Note that Eq. 1.42 essentially denotes the temperature-dependence of
viscosity t] which is implicit in Eq. 1.38.
TR = - C O S 0o = CTCOS 0 O (1.43)
The condition for the onset of plastic deformation is given by the so-called Schmid
law which states that a crystalline solidflows plastically when the resolved shear stress,
TRQ, acting along the slip direction in the slip plane reaches a critical value, rc:
a cos 0O cos Xo = a s i n x o c o s ^ o — Mo = rc. (1-44)
M is known as the Schmid factor, which has a maximum value of 0.5 corresponding
to the orientation 0O = Xo = 45°.
Fig. 1.6. A schematic diagram of a single crystal showing the orientations of the slip plane and
the slip direction.
7.5 Deformation of ductile single crystals 31
Consider the geometrical changes in the slip system as the initially cylindrical
crystal deforms plastically (Fig. 1.7). A reference gage length vector t0 along the
axis of the cylinder prior to deformation changes in both magnitude and direction
with the progression of slip. Let I be the instantaneous gage length vector at any
point during plastic deformation. It can be shown by simple geometrical arguments
that
« = «o + K R (Vn)b, (1.45)
where • denotes a dot product. In order to express I in terms of l0, consider
I • I = l0 • l0 + yll0 • n)2 (b b) + 2yRl0 . n) V b). (1.46)
Equivalently,
I2 = l02 (1 + 2yR cos 0o cos k0 + y£ cos2 0O). (1-47)
If yR is expressed in terms of the instantaneous and original gage lengths, I and £$,
respectively, and the initial orientation of the slip plane and slip direction 0O and k0,
we find that
YR
= (1.48)
In an actual tensile test on a single crystal, the ends of the crystal are gripped to the
testing machine and the gage length vectors £0 and I are confined to remain parallel
to the initial longitudinal axis of the cylinder (i.e. along the loading axis).
Consequently, the single slip displacement schematically illustrated in Fig. 1.7 is
tantamount to the rotation of both the slip plane and the slip direction toward the
tensile axis as deformation proceeds in a real experiment. The initial orientation
angles 0O and k0 will decrease with increasing plastic deformation.
The Schmid factor also relates the increment of shear strain dy& on a slip system
to the increment in longitudinal strain de. For instantaneous orientation angles 0
and k and small strain increments,
1
^ = H- = _L = (1 49)
de tR M cos 0 cos k'
When 0 = k = 45°, M = 0.5, rR = 0.5a.
The instantaneous value of resolved shear stress, rR, may be obtained by noting
that the glide plane, with the cross-sectional area ^4/cos0o, remains undistorted by
slip. Since the longitudinal axis at any point during slip is inclined at an angle k to
the slip direction,
p
xR = —cos 0o cos k = a cos 0o cos A. (1.50)
A
From Eq. 1.45, we note that
cos A = l-b/i= yj\ - ( £ 0 s i n V ^ ) 2 . (1.51)
Combining Eqs. 1.50 and 1.51, the instantaneous value of resolved shear stress can
be written as
32 Introduction and overview
Fig. 1.7. A schematic diagram of change in the gage length vector from £0 to £ due to slip.
The measurement of the applied force P and the instantaneous length of the
crystal I during a uniaxial test producing single slip in a single crystal can thus be
converted into a plot of the resolved shear stress rR and resolved shear strain yR
using Eqs. 1.52 and 1.48, respectively. It is seen from Eq. 1.52 that rR increases with
the elongation of the crystal (for afixedvalue of the applied force P). This phenom-
enon is known as 'geometrical softening'. It is important to note that, while the slip
system rotates toward the tensile axis in a monotonically loaded crystal, fully
reversed fatigue loads do not cause any orientation change.
Figure 1.8 shows a typical stress-strain curve at room temperature for an FCC
single crystal, oriented initially for single slip and subjected to uniaxial tension. Here
the variation of the resolved shear stress rR with the resolved shear strain yR exhibits
three distinct stages. Stage I commences at the critical stress r0 after an initial elastic
deformation. This region of 'easy glide' is characterized by primary slip and by
straight and uniformly spaced slip lines. As the crystal deforms and the slip systems
rotate with respect to the loading axis, secondary slip is activated. This onset of
secondary slip and the attendant decrease in mean slip distance generally marks the
beginning of stage II where the crystal exhibits a significant increase in the rate of
work hardening. With the progression of plastic deformation in stage II, the increase
in dislocation density and the propensity for cross slip promote the formation of
Exercises 33
III
Fig. 1.8. A typical stress-strain curve for an FCC single crystal exhibiting three distinct stages of
deformation.
Exercises
1.1 The design of the twin-engine Boeing 777 aircraft was launched in the late
1980s with the objective of capturing the long-distance air travel market.
The aircraft was designed to fill a gap between the four-engine 747 with a
passenger capacity of around 400 and the twin-engine 767 with a passenger
capacity of approximately 200. During the development of the 777, Boeing
had to face competition for the 300-350 passenger 777 aircraft from the
newer generation of planes introduced by rival manufacturers, i.e. the 323-
seat MD-11 from McDonnell-Douglas which replaced the DC-10 with more
efficient engines, and the four-engine A-340 and the twin-engine A-330 from
Airbus. The airlines which worked with Boeing in the development of the
34 Introduction and overview
111 forged an agreement early on in the design that its fuselage would be
much wider than that of the MD-11, A-330 or A-340.
(a) Speculate about the implications of the larger fuselage on the strength,
weight and power requirements.
(b) Speculate about the implications of the larger fuselage on damage tol-
erance considerations and design against fatigue fracture.
1.2 A circular shaft of length / and radius a is twisted at the ends by a torque T,
which results in an angle of twist a per unit length of the shaft. The shear
modulus of the material is G.
(a) Find the magnitude of the nonzero components of stress in the shaft.
(b) Derive expressions for the strain energy density and the total strain
energy.
1.3 For an isotropic elastic solid, derive expressions for the strain energy density
in terms of the components of stress or strain tensors for (a) plane strain and
(b) plane stress.
1.4 For a homogeneous and isotropic elastic medium, show that the principal
axes of the stress and strain tensors coincide.
1.5 The octahedral plane is defined as the plane which makes equal angles with
the principal stress directions.
(a) Show that the octahedral shear stress, which is the shear stress on the
octahedral plane, is
OW = \ V Ol - °lf + 02 - V3
1.8 A cubic crystal contains a screw dislocation. The Burgers vector of the
dislocation is parallel to [001]. A crack propagates rapidly in the crystal
along the (001) plane in the [110] direction. Sketch the geometry and orien-
tation of the steps formed on the fracture surface.
Part one
CYCLIC DEFORMATION
AND FATIGUE CRACK
INITIATION
CHAPTER 2
' Engineering alloys are used occasionally in monocrystalline form in some fatigue-prone structures. An
example is a gas turbine engine for aircraft in which the turbine blades are made of nickel-base super-
alloy single crystals. See Section 2.10 for the cyclic deformation mechanisms in this alloy system.
39
40 Cyclic deformation in ductile single crystals
U) (2.1)
where yvXi is the resolved plastic shear strain amplitude in the zth cycle and N is the
total number of cycles. For fully-reversed straining under a fixed plastic strain
amplitude y pl , T = 4yp\N. It is important to note that the parameter F is only an
approximate measure of global fatigue damage and that it does not accurately
capture the extent of permanent damage at low plastic strain amplitudes where a
significant fraction of dislocation motion can be reversible.
- compression —
• \ 600 S
yC J200
fit- ^
^ - "
1100
I50
H30 J
ten sion
,
-J20 0
-y^f^ r if
0
1/ ,
1
compression -m
15f
20 f- • " '
30 / •—• '
100
1 ^ ^ ^ ^
200 f ' ^ ^
600 L - - ^ ^ ^ ^
» tension
1
cally shows such a curve for FCC single crystals oriented for single slip. Actual
stress-strain data obtained for a number of FCC metals fatigued at different tem-
peratures are listed in Table 2.1.
There are three regions, marked A, B and C, which exhibit distinctly different
strain hardening characteristics in Fig. 2.2. At low values of plastic strain ampli-
tude (ypl < YPIAB)> denoted region A, work hardening occurs during cyclic loading.
(This hardening behavior is measured in terms of the saturation stress and is
different from the rapid cyclic hardening prior to saturation, at a fixed value of
yp\, discussed in Section 2.1.) Region A is followed by a 'plateau' in the stress-
strain curve (region B). This latter regime, where the saturation stress, r*, is inde-
pendent of the plastic strain, extends until YPIBC- A further increase in ypl results in
an increase in r*, stage C.
In region A, work hardening displayed by the cyclic stress-strain curve is almost
entirely due to the accumulation of primary dislocations. Microscopically, saturation
of the hysteresis loops corresponds to a state where a dynamic equilibrium is
achieved between bundles of edge dislocations and the surrounding matrix plied
42 Cyclic deformation in ductile single crystals
labyrinth
structures
threshold value
for crack formation
r pi, AB
Fig. 2.2. (a) Hysteresis loops with the resolved shear stress at saturation, r R , plotted against the
resolved plastic shear strain, ypl. The stress-strain curve is drawn through the tips of stable
hysteresis loops, (b) A schematic diagram showing different regimes of the saturation stress-
strain curve.
by screw dislocations. Under these conditions, fine slip markings are observed on the
free surfaces; the specimen could withstand an infinite number of fatigue cycles
because the cyclic plastic strain does not cause progressively degenerating damage.
One of the most visible features of cyclic saturation is the localization of slip along
bands. This process is nucleated at strain amplitudes corresponding to the beginning
of region B in the cyclic stress-strain curve (Fig. 2.2) and is intensified as the applied
plastic strain is increased. Early observations, e.g., Ewing & Humfrey (1903) and
Gough (1933), showed that fatigue failure initiated as a fine crack along those bands
where slip was particularly intense. These slip lines were termed 'persistent slip
2.2 Cyclic saturation in single crystals 43
Cu-2.0 Al (at.%) 1.0 x 10~4 3.0 x 10"3 33.0 Wilhelm & Everwin (1980)
(295 K)
Cu-5.0 Al (at.%) — — 32.0 Woods (1973)
(295 K)
Cu-16.0 Al (at.%) — — 20.0-25.0 Li & Laird (1994)
(295 K)
Cu-2.0 Co (at.%) 3.0 x 10"4 5.0 x 10"3 27.5 Wilhelm & Everwin (1980)
(295 K)
1.0 xlO" 4 7.5xlO~ 3 52.0 Mughrabi, Ackermann, & Herz
Ni(295K) (1979)
1.0 xlO" 4 8.0 x IO-3 50.0 Bretschneider, Holste & Tippelt
Ni(293K) (1997)
7.5 x 10~5 5.0 x IO-3 20.5 Bretschneider, Holste & Tippelt
Ni(600K) (1997)
— — 12.0-16.0 Bretschneider, Holste & tippelt
Ni(750K) (1997)
Ag(295K) 6.0 x IO-5 7.5 x 10"3 17.5 Mughrabi, Ackermann & Herz
(1979)
Al-1.6 Cu (at.%) 1.5 x 10~5 1.5 x 10~3 95.0
Lee & Laird (1983)
(295 K)
Fe-llNi-16Cr-2Mo — — 59.0
Yan et al (1986)
(wt%)(295K)
Fe-19Ni-llCr-2Mo — — 59.0 Kaneko, Morita & Hashimoto
(wt%)(295K) (1997)
bands' (PSBs) by Thompson, Wadsworth & Louat (1956) who found that in Cu and
Ni, the bands persistently reappeared at the same sites during continued cycling even
after a thin layer of the surface containing these bands was removed by electropol-
ishing. Numerous studies, including Laufer & Roberts (1966), Lukas, Klesnil &
Krejci (1968), Watt, Embury & Ham (1968), and Woods (1973), have conclusively
44 Cyclic deformation in ductile single crystals
demonstrated that the PSBs form through the bulk of the single crystals, and that the
bands of coarse slip merely mark their egress at the specimen surfaces.
Static deformation experiments after fatigue loading (Broom & Ham, 1959) and
microhardness measurements on fatigue-induced slip bands (Helgeland, 1965) reveal
that the PSBs are much softer than the matrix. These results imply that, during
saturation in the plateau region of the cyclic stress-strain curve, essentially the entire
deformation is carried by the PSBs. In fact, the very formation of the PSBs appears
to be closely related to the occurrence of the plateau. These slip bands first appear at
Kpi ~ Yv\,AB> a n d their volume fraction,/, increases linearly to nearly 100% as ypl is
raised to a value of yPisc- For Cu, Ni and Ag, fatigued at room temperature, the
ratio of the threshold saturation stress for PSB formation (rPSB ^ r*) to the shear
modulus (G) is approximately the same (~ 6.5 x 10~4), Mughrabi, Ackermann &
Herz (1979). Figure 2.3 shows the markings exhibited by PSBs on the surface of a Cu
single crystal subjected to 15 000 cycles of fatigue at ypl values of 1.5 x 10~3 and
Fig. 2.3. PSB markings on the surface of a Cu single crystal subjected to 15 000 cycles of fully
reversed fatigue loads at two different values of resolved plastic shear strain amplitude, ypl. (a)
ypl = 1.5 x 10~3. (b) yp] = 4.5 x 10~3. Width of the specimen = 4.7 mm. (From Winter, 1974.
Copyright Taylor & Francis, Ltd. Reprinted with permission.)
2.3 Instabilities in cyclic hardening 45
4.5 x 10 3. Note the increase in the volume of the crystal covered by the PSBs due to
the increase in ypl.
cyclic
deformation
0 2 4 6 8
cumulative resolved shear strain
Fig. 2.4. Resolved shear stress plotted against cumulative resolved shear strain for copper single
crystals subjected to tension and fatigue. (After Wilkens, Herz & Mughrabi, 1980.)
46 Cyclic deformation in ductile single crystals
o
X
.S 4
10 20 30 40 50
resolved shear stress (MPa)
Fig. 2.5. Strain bursts observed in a copper single crystal subjected to increasing stress
amplitude at 7.1 kPa/cycle at 90 K. (After Neumann, 1968.)
relative occurrence seems to be perfectly periodic in that they appear whenever the
stress amplitude is raised by at least 11.5% within about fifty fully reversed fatigue
cycles. These strain bursts have been observed in single crystals of Cu, Ag, Mg and
Zn (Neumann, 1968) and of Cu-Al alloys (Desvaux, 1970).
The effects of loading mode on the possible occurrence of strain bursts can be
rationalized from the arguments presented by Neumann (1974, 1983). If the crystal is
subjected to sufficient fatigue cycles (at a given stress amplitude), hardening due to
the mutual trapping of dislocations progressively reduces ypl. This effect continues
until the mean free path for dislocation motion is smaller than their mean spacing.
Consequently, the probability of close encounters among dislocations decreases. If
the stress amplitude is slowly raised, the disintegration of dipoles leads to an ava-
lanche of free dislocations. Macroscopically, this process is manifested in the form of
a strain burst. At the higher stress level, the released dislocations are trapped again
during subsequent deformation.
This discontinuous hardening trend is also known to occur locally during the very
early hardening stage of a constant plastic strain amplitude fatigue test. Neumann
suggests that whether such local strain bursts can be seen macroscopically depends
strongly upon their interactions throughout the gage length of the specimen. Under
increasing stress amplitude conditions, experiments appear to show the occurrence of
strain bursts (coherently) through the entire gage length. However, coherent strain
bursts are not compatible with constant plastic strain control. Therefore, the dis-
continuous hardening behavior adds up to asynchronously or slowly varying macro-
scopic plastic strain amplitude in a strain-controlled test. If the fatigue specimens
which exhibit strain bursts are subjected to monotonic tensile deformation, they
undergo easy glide of zero strain hardening where coarse slip steps are formed
(Broom & Ham, 1959; Neumann, 1968).
2.3 Instabilities in cyclic hardening 47
For example, cosine of the angle 0 between the normal to the plane (111)
and the direction [T23] is: (-1 + 2 + 3)/(Vl4>/3) = 4/(^14^3).
Similarly, cosine of the angle X between the slip direction [HO] and the
loading direction [T23] is: (—1 + 2 + 0 ) / ( A / I 4 > / 2 ) = - 3 / ( V l 4 v ^ ) .
For the FCC crystals which glide along the {lll}(110> slip system, the
three [UVW] ((110)) slip directions located on each of the four (hkl)
({111}) planes can be identified by recourse to the Weiss zone law which
states:
hU + kV + lW = 0. (2.3)
With the above information, the cosine of the angle between the slip plane
normal and the tensile loading axis, cos 0, and the cosine of the angle
More generally, if r^ and n 2 are the unit vectors normal to the two planes, then r^ • n 2 =
| n.! | - |n21 • cos</>. See Section 2.8.1 for further discussion.
48 Cyclic deformation in ductile single crystals
Table 2.2. Crystallographic geometric relationships for the FCC crystal with its
tensile axis initially along [123].
Slip (Plane)
system [Direction] Notation COS0 cos X cos 0 cos A
-3 -12
Primary A2
14V6
16
A3
1
A6
VT4V2 14V6
-3 -6
Conjugate B2
VT4V3 14V6
2 4
B4
10
B5
14V6
Cross-slip Cl 0
C3 0
C5 0
VT4V2
1
Critical (IiiXiio] Dl
14V6
12
D4
D6
14V6
between the glide direction on the slip plane and the tensile loading axis,
cos A, are determined for each of the twelve possible slip systems, as shown
in Table 2.2. For a given tensile load P and crystal cross-sectional area, A,
the last column of this table gives the initial Schmid factors, M, for the
different slip systems, and the maximum value of | cos0 • cos X\ identifies
the slip system with the highest resolved shear stress, as shown in Section
1.5.1. The last column of Table 2.2 reveals that for the given orientation of
the crystal, single slip occurs initially along the A3 slip system,
(ii) As slip deformation occurs along the A3 slip system, the axis of the
cylindrical crystal begins to rotate. Consequently, the stress axis
moves towards the [TOl] glide direction. This process is visualized most
2.3 Instabilities in cyclic hardening 49
010
Fig. 2.6. A stereographic projection showing the rotation of the loading axis, initially at [123],
towards the primary glide direction [TOl] until [112]. This rotation is marked by the arrow.
(2.4)
to £Q sin A
In the present case,
Likewise,
The initial few cycles of alternating strain produce dislocations that accu-
mulate on the primary glide plane (e.g., Basinski, Basinski & Howie, 1969;
Hancock & Grosskreutz, 1969).
Fully reversed cyclic loading produces approximately equal numbers of
positive and negative edge dislocations. One may envision the possibility
of frequent encounters between dislocations of opposite sign, which attract
one another. When such encounters occur over small distances, the strong
attraction between dislocations of opposite sign will trap the dislocations,
thereby creating a dislocation dipole. Only edge dislocations of opposite
sign are likely to form such dipoles because positive and negative screw
dislocations can easily cross slip and mutually annihilate (provided that
the stacking fault energy is sufficiently high). The process of mutual trapping
of edge dislocations continues until the entire dislocation arrangement
within the veins is composed of edge dislocation dipoles.
The generation of primary dislocations is a consequence of the geometrical
condition that, during fully reversed fatigue straining, there is no rotation of
the slip system with respect to the loading axis. Therefore, the primary slip
system remains the most highly stressed. Microscopy results by many
researchers, which document the absence of any lattice rotation between
adjacent channels, suggest that the average Burgers vector within the
veins is close to zero because of equal numbers of positive and negative
edge dislocations (e.g., Mughrabi, 1980). Thus, the veins do not produce
long-range internal stresses. One of the most notable distinctions between
monotonic and cyclic hardening of FCC single crystals at low amplitudes of
imposed strains is this absence of long-range internal stresses under fatigue
deformation. (The stresses due to the edge dislocation dipoles in the veins
are significantly more short-ranged (oc 1/r2) than those arising from the pile-
up of dislocations (oc l/^/r), where r is the radial distance from the core of
dislocation; see, for example, Neumann, 1983.) The absence of long-range
internal stresses has also been identified by X-ray measurements (Hartman
& Macherauch, 1963; Wilkens, Herz & Mughrabi, 1980).
With continued cycling, accumulation of dislocations occurs predominantly
in the form of mutually trapped primary edge dislocation dipoles.
These networks of edge dislocation dipoles are commonly referred to as
veins, bundles, or loop patches. The veins have an elongated shape; their
long axis is parallel to the primary dislocation lines and their cross sec-
tion normal to the long axis is equi-axed. The veins are separated by
channels, which are relatively dislocation-free and are of a size compar-
able to that of the veins. The width of the veins is about 1.5 (im in
copper fatigued at 20 °C. A reduction in temperature promotes a finer
dislocation structure.
The dislocation density within the vein is of the order of 1015 m~2 which
corresponds to a mean dislocation spacing of 30 nm. The dislocation density
2.3 Instabilities in cyclic hardening 51
within the channels is three orders of magnitude smaller, which implies that
the average dislocation spacing in the channels is comparable to the width of
the channels.
• The veins contribute to rapid hardening in the early stage of fatigue by
partially impeding dislocation motion on the primary slip system.
Increasing the number of cycles leads to an increase in both the dislocation
density within the veins and the number of veins per unit volume. This
results in an enlargement of the network of interconnected veins packed
tightly with primary edge dislocations which occupy up to 50% of the
volume of the material. In the dislocation-poor regions between the veins,
screw dislocations ply back and forth during cyclic straining.
Figure 2.7 is an example of the vein structure in a copper single crystal, oriented
for single slip under ypl control. This micrograph shows the view of the primary slip
plane which, in the notation used by Basinski, Korbel & Basinski (1980), is (111); the
primary slip vector is along [101] (which is normal to the vein structure). Primary
screw dislocations can be seen in the channels dividing the veins.
Fig. 2.7. A transmission electron micrograph of matrix vein structure in a section parallel to the
primary glide plane of a single crystal of Cu fatigued to saturation at 77.4 K. (From Basinski,
Korbel & Basinski, 1980. Copyright Pergamon Press pic. Reprinted with permission.)
52 Cyclic deformation in ductile single crystals
*.~l.55f (2.8,
are required. The channel diameter given in Eq. 2.8 represents the maximum distance
over which two ends of a semi-circular dislocation arc can be separated under a
resolved shear stress rs. Substituting the appropriate values for Cu, it is found that
dor & 0.6 um. This is of the order of the experimentally measured channel width of
1.5 um which separates adjacent veins in fatigued Cu.
relative amounts of the two phases (i.e. by changing/) within the plateau (region B)
of the saturation cyclic stress-strain curve. The parameters, ym and yPSB, in Eq. 2.9
correspond to y^AB and YPIBC> respectively, in Fig. 2.2 and Table 2.1. This line of
reasoning, albeit simplistic, provides an appealing rationale for the similarities in the
conditions that govern the formation of PSBs in single crystals of a variety of metals
and alloys.
Winter's two-phase model also has limitations (e.g., Brown, 1977). Firstly, the
model implies reversibility, contrary to the reality of a fatigue experiment where a
decrease in ypl does not lead to the disappearance of the PSBs. Secondly, the model is
not applicable for materials where fatigue loads alter the microstructure; for exam-
ple, precipitation-hardened alloys (in which cyclic straining can shear the strength-
ening precipitates) or work-hardened materials (in which fatigue softening occurs).
Thirdly, the two-phase model is not applicable to cyclic deformation involving dis-
location climb, i.e. above about half the melting point.
As the PSBs penetrate through the bulk of the crystal, the strain carried by them is
macroscopically reversible in that the local strain at the maximum value of the
applied tensile stress is identical to that at the compressive maximum (Finney &
Laird, 1975). On a polished surface, slip steps visible to the naked eye disappear
and reappear every quarter cycle. Although the surface slip steps form in proportion
to ypl, the displacements within the band are not fully reversed. This leads to the
formation of slip offsets and a rough topography within the bands which appears to
be the precursor to crack nucleation (see Chapter 4). There is considerable variation
in the thickness and distribution of slip, with the coarse PSBs consisting of narrower
slip bands known as micro-PSBs.
It is generally recognized that the PSBs are a pre-requirement for the formation of
fatigue cracks in pure crystals. Therefore, the observation of threshold stress (or
strain) for the formation of PSBs automatically implies the existence of a fatigue
(stress or strain) limit below which no cyclic failure occurs (Laird, 1976; Mughrabi,
1978).
gliding
screw bowing-out
, segment edge segment
;liding
screw segment
tens of micrometers
(c)
Fig. 2.8. Dislocation arrangements in FCC metals, (a) Vein structure in the matrix, (b) An
enlarged view of the dipolar walls and dislocation debris within a PSB. (c) A three-dimensional
sketch of PSB geometry formed in Cu at 20 °C. (After Mughrabi, 1980, and Murakami, Mura &
Kobayashi, 1988.)
The dislocation structure found within the PSBs is considerably different from
that of the matrix. The matrix contains, about 50% by volume, vein-like structures
consisting of dense arrays of edge dislocations. On the other hand, the PSB structure
is generated due to the mutual blocking of glide dislocations and the formation of
parallel wall (ladder) structures which occupy about 10%, by volume, of the PSBs
(Laufer & Roberts, 1966; Woods, 1973; Mughrabi, 1980). The walls are 0.03-
0.25 jim in thickness with a spacing of about 1.3 urn and they consist of dipoles.
The dislocation densities in the matrix veins and PSB walls are 1011—1012 cm"2 and
are two to three orders of magnitude greater than those in the in-between channels
containing screw dislocations. Weak-beam TEM studies of copper crystals reveal the
presence of about two-thirds vacancy dipoles and one-third interstitial dipoles of
primary edge dislocations (Antonopoulos, Brown & Winter, 1976; Antonopulos &
Winter, 1976). A schematic of the dislocation arrangements in the veins and in the
PSBs is given in Fig. 2.8.
Figure 2.9 is an arrangement of several electron micrographs showing the three-
dimensional geometry of the matrix veins and PSB structures in Cu. The (121) plane
clearly shows the ladder-like arrangement of the walls in the PSB, which are oriented
perpendicularly to the primary Burgers vector b. Figure 2.10 is a TEM micrograph
of a (121) section of a Cu crystal which shows the ladder structure in the PSB and the
matrix vein structure consisting of dislocation bundles.
2.5 Dislocation structure of PSBs 55
Fig. 2.9. A three-dimensional view, constructed from several TEM images, of the matrix vein
and PSB dislocations in Cu cycled to saturation at 20 °C at ypl = 1.5 x 10~3. The specimen
loading axis, indicated by the dashed line, is almost on the (121) plane and it makes an angle of
47° with the primary Burgers vector b. (From Mughrabi, Ackermann & Herz, 1979. Copyright
American Society for Testing and Materials. Reprinted with permission.)
The matrix veins accommodate plastic strains only of the order of 10 4, and hence
they undergo only microyielding. On the other hand, PSBs support high plastic shear
strains of the order of 0.01 and undergo macroyielding. This can involve dislocation
multiplication by the bowing-out of the edge dislocations (from the walls) and by
their transport along the channels; the screw dislocations in the channels may also
draw the edge dislocations out of the walls (see the schematic in Fig. 2.8(/?)). Figure
2.11 is an electron micrograph of a section parallel to the primary glide plane, (111),
of monocrystalline Cu at 20 °C. The primary edge dislocations bowing out of the
walls are also evident. The same sense of curvature is exhibited by dislocations of the
same sign.
Two different mechanisms have been proposed to rationalize the quasi-steady
state deformation of the saturation stress-strain curve. Deformation within the
matrix veins is believed to be accomplished by the back and forth ('flip-flop') motion
of dislocation loops that are produced by jogs during cross slip of screw dislocations
under cyclic straining (Feltner, 1965; Finney & Laird, 1975). It has been suggested by
Grosskreutz & Mughrabi (1975) that this flip-flop mechanism can accommodate
plastic strains of the order of 10~4, and hence accounts for the saturation behavior
56 Cyclic deformation in ductile single crystals
PSB
Fig. 2.10. TEM image of dislocation structures in a Cu crystal fatigued at ypl = 10 3 at room
temperature. A view of the (121) section revealing the matrix veins (M), PSB walls and screw
dislocations in the channels between the walls. (From Mughrabi, Ackermann & Herz, 1979.
Copyright American Society for Testing and Materials. Reprinted with permission.)
Fig. 2.11. TEM of a section parallel to the primary slip plane of single crystal Cu fatigued to
saturation at ypl = 5 x 10~ . Fast neutron irradiation was employed to pin the dislocations at
the peak tensile stress of the fatigue cycle. (From Mughrabi, Ackermann and Herz, 1979.
Copyright The American Society for Testing and Materials. Reprinted with permission.)
2.5 Dislocation structure of PSBs 57
in the veins either during rapid hardening or during saturation in region A. On the
other hand, a dynamic equilibrium between dislocation multiplication and annihila-
tion is considered responsible for saturation within the PSB in the plateau regime of
the cyclic stress-strain curve. Consequently, the local densities of edge and screw
dislocations are kept constant (Essmann & Mughrabi, 1979). Dislocation multiplica-
tion occurs by the bowing out of edge dislocations between the walls, whilst anni-
hilation occurs by climb of edge dislocations of opposite sign on glide planes 1.6 nm
apart in the wall structure of PSBs. Furthermore, the annihilation of screw disloca-
tions (on glide planes 50 nm apart) at room temperature is also believed to occur in
the dislocation-poor channels of the PSBs.
Equations 2.14 and 2.15 together must satisfy the condition that
/ c Ar c +/ w Ar w = 0. (2.16)
The local stresses, Eqs. 2.14 and 2.15, are long-range internal stresses that develop
due to different amounts of deformation in the walls and channels which have
different dislocation distributions. Thus, a crystal with a heterogeneous dislocation
distribution exhibits local deformation similar to that of a composite. This effect has
important implications for a wide variety of fatigue phenomena, such as cell forma-
tion (Sections 2.8 and 2.9), the Bauschinger effect (Chapter 3), cyclic slip irreversi-
bility and fatigue crack nucleation (Chapter 4).
The composite model discussed above rationalizes, in a simple manner, the
accommodation of plastic strains in the plateau regime of the cyclic stress-strain
curve. However, the development of quantitative criteria for the inception of a
fatigue crack requires detailed constitutive formulations of the inelastic deforma-
tion in the PSBs.
I2sd
superjog
(retained from
cross slip)
(a) (b)
Fig. 2.12. (a) Schematic illustration of the dislocation dipole. (b) Glide path for dipole flip-
flop.
2.5 Dislocation structure of PSBs 59
r
bow ^ ~T- (2.18)
Equating these two stresses, we find the condition for the stability of the
dipole loop to be
(2 20)
^ -
This is of the order of the stresses seen for Cu at room temperature,
(iii) The total dislocation density is
P = Pdipole x k = !02° x 0.5 x 10~6 m" 2 = 0.5 x 1014 m" 2 . (2.21)
The average glide path, schematically sketched in Fig. 2.12(6), is (V2 • sd).
Since there are two dislocations in the dipole, the average glide path per
dislocation is,
' Strictly speaking, the dipole passing and dislocation bowing processes should be treated as functions of
dislocation displacement.
60 Cyclic deformation in ductile single crystals
the plastic part accounting for the cumulative effect of slip in the PSBs (which leaves
the lattice undistorted as well as unrotated), and Fv is a factor representing the effects
of vacancy generation.
Let TR be the resolved shear stress acting in the slip system a along the direction s"
(i.e. a (110) direction) on a slip plane (i.e. a {111} plane) whose normal is nf\ If r is
the Kirchhoff stress tensor,
a
r ^ s V ; sa = ¥er and ma = F ^ V * , (2.25)
where the superscript T refers to the transpose of the tensor. The flow rule derived
from the kinematics of slip is written as (Rice, 1971):
ya r ® m01, (2.26)
where ya is the shear strain rate on the slip system a and ® denotes a vector dyadic
product. This constitutive formulation is completed by writing an equation for the
evolution of ya on the basis of the type of loading (e.g., fully reversed and yp\
controlled) and the material behavior (e.g., rate-independent plastic response).
t Details for extracting F e for FCC crystals can be found in Teodosiu (1982).
2.6 A constitutive model for the inelastic behavior of PSBs 61
= bpaw\ 1 1 , (2.27)
|lP(4) j
where b is the magnitude of the Burgers vector, pa is the dislocation density in the
primary slip system, and w is the distance of separation between the walls in the PSB.
The term [1 — P(TR)] denotes the subfraction of destabilized dislocations that are
trapped by the nearest wall, and 1/[1 — P(TR)] signifies the average number of jumps
taken by a dislocation, from one dislocation wall to a neighboring wall in the PSB,
before being trapped in a stable position. P(ra) can be determined directly from
experimentally measured stable hysteresis loops of TR versus ypl, similar to the
ones shown in Fig. 2.2(a).
(2.28)
Here haa is the self-hardening modulus, hac = xaclyac is the characteristic hardening
modulus, xac = CGb^/nna is the characteristic flow stress (with G being the shear
modulus and C, a nondimensional constant), and y" = {bpa)/(2^/ff) is a character-
istic glide strain. The density of obstacles created by forest dislocations, na, takes the
form
(2.29)
where f3 denotes all relevant slip systems other than the primary system a. The
interaction coefficients a0^, which depend on the nature of the dislocation junctions
' Equation 2.27 is an oversimplification in that it does not account for the link between the hardening
process and the motion of screw dislocations in the channels or the increasing densities of loops and
dislocation debris.
62 Cyclic deformation in ductile single crystals
* Note that the above argument does not take into account the process of annihilation of screw disloca-
tions in the channels. In addition, care should be exercised in analyzing the annihilation process since it
may involve dislocation climb or merely a mechanical collapse due to very high local interaction stresses.
2.7 Formation of PSBs 63
Fig. 2.13. A schematic showing the annihilation of dislocation loops and the attendant
production of vacancies.
edge segments necessarily involves dislocation climb until the area of the loop Ly
vanishes by generating point defects (which, as seen earlier, are predominantly
vacancies). Vacancy generation also has the concomitant effect of promoting a
steady elongation of the PSB along the nominal slip plane, which gives rise to surface
protrusions. The rate of deformation induced by dislocation climb due to the anni-
hilation of edge dislocations is found (Repetto & Ortiz, 1997) to be
F V " 1 = cv s" OS" = (\paylya) S" ® S". (2.31)
The rate of elongation of the PSB is thus established via the vacancy generation rate
(cY) and the known slip rate. The implications of this PSB elongation process, along
with that of vacancy diffusion, to fatigue crack initiation will be considered in
Chapter 4.
Fig. 2.14. The evolution of a PSB wall structure in the dislocation-poor region of the matrix
veins (marked by arrows), g = (111). yp\ = 4 x 1CT4. (From Holzwarth & Essmann, 1993.
Copyright Springer-Verlag. Reprinted with permission.)
2.7 Formation of PSBs 65
evident, with dislocation-poor interior regions in the veins. Consider the PSB in
this figure which cuts through a row of veins. From the geometry of the nascent
wall structure and the surrounding vein structure, it is noted that the walls
originate from the vein shells and that they have to move very little to establish
their spacing during PSB evolution. The destruction of veins is seen to begin
preferentially in the dislocation-poor regions where each vein forms two walls.
The scenario emerging from Fig. 2.14 is essentially the same as that put forth for
Ni by Mecke, Blochwitz & Kremling (1982), and for Cu by Jin (1989).
(2.32)
(2.33)
66 Cyclic deformation in ductile single crystals
For mechanical equilibrium, all dislocation structures must be relaxed, i.e. the net
stress on a dislocation line (due to the applied stress and due to all the other dis-
locations) must be zero. This can be accomplished by shifting the dislocations within
their slip planes (i.e. with yjfixed)into appropriate positions Xj. Mathematically, this
process reduces to equating the right hand side of Eq. 2.32 to zero, which results in n
nonlinear equations for the n unknowns Xj. In this way, the stability of veins can be
modeled by using various shapes of the finite Taylor-Nabarro lattices as the starting
configurations.
Figure 2.\5{a) shows such a relaxed configuration of a diamond-shaped section of
Taylor-Nabarro lattice in which all the dislocations are at their equilibrium positions
at zero applied stress. It is found that, for this section, the application of a stress
results in the emergence of dipolar walls of dislocations from the polarization of the
initial configuration, Fig. 2.\5{b). Figure 2.15(c) shows the equilibrium configuration
of a wall structure of dislocations. Here the ratio of wall spacing to wall height is of
the order of unity, in concurrence with the experimental observations of ladder
W
1T1T1T1
1T1T1T1T1T1
ITlTlTlTlTITiTl
ITiTlTATiTlTlTlTiTl
1T1T1T1T1T1T1T1T1T1T1T1
1T1T1T1T1T1TIT1T1T1T1T1T1T1
ITITITITITITITITITITITITITITITI
1T1T1T1T1T1T1T1T1T1T1T1T1T1T1T1T1T1
T1T1T1T1T1T1T1T1T1T1T1T1T1T1T1T1T
T1T1T1T1T1T1T1T1T1T1T1T1T1T1T
T1T1T1T1T1T1T1T1T1T1T1T1T
T1T1T1T1T1T1T1T1T1T1T
r1T1T1T1T
LT1T
T1T1T1T1T
T1T1T
(b) XT 1
IT IT IT 1
IT IT IT IT IT 1
IT IT IT IT IT IT IT 1
IT IT IT IT IT IT IT IT IT 1
IT IT IT IT IT IT IT IT IT IT IT 1
IT IT IT IT IT IT IT IT IT IT IT IT IT 1
IT IT IT IT IT IT IT IT IT IT IT IT IT IT IT 1
JX1T1T1T1T IT IT IT IT IT IT IT IT IT IT IT 1T1
TIT IT IT I T IT IT IT IT IT IT IT IT IT IT IT IT
T IT IT IT IT IT IT IT IT IT IT IT IT IT IT
T IT IT IT IT IT IT IT IT IT IT IT IT
T IT IT IT IT IT IT IT IT IT IT
T IT IT IT IT IT IT IT IT
T IT IT IT IT IT IT
T IT IT IT IT
T IT IT
T
(c) IT XT XT XT XT
XT XT XT XT JET
XT -I P XT XT XT
XT XI XT XT
Fig. 2.15. (a) and (b) show equilibrium states of finite Taylor-Nabarro lattices at r a = 0 and
r a = 0.425Tmax> respectively, (c) is the computed equilibrium structure of dipole walls at
Dy = bd/lp. Figure (a) is an example of a 9 x 9 quadrupole structure. Figure (c) is an example
of walls (parallel columns) each of which consists of four dipoles. (From Neumann, 1986.
Copyright Elsevier Sequoia S.A. Reprinted with permission.)
2.7 Formation of PSBs 67
structures shown in Fig. 2.10. For the arrangements seen in Fig. 2.15(c), the dipole
strength is bd/lp, where d is defined in Fig. 2.15(c) and the inset in Fig. 2.16. (It
should be noted that for an isolated dipole, the dipole strength is defined by the
relationship Dy = b(y+ — y~), where y+ is the y coordinate of the positive dislocation
and y~ is the y coordinate of the negative dislocation in the dipole, and b is the
magnitude of the Burgers vector.)
When the applied stress ra reaches a certain critical value, r max , the initial disloca-
tion configuration (made up of multipoles) begins to decompose into dipolar walls.
Figure 2.16 shows the variation of the decomposition stress, r max , calculated from
the foregoing numerical simulation, as a function of the total number of dislocations
used in the model. In this figure, r max is normalized by the decomposition stress, t max ,
of the most narrow elementary dipole of the configuration, with the separation
distance between the dislocations in the dipole being d in a direction normal to
the slip plane. r^ ax (oc b/4d) is the passing stress of two dislocations (say, the zth
and &th dislocations which have opposite signs, with yt — yk = d). The veins in this
2.0
compressed
walls of 2Nd dipoles
o
ex 1.0
o diamonds of 1 x Nd quadrupoles
8
0.0
0 2 4 6
size of dislocation configuration, NA
figure are composed of elementary quadrupoles (see inset in Fig. 2.16) which make
up a diamond-shaped Taylor lattice.
Figure 2.16 indicates that the wall structure is more stable than the vein structure
(at comparable values of r max ). This result provides a rationale for the experimental
observation that, at saturation, the decomposing veins cannot rearrange into a
different vein structure with smaller d values, but transform into a ladder structure.
This numerical model, albeit limited and very simplistic in its consideration of the
arrangements of dislocations in fatigued crystals, provides encouraging possibilities
for developing a physical basis for fatigue deformation.
dt dx
^ =D m ^ + Ppl (2.34)
at dxz
In these equations, the parameter P is related to the maximum stress or plastic strain
rate, x is the dislocation glide direction, and c measures the pinning rate of freed
dislocations by immobile dislocations. The function g(p{) is a dislocation generation/
loss function whose initial value is zero and whose derivate with respect to time is
positive at low dislocation densities (i.e. when dipole density increases) and becomes
negative at high densities (i.e. when increased dipole destruction occurs). The sub-
scripts T and 'm' denote quantities corresponding to the immobile and mobile
dislocations, respectively. (The reader may consult the original references for further
details.)
Solution of Eqs. 2.34 predicts instabilities in the form of oscillations in time and
spatial patterning. These two instabilities have been related to the occurrence of
strain bursts and the formation of PSBs, respectively. However, this analysis relies
on rather global assumptions on the diffusion of dislocations and ignores the specific
dislocation geometries within dipolar PSB walls and channels.
2.8 Formation of labyrinth and cell structures 69
Differt & Essmann (1993) have proposed a dynamic model for edge dislocation
walls within a reaction-transport modeling framework. In this work, the reaction
terms are consistent with the experimentally observed properties of fatigue-
induced dislocation structures (which overcome some of the limitations of the
Walgraef & Aifantis model). Two important length scales are introduced in the
reaction terms: (i) the critical annihilation distance of a dipole under the influence
of an applied stress and (ii) the critical distance for the spontaneous annihilation
of closely spaced dipoles. The analysis shows how the walls move. Edge disloca-
tions are deposited on the walls by the moving screws. If the fluxes on both sides
of the wall are not balanced, the wall is destructed on one side and reconstructed
on the other. The wall moves until the fluxes get balanced. This mechanism
rationalizes why a freshly-formed PSB is less periodic and imperfect than a
mature one.
In summary, the dislocation arrangements in fatigue can be broadly classified
into two basic groups (e.g., Glazov, Llanes & Laird, 1995) : (i) structures in which
equilibrium is maintained, and (ii) nonequilibrium self-organized dislocation struc-
tures. The former group includes the low-energy dislocation structure (LEDS)
discussed earlier in this section and includes the Taylor-lattice calculations. The
latter includes models of the type postulated by Walgraef & Aifantis. The non-
equilibrium structures have been shown to provide a rationale for the instigation of
fatigue instabilities such as the formation of ladder structures in PSBs and strain
bursts.
We close this section by noting that several approaches have emerged to ratio-
nalize the patterning seen in fatigue by recourse to computer simulations.
Hesselbarth & Steck (1992) have confirmed the Neumann model for equilibrium
structures through two-dimensional cellular automata simulations of stress-induced
patterning from an initial random configuration of edge dislocations. Devincre &
Pontikis (1993) have studied the periodicity of dipolar walls as a function of
applied stress and edge dislocation density, while full three-dimensional simulations
of dislocation structures under cyclic stressing have been undertaken by Devincre
& Kubin (1997).
2 um
Fig. 2.17. A view of the (010) section of a Cu crystal that was cycled to saturation at
ypl = 5 x 10~3, revealing the labyrinth structure. ((From Ackermann et al., 1984. Copyright
Pergamon Press pic. Reprinted with permission.)
rinth' and 'cell' structures are noticed for ypl > 2 x 10 3 . Figure 2.17 is a TEM
image of a (010) section of the Cu crystal that was subjected to fatigue at
ypl = 5 x 10~3. Note the formation of a labyrinth structure with its walls oriented
parallel to the (100) direction with a mean spacing of about 0.75 |im. The labyrinth
consists of two sets of orthogonal Burgers vectors; bx and b 2 denote the primary
and conjugate Burgers vectors, respectively. Labyrinth walls are also known to be
produced during cyclic deformation of Cu-Ni alloys (Charsley & Kuhlmann-
Wilsdorf, 1981), of ionic crystals (Majumdar & Burns, 1982) and of BCC metals
(e.g., Mori, Tokuwame & Miyazaki, 1979). The occurrence of walls of labyrinth
structures has been rationalized on the basis of a geometrical argument by
Dickson, Boutin & L'Esperance (1986), who considered a three-dimensional stack-
ing of twin dislocation loops of rectangular shape. The directions in which the
stacking of the loops was geometrically most favorable was shown to be consistent
with the crystallographic orientations of labyrinth structures actually observed in a
variety of metal crystals.
Ackermann et al. (1984) have suggested the following changes at the higher ypl
end of the saturation stress-strain curve (Fig. 2.2) for FCC crystals: matrix phase
with labyrinth structure —> PSBs and labyrinth structure —> cell structure.
Secondary slip (prevalent in region C) originates at the PSB-matrix interface
and spreads in the form of an expanding cell structure which fills the PSBs. The
transformation of all the PSBs into a cell structure appears to occur after 106
cycles. This marks the beginning of secondary hardening in region C. The above
structural changes reported for Cu have also been found in Ni (Mecke, Blochwitz
& Kremling, 1982). Figure 2.18 shows an example of a cell structure formed in Cu
in regime C.
2.8 Formation of labyrinth and cell structures 71
Fig. 2.18. A view of the (121) section of a Cu crystal that was cycled to saturation at ypl
1.45 x 10~ , revealing cell structures formed by multiple slip in regime C. The primary
Burgers vector is along b. (Photo courtesy of H. Mughrabi. Reprinted with permission.)
Problem:
(i) A single crystal of an FCC metal, with a (001) orientation along the stress
axis, is deformed until the onset of plasticity. How many equivalent slip
systems are activated? What is the Schmid factor for these slip systems? Is
the deformation accompanied by a change of axial orientation?
(ii) Answer the above questions for a BCC single crystal with a (111) orienta-
tion which deforms on slip systems of the type {TO 1} < 111).
Solution:
(i) A repeat of the calculations, similar to those listed in Table 2.2, readily
reveals that there are eight slip systems for this case with
M = |cos0-cosA| = l/(V3\/2) = 0.408. In other words, the slip sys-
tems A2, A3, B2, B4, Cl, C3, Dl and D4 have the same Schmid factor,
M. These eight slip systems comprise four {111} slip planes, each contain-
ing two (110) directions inclined equivalently to the stress axis [001]. The
resolved shear stress on the other four slip systems (A6, B5, C5 and D6) is
zero for this initial orientation because the four directions in the {111}
plane are perpendicular to the stress axis. Therefore, these slip systems are
not activated.!
The Schmid factor, M, can also be computed in a more concise manner,
for the slip system (11 l)[T01] for example, by ascribing the following
' I n a real experiment, however, errors in alignment and orientation may lead to the activation of slip
systems which differ from this predicted behavior. See Section 3.1 for a further discussion of this point.
72 Cyclic deformation in ductile single crystals
values: slip plane normal, n = [111], slip direction b = [101], and stress
axis, s = [001], such that
In view of the symmetry of the slip systems with respect to the stress axis,
no orientation change occurs.
(ii) For the BCC crystal, proceed similarly to the previous case. In this case,
there are six equivalent {110} (111) slip systems comprising three equiva-
lent (inclined) {110} planes, each containing two equivalent (111) slip
directions. The Schmid factor is also computed in a similar fashion for
these slip systems. For example, for the (110)[lll] slip system, assign:
n = [110], b = [111], and s = [111]. Substituting these values in Eq.
2.35 yields that M = 0.27. As in the previous case, in view of the sym-
metry of the slip systems with respect to the stress axis, no orientation
change occurs.
Table 2.3. Effects of crystallographic orientation and multiple slip on the cyclic stress-
strain response of FCC single crystals at 20 °C.
Loading
Metal axis Observation Reference
Cu [001] Higher hardening rate than Kemsley & Pater son (1960)
[111] in single slip
[111] No plateau Lepisto & Kettunen (1986)
[112] Higher cyclic hardening rate Jin & Winter (1984) and Jin
[012] in multi-slip than in duplex (1983)
[122] slip
[001]
[034] Pseudo plateau than in single Gong et al (1995)
slip
[117] No plateau Gong et al (1995)
[001] No plateau, no PSBs Gong, Wang & Wang (1997)
[Oil] A clear plateau over Li et al (1998)
ypl = 1.1 x 1 0 " 4 - 7 . 2 x 10" 3 ;
small, irreversible rotation of
slip system during symmetric
tension-compression loading
which causes deformation
bands to form
Ni [001] Pseudo plateau in regime B Mecke & Blockwitz (1982)
[111]
such a structure. The interactions among different slip systems in the labyrinth and the
attendant formation of Lomer-Cottrell locks causes a much higher cyclic hardening
rate in multi-slip orientations than in single glide. The labyrinths accommodate dif-
ferent imposed plastic strains by appropriately adjusting their channel widths: an
increase in yp\ is accommodated by a reduction in the channel width of the labyrinth.
Another noteworthy feature of multiple slip during cyclic deformation is the
apparent improvement in the fatigue limit. In the [001] specimens, the fatigue
limit, denned as the critical value of ypl below which (nonpersistent) slip bands do
not form, is approximately 1.7 x 10~4, compared to 6.0 x 10~5 for single slip fatigue
of Cu. Further implications of such multiple slip for fatigue deformation and for the
cyclic response in polycrystals will be discussed in the next chapter.
74 Cyclic deformation in ductile single crystals
b=(a/2)[101]
Fig. 2.19. A transmission electron micrograph of the labyrinth structure formed in a single
crystal of Cu fatigued in equal tension-compression along the [001] stress axis at ypl = 1.8 x
10~3 at room temperature. The TEM foil is parallel to (T20). The symbols 'p' (for primary)
and 'c' (for critical) denote the projections of [101] and [101] screw dislocation segments on
the (120) plane along the [425] and [425] directions, respectively. (From Wang, Gong &
Wang, 1997. Copyright Elsevier Ltd. Reprinted with permission.)
Single crystal Ni-base superalloys are also used as blades in the turbopump of the Space Shuttle main
engine.
2.10 Case study: A commercial FCC alloy crystal 75
Fig. 2.20. TEM micrograph of the initial microstructure showing the y/y precipitate
structure, g = {200}. (From Milligan & Antolovich, 1987. Copyright Metallurgical
Transactions. Reprinted with permission.)
Cr (10.4%), Co (5.3%) and W (4.1%), with the balance being Ni; the C content is 42
ppm. Figure 2.20 is the initial TEM micrograph showing the y/y precipitate structure of
this alloy prior to mechanical testing. This example also illustrates the evolution of
dislocation networks and stacking faults as a result of uniaxial cyclic loading and of
the interactions between dislocations and precipitates at different temperatures. The
results summarized here are from the work of Milligan & Antolovich (1987, 1991).
Distinct changes occur in the monotonic and fully-reversed cyclic deformation of the
PW 1480 alloy crystal in different temperature regimes. Orientation dependence of the
critical resolved shear stress in the family of {111} (110) slip systems, tension-compression
asymmetry as well as anisotropic strain hardening result from a highly anisotropic
octahedral slip, at temperatures typically below 760 °C. This trend has been attributed to
the ease of cube cross-slip and to a multitude of active slip systems. Above about 800 °C,
however, deformation is mostly isotropic, with the mechanism being largely governed by
the by-pass of y' particles by the dislocations which causes pronounced wavy slip. This
behavior is strain-rate sensitive, with increasing strain rate extending slip planarity and
anisotropic deformation of higher temperatures.
Figure 2.2\(a) shows a typical dislocation structure of PW1480 subjected to 6 cycles of
fully reversed strain-controlled fatigue. Dislocations and stacking faults with the y'
precipitates on the primary {111} slip planes are seen. The dislocation pairs (marked by
arrows) were determined to be of primary a/2(l 10) Burgers vector. Figure 2.2\{b) is from
the same area, with the primary slip plane viewed edge on. It is seen here that (i) the
dislocation pairs in the matrix are ostensibly in the same slip bands that contain the
faulted dislocation loops within the precipitates, and that (ii) the slip deformation is
highly planar. These micrographs also imply that the deformation mechanism involves
the shearing of the / precipitates by dislocations with the primary Burgers vector.
76 Cyclic deformation in ductile single crystals
R#
Fig. 2.21. Dislocation substructure in the superalloy crystal after six fully reversed cycles at
20 °C with ypl = 1.1 x 1013, and ypl = 8.7 x 103 s" 1 . (a) A bright-field TEM micrograph
showing stacking faults and faulted loops in the precipitate, and matrix pairs (arrows)
between the precipitates, b = {200}. (b) A bright-field micrograph of the same area looking
edge on. The planar nature of the structure is evident, g = {111}. (From Milligan &
Antolovich, 1991. Copyright Metallurgical Transactions. Reprinted with permission.)
0.2 \im
Fig. 2.23. Dislocations by-passing the y precipitates after 765 fatigue cycles at
ypl = 2.3 x 10~3 and ypl = 8.7 x 10~3 s"1 at 1093 °C. g = {200}. (Photograph courtesy of
W.W. Milligan. Reproduced with permission.)
77
78 Cyclic deformation in ductile single crystals
Faulted dislocation loops are left behind by this shearing process as deformation debris.
A more direct evidence for such shearing is available in Figs. 2.22{d) and (b) which show
the shearing of a / precipitate by {111} a/2 (110) dislocations after a plastic strain of
0.08% at 705 °C.
Figure 2.23 shows an example of the dislocation by-passing of / precipitates in the
same alloy subjected to 765 fatigue cycles. This process essentially homogenizes the
macroscopic fatigue deformation response which becomes isotropic in tension and com-
pression.
extrusion
intrusion
(a)
Fig. 2.24. (a) A series of steps resembling a staircase pattern produced by monotonic plastic
strain, (b) A rough surface consisting of hills and valleys produced by cyclic plastic strain.
saturation axial stress as a function of the axial plastic strain range during cyclic
deformation of a-Fe single crystals at 295 K. At low plastic strain amplitudes
(< 10~3), essentially no hardening occurs and the cyclic strain is a manifestation
of the motion of edge dislocations only. However, at higher strain amplitudes,
deformation proceeds by the large-scale motion of edge and screw dislocations
and culminates in the formation of a cell structure; pronounced cyclic hardening
as well as changes in the shape of the crystal are observed due to the asymmetric
slip of screw dislocations in tension and compression. These distinctions between
low and high strain fatigue are peculiar to BCC crystals. Although no PSBs have
been identified in either regime of plastic strain amplitudes, ill-defined bands of
slip, which could lead to crack nucleation, have been noticed. In agreement with
these findings, TEM investigations of dislocation structures ahead of fatigue
cracks (described in Chapter 4) have identified the existence of PSBs in polycrys-
talline Cu but not in pure a-Fe.
The following differences between FCC and BCC crystals point to some causes
for the distinctions in their fatigue response: (i) At 295 K and at low plastic strain
amplitudes, thermally-activated glide of screw dislocations as well as dislocation
multiplication are strongly suppressed in BCC a-Fe. (ii) Whereas FCC metals are
only weakly strain rate-sensitive, the flow stress of BCC metals is strongly depen-
dent upon the strain rate. For this reason, the cyclic stress-strain curves for BCC
crystals should be obtained at constant values of imposed strain rates. It is
generally seen that, as a consequence of dynamic strain-ageing,! high tempera-
tures, very low strain rates and the addition of impurity atoms (such as carbon,
nitrogen and oxygen) to the BCC metal promote cyclic damage that is more
similar to that found in FCC metals. Mughrabi, Ackermann & Herz (1979)
report that the addition of 30 weight ppm carbon to a-Fe single crystals leads
to cyclic stress-strain curves closer to those measured for FCC metals and slip
bands analogous to the PSBs. PSBs are also known to form in both the surface
and interior grains of polycrystalline low carbon steels (Pohl, Mayr &
Macherauch, 1980). These results show that any comparison of dislocation struc-
tures and cyclic slip characteristics reported by different investigators must be
made with caution because even a small impurity content can lead to marked
variations in fatigue micromechanisms.
' Dynamic strain-ageing refers to the phenomenon whereby certain materials (e.g., low carbon steels)
generally exhibit an increase in yield and fatigue strengths over certain temperature ranges as a result of
the interaction between dislocations and solute atoms (e.g., carbon and nitrogen). Details of the mechan-
isms of dynamic strain-ageing can be found in any textbook on mechanical metallurgy.
2.72 Cyclic deformation in BCC single crystals 81
Guiu & Anglada, 1980), effectively transforms an initially circular cross section of a
cylindrical crystal into an ellipse. Neumann showed that the shape change produced
by cyclic straining can be correlated with slip irreversibility, which is an important
factor for crack nucleation. Here we follow Guiu and Anglada for the derivation of
slip irreversibility due to shape changes in BCC crystals.
Consider a BCC crystal in which it is assumed that slip occurs on several different
planes in tension and compression in one direction defined by the unit vector b. Since
all these planes are parallel to b, they can be represented in terms of two basic
reference planes of the same zone with unit normal vectors i^ and n2, which can
be arbitrarily chosen. The glide strain in tension can be represented by the total glide
strain a l t in plane nx and by the total glide strain a2t in plane n2. Similarly, the total
glide strains in compression can be represented by a l c and a2c on planes nx and n2,
respectively.
In BCC crystals, any macroscopic slip plane can be visualized as being composed
of microscopic slip steps on planes of the {110} and {112} types. Assume that the
crystal is subjected to the same magnitude of plastic strain ep in both compression
and tension; the length of the crystal can then be taken to be unchanged. If the slip
direction for both cases is b, it can be shown that the net displacement after N
fatigue cycles of a point in the crystal is
lx(n 1 xn 2 )
Au(r) = 2Nyx (r.n)b,
n9
Here, r is the vector that locates the point under consideration with respect to the
origin of the coordinate system (Fig. 2.25), y\(= a l t — a l c ) is the net (irreversible)
shear strain on plane n l9 1 is the unit vector along the cylindrical crystal axis (i.e.
deformation axis), n is a vector which is perpendicular to both b and 1,
y = l^nj + y 2 n 2 | and y2 = a2t — a2c. The above result is most directly applicable
to BCC crystals which undergo shape changes as a consequence of glide along
(111). For such cases, a more convenient representation of Eqs. 2.36 is in terms of
the angles §, f, 0 t and 0 2 ; § is the angle between the tensile axis and the slip direction,
and 0 1? 02 a n < i f a r e the angles made by the reference planes n1? n2 and the maximum
resolved shear stress plane, respectively, with the plane of the same zone whose axis
is the slip direction. One finds that
(rn)b; ^
sinf 2cos§
and / g is the fraction of glide strain in plane i^ in tension which is not reversed in
compression, and e tot = 47Vep. If the initial diameter of the single crystal is do, it will
undergo a shape change into an ellipse which has major and minor diameters of d\
and J 2 , respectively, after N fatigue cycles. The following relationship is also
satisfied:
82 Cyclic deformation in ductile single crystals
Fig. 2.25. Nomenclature for the determination of shape changes induced by tension-
compression slip asymmetry during the cyclic straining of BCC single crystals. See text for
details. (After Guiu & Anglada, 1980.)
(2.38)
The slip irreversibility, Eqs. 2.36 and 2.37, is known to play an important role in
the nucleation of fatigue cracks in BCC crystals. Furthermore, microcrack nuclea-
tion at the boundaries of surface grains in polycrystalline a-Fe has also been
linked to the shape changes produced by the asymmetry of slip. Further discus-
sions of the effects of slip irreversibility on crack initiation will be provided in
Chapter 4.
results for Ti in order to compare and contrast its cyclic behavior with that of ductile
FCC metals and to identify micromechanisms which are specific to hexagonal
metals.
400
1120
300
200
1010
100
B was oriented near the (0001) corner, while specimen C was located near the middle
of the triangle. The saturated cyclic stress-strain curves (CSSC) for the three speci-
mens are plotted in Fig. 2.26. Orientations A and B represent the upper and lower
bounds, respectively, among the three cases considered here, while specimen C exhi-
bits an in-between response. Specimen B has a 'plateau-like' regime, similar to that of
FCC crystals. The dislocation substructures in each of the three fatigue specimens
were examined by TEM after the completion of the fatigue tests.
Gu et al. (1994) offer the following line of reasoning in an attempt to rationalize
the effect of crystal orientation on cyclic deformation in the a-Ti single crystals. (1)
Typically, the cyclic deformation is strongly influenced by the propensity for twin
formation. An increase in the occurrence of cyclic twins (in the sequence
B -> C -> A, among the three specimens considered here) causes a marked increase
in the cyclic hardening rate. (Under cyclic loading, {10T2}, {1121}, {1122} and {1123}
twins have been observed in Ti single and polycrystals.) (2) At fixed applied strain
amplitudes, orientations (such as Specimen C) which promote single slip and cross
slip give rise to planar dislocation dipole arrays and dislocation loops (similar to
fatigued FCC crystals), whereas cell structures are found in the specimens oriented
for duplex and multiple slip.
Exercises
2.1 Why does cyclic slip remain confined to the primary slip plane during the
formation of vein structure or the PSB structure?
2.2 Why are the vein structures and PSB structures in FCC crystals composed
mainly of edge dislocations?
Exercises 85
2.3 What are the characteristic dimensions associated with the geometry of the
vein structure and what is the physical basis for such dislocation configura-
tions? What are the effects of changes in test temperature (either increase or
decrease) on the geometry of dislocation arrangements within the vein struc-
ture and within the channels separating the veins?
2.4 Discuss the effects of stacking fault energy on the deformation of a ductile
solid in monotonic tension and in tension-compression fatigue.
2.5 A long crystal is bent to a semicircular shape with a radius of 20 cm. The
crystal has a square cross section (2 cm x 2 cm).
(a) If it is assumed that all bending is accommodated by the generation of
edge dislocations, calculate the total number of dislocations.
(b) If the magnitude of the Burgers vector of the edge dislocations is
0.32 nm, calculate the dislocation density.
2.6 Discuss the mechanisms responsible for dynamic strain-ageing.
2.7 There is a similarity between the hexagonal close-packed (HCP) and body-
centered cubic (BCC) crystal structures.
(a) Show which plane in the BCC structure is similar to the basal plane in
the HCP structure.
(b) Draw the arrangement of atoms in this plane and determine the stack-
ing arrangement normal to this plane in the BCC structure. Is the
stacking the same as in the HCP structure?
CHAPTER 3
86
3.1 Effects of grain boundaries and multiple slip 87
deformation within the bulk of poly crystalline Cu, of 100-300 urn grain size, by
examining TEM foils taken at various depths below the free surface. At strain
amplitudes of about 10~4, PSBs confined to a single slip system and of a wall
structure similar to that of single crystals were identified in the interior of the poly-
crystalline fatigue specimen. Pohl, Mayr & Macherauch (1980) have also observed
PSBs in the interior sections of fatigued polycrystalline low carbon steel. Although
PSBs can traverse through low angle boundaries, large angle grain boundaries are
impervious to them. When the strain amplitude is raised to values beyond 10~3,
labyrinth and cell structures are observed in polycrystalline copper, as in the case
of single crystals (Chapter 2).
Experimental studies of polycrystalline metals have also identified the existence of
regimes in the cyclic stress-strain curve where PSB formation has a significant effect
(Lukas & Kunz, 1985). Specifically, the saturation stress-strain curves for coarse-
grained Cu exhibit a region of low cyclic strain hardening (somewhat analogous to
the plateau for the single crystal); the occurrence of this region corresponds to a
continuous increase in the volume of the material occupied by the PSBs, which carry
a higher plastic strain than the matrix.
where Aa/2 and Aepl/2 are the applied uniaxial stress and plastic-strain amplitudes,
respectively, k is an experimentally determined material constant, and n{ is the cyclic
strain hardening exponent. The equation can be recast into a form amenable for use
with single crystals by employing the Taylor factor, MT (= 3.06 for randomly-
textured polycrystalline FCC metals):
Cyclic deformation in poly crystalline ductile solids
For fine-grained polycrystalline Cu, k' = 146 MPa and «f = 0.205 (Lukas & Kunz,
1985).
Figure 3.1 shows a comparison of the cyclic stress-strain curves for monocrystal-
line Cu, oriented for single slip and multiple slip, and polycrystalline Cu. The solid
line is the CSS curve for Cu single crystals oriented for single slip which shows a
plateau at a saturation stress of 28 MPa in regime B. The symbols are from the
experiments of Gong, Wang & Wang (1997) for [001] Cu single crystals which
have eight symmetric slip systems.! Note the absence of the plateau in the Cu multi-
slip crystal. The dashed line in Fig. 3.1 is the power-law function, Eq. 3.2, for Cu
polycrystals, corrected for the Taylor factor. It can be inferred from Fig. 3.1 that the
absence of a plateau in the polycrystalline FCC metals is similar to that in the
multiple-slip Cu single crystal. %
As a general trend, two factors clearly distinguish polycrystalline FCC metals
from single crystals oriented for single slip:
' See the worked example in Section 2.8 for the identification of the symmetric slip system for the [001]
orientation. Although all eight systems would, in principle, be expected to have the same Schmid factor,
small errors during the alignment, machining or mounting of the fatigue specimen can lead to a pre-
ferentially higher Schmid factor in one of the eight systems. On the basis of their slip trace observations,
Gong et al. (1997) identify the B4 system to operate first as the primary system for which the resolved
shear stress and plastic shear strain are computed.
+ It is also of interest to note here that the work of Mughrabi & Wang (1981) showed an excellent
agreement between the cyclic deformation results at low plastic strain amplitudes (regime A) for Cu
single crystals (single slip orientation, where the effects of incompatibility stresses were ignored) and
polycrystals by employing the Sachs orientation factor. Above regime A, they found that the effective
orientation factor was larger than the Sachs factor, but smaller than the Taylor factor.
3.2 Cyclic deformation of FCC bicrystals 89
60 p -
40
20
Fig. 3.1. A comparison of the cyclic stress-strain (CSS) curves of Cu single crystals (—) and
polycrystals ( ) at 20 °C. The dashed line is a plot of the stress-strain response of Cu
polycrystals (from Lukas & Kunz, 1985), corrected by the Taylor factor, M T . The symbols (•)
denote the CSS response of Cu single crystals oriented for multiple slip with the loading axis
along [001]. (After Gong, Wang & Wang, 1997.)
where the subscripts 1 and 2 denote the [345] (single-slip orientation) and [117]
(double-slip orientation) components, respectively, Mx and M2 are the Schmid fac-
tors for the primary slip systems BA of the two crystals, as and rs are the saturation
values of the axial stress applied to the crystal and the resolved shear stress, respec-
tively, and 6pi is the applied axial plastic strain amplitude. Figure 3.2 is a plot of rs vs
ypl for the [345]/[Tl7] Cu bicrystal for symmetric tension-compression loads with
plastic strain control. Note the absence of a plateau in the CSS curve. Also plotted
here are the stress-strain data for a coarse-grained Cu polycrystal with a grain size of
45
***
I 35 ,6°
O bicrystal
25 A polycrystal
_j I
15
1(T 10"
Fig. 3.2. Cyclic stress-strain curves of [345]/[117] Cu bicrystal (after Hu & Wang, 1997) and
coarse-grained Cu polycrystal (after Lukas & Kunz, 1985) appropriately modified by the Taylor
factor.
3.3 Cyclic hardening and softening in polycrystals 91
1.2 mm. For the Cu polycrystal, as and epl were converted into rs and yp\ using the
Taylor factor, MT = 3.06 in the following manner: rs = <rs/MT and yp\ = MTepl.
The CSS curve of the bicrystal overlaps with that of the coarse-grained polycrys-
tal, when modified appropriately by the Taylor factor, Fig. 3.2. (Recall that a similar
overlap was demonstrated in Fig. 3.1 between a Cu single crystal oriented for multi-
slip and a Cu polycrystal.) The foregoing results illustrate that under some condi-
tions, it is possible to correlate the cyclic deformation response of polycrystals with
the corresponding behavior seen in single crystals and bicrystals.
A A A
vVVvf V- v -y -
y_v
Fig. 3.3. Phenomena associated with transient effects in fatigue, a, e and / denote stress, strain
and time, respectively.
uration representative of the saturated state is reached. Beyond this point, the hys-
teresis loop remains essentially the same cycle after cycle over the life of the test
specimen. The parameters used to describe the salient features of cyclic hysteresis
loops are defined in Fig. 3A(a). The locus of the tips of stable hysteresis loops
provides the cyclic stress-strain curve, Fig. 3.4(6).
Stress- and strain-controlled fatigue represent extremes of fully unconstrained and
fully constrained loading conditions. In real engineering components, there is usually
some structural constraint of the material at fatigue-critical sites. It thus seems
appropriate to characterize fatigue response of engineering materials on the basis
of data obtained under strain-controlled fatigue rather than cyclic stress-controlled
conditions.
Strain-controlled tests have gained increasing use in the determination of CSS
curves for engineering alloys. Three commonly used strain-controlled test methods
are indicated in Fig. 3.4(c). In the constant amplitude test, the specimen is cycled
within a constant plastic strain limit (until failure) to obtain a single stable
hysteresis loop. Multiple test specimens are needed to determine the entire CSS
curve using this method. In the multiple step method, a specimen is cycled
between constant plastic strain limits until a saturation loop results. Then the
plastic strain limits are incremented until another stable hysteresis loop is
obtained. This process is continued until the entire CSS curve is measured
from a single test specimen. In the incremental step method, the specimen is
subjected repeatedly to a strain pattern comprising linearly increasing and
decreasing amplitudes, from zero to a certain maximum total strain. The resulting
stable hysteresis loop provides the CSS plot. In some alloys exhibiting planar slip
deformation, the incremental step method provides a CSS response which is
different from the other direct methods because of the variations in the develop-
ment of dislocation structures.
3.3 Cyclic hardening and softening in polycrystals 93
cyclic stress-
strain curve'
I- 0
Ao-
constant plastic
strain limit
A A A A
V V V V V
multiple step,
increasing plastic
AY AA
VAV
strain limit after
saturation at each
step
incremental step,
A A repeated patterns
consisting of linearly
increasing and
decreasing strain limits
v
Fig. 3.4. (a) A schematic of a stable hysteresis loop and the nomenclature. Aee, Aep and Ae
denote the elastic, plastic and total strain range, respectively, (b) Cyclic stress-strain curve
drawn through the tips of stable hysteresis loops, (c) Procedures for obtaining cyclic stress-
strain curves.
(3.4)
Copper-base
OFHC Annealed 20/140 0.40/0.24
Brass 365 As-rolled 172/248 0.13/0.21
Cu-Be 172 As-drawn 641/490 0.02/0.15
Aluminum-base
2024 T4 303/448 0.20/0.09
6061 T651 290/296 0.04/0.10
7075 T6 469/517 0.11/0.10
Iron-base
SAE 1015 Normalized 225/240 0.26/0.22
Ferrovac E Annealed 48/159 0.36/0.19
SAE 1045 Q+T 1365/825 0.08/0.15
AISI 4340 Q+T 1172/814 0.07/0.15
Mar M-300 Annealed 952/800 0.03/0.08
strain hardening exponent. The typical range of nm for alloys is 0-0.5. In the applied
mechanics community, the strain hardening exponent is often denoted by n = l/nm.
Here n = 1 for a linear elastic material and n = oo for an elastic-perfectly plastic
solid.
In an analogous fashion, the cyclic stress-strain response is characterized by the
relationship
Ae Aa
(3.5)
~2E 1A
where A' is the cyclic strength coefficient and nf is the cyclic strain hardening expo-
nent. For most metals, nf varies between 0.1 and 0.2 despite vast differences in their
cyclic hardening and softening characteristics. Table 3.1 provides a list of the strain
hardening characteristics in some common engineering alloys. As a general rule-of-
thumb, well-annealed, polycrystalline metals of high purity exhibit cyclic hardening
due to dislocation multiplication, as evidenced by an increase in the stress amplitude
3.4 Effects of alloying, cross slip and stacking fault energy 95
with fatigue cycles (at a fixed strain amplitude); work-hardened materials undergo
strain softening under cyclic loading. The rearrangement of prestrain-induced dis-
location networks due to fatigue causes cyclic softening.
' It is now generally recognized that the ease of cross slip plays a decisive role in determining the slip
mode. Stacking fault energy, however, is not the only parameter influencing cross slip. For example,
Gerold & Karnthaler (1989) demonstrate that short range order can also strongly influence cross slip.
96 Cyclic deformation in poly crystalline ductile solids
monotonic cw
monotonic cyclic cw
cold-worked (cw) |3
cyclic annealed
—
cyclic
— \ — ^ —
s* monoton r monotonic
a nnealed annealed
plastic strain plastic strain
(a) (b)
Fig. 3.5. (a) Schematic showing that the cyclic stress-strain curve is independent of prior
deformation history in wavy slip materials, (b) History-dependent behavior for planar slip
materials. (After Feltner & Laird, 1967a.)
and from a literature review, Plumtree & Pawlus (1988) developed the following
empirical relationship for the dependence of saturation stress on cell size:
(3.6)
In Eq. 3.6, crs is the saturation stress, a0 is the back stress, E is Young's modulus, b is
the magnitude of the Burgers vector, Xs is the linear intercept cell size and B is a
material constant which increases in proportion to the stacking fault energy (SFE).
The works of Pratt (1967), Feltner & Laird (1967b), Abdel-Raouf & Plumtree (1971),
Saga, Hayashi & Nishio (1977) and Kayali & Plumtree (1982) collectively show that
the constant B is 7.8 for Al (SFE = 200 x 10~3 Jm" 2 ) and 3.6 for Cu (SFE = 40 x
10~3 Jm~2). Equation 3.6 does not appear to be a function of the type of deforma-
tion in that it describes the steady-state flow stress-cell size data for both monotonic
and cyclic loading conditions.
For aluminum fatigued at a total strain range of 1 % at room temperature, the
cell size and the misorientation between neighboring cells remains constant from
the onset of saturation until final failure despite noticeable changes in the cell
morphology. One may then infer that the dislocation density remains relatively
constant upon the attainment of saturation. A survey of relevant literature shows
that the operative mechanism during cyclic saturation is the irreversible bowing of
dislocation segments from the cell walls. After being emitted from the cell walls,
the dislocation segments traverse the cell and enter the adjacent walls where they
are annihilated by dynamic recovery. This equilibrium between work hardening
(dislocation generation) and dynamic recovery (dislocation annihilation) is
believed to result in a constant maximum stress and dislocation density during
the saturation stage.
3.6 The Bauschinger effect 97
work hardening phenomena, and for rationalizing such fatigue effects as mean stress
relaxation and cyclic creep (Chapter 8). For example, many commercial aluminum
alloys containing nonshearable strengthening precipitates (such as the peak-aged and
over-aged 7075 alloys used in aircraft applications) are stretched prior to temper
treatments to relieve thermal residual stresses. Since many of these alloys are known
to exhibit Bauschinger effects, low flow stresses may result under service conditions if
the material is loaded in a direction opposite to the stretching direction. It is also
known that the Bauschinger effect in precipitation-hardened commercial alloys can
persist even after the cyclic hysteresis loops are stabilized. On a more fundamental
level, the Bauschinger effect can be used to identify the contributions to strain
hardening from different kinds of dislocation mechanisms. The study of the
Bauschinger effect is, therefore, commonly regarded as a 'litmus test' for the validity
of strengthening theories in the sense that any complete hardening theory must be
capable of quantitatively accounting for the Bauschinger effect.
3.6.1 Terminology
One of the common methods of quantifying the Bauschinger effect involves
the definition of the reverse strain. This reverse strain is the magnitude of additional
strain after load reversal which makes the reverse yield stress equal in magnitude to
the maximum flow stress attained in the forward deformation. However, a realiza-
tion of the differences between forward and reverse flow stresses at any strain value
can be achieved by recourse to the construction schematically depicted in Fig. 3.6. In
Fig. 3.6(tf), ABC represents the forward deformation in uniaxial tension, with C
being the point of unloading. CD is the tensile unloading segment and DEF is the
reverse (compression) loading segment. The magnitudes of the stress and the accu-
mulated strain are replotted in Fig. 3.6(b) irrespective of the direction of loading.
|e| (accumulated)
(a) (b)
Fig. 3.6. (a) Schematic of the stress-strain curve for fully reversed loading, (b) Only the
magnitudes of the stress and the accumulated strain are replotted to illustrate the Bauschinger
effect.
3.6 The Bauschinger effect 99
Here, ABCD represents the tensile segment and DEF is the compression loading
portion. If the forward hardening segment is extrapolated (until point C'), the
instantaneous difference between the flow stress levels Aab in the (nearly parallel)
segments CC' and EF provides an indication of the Bauschinger effect in terms of
stress and characterizes the extent of 'permanent softening'. Similarly, the difference
in strain values Aeb between the forward and reversed deformation at the maximum
forward tensile stress amplitude (point C) characterizes the Bauschinger strain.
3.6.2 Mechanisms
The origins of the Bauschinger effect are related to the changes in disloca-
tion substructure induced by reversed loading and in the changes in the internal
stress systems. In polycrystalline metals where dislocation walls and subgrain bound-
aries form during forward straining, the dissolution of cell walls or sub-boundaries
upon stress reversals is considered a contributing factor to the Bauschinger effect
(Hasegawa, Yakou & Kocks, 1986). Furthermore, long-range internal stresses
induced by strain incompatibility between the PSB walls and channels can lead to
easier reverse flow in materials which form well-defined PSBs.
For particle-hardened alloys, the mechanistic basis for the Bauschinger effect is
often provided in terms of the interaction of dislocations with the strengthening
particles (Orowan, 1959). Age-hardened alloys can be broadly classified into two
groups: (i) those containing precipitates which are coherent with the matrix and
which can be sheared by dislocations, and (ii) those containing larger semi-coherent
or incoherent particles which are not penetrable by dislocations. The two types of
particles can give rise to very different hardening response in monotonic and cyclic
loading. Furthermore, the Bauschinger effects seen in the two cases are also dis-
tinctly different.
When the matrix contains permeable particles, mobile dislocations cut through
these barriers with essentially no dislocation pile-up. If the material is subjected to a
compressive stress following a tensile stress, the impingement of the shearable bar-
riers with dislocations once again leads to a reverse flow stress comparable in mag-
nitude to that seen in forward deformation due to the paucity of dislocation pile-up.
Consequently, there is little contribution to the flow stress from internal stresses
(Wilson, 1965; Stoltz & Pelloux, 1976).
In the case of alloys with coarse, incoherent and impermeable particles, the mono-
tonic stress-strain curve exhibits a large hardening rate. For these alloys, a simple
model to rationalize the Bauschinger effect is often formulated in terms of the
following three factors which influence the forward yield stress: (i) a contribution,
a0, to strength from solid solution hardening and the stress to bow out the first set of
dislocations past the obstacles, (ii) forest hardening, ad, due to the interactions of
mobile dislocations with forest dislocations, and (hi) a mean internal or back stress,
100 Cyclic deformation in poly crystalline ductile solids
<7M>which is exerted on the matrix by the particles. The total flow stress during
forward deformation is
orf = cr0 + crd + a^. (3-7)
At reverse strains of the order of the forward strain, the deformation must be cap-
able of overcoming cr0 and ad. However, ^ now assists reverse deformation, rather
than opposing it and hence the total reverse flow stress becomes
a r = cro-\-crd -OM> (3.8)
From Eqs. 3.7 and 3.8, Aab in Fig. 3.6(7?) becomes
Aa b = <r f -cr r = 2a^. (3.9)
The back stress which arises from the internal stress system in the material is very
localized in the matrix, and it is believed to be a consequence of the inhomogeneity of
plastic deformation on a microscopic scale. The term Aab is sometimes referred to as
'permanent softening'.
A large Bauschinger effect has been documented in Al-4Cu alloys containing
nonshearable 6' (CuAl2) precipitates, Al-Cu-Mg alloys containing S' (Al2CuMg)
precipitates, and Al-Cu-Zn-Mg alloys containing rj (MgZn2) precipitates (Wilson,
1965; Abel & Ham, 1966; Stoltz & Pelloux, 1976; Wilson & Bate, 1986). Using X-ray
diffraction measurements of directional lattice strains in two-phase cubic alloys,
Wilson (1965) demonstrated that reverse loading destroys the internal stresses, redu-
cing them to zero at some strain value. At this point, the stress difference between the
forward extrapolated and the knee portion of the reverse stress-strain curves, Fig.
3.6(6), was equal to 1.9OM. Here the mean stress in the matrix, a^, was estimated
using X-rays after unidirectional plastic deformation. Note that this experimental
correlation is quantitatively consistent with the prediction of Eq. 3.8.
Some of the most comprehensive studies of the Bauschinger effect have been
conducted on dispersion-strengthened metals. In their study of plastic deformation
in Cu-SiO 2 , Brown & Stobbs (1971a,b) and Atkinson, Brown & Stobbs (1974)
related the internal stresses to the formation of dislocation shear (Orowan) loops
around hard particles on many slip planes. In the unrelaxed state typical of low
temperatures and low strains, there are two contributions to strengthening: (i) A
homogeneous mean stress in the matrix is produced by the Orowan loops left around
the particles. This stress state is amenable to a transformation strain analysis because
the Orowan loops may be regarded equivalent to the transformation strains in
Eshelby's classical inclusion problem (Eshelby, 1957). This mean internal stress,
<7M, in the matrix opposes continued forward deformation during tensile loading,
(ii) The Orowan loops also give rise to an additional inhomogeneous stress locally at
the particle because the presence of the loops around the particles repels successive
dislocations. This increase in internal stress over and above the initial Orowan stress
has been termed the 'source-shortening stress' by Atkinson, Brown & Stobbs (1974).
The occurrence of a Bauschinger effect upon load reversal is then viewed as a con-
sequence of plastic relaxation which can arise due to (a) the removal of Orowan
3.7 Shakedown 101
3.7 Shakedown
Ductile metals are often subjected to cyclic loads in such a manner that the
early fatigue cycles lead to the build-up of residual stresses. Repeated contact loading
in ball bearings and railway rails, for example, commonly engenders plastic yielding.
A consequence of this plastic flow is the generation of residual stresses, which can
possibly be of such a magnitude that a steady-state is attained after some load
reversals wherein a closed cycle of entirely elastic reversed deformation is promoted.
For this situation, there is no net accumulation of plastic strain in subsequent cycles
and the system is said to have undergone shakedown. In other words, the residual
stresses generated during the early load reversals alleviate the applied loads by
inhibiting further plastic deformation in subsequent cycles, and induce a state of
reversible elastic response. Note that during shakedown, the maximum applied load
alone is of a magnitude which violates the yield condition.
The limiting value of the applied load below which no continued accumulation of
plastic strain is possible during cyclic loading is known as the shakedown limit. If the
shakedown limit is exceeded, plastic strains continue to accumulate during each cycle
and this phenomenon is commonly known as ratchetting, cyclic creep or incremental
collapse.
The conditions governing the occurrence of shakedown can be formulated in
terms of the so-called shakedown theorems, for elastic-perfectly plastic solids:
' If the ductile solid is reinforced with a brittle phase, the overall Bauschinger effect for the composite can
be rationalized even when the plastic deformation of the matrix is described by an isotropic hardening rule.
The Bauschinger effect in this case arises from the constrained flow of the matrix material between the
brittle particles (e.g., Llorca, Needleman & Suresh, 1990).
3.8 Continuum models for uniaxial and multiaxial fatigue 103
C
D
D
(a) (b)
Fig. 3.7. (a) Shapes of hysteresis loops associated with (a) isotropic hardening and (b) kinematic
hardening.
approximated by the straight line A'B''. Upon load reversal at B', the behavior
follows elastic unloading line BC\ Subsequent plastic compression is represented
by the dashed line CD' which is parallel to A'Bf. If c is assumed to be a function of
the stress invariants, the slope of the stress-strain curve at C will depend on the value
of the stress and hence on the location of C. Note that the kinematic hardening
model does predict the existence of the Bauschinger effect. This theory has been
implemented into many finite element codes.
Consider now the case of tension-compression loading over many cycles. The
kinematic hardening rule predicts that a steady state of alternating plastic flow
will set in after the first cycle of loading. On the other hand, the isotropic hardening
model suggests that the specimen will 'shake down' to an elastic state. However, as
seen in Figs. 3.3 and 3.4, a steady state of plastic strain amplitude is reached only
after an initial transient behavior. Thus, it is noted that simple isotropic and kine-
matic hardening rules may not provide an adequate description of plasticity, when a
material is subjected to periodic unloading and reloading along a different stress
path (e.g., Mroz, 1967).
In this section, a brief summary of some prominent models for cyclic plasticity is
presented, and their strengths and limitations are pinpointed. More comprehensive
reviews of these formulations are available in the literature (Drucker & Palgen, 1981;
Dafalias, 1984; Chaboche, 1986). Any complete model for cyclic plasticity must be
capable of rationalizing the following fatigue characteristics:
Many models for cyclic plasticity have been proposed over the years which ratio-
nalize the foregoing cyclic phenomena with varying degrees of success. In addition to
the Prager-Ziegler kinematic hardening model described earlier in this section, the
available approaches to modeling cyclic plasticity can be classified into the following
groups: (i) the parallel sub-element model, (ii) field of work hardening moduli,
(iii) two-surface models, and (iv) other developments involving combined
isotropic-kinematic hardening models or internal variable concepts. The following
sections describe the features of each of these approaches.
(1) When the material is loaded in tension, the weakest element yields first at a
stress ox .
(2) If loading is continued further, the second weakest element yields at a tensile
stress a2.
(3) The total load on the material is a2- A (where A is the total cross-sectional
area), whereas the total load on element 1 is ct\Ai, where A\ is the area of
element 1. Upon unloading, the residual stress on element 1 equals
—(<j2 — or\) while the residual stress on each of the other (n — I) elements
(which are all elastic at this point) is (a2 — cr{)/(n — 1).
(4) If forward loading were to be continued beyond a2 to a far-field tensile
stress, a3, the residual stress on element 1 would become —(a3 — ax) and
3.8 Continuum models for uniaxial and multiaxial fatigue 105
(a)
Fig. 3.8. (a) Masing's parallel sub-element model, (b) Three types of kinematic hardening
behavior which can be extracted from the sub-element model. (After Asaro, 1975.)
on element 2, —(<J3 — a 2 ) and so forth. For this case, reverse plastic straining
would begin at —aR where |a R | = ox + a2 — cr3.
(5) If the forward tensile loading curve has the form a = / ( e ) , then the reverse
loading curve takes the form o = 2/rte).
On the basis of the Masing sub-element approach, Asaro (1975) presented micro-
mechanical arguments for three types of kinematic hardening. The premise here is
that, at fixed values of strain rate e and temperature T, the applied stress required to
achieve a certain mechanical state is a function of the internal structure such that
a = o(ot\, a2, a 3 , . . . ) . (3.11)
It is assumed that the internal structures form in the indicated sequence Qf 1 ,a 2 ,a 3
during forward loading and cause the yield surface to translate by the increment
d£y(c*i, of2, of 3 ,...). The order in which the recovery of individual events at occurs
during reverse loading determines the type of kinematic hardening.
If ai,«2» a3> e^c- (which are the microstructural variables determining the flow
strength) are viewed as being the plastic strains in the various sub-elements, then
one has the situation where the recovery has the sequence 2a l5 2a 2 , 2a 3 , etc. In other
words, element 1 deforms plastically twice as much in compression before element 2
yields as it did originally in tension. It is also implied here that (3cr/da1) is not a
function of a 2 , a 3 , etc. and likewise for (9<r/da2), (3or/da3), etc. This sequence, when
represented by a stress-strain plot, results in the type I behavior schematically shown
as loop OABCDEGHJB in Fig. 3.8(&). The type I kinematic hardening model ratio-
nalizes the Bauschinger effect in a number of alloys with shearable precipitates. In
these materials, dislocation cells are envisioned as the elastic-plastic elements which
generate the internal stress systems. The type I sub-layer model has also been found
106 Cyclic deformation in poly crystalline ductile solids
Fig. 3.9. (a) Representation of the stress-strain curve by regions of constant tangent moduli, (b)
Representation in stress space. (After Mroz, 1967.)
identical to that of EHK. Upon reaching point E, deformation follows a steady cycle
EHKNE.
Mroz also extended the above model to situations involving nonproportional
multiaxial loading. As an example, consider the case where the specimen is unloaded
partially to a stress point Q inside So from the stress point E, Fig. 3.9(6), whereupon
the stress point moves along QR contacting the surface So at T. The surface So must
move such that the point T makes contact with the surface S^ without intersecting it.
(Therefore, translation will not occur along the normal at T, i.e., along the extra-
polation of O0T.) Thus T will move to a point U on S}. As the stress point moves
along 77?, the surface So will touch Sx at W and subsequently they move together to
touch S2 at Z and so on. When the stress path meets the surface S4, the work
hardening modulus on the loading path becomes equal to that at E.
Mroz's geometrical model can be mathematically stated using a typical situation
sketched in Fig. 3.10. Si and Sl+{ are two yield surfaces whose centers are at O{ and
3.8 Continuum models for uniaxial and multiaxial fatigue 109
Fig. 3.10. Two yield surfaces Si and *S/+1; the translation of surface 5/ along PR is defined by its
relative position with respect to S[+l. (After Mroz, 1967.)
O/+1, respectively. These centers are defined by the position vectors $$ and ^ / + 1 \
respectively, from the origin O. Sj and 5/+i, respectively, are defined by the following
equations:
Pii - 4°
4°) - (otfV1 = 0, (^ - 4/+1)) - {4 =0, (3.15)
l
where/ is a homogeneous function of order nx of its arguments and a 0 and <TQ/+1) are
constants. If P lies on the surface Sh the instantaneous translation of S[ will occur
along PR, where R is a point on S /+1 corresponding to the same direction of outward
normal. The position of R is determined by drawing from O/+1 a vector Oi+\R
parallel to OjP. From the homogeneity of/ in Eq. 3.15 and by denoting the stresses
at P and 7? by off and oV+l\ respectively, one obtains
(3.17)
The parameter d^ is obtained from the continuity condition that the stress point
remain on the yield surface,
l ; r - = 0. d<7 = (3.18)
The Mroz formulation captures many of the salient features of uniaxial fatigue
deformation described earlier in this section. However, it does poorly for asymmetric
cyclic deformation (White, Bronkhorst & Anand, 1990).
Fig. 3.11. Schematic illustration of the line bounds in stress-strain space. (After Dafalias «
Popov, 1975.)
3.8 Continuum models for uniaxial and multiaxial fatigue 111
value of Ep changes from point G to point H. The third part HX' also represents
plastic behavior; however, Ep has a constant value in the region. This third part lies
on lines such as XX' or YY' which provide bounds.
Dafalias & Popov postulated that the instantaneous value of the plastic modulus
Ev is determined by (i) the relative position of the current plastic loading point with
respect to the bounding line (<5ys in Fig. 3.11) and (ii) the amount of plastic work,
wp = Jcrde p , accumulated during plastic deformation prior to the elastic deforma-
tion preceding the current plastic state. The value of 8ys at the initial yield point is <5in.
All loading states lying on a line drawn parallel to XX' in Fig. 3.11 have the same
values of 8ys and Ep.
The generalization of the above model to multiaxial loading conditions in stress
space is schematically illustrated in Fig. 3.12. This figure shows two circles, where the
inner circle with its center at k represents the loading surface and the outer circle with
its center at r represents the bounding surface. Let point a on the loading surface
represent the current plastic state of the material. Given point a, there is a corre-
sponding point b on the bounding surface, and the distance between a and b, denoted
as 8ys, determines the value of the generalized plastic modulus at point a for the
multiaxial case. Point b can be defined in a number of ways: (i) if the two surfaces are
congruent, b can be taken as the point determined from the condition of congruency
with respect to a; (ii) b can be obtained by the intersection of the normal to the
loading surface at a with the bounding surface; or (iii) b can be taken as the point of
intersection of the line drawn through ka with the bounding surface, as shown in Fig.
3.12. If ay are the coordinates at a and a* are the coordinates at b, the distance, <Sys,
can be denned as
Let K be the generalized plastic modulus for the multiaxial case. Assuming the
associated flow rule, Eq. (1.25), and that the plastic strain increment dep is proper-
Fig. 3.12. Schematic illustration of the loading and bounding surfaces in stress space and of the
motion of these surfaces during multiaxial loading. (After Dafalias & Popov, 1975.)
112 Cyclic deformation in poly crystalline ductile solids
tional to the projection da of the stress increment da^ on the unit normal co to the
loading surface,
del-= ^ w t j . (3.20)
In Fig. 3.12, c is the point on the bounding surface where the outward normal to it
lies on the same direction as the normal to the loading surface. If m is the unit vector
along the line that joins a and c, the translation of the bounding surface along m
fulfills the condition that the point of contact is also the current stress state.
Dafalias & Popov formulated various conditions for the deformation and transla-
tion of the loading surface as well as of the bounding surface according to different
hardening rules, particularly with reference to well known kinematic hardening rules.
In general, the inner yield surface is taken to follow kinematic hardening rules while
the outer yield surface follows isotropic hardening. The use of the two-surface model
to rationalize cyclic creep is illustrated in Section 3.9.
Modifications of the two-surface models of cyclic plasticity have been examined by
Moosbrugger & McDowell (1989) within the context of various isotropic and kine-
matic hardening formulations. These workers also show that the two-surface models
for rate-independent plasticity offer superior correlation with experimental data on
nonproportional cyclic deformation in stainless steels.
{a) (b)
Fig. 3.13. Cyclic creep under (a) tensile and (b) compressive mean stress.
114 Cyclic deformation in poly crystalline ductile solids
Fig. 3.14. A rationale for the occurrence of cyclic creep in terms of the bounding surface
concept. (After Dafalias & Popov, 1975.)
Therefore, from Section 3.8.3, the plastic modulus is smaller for the stress states lying
on the loading paths k2o2 than for the ones on kxox. The cyclic loops, therefore, are
not closed and they progressively shift to the right of the strain axis as shown in Fig.
3.14. This argument thus provides one rationale for the occurrence of cyclic creep.
With continued shift to increasing mean strains, the distance between a = k\ and
XX' and that between a = k2 and YY' tend to become equal. At this point, the
plastic moduli also become equal and the loops become stabilized.
Cyclic creep or ratchetting has major implications for fatigue in a variety of
engineering applications. For example, in rolling or sliding contact fatigue, combi-
nations of high normal and shear tractions are imposed on a thin layer of material
near the contacting surfaces. Within this layer, which is 10-50 jim thick in gears and
bearings and about 2 mm thick in railway track, shear strains as high as 100% are
accumulated with repeated applications of the load. Under conditions of free rolling
or low traction (where the traction coefficient, i.e. the ratio of the shear to the normal
traction, /xt < 0.25), an unsymmetrical cycle of shear is imposed on the highly
deforming region which is confined beneath the surface. For high traction
(/xt > 0.25), on the other hand, the critically stressed material lies at the surface.
For this latter case, the material is subjected to a nonproportional load cycle which is
made up of tension, followed by shear, followed by compression. An example of the
application of cyclic creep models to contact fatigue problems is found in the work of
Bower & Johnson (1989), who employed phenomenological nonlinear kinematic
hardening models for analyzing the effects of strain hardening on cyclic creep con-
tact fatigue. Further discussions of cyclic creep and ratchetting can be found in
Section 13.4.4.
3.10 Metal-matrix composites subjected to thermal cycling 115
IA71
D F Time
(b)
Fig. 3.15. (a) Geometry of the representative volume element for the thermal cycling analysis for
the metal-matrix composite, (b) Thermal loading history.
116 Cyclic deformation in poly crystalline ductile solids
r{ < r < ro. T h e v o l u m e fraction of the ceramic particle is, / p = (rj/r o ) 3 , while t h a t
occupied by the metal is (1 -fv). The concentration of the particles,/p, can be dilute
or nondilute with only the proviso that the particles be well dispersed within the
matrix without forming an interpenetrating composite. For the small strain analysis
considered here, the radial and tangential strains are related to the radial displace-
ment u by
^ + ?(<xr-or,) = 0. (3.22)
If both the matrix and the particle initially deform elastically,t the stress-strain
relations are written as
J'^^ (3.23)
where E is Young's modulus, v is Poisson's ratio, and a is the thermal expansion
coefficient, with the subscripts 1 and 2 denoting the matrix and the particle, respec-
tively.
Consider a uniform change in temperature, AT, from an initial stress-free tem-
perature. For an increase or a decrease in temperature, A 7 > 0 o r A T < 0 , respec-
tively. For this pure thermal loading case, where the composite is free of any external
kinematical constraint, the appropriate outer boundary condition for the volume
element in Fig. 3A5(a) is that ar = 0. The stresses in the spherical particle are then
readily determined from straightforward thermoelastic analysis to be
2El (a2-ax)(l-fp)AT
v P cr p p 5 (3.24)
3(1-
the maximum effective stress develops at the interface which is the site for the onset
of plastic flow. The temperature change necessary to initiate plastic flow at the
interface, A7"1? is found by setting (crQ)l = ay at r = ri? where ay is the yield strength
of the matrix:
(3.28)
This equation provides a direct connection between the size of the plastic zone rp and
the magnitude of thermal strain (a2 — a{)ATi, and reduces to Eq. 3.28 when rp = r{.
As the plastic zone continues to spread under a monotonic temperature change
| AT|, another critical value of | AT|, which we shall term | A7"31, is reached at which
the entire matrix becomes plastic. The magnitude of AT3 is determined by setting
rp = ro in Eq. 3.29:
- v O f l 2M eli 1
(3.30)
3
-«ill/P J
Now consider temperature cycles, 0 < |A7"| < ATa, commencing at the stress-free
temperature,! Fig. 3.15(&). The first unloading in the thermal cycle corresponds to
the excursion from point A to point B.
If the yield strength of the matrix is the same in tension and compression, it can be
readily shown that there exists a characteristic temperature change, AT2 = 2AT1?
' Equations 3.28 and 3.30 pertain to thefirstthermal loading ramp from | AT| = 0 to \AT\ = ATa (point
A in Fig. 3.15(6)). In general, AT and ATa can be positive or negative. For simplicity, we consider
positive values of the characteristic temperatures in subsequent discussion.
118 Cyclic deformation in poly crystalline ductile solids
below which a zone of reverse plasticity does not occur. In other words, if
|A7a| < AT2, there is no accumulation of plastic strains during thermal cycling.
Therefore, A T2 represents a shakedown limit for the thermal fatigue of a metal-
matrix composite. For \AT.d\ < AT2, only elastic conditions prevail after the first
unloading (i.e. after point B).
If, on the other hand, |ATa| > AT2, a zone of reversed plastic flow of radius rc
develops at the particle-matrix interface. Repeated thermal cycling causes rc to
expand outward. Referring to Fig. 3.15(6), if the temperature is first increased
(decreased) from some initial stress-free temperature (point O) to a maximum (mini-
mum) value at point A, and then decreased (increased) to the current temperature
A T, the size of the reversed or cyclic plastic zone rc is given by
\(a2-al)(AT!i-AT)\ =
2iog
ftH 6
2<7y(l —^ i ) [ i - c i n - i " i i _ _ i ' c i , - i i / - c \i
The right hand sides of Eqs. 3.29 and 3.31 differ only by a factor of 2 and by a
( 3 31)
change from rp to rc. A remarkable feature of Eqs. 3.28-3.31 is that both the
monotonic and cyclic plastic zones initiate at the particle-matix interface and spread
monotonically outwards during cyclic variations in temperature.
As the cyclic plastic zone spreads outwards, there exists another critical tempera-
ture at which the entire matrix begins to undergo reversed plastic yielding. This
characteristic temperature AT4 is obtained by setting rc = r0 in Eq. 3.31, from
which it is readily seen that AT4 = 2AT3. Figure 3.16 schematically shows the
spread of rp and rc for different values of A Ta with respect to the various character-
istic temperatures.
For the uniform spatial distribution of spherical particles, the conditions that
\AT{\ < \AT2\ and that lAT^I < |Ar 3 | always hold. However, the condition that
IA 721 < IA 7^ | need not always be true, i.e. the first monotonic temperature change
from O to A in Fig. 3.15(6) may cause complete yielding of the matrix with no cyclic
plastic zones induced upon subsequent unloading (from A to B). From Eqs. 3.28 and
3.29 and from the condition for shakedown (AT2 = 2 A 7^), it can be shown that
there exists a critical concentration of the reinforcement, / p = /p*, at which
A 7^ = A 7*3, which obeys the equation:
The value of/p is unique for afixedcombination of the matrix and reinforcement,
and is bounded by 0.203</p <0.586. If/p > / p , AT2 > AT3, and the composite
matrix undergoes no plastic strain accumulation during thermal cycling, although
the matrix is fully yielded during the first thermal excursion from the initial stress-
free state.
3.10 Metal-matrix composites subjected to thermal cycling 119
\ATa\ < A77! ATX < |Ar a | < AT3 AT3 < \ATt
(b)
(c)
AT3 < \ATa\ < AT2 A7\ < \ATa\ < AT4 AT4 < \ATa\
Q elastic response
£ 2 plastic zone (monotonic)
8 2 reversed plastic zone (cyclic)
Fig. 3.16. The evolution of monotonic and cyclic plastic zones at different temperature
amplitudes, (a) Monotonic thermal loading corresponding to point A in Fig. 3.15(7?).
(b) Temperature cycling for AT2 < AT3 corresponding to points B, C, D,... in Fig. 3.15(6).
(c) Temperature cycling for AT2 > AT3 corresponding to points B, C, D,... in Fig. 3.15(6).
(3.33)
Since the radial stress and the effective stress (and hence the tangential stress) are
continuous across the plastic zone boundary, the plastic strains are also continuous.
120 Cyclic deformation in poly crystalline ductile solids
From Eq. 3.33, the effective plastic strain is found which, for the present geometry,
reduces to
1
g (3.35)
because of proportional plastic strains. At the initial stress-free temperature (point
O), 4 = 0.
Beginning with the first thermal excursion O-A, the accumulated plastic strain is
found by substituting Eq. 3.34 in Eq. 3.35 and integrating Eq. 3.35:
,,<,<,„. ,3.36)
The reversed flow zone size rc in Eq. 3.38 is given by Eq. 3.31. The first term on the
right hand side of Eq. 3.38 gives e^ T during the first temperature excursion from O
to A, and the second term gives the accumulated value in the next (NT — 1) tem-
perature reversals. It should be noted that the rate of plastic strain accumulation in
Eqs. 3.37 and 3.38 is the same, i.e. the second terms on the right hand side of these
two equations are identical. Thus, the difference in the magnitude of the accumu-
lated plastic strain is only that due to the difference developed in the first tempera-
ture excursion.
(1) For cycling between fixed temperature limits, the four characteristic tem-
peratures, ATh / = 1 , . . . , 4 , are constants for an elastic-ideally plastic
matrix. For a strain-hardening matrix, however, these temperatures change
with the number of thermal cycles; they can still be defined based on the
plastic strain distribution.
(2) The accumulation of plastic strain near the particle-matrix interface
increases the flow strength of the hardening matrix. Further accumulation
of plasticity is thereby suppressed.
(3) The result of the preceding section that plastic strain accumulation occurs
only within the cyclic plastic zone, still applies to the hardening matrix. The
rate of accumulation, however, is affected by the hardening rate.
Consider a matrix alloy with isotropic, linear strain hardening //, which
captures the cyclic hardening characteristics of the matrix. The matrix yield
strength ay is now modified to include hardening in the following way:
cry +Heller). Let H = 27/(1 - vx)/Ex. It can be readily shown (Olsson,
Giannakopoulos & Suresh, 1995) that the plastic strain increment during each
load reversal is explicitly given by
For H = 0 (no hardening), the results of the preceding section are recovered. An
examination of Eq. 3.40 reveals that Aej^ 7 -> 0 as NT -> oo. Therefore, unlike the
case of an ideally plastic matrix for which the plastic strain accumulation during
thermal fatigue is unbounded, the accumulated plastic strain for a strain-hardening
matrix asymptotically approaches a limiting value at large numbers of thermal cycles
in the following manner:
(^)3|[(^)3] (3-40)
where Ae^ 1 is the plastic strain accumulated after the first thermal excursion. The
limiting strain in Eq. 3.40 has a maximum value at the particle-matrix interface. If
the ductility of the matrix alloy exceeds this maximum value, an endurance limit for
thermal fatigue is expected. This temperature endurance limit is higher than A T2
because of strain hardening.
All of the foregoing analytical results pertain to situations where Eu v1? a1? a2,
ay and H are temperature-independent. The same approach can be adapted for
analyzing thermal fatigue by including the temperature-dependence of these prop-
erties by recourse to numerical simulations (see, for example, Olsson et al.,
1995).
122 Cyclic deformation in poly crystalline ductile solids
(i) Substituting the numerical values of the various terms in Eq. 3.28, we
find that the temperature change, from the initial stress-free temperature
(250 °C) at which plastic yielding begins is: | AT^ | = 172 °C, i.e. at 250 -
172 - 78 °C.
(ii) To find the plastic zone radius rp for a temperature change of
\AT\ = 225 °C, replace A ^ in Eq. 10.2 by \AT\. Substituting the appro-
priate numerical values for |A!T| and the various material parameters, it
is seen that
/r\3 /r\ 3 /r\3
1.0467M -0.2333 log -^1 =1.0644, or U « 1.025. (3.41)
\ri/ Vi/ VJ
The volume fraction of the matrix which has undergone plastic yielding
upon cooling from the processing temperature to room temperature is:
J J /• f A. \ 3 1
-1 . (3.42)
Substituting the value of rp from Eq. (2) into this equation, it is seen that
Kpl « 0.63%.
(iii) We note that the characteristic temperature change below which a zone
of reversed plastic flow does not develop in the matrix is:
|AT 2 | = 2|A7^!| = 344 °C. Since the temperature range for thermal
cycling |AT| = 225 °C < |AT 2 |, it is apparent that repeated thermal
cycling between room temperature and the processing temperature will
not lead to any continued accumulation of plastic strains in the matrix,
(iv) (a) As the yield strength decreases with increasing temperature, both A 7^
and A T3 will be lowered compared to the case where the yield strength is
independent of temperature, (b) The monotonic plastic zone size, rp,
increases because of the lower yield strength at higher temperatures.
There is a corresponding increase in the volume of the matrix material
which has undergone plastic yielding.
' Near the free edges of the bilayer where the interface intersects the free surfaces, the stresses have to be
modified locally so as to satisfy the stress-free boundary conditions at the free surfaces of the uncon-
strained bilayer plate. Consequently, there develops a three-dimensional stress state which comprises
both in-plane and out-of-plane normal and shear stresses. The size of this 'edge zone', measured from
each edge, is of the order of the total layer thickness. The analysis presented in this section is valid only
away from this edge-zone.
3.11 Layered composites subjected to thermal cycling 125
layer 1
layer 2
(a)
|AJC|
onset of
inelastic deformation ideally plastic
\
elastic ^^ If
' ^ elastic
residual
curvature
X 1
unloading
onset of reverse
inelastic deformation
1 _ i\AT\
(b) AT3
Fig. 3.17. (a) Geometry of the bilayer and the associated nomenclature, (b) Schematic
representation of the variation of curvature with temperature for a metal-ceramic bilayer where
the metallic layer is elastic-perfectly plastic. All material properties are assumed to be
independent of temperature.
The thermoelastic strain in the bilayer, in regions away from the free edges, con-
sists of two parts: (i) an in-plane normal strain, e0, which arises from a uniform
stretch or contraction, and (ii) the strain due to bending, KRZ, where z is the thickness
coordinate:
€xx(z) = eyy{z) = e(z) = eo + KRZ. (3.43)
The subscripts T and '2' refer to quantities associated with layers 1 and 2, respec-
tively, in Fig. 3.11 (a). Static equilibrium dictates that the net force and the net
126 Cyclic deformation in poly crystalline ductile solids
moment arising from the stresses in Eq. 3.44 should be offset by any externally
imposed force Fap and moment, M ap . For the unconstrained bilayer plate subjected
only to a uniform temperature excursion, these force and moment equilibrium con-
ditions give:
and
(3-49)
Note that the stresses vary linearly with z within each layer to a maximum value at
the interface, and that there occurs a sharp jump in the magnitude of the stress at the
interface between the two layers. While the foregoing analysis pertains to a bilayer,
the same approach can be used to analyze the thermoelastic deformation of a multi-
layer comprising any number of layers. In such a case, the equilibrium equations, Eq.
3.45, can be solved numerically using a personal computer where additional effects
3.11 Layered composites subjected to thermal cycling 127
In addition, Eqs. 3.48 and 3.49 give, for the thin-film limit,
O\\z=zhx ^ —Eiipt\ —a2)AT, and cr\\z=o ^ —Ei{ot\ —a2)AT. (3.51)
In other words, the equi-biaxial stress in the thin film is essentially uniform. It is also
readily seen from Eq. 3.49 that, for hx <^ h2, the magnitude of the stresses in the thick
substrate is very small.
Combining Eqs. 3.47 and 3.51, and denoting the various parameters associated
with the film and the substrate with the subscripts 'film' and 'sub', respectively,
(3.52)
' In view of its simplicity, the Stoney equation, Eq. 3.52, is commonly used to determine the thin film
stresses in the microelectronics and structural coatings industries where scanning laser interferometry
methods are widely used to determine the radius of curvature of the thin-film/substrate system before
and after thermal excursions.
128 Cyclic deformation in poly crystalline ductile solids
shaped on the thin-film side (i.e. positive /cR), then the stress in the film should be
compressive. From Eq. 3.50, we see that such a situation arises when the coefficient
of thermal expansion of thefilmis higher than that of the substrate and the bilayer is
subjected to heating from a stress-free initial reference temperature.
(3 53)
-
where the various parameters are defined in Eq. 3.48.
If now the temperature continues to change monotonically beyond lAT^I, the
plastic zone which initiates at the interface spreads outwards to the free surface of
the metallic layer. After a further temperature change, there occurs a critical condi-
tion, \AT\ = \AT3\ that the entire metallic layer becomes fully plastic, where
(3.54)
If the metallic layer does not strain harden, this limit temperature for full yielding
also signifies the condition for a limiting curvature, /cR L. That is, any further change
in temperature beyond lAT^I does not cause any change in the curvature of the
bilayer. This limiting curvature is
Exercises 129
h T , , , , , , (3-55)
"2^2
Exercises
3.1 It was shown in Chapters 1 and 2 that the resolved shear stress in a single
slip system is related to the applied stress by the Schmid factor, M. For a
poly crystal, a = M T r, where M T is commonly referred to as the Taylor
factor. The value of M T is computed such that the continuity of slip at
the grain boundary satisfies the requirement for five independent slip sys-
tems to operate in each grain. The values of MT are computed by invoking
the principle of virtual work. Convince yourself, by consulting appropriate
130 Cyclic deformation in poly crystalline ductile solids
(b) Show that the so-called 'permanent softening' is expected only in one of
the two cases and that the amount of permanent softening is equal to
twice the internal back stress in the soft elements.
(c) Considering both cases, can permanent softening be considered an
unambiguous measure of the back stress?
(d) Describe the occurrence of the Bauschinger effect in terms of deforma-
tion-induced internal stresses and the yielding of the softer elements
upon load reversal.
3.8 Discuss the effects of cyclic strain hardening on the shakedown limit derived
in Section 3.10.2 for the metal-matrix composite subjected to thermal cycling.
3.9 An aluminum film, 1 urn in thickness, is deposited onto a silicon substrate
which is 500 fim thick and 100 mm in diameter. The isotropic properties of
Al and Si are: EAl = 66 GPa, vA1 = 0.33, aM = 23 xlO'6 °C~\ Esi = 130
GPa, vsi = 0.28, asi = 3xl0~ 6 °C~1. At some reference stress-free tem-
perature, this thin-film/substrate system is flat (i.e. zero curvature). This
bilayer is now uniformly cooled by 50 °C.
(a) What is the average stress in the aluminum film?
(b) Is it tensile or compressive?
(c) Describe the direction in which the bilayer bends during the above
thermal excursion.
(d) If the yield strength of the thin aluminum film is 140 MPa, what is the
temperature change needed to cause plastic yielding in the aluminum
film?
(e) If the thin-film/substrate system is thermally cycled between the stress-
free initial temperature and some high temperature TcyciQ9 what is the
minimum value of r cycle needed to induce fully reversed plastic flow in
the entire aluminum film?
3.10 A 50 mm x 50 mm bilayer plate is made by diffusion bonding a plate of pure
Ni, 3 mm in thickness, to a plate of pure A12O3, 2 mm in thickness, at
827 °C. The isotropic properties of Ni are: Em = 214 GPa, vNi = 0.31,
and a Ni = 17.8 xlO" 6 °C" 1 at 827 °C and 13.4 xlO" 6 °C" 1 at 20 °C. The
yield strength of Ni as a function of temperature, <7yNj(r), are: 148 MPa
(20 °C), 140 MPa (227 °C), 115 MPa (427 °C), 69 MPa (627 °C) and 45 MPa
(827 °C). The isotropic properties of the polycrystalline A12O3 plate are:
£AI 2 O 3 = 380 GPa, vAl2o3 = 0.25, and aAl2o3 = 9.4 x 10~6 °C~l at
827 °C and 5.4 x 10"6 °C~l at 20 °C. You may ignore the strain hardening
characteristics of Ni for the purpose of this problem.
(a) If the bilayer is uniformly cooled to room temperature (20 °C), what is
the temperature at which plastic yielding begins during cooling from the
bonding temperature?
(b) Is it possible to cause yielding of the entire Ni layer before reaching the
room temperature?
CHAPTER 4
132
4.1 Surface roughness and fatigue crack initiation 133
where slip bands emerge at the free surface. The valleys so generated function as
micronotches and the effect of stress concentration at the root of the valleys
promotes additional slip and fatigue crack nucleation.
Fig. 4.1. (a) Intrusions and (b) extrusions along slip bands in polycrystalline Cu fatigued at
-183 °C. (From Cottrell & Hull, 1957. Copyright The Royal Society, London. Reprinted with
permission.)
134 Fatigue crack initiation in ductile solids
form of an extrusion at the specimen surface. Although Mott's proposal formed the
basis for a number of subsequent models for surface roughening, its basic feature
that screw dislocations travel in a closed circuit has not been convincingly substan-
tiated by experiments. Kennedy (1963) emphasized the need for a gating mechanism
which would modify the forward-reverse oscillations of screw dislocations into irre-
versible displacements. The formation of obstacles to dislocation motion, such as
creation of jogs as a consequence of edge-screw intersections and the intersection of
two screw dislocations with a third dislocation at a node in a free surface, have all
been suggested as possible gating mechanisms which would provide net irreversible
slip during fatigue (see Lin & Lin, 1979 for a critical review).
The first quantitative statistical model for random slip leading to the formation of
hills and valleys on fatigued surfaces was published by May (1960a,b) who adapted a
variation of Mott's cross slip mechanism. The assumption here is that the reverse
glide of dislocations is shifted from the forward path in a random manner. If the
amount of this shift is comparable to the width of the slip band, this is tantamount to
stating that random distribution of slip in each half-cycle is independent of the
distribution in the previous cycles. Thus, hills and valleys are formed on the surface,
with subsequent slip concentrating in the valleys in proportion to their depths. May
assumed that if f(z, N) is the fraction of the valleys (of width w) with a depth
between z and z + dz after TV cycles of fatigue, /(z, N) obeyed a diffusion equation
where k and fi are factors of the order of unity, b is the magnitude of the Burgers
vector, and y is the plastic strain in the slip band which is equivalent to yPSB in Eq.
2.9. Solving Eq. 4.1, May showed that
where F is a slowly varying function of z and N. For small values of N, the exponential
factor is very small and the deepening of the valleys would not be significant. The main
criticism of this statistical model is that it does not contain a sufficient number of
physical variables which incorporate the random slip process in a realistic form.
Cu single crystals, ypl and the slip offset (denoted by ndb, where nd is the number of
dislocations and b is the modulus of Burgers vector) were related by the expression,
y pl oc (ndb)m*. (4.3)
For Cu single crystals subjected to a plastic strain amplitude in the range of 10~3 to
10"2, mp ^ 0.78 and ndb = 0.3-3 urn.
A technique, known as the taper-sectioning method, introduced by Wood (1958),
has allowed high-resolution imaging of surface morphology in fatigued crystals. In
this method, the specimen is sectioned along a plane which is oriented at a small
angle a (i.e. a few degrees) to the specimen surface. The profile of the surface, as
observed on the sectioned plane, is magnified by a factor of (1/ sin a), over and above
the magnification obtained by other visual methods such as scanning electron micro-
scopy, optical microscopy and optical interferometry. Hunsche & Neumann (1986)
have refined this technique to obtain sections with sharp edges normal to the speci-
men surface so that the surface features can be recorded to a resolution of 20 nm in
the scanning electron microscope. Basinski & Basinski (1984), Hunsche & Neumann
(1986), and Ma & Laird (1989a,b) have utilized this method to examine the details of
surface roughening in fatigued Cu. Their results collectively indicate the following
general trends:
(1) The surface of the fatigued crystal is covered with PSB extrusions, intrusions
and protrusions. A protrusion is a surface uplift (a large extrusion), many
micrometers in height, where a macro-PSB, tens of micrometers wide and
containing tens of matrix and/or PSB lamellae, emerges at the free surface.
A protrusion may contain several intrusions and extrusions. Figure 4.2 is a
scanning electron micrograph obtained using the sectioning method which
Fig. 4.2. Protrusions with extrusions and intrusions on the surface of a Cu crystal fatigued at
room temperature for 120000 cycles at ypl = 0.002. (From Ma & Laird, 1989a. Copyright
Pergamon Press pic. Reprinted with permission.)
136 Fatigue crack initiation in ductile solids
The contour of a PSB profile, imaged directly by focusing on the specimen edge, is
provided in Fig. 4.3. This figure shows a protrusion on the side surface of a Cu
specimen fatigued at 77 K for 35 000 cycles at ypl = 0.002. The loading axis is along
the vertical direction and b is the direction of the primary Burgers vector. A similar
extrusion/protrusion is found on the opposite side of the crystal (not shown in Fig.
4.3).
Numerical simulations of the random slip processes have also been attempted to
quantify the extent of surface protrusions produced by fatigue. Differt, Essmann &
Fig. 4.3. The contour of a PSB profile created in a Cu crystal. (From Differt, Essmann &
Mughrabi, 1986. Copyright Taylor & Francis, Ltd. Reprinted with permission.)
4.2 Vacancy-dipole models 137
7
5RH
:i
1-
2- nzi
(a)
S ^ interface
dislocation
Fig. 4.4. (a) The critical annihilation distance for screw and edge dislocations, (b) Mechanism of
extrusion formation by combined glide and dislocation annihilation, (c) Irreversible slip in the
PSB creating effective interfacial dislocations which put the slip band in a state of compression.
(d) The combined effects of applied stresses and internal stresses. Bigger arrows indicate
repulsive forces on interfacial dislocations and smaller arrows denote forces caused by the
applied load. (After Essmann, Gosele & Mughrabi, 1981.)
hilation, the to-and-fro motion of dislocations within the walls and channels of the
PSB would be reversible and no permanent changes in surface topography would
result. Essmann et al. propose the following sequence of events:
(a) Dislocations that are generated at dislocation sources (e.g., point S in Fig.
4.4(6)) are terminated by mutual annihilation before the reversal of strain.
(b) The annihilation of vacancy-type dipoles, shown in Fig. 4.4(7?), is the dominant
point defect generation process. Dislocations moving during the tensile portion of
the fatigue cycle are denoted by solid symbols and those moving during the com-
pression portion by open symbols. During tensile loading, slip is transmitted across
the specimen by the sequence of microscopic processes extending from A to A'.
(c) At locations where the edge dislocations are annihilated (e.g., the PSB walls in
Cu), the plane on which slip is dominant is changed because of the annihilation
process. Therefore, the effective slip plane A-A' is not parallel to the primary
Burgers vector b, but is slightly inclined to b. Slip steps are created at surface loca-
tions A and A' during the tensile portion of fatigue.
(d) On reversing the strain into compression, slip steps are formed at B and Bf by a
similar process. The steps A-B and A'-Bf thus constitute an extrusion. If interstitial-
type dipoles, rather than vacancy-type dipoles, are considered, then intrusions,
rather than extrusions, form by a process analogous to that described in Fig. 4.4(6).
(e) The extrusion in Fig. 4A(b) ceases to grow when the concentration of vacancies
formed by edge dislocation annihilation attains a saturation value, [Cv]sat
(%3x 10~4 for Cu), within the slip band. At saturation, the effective slip plane no
longer deviates from b.
if) While Fig. 4.4(6) illustrates the formation of extrusions by two microscopic slip
processes, Fig. 4.4(c) schematically shows this phenomenon for the situation invol-
ving the superposition of multiple slip processes. The path X-Y denotes the zig-zag
glide of a combined slip process aided by annihilation, just as in Fig. 4.4(6). For
clarity, the other paths are merely represented by straight lines. These lines join edge
dislocations which have either survived the annihilation process and arrived at the
free surface or have been deposited at the PSB-matrix interface. These latter inter-
face dislocations have the same sign and give rise to internal stresses. Thus, the net
result of the irreversible slip process after one cycle is a row of edge dislocations at
the PSB-matrix interface. The extra half planes of atoms of these edge dislocations
face into the PSB.
(g) If all the interface dislocations emerge at the free surface, the resulting surface
roughness of the PSB lamellae in the direction of the active slip vector is given by
e = [Cv]sar4>/cos0, (4.5)
where d0 is the diameter of the crystal and 0 is the angle between b and the specimen
surface. If all the dislocations remain at the PSB-matrix interface, the mean separa-
tion S[ of the interface edge dislocations is
(4.6)
140 Fatigue crack initiation in ductile solids
Taking typical values for b and [Cv]sat f° r Cu, one obtains s-x ^ 1 urn.
(h) The arrangement of interface dislocations in Fig. 4A(c) leads to an elastic
compressive stress within the PSB acting along b and to a tensile stress in the matrix
adjoining the PSB. Essmann et al. estimate that this compressive stress in the PSBs is
of the order of 2MPa for Cu.
(f) The combined effect of the applied stress and the internal stress produced by
the interface dislocations is shown in Fig. 4A(d). The bigger arrows denote the
internal stress arising from the mutual repulsions of the interface dislocations. The
smaller arrows refer to the stress resolved in the direction of the PSB due to the far-
field axial load, which reverses sign during every half fatigue cycle. Thus, A and A'
serve as stress concentration points in tensile loading where the internal stress and
the applied stress combine to produce high local stresses. B and Bf are stress con-
centrating sites during compression where the two stresses oppose each other.
Starting with a set of initial assumptions similar to those of Essmann et al.,
Antonopoulos, Brown & Winter (1976) developed a model of dislocations at PSB-
matrix interfaces by considering a continued increase in the density of vacancy
dipoles during fatigue. Their approach is different from the foregoing model of
Fig. 4.4 in that Antonopoulos et al. did not consider the annihilation of vacancy
dipoles (which are continually replenished) to form vacancies. They concluded that
the material in the PSB isfiber-loadedin tension parallel to b after the attainment of
cyclic saturation. This prediction is contradictory to that of Essmann et al. A pos-
sible clue to this apparent contradiction can be obtained by noting that both models
assume the sign of the internal stress to remain unchanged during fully reversed
loading. Brown & Ogin (1985) have pointed out that if the effective slip plane
does not switch (from A—A to B—B! in Fig. 4.4) as the applied load is changed
from tension to compression, then the internal stress also changes sign. Despite
their differences, both models clearly pinpoint the significant role of vacancy dipoles
and interfacial dislocations in promoting surface roughness. Both groups of authors
also propose that cracks initiate at the surface steps created at the PSB-matrix
interface. This prediction is consistent with a variety of experimental observations,
to be described in Section 4.3.
Micromechanical models have also been proposed to describe the formation of
intrusions and extrusions on the surfaces of metals due to glide on parallel planes
(Lin & Ito, 1969; Lin & Lin, 1979; Tanaka & Mura, 1981). A feature common to
these analyses is the assumption that the forward and reverse slip displacements
during a fatigue cycle are accommodated within two closely-located, parallel layers,
i.e. the most favorably oriented slip planes. Such an assumption apparently finds its
basis from the experiments of Forsyth (1953) and Charsley & Thompson (1963), who
found that the slip plane accommodating plastic deformation during the forward
(tensile) loading and the one during reversed (compressive) loading are closely
spaced, but distinct from each other. Both slip planes are still part of the same
slip band.
4.3 Crack initiation along PSBs 141
clearly established that, in materials that form PSBs, crack nucleation and early
crack growth occur in the PSB. Figure 4.6 is a TEM image showing two PSBs (of
length ~ 100 jam, which is comparable to the grain size) in a Cu specimen where a
surface layer, approximately 2 jam thick, containing intrusions has been removed by
electropolishing. A nascent crack is seen within one of the PSBs and the presence of
the crack does not appear to modify their dislocation structure. An optical micro-
graph of the crack is also shown in the inset. A similar TEM image of the Cu
specimen obtained by Katagiri et al. also revealed cracks nucleating along the
PSB-matrix interface at the root of a surface intrusion.
20 jim
electron
diffraction pattern
Fig. 4.6. A nascent fatigue crack along the ladder structure of a PSB in fatigued, polycrystalline
copper. Inset at left is an optical micrograph showing the location of the crack with respect to
the free surface. (From Katagiri et al., 1977. Copyright Metallurgical Transactions. Reprinted
with permission.)
4.5 Computational models for crack initiation 143
crystals, one would expect sufficient time to be available for such diffusive processes,
even at room temperature.
The evolution of vacancy concentration can then be estimated on the basis of the
following considerations and approximations (Repetto & Ortiz, 1997). (1) The stress
concentrations arising at the free surface by the roughening induced by the egress of
the PSB produces strain energy density gradients, which in turn promote stress-
assisted diffusion. (2) The vacancy concentration at the free surface remains at its
equilibrium value given by
where AGV is the incremental change in free energy per vacancy, k is Boltzman's
constant, and T is the absolute temperature. (3) An effective diffusion coefficient for
vacancy mobility by both pipe and lattice diffusion is determined from a rule-of-
mixture type approximation based on the dislocation density. (4) Since the screw
dislocations in the channels between the walls are parallel to the direction of vacancy
flux to the free surface, they are postulated to contribute more strongly to vacancy
diffusion than edge dislocations.
With the above line of reasoning, the flux of vacancies from the PSBs to the free
surface is expected to follow the diffusion equation:
where Z)lat and Dp[pQ are the lattice and pipe diffusion coefficients, respectively, I is
the identity tensor, b is the magnitude of the Burgers vector, ps is the density of screw
dislocations in the channels, s is the direction of the Burgers vector in the unde-
formed configuration of the crystal, R is the universal gas constant, and W is the
elastic strain energy density. The last term on the right hand side of Eq. 4.8 is the
vacancy generation rate defined in Eq. 2.31. The symbol Vo is the material gradient
operator defined such that (VQ/) 7 = 3//3X 7 , where (X{, X2, X3) refer to the material
reference frame defined with respect to the undeformed configuration of the crystal.
The term within the square brackets in Eq. 4.8 equals - J v , where J v is the vacancy
flux through the crystal.
The net outward flow of vacancies causes the surface of the crystal to move
inward, thereby forming an intrusion. The outward velocity of the vacancies,
relative to the undeformed configuration of the crystal, is Vv = J v /c v . If one
considers a small area on the undeformed surface of the crystal with a unit
outward normal N, the inward velocity of the surface region due to the egress
is VN = J v - N.f
' It is worth noting that the possibly significant process of annihilation of screw dislocations in the
channels is not taken into account in this formulation.
4.5 Computational models for crack initiation 145
|u,m
376.5 -
376.0 -
375.5
375.0 -
Fig. 4.7. Surface roughening in a [125] Cu single crystal oriented for single slip under symmetric
tension-compression loading with ypl = 6x 10~3. The figure shows the deformed mesh from the
finite-element simulation after about 65 000 cycles. (After Repetto & Ortiz, 1997.)
146 Fatigue crack initiation in ductile solids
AL Aa
where AL/L is the fractional change of the external edge dimension of the
crystal due to the introduction of the defects, and Aa/a is the fractional change
of the lattice parameter (as measured by X-ray diffraction) due to the defects.!
Solution:
In order to arrive at the desired result, carry out the operation of intro-
ducing vacancies in the crystal in the following steps:
Step 1:
Create the vacancies inside the crystal by taking atoms from the interior
and placing them on various free surfaces of the crystal. Apply, however, a set of
body forces around the vacant sites so that no strains develop due to atomic
relaxation. If Lt (i = 1, 2, 3) are the linear dimensions of the crystal, and if ALt
denote the corresponding changes in linear dimensions, the total fractional
volume change is
x 2
- V — _|_ _|_ J (A Q\
But,
a
^ Jstep2 L ^ Jstep2 L Jstep2
' The author thanks Professor R.W. Balluffi of the Massachusetts Institute of Technology for bringing
this problem to his attention.
4.6 Environmental effects on crack initiation 147
However,
3
Jstepl [irl = = 3 ^ 1 = 3[-1.
L ^ Jstep2
L ^ J total
'//////
tension '////MY
compression
V///////////
V
second tension WZW/'
incipient crack
Fig. 4.8. A model for fatigue crack nucleation near a free surface by the synergistic effect of
single slip and environmental interactions. (After Thompson, Wadsworth & Louat, 1956, and
Neumann, 1983.)
(1) Cross slip of screw dislocations and different paths for their forward and
reverse glide during a complete fatigue cycle.
(2) The extrusions, with a triangular cross section (base width ^ 1 — 2 um and
height ~ 2 — 3 |im), grow at rates of 1 — 10 nm (cycle)"1, whereas the growth
rate of protrusions is an order of magnitude smaller.
(3) Random distribution of slip (independent of prior history) with the progres-
sive, preferential deepening of valleys at surfaces.
(4) Dislocation-dislocation interactions leading to the formation of nodes, jogs
or dislocation locks which impede motion during part of a fatigue cycle.
(5) Production of point defects during saturation, due to the dynamic equili-
brium between dislocation generation and annihilation.
(6) Irreversibility due to shape changes (see Section 2.12.1) as well as differences
in dislocation back stress due to slip on different glide planes during the
tension and compression portions of fatigue.
(7) Reduction in slip displacement during unloading due to the adsorption of an
embrittling species or due to the oxidation of slip steps, and the attendant
creation of net slip irreversibility.
4.8 Crack initiation along grain and twin boundaries 149
20 nm |
Fig. 4.9. (a) Nucleation of flaws (denoted by arrows) along a grain boundary. (From Figueroa
& Laird, 1983. Copyright Elsevier Sequoia, S.A. Reprinted with permission.) (b) White light
interferograms showing slip-step formation at grain boundary in fatigued Cu. (From Kim &
Laird, 1978. Copyright Pergamon Press pic. Reprinted with permission.) The dark diagonal
lines parallel to the arrow are fiducial markers whose separation is 100 urn.
4.8 Crack initiation along grain and twin boundaries 151
in BCC single crystals. The surface roughness created by similar shape changes in the
near-surface grains of polycrystalline BCC metals, such as a-iron, can cause inter-
granular crack nucleation (Mughrabi, Herz & Stark, 1981).
The process of slip involves a simple translation of atoms across a glide plane such
that a rigid block of solid on one side of the slip plane moves with respect to the
other in the direction of slip. Slip occurs by translations in whole multiples of the
Burgers vector, so that the relative crystallographic orientation of different regions in
a slipped material remains the same. On the other hand, a twin boundary is a surface
where the atom positions in the twin on one side of the boundary are a mirror image
of those in the untwinned matrix material on the other side of the boundary.
Therefore, one observes a shape change in a twinned body.
Although twin boundaries are grain interfaces with the lowest energy, their role in
crack nucleation has long been known (e.g., Thompson, Wadsworth & Louat, 1956;
Boettner, McEvily & Liu, 1964; Neumann & Tonnessen, 1988). In FCC metals, twin
boundaries are parallel to the slip planes so that the PSBs can fit into the region of
high local stresses at the boundary. Therefore, the geometric relationship between
the boundary and the slip plane may provide possible clues to the role of twins in
fatigue crack nucleation. An intriguing aspect of fatigue crack nucleation at twin
boundaries is that, in a stack of lamellar twins, there is a propensity for slip bands
and cracks to form only at every other twin boundary (Boettner, McEvily & Liu,
1964). This trend has also been studied in greater detail in the context of annealing
twins formed in polycrystalline Cu, Ni and austenitic stainless steel (Neumann &
Tonnessen, 1988). Figure 4.10 shows an example of fatigue crack nucleation at every
other twin boundary in Cu fatigued at room temperature.
30 nm
Fig. 4.10. Nucleation of fatigue cracks along every other twin boundary (indicated by arrows) in
polycrystalline Cu fatigued at room temperature. (From Neumann & Tonnessen, 1988.
Reprinted with permission from P. Neumann.)
152 Fatigue crack initiation in ductile solids
Using the taper sectioning technique (discussed in Section 4.1.2) and electron
channeling method in the SEM, Neumann & Tonnessen have detected the orienta-
tions of grains and the nucleation of microcracks at twin boundaries in FCC metals.
They found that, at low imposed stress amplitudes, PSB formation within the grains
was suppressed. However, PSBs were found exclusively parallel to and coincident
with twin interfaces. Careful grain orientation measurements revealed that, even
when slip activity ceases within the interior of grains, slip bands are activated at
some twin interfaces as a consequence of local stress concentrations.
Neumann & Tonnessen have rationalized the observations of fatigue crack for-
mation at every other twin boundary utilizing a mechanism which relies on the
elastic anisotropy of the material containing the twins. For example, the shear
modulus of Cu varies with direction by as much as a factor of 3.2. In order to ensure
strain compatibility at twin boundaries in the elastically anisotropic material, inter-
nal stresses must be generated in the vicinity of the twin boundaries. Consider a stack
of lamellar twins, where the crystallographic orientation of the lamellae changes
back and forth from that of the matrix to the twin to the matrix as one traverses
across the boundaries. With the change in orientation, there is also a change in the
direction of internal stresses. The internal stresses act in concert with the resolved
stresses from the applied loads at every other twin boundary. When the resultant
stress is of sufficiently high magnitude, a PSB is formed near the twin-matrix inter-
face and eventually develops into a fatigue crack. At the alternate boundaries, the
internal stresses oppose the resolved stresses so that slip is obstructed. Neumann &
Tonnessen used this approach to predict the internal stressfieldin the vicinity of twin
boundaries using elasticity theory. Their simulation, in conjunction with electron
channeling measurements of orientation of grains, correctly predict the twin bound-
aries at which fatigue cracks are likely to nucleate.
Fig. 4.11. Scanning electron micrograph showing the nucleation of a fatigue crack normal to the
tensile axis (vertical direction) at the site of an MnO-SiO 2 -Al 2 O3 inclusion which is partially
debonded from the 4340 steel matrix denoted M. (From Lankford & Kusenberger, 1973.
Copyright Metallurgical Transactions. Reprinted with permission.)
154 Fatigue crack initiation in ductile solids
• Al 2 CuMg (S phase)
X Al 7 Cu 2 Fe(/3 phase)
£ 2
5 10 15
particle thickness (|im)
Fig. 4.12. Relative probability of crack initiation versus the constituent particle thickness
normal to the stress axis for S and f$ inclusions in 2024-T4 aluminum alloy. (After Kung & Fine,
1979.)
probability for the initiation of fatigue cracks at two different types of constituents,
S-phase and /3-phase particles, in a commercial 2024-T4 aluminum alloy as a
function of the particle thickness, measured in the direction normal to the stress
axis. Here, the number of particles in the vicinity of which matrix cracks were
initiated was determined as a function of the particle size. This number was divided
by the particle size distribution to give the relative fatigue crack initiation prob-
ability curves (Kung & Fine, 1979). Note the precipitous increase in crack nuclea-
tion probability with an increase in the size of the inclusion and the scatter
associated with the measurements due to the variability in the size and distribution
of the inclusions.
(c) In high strength nickel-base superalloys, crack initiation has been identified
with the existence of large defects, either pores or nonmetallic inclusions (e.g.,
Hyzak & Bernstein, 1982). At room temperature, crystallographic cracking at or
near the surface is initiated at the sites of the defects at both low and high strain
ranges. At an elevated temperature of 760 °C, low strain range fatigue results in
crack nucleation at the interior of the specimen. Figure 4.13 shows an example of
this process in a complex nickel-base superalloy (made by powder metallurgy
methods conforming to a commercial designation AF-115 and consisting princi-
pally of Ni-Cr-Co-W-Ti-Al-Mo-Hf-Cb-C) where subsurface crack initiation
occurs at an HfC>2 inclusion. At high strain range values, however, near-surface
crack nucleation is dominant.
4.9 Crack initiation in commercial alloys 155
Fig. 4.13. Subsurface fatigue crack initiation at an HfO2 inclusion in an AF-115 nickel-base
superalloy at 760 °C. (From Hyzak & Bernstein, 1982. Copyright Metallurgical Transactions.
Reprinted with permission.)
particle near the site of dislocation pile-up. The second stage, i.e. crack advance
inside the matrix, was assumed to occur when the total energy of the system attained
a minimum. The total energy comprises four terms: the elastic strain energy from the
stress field of the piled-up dislocation array, the effective surface energy needed for
crack advance, the work done by the applied stress in opening the crack, and the
elastic strain energy of the crack under the applied stress field.
Tanaka & Mura (1982) presented an extension of the parallel layer model for
surface roughening and slip band fracture to include crack initiation from interme-
tallic particles in high strength steels and aluminum alloys. The initiation of the crack
was assumed to be determined by the energy criterion that the fatigue flaw initiates
when the self strain energy of dislocation dipoles accumulated at the inclusion
reaches a critical value. Tanaka & Mura considered three different processes of
fatigue crack initiation: a slip band crack emanating from a debonded inclusion, a
slip band crack initiating from an uncracked inclusion and inclusion cracking due to
the impingement of slip bands. For the last mechanism, which is believed to be
representative of inclusion cracking in aluminum alloys, the solution was obtained
using Eshelby's equivalent inclusion method (Eshelby, 1957).
Corrosion pits are typically smaller than a millimeter in depth and serve as micro-
notches which locally elevate the stress level. Furthermore, the pH level of the
corrosive medium inside the pit can be more acidic than that in the bulk, causing
possible acceleration in the rate of fatigue crack growth. Experimental results
obtained for Ni-Cr-Mo-V steels, austenitic stainless steels and aluminum alloys
4.11 Crack initiation at stress concentrations 157
Fig. 4.14. A fatigue crack initiated at corrosion pits in stress relief groove in a low pressure
turbine rotor made of Ni-Cr-Mo-V steel. (From Lindley, 1982. Reprinted with permission
from T.C. Lindley.)
have established that the formation of corrosion pits on the initially smooth surfaces
of the fatigue specimen results in a significant reduction in the fatigue strength.
Figure 4.14 shows an example of fatigue cracks initiated at corrosion pits in stress
relief groove in a low pressure turbine rotor made of a Ni-Cr-Mo-V steel. The rotor
consists of stepped shafts with shrunk-on discs which carry the turbine blades. A
combination of the steady mean stress due to the shrink fit and the pulsating stresses
caused by the self-weight bending resulted in the initiation of fatigue cracks at
corrosion pits. In the case of the turbine component shown in Fig. 4.14, the fatigue
cracks led to the complete failure of the low pressure turbine shaft.
' The compression fatigue failure of upper spar cap on the wing of an F-15 military aircraft is a typical
example (see Rich, Pinckert & Christian, 1986).
+ A case study of fatigue cracking under cyclic compression in a total hip femoral component is presented
in Chapter 10.
4.11 Crack initiation at stress concentrations 159
-time
uIT
n min
,-<cj
(a)
Fig. 4.15. Schematic showing (a) the loading of a notched specimen in cyclic compression and
(b) typical variation of crack length, measured from the notch tip, as a function of the number
of compression cycles.
behavior of 'nonpropagating' cracks nucleated under cyclic tension (Chapter 7), the
mechanisms underlying the two processes are different.
Observations of controlled crack initiation in cyclic compression of notched metal-
lic materials were first reported in the 1960s. Hubbard (1969) reported a fracture
mechanics-based study of crack growth in a center-notched plate of 7075-T6 alumi-
num alloy. He found that fatigue cracks grew from the tip of the notch over distances
of several millimeters. Similar observations have been made subsequently in a variety
160 Fatigue crack initiation in ductile solids
50 nm
Fig. 4.16. Examples of mode I fatigue cracks initiated at stress concentrations under far-field
cyclic compression :(a) Ti-48 Al intermetallic with a predominantly y-phase micro structure. (6)
Al-3.5 Cu alloy reinforced with 20 volume % of SiC particles. The cyclic compression loading
axis is vertical in both cases. (Photographs courtesy of P.B. Aswath and Y. Sugimura,
respectively.)
of ferrous and nonferrous alloys (Saal, 1971; Reid, Williams & Hermann, 1979;
Suresh, 1985b; Pippan, 1987).
The mechanism by which a fatigue crack initiates and advances in a direction
normal to the imposed compression axis is dictated by the development of a cyclic
plastic zone ahead of the notch tip upon unloading from the far-field compressive
stress. In zero-tension fatigue, there develops a region of reversed flow ahead of a
tensile crack within which residual stresses comparable in magnitude to the flow
4.11 Crack initiation at stress concentrations 161
stress in compression exist.f If one considers the case of a 'sharp' nonclosing notch
which is subjected to a zero-compression-zero fatigue cycle, it is seen that the reverse
flow induced within the monotonic plastic zone ahead of the notch tip upon unload-
ing from the maximum compressive stress generates a zone of residual tensile stresses
at the notch tip (Fig. 4.17). Full field finite element simulations of the generation of
residual tensile stresses in notched plates of ferrous alloys have been reported by
Holm, Blom & Suresh (1986). Quantitative and in-situ measurements of the evolu-
tion of residual tensile stresses ahead of stress concentrations subjected to cyclic
compression loading have been reported by Pruitt & Suresh (1993); see Chapter 6.
Residual stresses are induced ahead of the notch tip during unloading from the
far-field compressive stress because there is no contact (closure) in the wake of the
notch tip. (If a long, sharp fatigue crack, rather than a notch, is subjected to cyclic
compression, such a residual tensile field may not be generated because of the com-
plete closure of the crack during far-field compression loading and unloading.) Once
a fatigue crack emanates from the notch tip, the faces of the crack tend to remain
partially or fully closed during some portion of the loading cycle. Experimental
load
VV\ time
load
time
0
W
Fig. 4.17. (a) A schematic of a zone of residual compression ahead of a sharp notch (with a
small included angle at the notch tip) subjected to cyclic tension in an elastic-perfectly plastic
solid. rc is the cyclic plastic zone defined in Eq. 9.74. (b) A zone of residual tension for the
nonclosing notch subjected to cyclic compression.
' As shown in Section 9.6, the size of the cyclic plastic zone ahead of a stationary fatigue crack in an
elastic-perfectly plastic solid subjected to zero-tension cyclic loading in plane stress is about one-quarter
the size of the monotonic plastic zone.
162 Fatigue crack initiation in ductile solids
measurements of crack closure (Suresh, Christman & Bull, 1986) reveal that as the
length of the fatigue crack increases, the fraction of the loading cycle during which
the crack remains open progressively diminishes. This increasing closure causes the
crack to arrest completely after growth over a distance a*, as shown in Fig. 4.15. The
total distance of crack growth ahead of the notch is a complex function of such
variables as the size of the residual tensile zone created during the first cycle, the
stress state, load range, notch tip geometry and the microscopic roughness of the
fatigue crack faces. The distance a* is dependent upon the rate of exhaustion of the
residual tensile zone and the rate of increase in closure stress with increasing fatigue
crack length.
As crack advance under far-field cyclic compression is governed by local tensile
stresses, the influence of micro structure on crack growth behavior is found to be
similar to that seen under far-field cyclic tension. However, the mechanisms of
fracture surface contact and abrasion are different for the two cases.
Since the size and shape of the monotonic and cyclic plastic zones and the extent
of crack closure are strongly influenced by whether plane stress or plane strain
conditions prevail (see Fig. 9.15 and Chapter 14), the stress state is expected to
have a marked effect on the characteristics of crack initiation and growth in notched
components subjected to cyclic compression. Plane stress conditions, where the
monotonic and reversed plastic zone sizes directly ahead of the notch tip are
about three times greater than those for plane strain, Eq. 9.77, a substantially faster
rate of crack initiation and a greater crack growth distance a* are promoted in plane
stress than in plane strain. Holm, Blom & Suresh (1986) conducted a numerical
simulation of the effects of stress state on crack growth in edge-notched plates of
a bainitic steel under cyclic compression using elastic-plastic finite element calcula-
tions with an isotropic hardening model. Geometrical aspects of crack propagation
were modeled by releasing the crack tip node at the peak of each compression cycle
(amax), by changing the boundary conditions, and by solving the contact problem to
determine the stress level of the compression cycle (acl) at which the freshly formed
crack faces would first contact during the loading portion. Their results reveal that
the crack remains open during a larger fraction of the compression cycle in plane
stress than in plane strain.
Exercises
4.1 The roughening of the surface of a material by the formation of slip steps
plays an important role in the nucleation of fatigue cracks. Consider a cube
which is made of an FCC single crystal. One of the corners of the cube is
located at the origin of the Cartesian coordinate system (with axes x, y and
z, and unit vectors along the axes i, j and k, respectively). A closed disloca-
tion loop lies on the plane x — a/2, where a is the edge length of the cube.
Exercises 163
The loop consists of dislocation segments of pure edge, pure screw and
mixed edge-screw characters. If the loop expands in its own plane under
the influence of an applied stress, slip steps will be formed on some faces of
the crystal when all segments of the loop intersect the faces of the crystal.
Indicate the faces of the cube on which the slip steps will form in the
following cases:
(a) The Burgers vector of the dislocation loop is b = b\.
(b) The Burgers vector of the dislocation loop is b = bk.
4.2 An edge dislocation (±x) is located on the plane x = x\\ x, y and z are the
axes of the Cartesian coordinate system and i, j and k are the corresponding
unit vectors along these coordinate axes. The Burgers vector of J_i is bi = b\
and the dislocation line is parallel to k. A second edge dislocation line J_2>
also oriented parallel to k, is at the origin. Calculate the glide and climb
forces J_! would experience due to the presence of ±2> m terms of xx and 0
(i.e. the angle between the x-axis and the line on the x-y plane connecting the
two dislocations) for the case where the Burgers vector of J_2 *s ^2 = bi.
4.3 A crystal contains a single edge dislocation (Burgers vector, b = bi and
dislocation line vector parallel to k, where i, j and k are the unit vectors
along the Cartesian coordinate axes, x, y and z, respectively).
(a) The crystal is subjected to a tensile stress at = axx. Calculate the force
on the dislocation. Is it a glide or a climb force?
(b) The stress is now reversed into compression with the compressive stress
<TC = — 2oxx. Recalculate the magnitude and direction of the force on the
dislocation.
(c) Find the magnitude and direction(s) of the maximum force on a screw
dislocation (oriented parallel to k with a Burgers vector, b = b k) in a
crystal subjected to a shear stress, oxz.
4.4 Consider two parallel screw dislocations of the same sign. Obtain an expres-
sion for the force on the dislocations as a function of their relative positions.
Comment on the stability of this arrangement.
4.5 Describe the process of point defect production by the annihilation of two
edge dislocations of opposite signs which are separated by two atomic
planes. The extra planes of atoms in both the dislocations are on the outside
of the slip planes for the dislocations. Use schematic diagrams to show the
orientations, glide directions, and atomic arrangements before and after
annihilation. Are the point defects vacancies or interstitials?
4.6 Consider two parallel edge dislocations of the same sign. Let 0 be the angle
between the line connecting the two dislocations and the direction of their
Burgers vectors.
(a) Calculate the variation of the glide force and the climb force for the two
dislocations as a function of the relative positions of the dislocations
(i.e. as a function of 0).
164 Fatigue crack initiation in ductile solids
(1) Frictional sliding of the mating faces of microcracks that are nucleated at
grain boundaries (in single phase systems), at interphase regions (in multi-
phase systems), and along the interfaces between the matrix and the rein-
forcement (in brittle composites) under the influence of the applied loads.
165
166 Cyclic deformation and crack initiation in brittle solids
(2) Progressive wear and breakage, under repeated cyclic loading, of bridging
ligaments which connect the faces of microcracks and long flaws in brittle
solids at low and elevated temperatures.
(3) Wedging of the mating surfaces of microscopic and macroscopic flaws by
debris particles which are formed as a consequence of repeated contact
between the crack faces, especially under fully compressive or tensile-com-
pressive cyclic stresses.
(4) Microcracking due to the release of thermal residual stresses at grain bound-
aries and interfaces, which gives rise to a permanent transformation strain.
(5) The inelastic strain arising from shear or dilatational transformations such
as mechanical twins or martensitic lamellae.
(6) The viscousflowof glassy phases that are introduced during processing and/
or formed as a result of environmental interactions at elevated temperature,
and the associated interfacial cavitation in ceramics and ceramic composites
during high temperature fatigue. The strain-rate dependence of viscous
deformation causes the fatigue response of the brittle solid with glassy
films to be both time-dependent and cycle-dependent.
fracture as the component of the normal tensile stress on the ensuing crack plane.
This inference is also supported by experimental observations which show that
cracks in semi-brittle solids are nucleated as easily in compression as in tension.
(This behavior is distinctly different from that of brittle solids, which are many
times stronger in compression than in tension.) Semi-brittle solids generally do not
contain a sufficient number of slip systems to accommodate plastic strains. Recall
from Chapter 3 that five independent slip systems are needed to ensure strain com-
patibility in a polycrystalline solid. Therefore, the initiation of a brittle crack may be
the principal factor responsible for relieving the strains accommodated by a limited
amount of slip in these materials. Damage evolution by craze formation is another
mode of semi-brittle deformation in polymers, which is discussed in the next chapter.
Increases in temperature tend to reduce the degree of brittleness in a material.
While the classification in Table 5.1 is primarily intended for quasi-static loading
conditions, it should be noted that strain rate and temperature strongly affect the
degree of brittleness in many materials.
or in the immediate vicinity of the crack tip. In brittle solids, however, it is generally
not so straightforward to identify a clear cyclic effect. This difficulty arises because
fluctuations in applied loads can lead to a large influence on the cyclic stress-strain
curve and in the crack initiation/propagation life (compared to static loads of the
same peak value) even when there are no discernable differences in the deformation
and damage mechanisms between the static and cyclic loading cases. In this chapter,
and in Chapters 6, 11 and 12, we demonstrate the following effects of cyclic loading
on deformation and cracking in brittle solids.
(1) Cyclic loading resulting in an increased hysteresis or gradual shift in the
stress-strain curve as a result of progressive damage evolution involving
microcracking, crazing, cavitation or phase transformations at both low
and high temperatures.
(2) Cyclic response of semi-brittle ionic crystals at elevated temperatures
wherein the dislocation structures are apparently similar to those of fatigued
ductile FCC crystals at room temperature.
(3) Elevated temperature cyclic response of ceramic composites in which the
cyclic deformation characteristics at the tip of a crack are distinctly different
from those immediately ahead of a statically loaded crack.
In addition, it is shown in this chapter and in Chapters 6, 11 and 12 that an
identifiable fatigue effect, as seen by an enhanced or reduced time to failure or
crack propagation rate compared to a static load of the same peak value or mean
value, can occur in many brittle solids at room and elevated temperature, even when
the mechanisms of deformation and damage are the same under both static and cyclic
loads. The following processes which lead to such fatigue effect are considered in this
connection.
(1) The formation of crazes during cyclic loading results in cyclic softening in
brittle polymers (next chapter).
(2) The inducement of a permanent deformation (such as microcracking or
crazing) within the cyclic damage zone ahead of the notch in a brittle cera-
mic or polymer at room temperature results in a mode of crack initiation
and growth under cyclic loads which is distinctly different from that
observed under monotonic compression loads (see Chapters 6, 11 and 12).
(3) The progressive breakdown of bridging ligaments in the wake of a fatigue
crack results in a much higher crack velocity at room temperature under
cyclic loads than under sustained loads of the same peak stress intensity
(Chapter 11).
(4) The bridging of the wake of a fatigue crack by glassy ligaments (formed
from the viscous flow of the glassyfilmsleft from the processing additives or
formed in-situ as a result of environmental interactions) leads to a much
lower crack velocity at high temperature under cyclic loads than under
sustained loads of the same peak stress intensity (Chapter 11).
53 Highly brittle solids 169
5.5./ Mechanisms
There exist several possibilities for introducing crack nuclei during the fab-
rication and service of a brittle solid:
(a) Brittle solids contain a population of small microscopic flaws, commonly
known as Griffith flaws. The presence of these flaws can cause marked reductions
in fracture strength. On the free surface, the Griffith flaws can be initiated due to the
impingement of hard dust particles, such as quartz, which are prevalent in the atmo-
sphere. Within the bulk, defects such as pores, inclusions or gas bubble entrapments
are likely to develop in a commercially-processed material. These internal defects
serve as potential sites for the nucleation of a dominant crack.
(b) The free surface is almost invariably 'rough' on an atomic level. Surfaces
typically consist of steps, grooves, ridges, pits, etc., as a result of crystal growth,
dissolution, cleavage or ion bombardment, even when the surface preparation tech-
niques and the specimen surfaces are 'clean'. These atomically rough surface features
can serve as local stress raisers in brittle solids where atomic bond rupture is the
principal mode of failure.
(c) In materials such as ceramics, rocks, cement mortar and concrete, distributed
microcracking in the bulk is known to occur along grain facets and/or interfaces. In
noncubic, single phase brittle solids and brittle composites, residual stresses gener-
ated at grain boundary facets and interfaces give rise to microcracking during cool-
ing from the processing temperature as a result of thermal contraction mismatch
between adjacent grains or phases. Furthermore, the residual stresses may aid in the
nucleation of intergranular flaws under the influence of an external stress. In trans-
formation-toughened ceramics (to be discussed in Section 5.5), microcracking occurs
in conjunction with stress-induced martensitic transformations.
(d) Brittle materials, when exposed to certain embrittling environments, can suffer
strength degradation and increased susceptibility to flaw nucleation. For example,
the large sodium ion in the glass network is replaced by a smaller species, such as H +
in an acid solution or Li+ in a molten salt. Furthermore, local devitrification of glass
can provide a preferential site for crack nucleation.
170 Cyclic deformation and crack initiation in brittle solids
(5.1)
where 7VC is the number of microcracks per unit volume, S is the area of a microcrack
and P is its perimeter. The symbol { } denotes a volume average.
Fig. 5.1. (a) A zone of grain boundary microcracks formed ahead of a single edge-notch in an
A12O3 subjected to uniaxial compressive stresses in a direction normal to the plane of the notch.
(From Suresh & Brockenbrough, 1988. Copyright Pergamon Press pic. Reprinted with
permission.) (b) Microcracks ('me'), denoted by arrows, as seen in a TEM foil taken 0.5 Jim
from the tensile fracture surface in ZrO 2 -toughened A12O3. (From Ruhle, Clausen & Heuer,
1986. Copyright American Ceramic Society. Reprinted with permission.)
5.3 Highly brittle solids 171
three-dimensional slits
random pennies
two-dimensional slits
Fig. 5.2. Variation of the elastic modulus E for a microcracked solid, normalized by its modulus
Eo when no microcracks exist, is plotted as a function of the microcrack density (3 for the
indicated crack systems. (After Laws & Brockenbrough, 1987.)
/ 1
Fig. 5.3. Stress-strain curve for a microcracking material subjected to a zero-tension-zero load
cycle. The strain axis is enlarged for clarity.
53 Highly brittle solids 173
Giannakopoulos, 1990) and at a critical mean stress (e.g., Hutchinson, 1987) have
been considered. Other constitutive models for isotropic microcracking have also
been proposed where microcrack nucleation between the threshold and saturation
stages is considered to be governed by an effective stress a. For example,
Charalambides & McMeeking (1987) use the following small strain, nonlinear elastic
constitutive relation to characterize the deformation of a microcracking solid:
EetJ = [h(d) + v]^ - vakk8tj, (5.2)
where atj and etj are components of the stress and strain tensors, respectively, v is
Poisson's ratio, 8^ is Kronecker's delta (defined in Section 1.4),
> (5-3)
With respect to the different regimes of the loading curve in Fig. 5.3, Charalambides
& McMeeking assumed that
P=0 for a < a0,
ft = k{a — a 0 ) for <70 < a < as,
/3 = ps = k(as-G) for a>as, (5.5)
where k is a factor which governs the rate of microcracking with stress.
In an independent study, Brockenbrough & Suresh (1987) used a similar assump-
tion of penny-shaped flaws to develop a constitutive model for their numerical
simulation of compression fatigue crack nucleation in highly brittle solids. Using
in situ video photography and acoustic emission measurements, they measured the
threshold stress <x0 f ° r microcrack nucleation in edge-notched specimens of mono-
lithic alumina loaded in uniaxial cyclic compression (Fig. 5.\a shows notch tip
microcracking from one such test). Microcrack nucleation was assumed to follow
the relationship:
- - 1 ) for |<x|>|a o |, £ < & ,
Fig. 5.4. Constitutive behavior of a microcracking brittle solid in cyclic compression. The strain
axis is enlarged for clarity.
from the far-field compressive stress. The development of permanent strains after
one compression cycle can then be quantified by an unloading parameter,
X— 1 — (5.7)
Pmax
The unloading path B in Fig. 5.4 corresponds to the idealized situation where all the
microcracks, of density /3 max (= /3S if saturation occurs) existing at the maximum far-
field compressive stress, gradually close upon unloading. In this case, fiu = j#max?
X = 0 and no permanent strains exist in the fully unloaded state. Path D represents
the other extreme case where all the microcracks nucleated during compression
loading are blocked by the presence of debris within them or they are locked in
friction. Here, X = 1 and unloading occurs with the same slope as the initial loading
portion of curve A. If the frictional sliding taking place between the faces of the
microcracks during compression loading is partially reversed upon unloading,
0 < Pu < Anax> 0 < A. < 1, and unloading occurs along path C. Thus the linear
unloading parameter X conveniently characterizes permanent strains representing
the entire range of linear unloading paths. The elastic secant moduli during unload-
ing are given by
Eu = E0X + Em(\ - XI vu = v0X + v m (l - X). (5.8)
Em and vm are the values of Young's modulus and Poisson's ratio, respectively, at
the maximum far-field compressive stress.
5.3 Highly brittle solids 175
Using a finite element analysis, Brockenbrough & Suresh (1987) showed that when
the unloading path leads to permanent strains, i.e. for k > 0, the resulting residual
stresses that arise in the matrix material in the vicinity of a stress concentration are
distinctly different from those induced under monotonic loading conditions. This
effect of permanent strains causes a mode of failure which is unique to cyclic loading
conditions. More significantly, the results imply that kinematic irreversibility of
microscopic deformation (in this case, the differences in the opening and closing
of microcracks) occurring during fatigue in a brittle solid is qualitatively similar to
the development of stress-strain hysteresis due to slip irreversibility in metal fatigue.
Note the similarity of the above formulation for the compression fatigue of brittle
solids to the process of compression fatigue in metals discussed in Section 4.11. A
similar conceptual framework was used by Lawn et al. (1994) to rationalize the
progressive evolution of microcracking during cyclic indentation of brittle ceramics.
A constitutive model similar to that shown in Fig. 5.4 has also been used to predict
the size and shape of the cyclic damage zones developing ahead of tensile fatigue
cracks in microcracking ceramic materials, Suresh & Brockenbrough (1990). These
cyclic damage zones are taken up for discussion in Chapter 11.
' Usually, for comparison of times to rupture under static and cyclic loads, the maximum nominal stress
corresponding to the fatigue cycle is taken to be the same as that of the static stress for smooth specimens.
176 Cyclic deformation and crack initiation in brittle solids
extrinsic factors
promoting a
beneficial effect
of cyclic loading ^ ^ — —
*» "^
) ruptiire (1<3g scale)
time-dependent •
rupture
^ ^ no fatigue effect
controlled by ~^»^ i
(ii
environment synergistic * i ^ ^
IU11
effects of . ^ ^
+•"
environment 1 ^^ ^
and fatigue | cycle-dependent failure
causing detrimental effect of fatigue
cyclic frequency (log scale)
Fig. 5.5. A schematic illustration of possible beneficial or detrimental effects of cyclic loading on
the time to rupture in brittle solids.
to form an amorphous SiO2 glass phase. The viscous flow of this phase at the
elevated temperature leads to the nucleation of cavities and microcracks along the
interfaces between the alumina matrix and the SiC particles. Figure 5.6(a) shows an
example of interfacial cavities formed at every corner of a SiC particle in an A12O3-
33 volume% SiC whisker composite fatigued in 1400 °C air. The presence of the
amorphous interfacial film and the kinematically irreversible cyclic displacements
associated with the opening and closing of the interfacial microcracks promote
tensile fatigue deformation mechanisms which can be different, in some cases,
from those seen under sustained tensile loads. The reinforcement phase also breaks
under cyclic loading conditions; Fig. 5.6(b) is a micrograph of a SiC whisker broken
by cyclic tensile loads in 1400 °C air. In this figure, the meniscus of the silica glass
phase can be seen within the broken whisker.
Environmental effects at high temperatures can influence deformation and frac-
ture in brittle solids subjected to cyclic loads in a manner which is different from that
observed under static stresses. If the material does not contain any macroscopic
cracks or stress concentrations, the fatigue mechanisms described above are confined
to the near-surface region, where oxygen is available. If through-thickness stress
concentrations are present in the material, the transport of the environment to the
tip of the defect causes a damage zone to develop under the influence of an applied
stress. In the example shown in Fig. 5.6, the oxidation of SiC whiskers giving rise to
interfacial microcracking is essentially the same for monotonic and cyclic loading
conditions. However, mechanisms associated with microcrack opening and closure,
bridging of the flaws by reinforcement particles and the breaking of debonded whis-
kers are affected in different ways depending upon whether the composite is sub-
jected to monotonic or cyclic loads.
Direct tensile fatigue tests at 1000-1200 °C on hot-pressed Si3N4 unidirectionally
reinforced (along the tensile axis) with 30 vol.% SiC (SCS-6) fibers also reveal a
gradual reduction in the elastic modulus with the progression of fatigue damage
(Holmes, 1991). No such changes in compliance were observed in specimens which
are subjected to low stress cycles below the endurance limit (at 2 x 106 cycles).
Fatigue-induced changes in elastic properties were observed at maximum stress levels
that were above the monotonic proportional limit, with both mechanical fatigue and
creep influencing progressive damage. This regime of fatigue is characterized by
decreasing stiffness, increasing stress-strain hysteresis, and strain ratchetting (cyclic
creep). However, when the maximum stress level in fatigue is below the monotonic
proportional limit, only creep deformation occurs. This creep regime of loading is
characterized by strain ratchetting, but no change in elastic properties. Holmes has
also shown that the fatigue life deteriorates markedly with decreasing tensile load
ratio R. Figure 5.7 contains experimental data on the changes in the cyclic stress-
strain hysteresis loops with increasing number of fatigue cycles. Note the occurrence
of cyclic creep (as in metals, Section 3.9) and of increase in specimen compliance due
to repeated stress cycles.
178 Cyclic deformation and crack initiation in brittle solids
0.2 n
Fig. 5.6. Microscopic deformation mechanisms ahead of a crack tip in an Al 2 O 3 -33 volume%
SiC whisker composite fatigued at a stress ratio, R = crmin/crmax = 0.15 and a load frequency of
0.15 Hz (sinusoidal waveform) in 1400 °C air. (a) TEM photograph showing nucleation of
cavities at the interfaces between SiC whiskers and matrix A12O3 grains, (b) A SiC whisker
broken under cyclic loads. The meniscus of the amorphous glass phase can be seen within the
broken whisker. (From Han & Suresh, 1989. Copyright American Ceramic Society. Reprinted
with permission.)
5.4 Semi-brittle solids 179
300
200
100
0.1 0.2
strain (%)
Fig. 5.7. Uniaxial tensile cyclic stress-strain behavior of a Si 3 N 4 -SiC fiber composite at
maximum stress levels above the proportional limit (196 MPa). The number of stress cycles is
indicated along with each hysteresis loop. Test temperature, T = 1200 °C, laboratory air
environment, R = 0.1, and vc = 10 Hz. Number of cycles to failure, Nf — 6.5 x 104. (After
Holmes, 1991.)
the well known 'Petch' relationship (Petch, 1953) for the grain size-dependence of
yield strength:
o fe (59)
where rxy is the resolved shear stress on the glide plane, r®v is the friction stress
(which is to be overcome before the dislocations glide on the slip plane), G is the
shear modulus and d% is the grain size of the material. Equation 5.9 is derived by
assuming that the Frank-Read source is located at the center of the grain.
Evidence of dislocation pile-up at grain boundaries and of the attendant nuclea-
tion of a crack at the boundary is available for a number of semi-brittle solids. The
birefringence of transmitted polarized light in Fig. 5.8(a) shows stress concentra-
tions, generated at the tip of slip bands obstructed by a grain boundary, in a bicrystal
of MgO. Transgranular crack formation at the site of slip band obstruction at the
grain boundary is evident in the micrograph of the etched MgO bicrystal, Fig. 5.8(6).
Figure 5.9 illustrates some mechanisms by which the pile-up of dislocations can
nucleate a brittle crack. The nucleation of a microcrack or a wedge-shaped cavity by
the pile-up of dislocations at an obstacle such as a grain boundary (GB) is shown in
Fig. 5.9(a). The stress gradients ahead of a dislocation pile-up are similar to those
found in front of a shear (mode II) crack. If the interface in Fig. 5.9(a) is weak,
preferential cracking occurs along the interface.
The crack nucleation mechanism shown in Fig. 5.9(6), which was first proposed by
Cottrell (1958), is a process in which two intersecting slip planes provide the nucleus
for a crack, even in the absence of a pre-existing obstacle to slip. This process has
also been suggested as a mechanism for the initiation of subsurface fatigue cracks
along {001} cleavage planes of /3 phase in Ti alloys composed of a-fi duplex micro-
structures (Ruppen et al., 1979).
Fig. 5.8. {a) Stress concentrations revealed by the birefringence of transmitted polarized light in
an MgO bicrystal at a location where a grain boundary obstructs slip. (From Ku & Johnston,
1964. Copyright Taylor & Francis, Ltd. Reprinted with permission.) (b) Transgranular cracks
formed at sites where slip is impeded by the grain boundary in the MgO bicrystal. (From
Johnston, Stokes & Li, 1962. Copyright Taylor & Francis, Ltd. Reprinted with permission.)
182 Cyclic deformation and crack initiation in brittle solids
(a)
Fig. 5.9. Mechanisms for the nucleation of cracks by (a) dislocation pile-up at a grain boundary
(GB) and (b) dislocation reactions.
a 4001]. (5.10)
J (ioi) + 2 ^
Thus, the Burgers vector of the product dislocation is a[001].
(ii) Note that the energy of a dislocation is proportional to the square of the
magnitude of the Burgers vector. The sum of the energies of the two
reacting dislocations is proportional to 3a /2. The energy of the product
dislocation is proportional to a . Since there occurs a net reduction in
energy, this reaction is energetically favorable.
(iii) The product dislocation is of pure edge character, whose extra plane of
atoms lies parallel to the (001) cleavage plane of BCC a-iron. Since this
dislocation is not favorably oriented for slip (i.e. {110} plane and (111)
direction), it cannot glide. It is a sessile dislocation and forms an obstacle
to other dislocations gliding down the (101) and (TOl) planes.
Fig. 5.10. Intrusions and extrusions formed on the surface of fatigued AgCl crystal. (From
Forsyth, 1957. Copyright The Royal Society, London. Reprinted with permission.)
opments comparable to those found in cyclically strained FCC metals. It has, how-
ever, been shown by Argon & Godrick (1969) that the elevated temperature fatigue
deformation of LiF is similar to the room temperature cyclic deformation character-
istics of ductile FCC metals. They found that above 673 K (which is 59% of the
absolute melting temperature), cross slip and dislocation climb were favored. Cyclic
loading in this temperature regime produced pores throughout the highly strained
volume of the crystal. Continued cyclic straining resulted in a gradual change in the
density of the crystal as a consequence of cavitation. Argon and Godrick measured a
fractional density change of 3 x 10~8 per cycle in LiF crystals fatigued at 783 K at a
strain amplitude of 2.5 x 10~3. Similar pore development was also observed in AgCl
crystals which were fatigued above 423 K (58% of the absolute melting temperature).
Majumdar & Burns (1981) also employed direct push-pull fatigue loading in
smooth specimens of LiF crystals at elevated temperatures and showed that disloca-
tion banding occurred within subgrains. Microcracking also appeared to take place
along the (110) directions at low strain amplitudes and at large numbers of fatigue
cycles. Associated with the bands are alternate regions of high and low dislocation
density which seem to be sites where dynamic recovery occurs. As the temperature is
raised, the behavior of the LiF crystal appears to resemble more closely that of FCC
metals. A TSB-like' slip pattern emerges in the fatigued crystal at a temperature of
573 K, and at low strain rates and strain amplitudes. Ladder-like dislocation struc-
tures appear to exist within the PSBs, Fig. 5.11. The arrangement and the spacing of
dislocations within the ladders of PSBs, however, are different from those of ductile
crystals. The fatigued crystal also exhibits a plateau where the saturation value of the
shear stress is independent of the plastic strain amplitude as in FCC crystals (Fig.
2.2). Further increases in test temperature and strain amplitude cause a cellular
structure to form, similar to the trend seen in regime C of Fig. 2.2.
184 Cyclic deformation and crack initiation in brittle solids
Fig. 5.11. PSB-like dislocation structure in LiF single crystal fatigued at 573 K. A6 p /2 = 0.5%,
and € — 10~3 s" 1 . Note that the rungs of the PSB ladder structure are bent, as, for example, at
location A. The curved dark lines running across the micrographs are cleavage steps and their
positions oscillate with the PSB structure, probably as a result of local stresses. (From
Majumdar & Burns, 1982. Copyright Pergamon Press pic. Reprinted with permission.)
Majumdar & Burns (1987) also conducted fully reversed fatigue tests on MgO
single crystals at 743 K. They found that dense bundles of dislocations developed
as a consequence of reversed straining, similar to the vein structure evolving from
the early stages of fatigue in FCC metals (Fig. 2.2). These bundles were aligned
normal to the Burgers vector. Bowed out screw dislocations were observed
between the edge dislocation bundles suggesting that the screws were largely
mobile.
In summary, one of the principal contributing factors for the pronounced brittle-
ness of ionic crystals at low temperatures is the limited possibility for cross slip.
However, when certain combinations of temperature and strain rate favor cross slip,
it is not surprising to observe the aforementioned similarities between their fatigue
deformation characteristics and those of ductile FCC metals.
5.5.1 Phenomenology
Tetragonal (/) to monoclinic (m) phase changes occur as a martensitic trans-
formation in ceramics which contain metastable tetragonal ZrO2. This tetragonal
phase may be present in a stable cubic matrix phase in the form of a precipitate (as in
partially stabilized zirconia, PSZ), or a dispersoid (as in ZrO2-toughened alumina,
ZTA), or may be formed as the fine matrix phase in the (nearly) 100% t-ZrO2
polycrystals, TZP. Since the seminal paper of Garvie, Hannick & Pascoe (1975)
on this topic, it has been acknowledged that the dilatational and shear strains
accompanying the / to m transformation can account for the remarkable toughening
properties of ZrO2-containing ceramics at low temperatures (typically below 700 °C).
Among the various transforming ceramic micro structures, a large body of
research has centered around the monotonic and cyclic deformation and fracture
characteristics of ZrO 2 , partially stabilized with MgO (commonly referred to as Mg-
PSZ). Figure 5A2(a) is a micro structure of a peak-aged (maximum strength) Mg-
PSZ containing 9 mol.% MgO. This material is composed of cubic phase zirconia
grains, of 50jim average diameter, with the MgO in solid solution. Lens-shaped
tetragonal precipitates, which are 300 nm long and metastable at room temperature,
populate the interior of the grains. The tetragonal oaxis of the precipitates is parallel
to their smallest dimension. The precipitates are oriented within the cubic phase
grains in such a way that their oaxis is parallel to one of the three cubic axes.
Experimental studies by Chen & Reyes Morel (1986) and others reveal that the
mechanism by which microscopic strains induced by martensitic transformation are
converted to macroscopic plastic strains is via shear localization. Figure 5.\2(a)
shows an interior section of the material, deformed under a hydrostatic compressive
stress of 200 MPa, showing shear bands within the grains. It is seen that the shear
bands, which span the entire grain, have different orientations in different grains; the
bands within individual grains appear to be parallel. In order for the transformation
of individual tetragonal particles to cause a macroscopic shear strain via shear
banding, it appears necessary that the particle transformation be correlated, as
shown in Fig. 5A2(b).
Shear bands in 'transformation plasticity' can thus be deemed functionally equiva-
lent to the slip bands in 'dislocation plasticity' of polycrystalline metals. Although
the shear characteristics of the two phenomena are similar in this respect, there are
also some major differences between them. While dislocation plasticity is volume-
preserving, transformation plasticity induces both microscopic and macroscopic
dilatational strains. For unconstrained t -> m transformation in Mg-PSZ, the max-
imum amounts of volumetric and shear strains are 0.04 and 0.16, respectively. When
embedded in an elastic matrix, correlated transformation of the particles leads to the
186 Cyclic deformation and crack initiation in brittle solids
(b)
Fig. 5.12. (a) Transgranular shear band formation due to martensitic transformation. (From
Chen & Reyes Morel, 1986. Copyright American Ceramic Society. Reprinted with permission.)
(b) Correlated transformation of particles leading to the formation of a shear band.
5.5 Transformation-toughened ceramics 187
nucleation of shear bands, whose orientation varies from grain to grain. Thus, the
average shear strain over the particle for constrained transformation is less than 0.16,
although the dilatant transformation strain is still 0.04 for the particle. It is also
known that martensitic transformation can lead to microcracking as a consequence
of the intersection of shear bands and grain boundaries, as well as by the decohesion
of the transformed particle from the surrounding matrix. The opening of a popula-
tion of microcracks also produces macroscopic dilatational strains.
Permanent phase changes cause stress-strain hysteresis in transforming ceramics
upon loading and unloading, similar to the behavior found in metallic materials.
Figure 5.13 is a stress-strain diagram of the peak-aged Mg-PSZ subjected to one
cycle of uniaxial tensile loading. Beyond a tensile stress of about 275 MPa, fully
irreversible phase transformation takes place; the resulting constitutive response
becomes highly nonlinear. Elastic unloading is observed in the nonlinear regime;
reloading occurs with an elastic modulus which is identical to that of the initial
elastic regime. These results indicate how nonlinear effects associated with marten-
sitic phase transformations can provide a mechanism for stable fatigue damage to
occur in nominally brittle solids.
400
200
1 2
strain (x 103)
Fig. 5.13. Uniaxial tensile loading and unloading behavior of peak-strength Mg-PSZ. (After
Marshall, 1986.)
188 Cyclic deformation and crack initiation in brittle solids
Lambropoulos, 1983). These models, which are described in some detail below,
neglect the shear component associated with the transformation and invoke the
assumption that the dilatant transformation occurs at a critical mean stress am.
In the analysis of Budiansky et al., the constitutive behavior is formulated for a
linear elastic matrix with embedded metastable particles which undergo irreversible
inelastic volume expansion. Assume that the matrix material deforms linearly under
both hydrostatic tension and compression with bulk modulus B, according to
1
c>m = —<yjrk = (5.11)
where otj and etJ are stress and strain tensors, respectively, and ekk is the total
dilatation.
When the mean stress due to a monotonically increasing load is less than a critical
value (7^, the particles satisfy Eq. 5.11 with the same bulk modulus B, as shown in
Fig. 5.14. However, once am > o^, the incremental response of the particle is gov-
erned by Bf where
&m = B'ekk. (5.12)
The inelastic or transformed portion of the dilatation 0p is the difference between the
total and elastic dilatation:
crl
In this model, the particle and the matrix are assumed to exhibit the same shear
behavior; the shear modulus of the composite is G at all strains. The incremental
response of the composite for am > a^ is
a = + (515)
= Bekk
P = 200 MPa, are plotted in Fig. 5.15. A, R and V scale with the applied differential
stress in the ratio of —2 : 3 : 4.
The yield condition for transformation plasticity, which can be derived from the
multiaxial compression experiments, is
(5.20)
where a e is the effective stress, Eq. 1.27, am is the mean pressure, and a* and a^ are
measures of hardness.
The experiments of Chen & Reyes Morel also suggest the following yield criterion
consistent with Eq. 5.20:
Yc= 70c + aci>, (5.21)
c
where YQ and Y are the compressive yield stress values at pressures of 0 and P,
respectively, and ac is a constant, which is about two for a wide range of strain
values, except for very small and very large strains. Experiments on Mg-PSZ suggest
that a* = 3Fo/5 and a^ = O.57o- The numerical value ac = 2, along with the
assumption of normality flow, produces a ratio A : R : V of — 2 : 3 : 4, which is
consistent with the results of Fig. 5.15. Furthermore, since this formulation is phe-
nomenological, it also accounts for the effects of microcracking (induced by trans-
formation) on deformation.
0.018
0.016
0.014
0.012
1 0.010
I 0.008
"3,
0.006
0.004
0.002
Fig. 5.15. Experimentally determined variation of axial (^4), radial (R) and volumetric (V)
strains plotted as a function of the differential axial compressive stress E for Mg-PSZ
(maximum strength condition) under an imposed hydrostatic pressure, P = 200 MPa and a
strain rate, 6 = 1 0 . (After Chen & Reyes Morel, 1986.)
5.6 Fatigue crack initiation under far-field cyclic compression 191
Under cyclic compression loading conditions, however, brittle solids with stress
concentrations exhibit a completely different mode of crack initiation which is
macroscopically similar to that found in metallic materials (Section 4.11). When
notched plates of brittle solids are subjected to some combinations of (cyclic com-
pression) stress amplitude and mean stress, confined microcracking occurs at the tip
of the notch (see Fig. 5Aa). If even a fraction of this microcracking deformation at
the notch tip is permanent (i.e. when microcracks do not open and close the same
way during compression loading and unloading), residual tensile stresses are created
within the microcrack zone upon unloading from the maximum far-field compres-
sion stress. Similarly, permanent strains associated with stress-induced phase
changes, frictional sliding, or creep can also cause residual tensile stresses to develop
ahead of stress concentrations under far-field cyclic compression. Examples of fati-
gue crack growth in cyclic compression ahead of stress concentrations in brittle
solids are shown in Figs. 5A6(a) and (b).
Brockenbrough & Suresh (1987) conducted a finite element simulation of near-
tip fields in notched plates of a polycrystalline aluminum oxide subjected to
uniaxial cyclic compression. They used a constitutive model for microcracking
which was described earlier in Fig. 5.4 and in Eqs. 5.4-5.8. Their predictions
of the variation of residual stresses normal to the plane of the notch, ayy
(which is the stress ayy perpendicular to the plane of the notch, normalized by
the product of the maximum far-field compressive stress a°° and the elastic stress
concentration factor for the notch tip Kt), are plotted in Fig. 5.17 as a function
of the distance directly ahead of the notch tip x, normalized by the notch tip
radius p. These computations were made using the following values for the vari-
ables in Eq. 5.6: cro/(cr°°Kt) = 0.0076, A = 0.004, n = 1, and & = 0.4 for penny-
shaped microcracks. When the microcracking deformation ahead of the notch tip
leaves no permanent strains, i.e. when X = 0, (see Eq. 5.7 and Fig. 5.4), essentially
no residual stresses are induced ahead of the notch tip after one compression
cycle. On the other hand, when A > 0, a region of large residual tension is created
at the notch tip after the far-field compressive stress is removed. Note that
residual stresses are self-equilibrating. A zone of residual tension in the immediate
vicinity of the notch tip is accompanied by a zone of residual compression away
from the notch tip, Fig. 5.17.
The effect of this residual stress zone is that residual tensile stresses easily exceed
the tensile strength of the brittle solid over a distance of the order of the notch root
radius. This implies that a mode I crack will develop over this distance upon unload-
ing from the far-field compression stress, an inference which is supported by experi-
mental observations. Once a fatigue crack initiates from the notch tip, its rate of
growth during subsequent compression cycles is dictated by such factors as the
exhaustion of the residual stress zone created during the first cycle, formation of
5.6 Fatigue crack initiation under far-field cyclic compression 193
r . '"
(b)
Fig. 5.16. Examples of mode I fatigue cracks initiated at stress concentrations under far-field
cyclic compression: (a) Polycrystalline A12O3. (b) Cement mortar. The compression axis is
vertical in both cases. (From Ewart & Suresh (1986) and Suresh, Tschegg & Brockenbrough
(1989), Reprinted with permission.)
debris particles of the brittle solid due to repeated contact between the crack faces,
the generation of a residual stress field in subsequent cycles, and the development of
closure due to an increase in crack length. Experiments by Ewart & Suresh (1987) on
polycrystalline alumina show that the high frequency contact between the crack faces
generates debris particles of the ceramic, typically of the order of 1 jim in size, within
the crack. The presence of the debris particles promotes a wedging effect. Periodic
removal of the debris particles by ultrasonic cleaning of the crack leads to a sig-
nificant increase in the total distance of crack growth (Fig. 5.18). In ceramics with
grain sizes in the range 1-30 jim, crack growth over a distance of the order of 1 mm
194 Cyclic deformation and crack initiation in brittle solids
U.JU
0.45 -
0.40 -
0.35
0.30
U A= 0.75
0.20
•\i~ A
= 0.50
0.15
0.10 \ y\ A = 0.25
0.05 A
^0.00
0.00
^ — = 1 ^ 0.50
=^-0.75
-0.05
-0.10 i i t i i i
0 8 16 24 32
number of compression cycles, N (x 10~4)
Fig. 5.18. Variation of fatigue crack length a, measured from the notch tip, as a function of the
number of compression cycles in a-alumina of grain size = 1 8 urn (curve A). Curve B shows the
increase in crack growth rates as a consequence of reducing crack closure by the removal of
debris particles from the crack after every 5000 compression cycles using ultrasonic cleaning.
(After Ewart & Suresh, 1986.)
5.6 Fatigue crack initiation under far-field cyclic compression 195
has been observed under fully compressive far-field cyclic loads. The fatigue cracks
arrest after growth over this distance because of the development of crack closure in
cyclic compression and the exhaustion of the residual tensile field.
At the maximum far-field compressive stress, there exists a state of compression
immediately ahead of the notch tip. Complete unloading, however, gives rise to a zone
of residual tension at the notch tip. Numerical simulations by Brockenbrough &
Suresh (1987) reveal that residual tensile stresses are generated only after unloading
occurs below a certain critical value, crcr, of compressive stress, i.e. when
<rcr < <7°° < amax, Fig. 5.17. This result implies that the mean stress of the compression
fatigue cycle will have an important effect on the magnitude and extent of the residual
stressfield.As the mean stress is pushed far below the zero level, the extent of residual
tension will decrease and, consequently, crack initiation from the notch tip will become
more difficult. Such predictions have been confirmed independently by experimental
studies of the effects of cyclic compressive mean stress on crack initiation in /3-alumina
(James, Tait & Mech, 1991) and in brittle polymers (Pruitt & Suresh, 1993).
An important feature of the phenomenon of crack initiation from notches under
cyclic compression is that both monolithic and composite (brittle or ductile) solids
with vastly different microscopic deformation modes exhibit a macroscopically simi-
lar mode I fatigue crack growth behavior. The principal reason for this universal
trend is that residual tensile stresses are induced within the notch tip damage zone
during cyclic compression as long as permanent deformation occurs ahead of the
notch tip; such permanent deformation can be a consequence of dislocation plasti-
city, phase transformation, microcracking, interfacial sliding or creep. Since the zone
of residual tension is embedded within a compressive residual stress field, crack
initiation and growth in cyclic compression is intrinsically stable even in brittle
solids. Results of numerical analysis of the residual stress fields ahead of notches
subjected to cyclic compression have been reported by Suresh & Brockenbrough
(1988) and Suresh (1990a) for single phase ceramics, transforming ceramics, creeping
solids, and cement mortar.
Experimental studies of crack initiation in cyclic compression in ceramic compo-
sites have pointed out the potentially deleterious effects that fatigue loads can have on
the service life of a structural component (see, for example, Suresh, 1990a). Consider,
for example, the case of hot-pressed Si3N4 which is reinforced with SiC whiskers. It is
known that the addition of 20-30 volume% SiC to the Si3N4 matrix can lead to an
increase in fracture toughness by more than a factor of two over that of the unrein-
forced matrix material. However, when the composite contains stress concentrations,
the application of cyclic compressive loads causes fatigue cracks to initiate more easily
in the composite than in monolithic Si3N4. This effect can be rationalized by noting
that the stress-strain curve for the composite is more nonlinear than that for the
matrix material. Unloading from a far-field compressive stress can promote a higher
degree of permanent deformation which, in turn, may lead to larger residual tensile
stresses ahead of the stress concentration (see Fig. 5.17).
196 Cyclic deformation and crack initiation in brittle solids
(i) Four experiments are conducted where amin is held fixed and constant-
amplitude compressive stress cycles with the following R ratios are used:
(a) 2, (b) 10, (c) 30, and (d) oo (which corresponds to zero-compression
cyclic loading with a max = 0). How would you expect the initial rate of
crack growth and the maximum distance of crack growth under cyclic
compression (before complete crack arrest) to vary as a function of R for
these four cases?
(ii) Three additional experiments are conducted where <7max is held fixed and
the following R ratios are used: (a) 2, (b) 10, and (c) 30. How would you
expect the initial rate of crack growth and the maximum distance of crack
growth under cyclic compression (before complete crack arrest) to vary as
a function of R for these three cases?
Solution:
On the basis of the information provided, assume that the trends pre-
dicted by the simulations in Fig. 5.17 apply to the polycrystalline ceramic con-
sidered here.
Exercises 197
(i) It is evident from the preceding section and the given information that,
for fixed a min , the extent of permanent damage developed ahead of the
notch during compression loading is the same in all four cases. The extent
of residual tensile stresses generated upon unloading then is dependent on
the <rmax. That is, the closer is the value of amax to zero far-field stress (and
hence the higher the R ratio), the larger would be the tensile stress gen-
erated at the notch tip. Therefore, the maximum tensile residual stress
field (or a distance ahead of the notch tip over which a tensile stress of
some level is developed) would be expected to increase with an increase in
the applied R ratio. Consequently, the initial rate of crack growth and the
maximum distance of crack growth under cyclic compression (before
complete crack arrest) would both increase with an increase in R ratio.
(ii) For a fixed value of applied a max , amin increases with increasing R. Larger
the value of R, greater would be the amount of permanent deformation
(in this case, microcracking) at the notch-tip. As a simple approximation,
one would then expect X to be higher for higher values of R. From Fig.
5.17, it could then be argued again that the extent of tensile residual stress
field, the initial rate of crack growth and the maximum distance of crack
growth under cyclic compression (before complete crack arrest) would all
increase with an increase in R ratio.
Exercises
5.1 Two dislocations in BCC a-iron with Burgers vectors a o /2 [111] and
ao/2 [111] (where a0 is the lattice dimension) glide along two intersecting
{110}-type slip planes meet.
(a) Write down the dislocation reaction and show that it is energetically
favorable.
(b) Discuss the orientation of a possible cleavage crack which could be
triggered by this Cottrell mechanism.
5.2 A cubic crystal contains a mixed dislocation (i.e. a dislocation with com-
bined edge and screw components) with a Burgers vector parallel to [001].
What would be the orientation and geometry of the steps on the cleavage
fracture surface for a crack propagating along the cleavage plane (001)?
Discuss various possibilities for the crack-dislocation intersection.
5.3 Consider a brittle elastic solid which is subjected to cyclic loading. The
material is first loaded in uniaxial tension. At a threshold tensile stress a T ,
microcracks initiate in the material; a further increase in tensile stress to a
peak value of ^Tmax results in a progressive increase in both the number of
microcracks per unit volume and the average size of the microcracks, and in
198 Cyclic deformation and crack initiation in brittle solids
the release of the residual thermal strain. The specimen is unloaded at crTmax.
During unloading, the microcracks remain open until a far-field tensile
stress of a Tcont . Below orTcont, lowering the far-field stress to zero and sub-
sequent load reversal into compression results in a gradual recovery of
stiffness until all the microcrack surfaces are closed (where the far-field
stress is trCclose). Further increases in compressive stress to a peak value of
a Cmax are borne by the fully dense elastic solid. Unloading from the far-field
compressive stress results in the elastic recovery of a fully dense solid until
the microcracks reopen at a far-field compressive stress of a Copen , with
I^Copenl > I^Cclosel-
(a) Plot the variation of the far-field stress against the average inelastic
strain (i.e. total strain minus the elastic strain for the fully dense
solid) for one full fatigue cycle involving zero-tension-zero-compres-
sion-zero loading.
(b) How is the stress-strain curve in (a) affected by the presence of a popu-
lation of pre-existing microcracks prior to fatigue loading.
(c) Suppose that, in (a), frictional sliding occurs between the faces of the
microcracks (as, for example, along grain boundaries or shear bands)
upon unloading from the far-field compressive stress. Schematically
sketch the stress-strain curve by incorporating the sliding mechanism.
5.4 Cyclic indentation of a brittle solid exhibits some features which are quali-
tatively similar to those discussed in connection with the cyclic compression
loading of a notched brittle solid. Discuss the similarities and differences
between the initiation of a fatigue crack in a notched brittle solid subjected
to cyclic compression loading and the cracking that occurs beneath the tip of
an indenter repeatedly pressing against the surface of a brittle solid.
5.5 The mechanism for the nucleation of a crack by the pile-up of dislocations,
Fig. 5.9(#), at an obstacle (such as a grain boundary) was proposed by A.N.
Stroh (Proceedings of the Royal Society, London A223, p. 404, 1954, and
A232, p. 548, 1955). Since the dislocation pile-up leads to stress concentra-
tion in much the same way as a mode II crack, the near tip stress fields ahead
of a mode II crack, Eqs. 9.47, can also be used to model the fields ahead of
piled-up dislocations. Stroh postulated that cleavage fracture will nucleate
at an obstacle when the maximum local tensile stress, aee reaches a critical
value.
(a) Using Eq. 9.47, show that aee is a maximum at an angle of-70.5° from
the plane of dislocation pile-up.
(b) Following a procedure similar to that used in the previous problem on
the Petch relationship, show that the cleavage fracture stress takes the
form:
aF = ai+kFd~l/2,
Exercises 199
200
6.1 Deformation features of semi-jnoncrystalline solids 201
complete crystallization in polymeric solids arise from the very existence of the long-
chain molecule and of the chain branches and side groups. Consequently, the struc-
ture of a polymer can be fully amorphous or of a semi-crystalline arrangement in
which folded molecular chains are formed amid an amorphous phase.
With the exception of some modes of deformation such as craze formation or the
rotation of molecular chains, the mechanisms of deformation and failure in poly-
meric solids exhibit many similarities to those discussed earlier in this book for
metals and ceramics. Under cyclic loading, polymers display deformation modes
(such as stress-strain hysteresis and cyclic softening) and subcritical crack growth
analogous to atomic solids. It was shown earlier in the context of fatigue in metals
and alloys (Chapters 2-4) and in ceramic materials (the preceding Chapter) that
kinematic irreversibility of microscopic deformation is an important reason for the
onset of true mechanical fatigue effects. In polymeric solids, such kinematically
irreversible deformation can be manifested as crazing, shear band formation, rota-
tion or other changes in the orientation of molecular chains, or a combination of
these mechanisms.
In this sense, crazes lead to inelastic strains in much the same way as the shear
and/or dilatant transformations in metals and ceramics (such as mechanical twins
or martensitic lamallae). Furthermore, purposely promoting the formation of
crazes at lower stress levels in an attempt to develop appreciable dilatational
plasticity is viewed as a possible means of toughening polymers (e.g., Argon,
1989). This approach is conceptually similar to the mechanisms of microcrack or
transformation toughening in brittle solids (see Chapter 5). Cyclic deformation and
the subcritical advance of fatigue fracture in many polymers are dictated by the
nucleation, growth and breakdown of crazes.
A craze contains fibrils of highly oriented molecules (craze matter) separated by
porous regions. The density of the craze matter is only 40 to 60% of the matrix
density and the molecular fibrils are oriented along the direction of the maximum
tensile stress. Figures 6.1 (a) and (b) are electron micrographs of a newly formed craze
Fig. 6.1. (a) A newly formed craze in a thin slice of PS. Note the orientation of the craze normal
to the tensile stress axis (indicated by the arrow) and of the fibrils parallel to the tensile stress
axis, (b) An electron micrograph of the central section of another craze. (From Beahan, Bevis &
Hull, 1971. Copyright Taylor & Francis, Ltd. Reprinted with permission.)
6.1 Deformation features of semi-jnoncrystalline solids 203
in a thin slice of PS which was loaded on a mini-tensile straining device. Note that
the craze is oriented normal to the uniaxial tensile stress and that the fibrils within
the craze are aligned with the tensile axis. (The craze geometry is discussed in further
detail in Chapter 12.) It is generally known that the criterion for the nucleation of a
craze in a three-dimensional stress state is of the form:
(6.1)
where <rmax and amin are maximum and minimum principal stresses, respectively,
A(T) and £l\(T) are material constants which depend on the temperature, and aH
is the hydrostatic stress (Section 1.4). Even if the overall hydrostatic stress is nega-
tive, a craze can advance if there exists one tensile stress component (with the craze
extending normal to the tensile stress direction). The nucleation of crazes in crazable
polymers has been investigated in detail, and the criteria for their formation have
been developed in terms of the tensile hydrostatic stress component and the devia-
toric stress component of the imposed stress state (e.g., Argon & Hannoosh, 1977;
Argon, 1989).
The growth of crazes is also a topic of considerable interest because cracking in
many polymers is preceded by the formation of a craze. In this sense, the craze zone
ahead of a crack in a polymer is somewhat analogous to the plastic zone in front of a
crack in a ductile metallic material. Under an imposed stress, the craze extends by
drawing more polymer from its surface into the fibril while the fibrils themselves
deform by creep, Kramer & Hart (1984); see Section 12.2 for further details.
Shear localization is also a prominent feature of deformation and failure in many
polymers. At stress levels lower than the tensile strength of the glassy polymer,
'plastic' deformation can be initiated by the formation of shear bands. In polymers
susceptible to shear banding, the onset of 'yielding' is associated with the inception
of shear bands. Figure 6.2 shows shear bands in plastically stretched PETP. Shear
bands are always oriented along the direction of the maximum shear stress.
Fig. 6.2. Shear bands (sb) and crazes (c) in plastically stretched PETP. (From Argon, 1980.
Copyright Academic Press. Reprinted with permission.)
(2) The second major distinction between fatigue of metals and polymers is the
degree to which the loading rate influences the stress-strain characteristics
and failure modes. For many polymeric materials, even room temperature is
a significant fraction of the homologous temperature. Furthermore, hystere-
tic damping effects are substantial in thermoplastics as a result of their
strong nonlinear viscous behavior, which is not the case for metals. These
factors, coupled with the poor thermal diffusivity of polymers, can result in
marked increases in temperature during cyclic deformation at sufficiently
high strain rates. The attendant thermal softening becomes an important
consideration and may even dominate over any intrinsic mechanical fatigue
effects. These interactions between adiabatic thermal effects and mechanical
fatigue are complex. For certain combinations of stress amplitudes and
strain rates, thermal effects exacerbate the fatigue failure process while, in
other cases, the combination of the thermal and mechanical effects is not
deleterious to fatigue life. The imposition of low strain rates to circumvent
6.2 Cyclic stress-strain response 205
25 MPa i-
12
strain (%)
(b)
Fig. 6.3. Cyclic softening in PC subjected to strain-controlled fatigue at 298 K. (a) Change in the
size and orientation of the hysteresis loops with the progression of fatigue deformation, (b)
Stress-strain response in monotonic tension and fatigue. (From Rabinowitz & Beardmore,
1974. Copyright Chapman & Hall. Reprinted with permission.)
stress-strain curve in monotonic and cyclic loading can also be obtained in a similar
fashion. The origin of the differences between monotonic and cyclic response is
linked to the molecular rearrangements. During cyclic deformation, the strains are
accommodated by molecular rearrangements at the microscopic level, whereas
monotonic loading promotes more macroscopic permanent deformation associated
with molecular rearrangements.
6.2 Cyclic stress-strain response 207
Fig. 6.4. Examples of failure due to cyclic thermal softening (top) and mechanical fatigue
(bottom) in PMMA. The total length of the test specimen is 110 mm. (From Constable,
Williams & Burns, 1970. Copyright Council of the Institution of Mechanical Engineers.
Reprinted with permission.)
208 Cyclic deformation and crack initiation in noncrystalline solids
f
Lf, \E*\ = ^ = J(Ef + {Ef. (6.3)
6
£ is known as the storage modulus and it denotes the ratio of the stress in phase
with the strain to the strain. The imaginary number i = V—T. E is the loss
modulus and it is the ratio of the stress which is 90° out of phase with the strain
to the strain. The linear viscous deformation due to sinusoidal fatigue loading
can also be characterized in terms of the complex compliance,
where, analogous to the storage modulus and loss modulus, D' and D" denote
the storage compliance and loss compliance, respectively. The entity
tan 8 = E /E = D"ID' is known as the loss tangent.
(i) Find the rate of hysteretic energy dissipated per fatigue cycle.
(ii) If H represents the heat transfer coefficient for loss of heat from the
specimen surface to the surroundings, and T and To are the instantaneous
specimen temperature and the ambient temperature, respectively, derive
an expression for the rate of temperature increase assuming adiabatic
heating conditions.
Solution:
(i) The rate of hysteretic energy dissipated as heat, Q, per unit volume of the
material during fatigue loading is given by
where k is the strain rate and the superscripts ' and " indicate the real and
imaginary components, respectively (Constable, Williams & Burns, 1970).
Combining Eqs. 6.2 and 6.5 with the result that o1 = a/2(l + tan2 6), one
obtains the energy loss per stress cycle,
tan
' (6.6)
E l+tan2<5
The average energy dissipation rate per unit volume is
Q= co_ = nvA tana = ^ (6J)
* ^ In E l+tan 2 5 ° V
For cyclic loading with a zero mean stress, the peak stress value of the
fatigue cycle is the same as the stress amplitude Aa.
(ii) If adiabatic heating conditions prevail (i.e. heating in which all of the heat
generated within the polymer is manifested as a temperature rise and
none is lost to the surroundings), the time rate of change of temperature
dT/dt is given by
6.2 Cyclic stress-strain response 209
dT nvcD/fa0
(6.8)
~d7
where p is the mass density and cp is the specific heat. In reality, however,
some heat is lost to the surroundings. Equation 6.8 may be modified to
account for heat loss:
dT nvcD"crQ HA
(T-To). (6.9)
~d7 pcp pcp V
Here A and V are the surface area and volume of the fatigue test speci-
men, respectively. Note that the loss compliance D" depends strongly on
both tempeature and strain rate. As the specimen temperature increases
and approaches a critical softening temperature, the specimen becomes
too soft to support the load and suffers catastrophic fracture.
1JJJ J 1 1
F
i
103 104 105 106 107
number of cycles to failure, Nt
Fig. 6.5. Effect of the applied stress range ACT on temperature rise in PTFE subjected to stress-
controlled fatigue. The symbol x denotes failure of the specimen. (After Riddell, Koo &
O'Toole, 1966.)
210 Cyclic deformation and crack initiation in noncrystalline solids
number of cycles. The rate of initial elevation in temperature is higher for the larger
values of Aa. However, when Aa < Aae (i.e. for curve F), the temperature increase
is not sufficient to cause thermal failure. Consequently, the temperature stabilizes
after prolonged fatigue loading, and the specimen is essentially capable of sustaining
an infinite number of fatigue cycles.
Koo, Riddell & O'Toole (1967) performed fatigue experiments in an attempt to
quantify the effect of thermal softening on fatigue life in three fluoropolymers:
PTFE, polychlorotrifluoroethylene (PCTFE), and polyvinylidenefluoride (PVF2).
They derived estimates of the loss compliance D" during fatigue on the basis of
dynamic modulus measurements using a torsional pendulum. It was found that
hysteretic heating caused a significant increase in loss compliance (Fig. 6.6). With
an elevation in material temperature, the specimen became too soft to fail by purely
mechanical fatigue, but instead suffered a loss in fatigue strength by thermal soft-
ening. This damage was at least partially recoverable by annealing the specimen in
the early and intermediate stages of temperature rise (see Fig. 6.5). The most sig-
nificant effect of temperature rise on fatigue damage was observed in the stress cycles
just prior to final failure.
2.0 x l O 1 1
2 1.5 xlO"11
x
£ 1 x 10~u
Q 12
5x10
I I 1
20 60 100 140
Fig. 6.6. Change in loss compliance D" due to temperature rise in PTFE subjected to stress-
controlled fatigue at room temperature at a cyclic frequency of 30 Hz. (After Koo, Riddell &
O'Toole, 1967.)
6.3 Fatigue crack initiation at stress concentrations 211
lOOMPar-
Fig. 6.7. Anomalous fatigue deformation of PC at 77 K where craze formation leads to cyclic
softening only in the tensile portion of cyclic loading. (From Rabinowitz & Beardmore, 1974.
Copyright Chapman & Hall. Reprinted with permission.)
loop remains stable in the compression portion. This type of anomalous softening is
also seen in the stress-strain response of polymers when the deformation mechanism
involves the stable growth of microscopic cracks under fatigue loading (Beardmore
& Rabinowitz, 1975).
The overall fatigue response of a polymer is dictated by a combination of factors
involving the molecular structure, deformation modes, and cyclic loading conditions
(Hertzberg & Manson, 1980, 1986), which include:
(1) polymer composition, molecular weight and distribution, and thermody-
namic state,
(2) structural and morphological changes induced by the mechanical loads and
the environment, such as bond breakage, molecular alignment and disen-
tanglement, or crystallization,
(3) the type of deformation, such as elastic, linear viscoelastic or nonlinear
viscoelastic response,
(4) the mode of microscopic failure, such as crazing or shear banding,
(5) thermal softening, and
(6) the time-scale of the experiment vis-a-vis the kinetic rate of the processes
causing structural changes.
the nucleation and growth of fatigue cracks along the plane of the notch. A similar
phenomenon was reported for polymeric materials by Pruitt & Suresh (1993).
Figures 6.8(#) and (b) show examples of fatigue crack growth normal to the far-
field cyclic compression axis in notched specimens of an untoughened polystyrene
and a high-impact polystyrene comprising 7.5 wt% butadiene rubber in the form of
gel particles with an average diameter of 1-2 urn. (The rubber particles are added to
the polystyrene to enhance its toughness through increased craze formation.)
Inelastic deformation at the tip of notch, arising from such irreversible deforma-
tion processes as shear localization and rotation of molecular chains, generates a
zone of residual tensile stresses upon unloading from the first compression cycle. If
the magnitude of such compressive stresses exceeds the craze strength, crazes
oriented parallel to the plane of the notch and normal to the far-field compression
{<*)
0.1 mm
0.1 mm
Fig. 6.8. Fatigue crack initiation and growth normal to the cyclic compression axis in (a) an
untoughened PS (weight-average molecular weight, M w = 300 000 and polydispersity = 2.4),
and (b) a high-impact polystyrene comprising 7.5 wt% butadiene rubber in the form of gel
particles with an average diameter of 1-2 jam (M w = 240000 and polydispersity = 2.8). The
compression axis is vertical. (From Pruitt & Suresh, 1993. Copyright Taylor & Francis, Ltd.
Reprinted with permission.)
6.4 Case study: Compression fatigue in total knee replacements 213
axis (i.e. normal to the local maximum tensile stress) are induced ahead of the notch-
tip. This provides a strong kinematically irreversible damage mechanism for the
generation of residual tensile stresses in the subsequent cycles and for the advance
of the crack.
The white region immediately ahead of the notch in Fig. 6.8(Z?) is approximately
indicative of the region in which crazing occurs during cyclic compression. Figure
6.9(a) shows a transmission electron micrograph of a typical craze observed within
this region during the cyclic compression loading of the toughened polystyrene.
Figure 6.9(6) shows the craze penetrating through the rubber particle and the
matrix. The features of the craze formed under imposed cyclic compression are
the same as those produced during monotonic or cyclic tension (Pruitt & Suresh,
1993).
In-situ photoelastic and laser interferometric measurements have also been carried
out in notched plates of a photoelastic resin to quantify the evolution of residual
tensile stresses ahead of the stress concentration upon unloading from the far-field
compression axis. Figure 6.10 shows the evolution of an increasing tensile residual
stress field at the notch tip upon unloading from a maximum applied compressive
stress of-16.5 MPa. Plotted in Fig. 6.10 are the contours of constant oyy (i.e. stress
normal to the plane of the notch) at different stages of unloading. At an applied
compressive stress of-2.76 MPa, tensile stresses with a magnitude in excess of +4.96
MPa span a distance of 0.07 mm ahead of the notch tip. Upon unloading to -0.92
MPa, the stresses exceed +7.6 MPa over a distance of 0.11 mm. Further unloading
to -0.55 MPa causes the residual tensile stresses to exceed + 9.1 MPa over a distance
of nearly 0.1 mm. Given that the tensile strength of the brittle photoelastic resin is
only 6.7 MPa, the stress measurements shown in Fig. 6.10 provide a justification for
the nucleation of a fatigue crack ahead of the notch under cyclic compression load-
ing. The overall initiation and growth characteristics of compression fatigue cracks
in polymers are qualitatively similar to those of metals and ceramics (see Sections
4.11 and 5.6).
Fig. 6.9. (a) A transmission electron micrograph of a typical craze produced ahead of the notch
during the cyclic compression loading of the toughened polystyrene, (b) shows the craze
penetrating through the rubber particle and the matrix. The far-field compression axis is
approximately perpendicular to the craze in both figures. (From Pruitt & Suresh, 1993.
Copyright Taylor & Francis, Ltd. Reprinted with permission.)
As the articulating surfaces of the knee joint move during flexion, the polymer
component is subjected to complex stress distributions within and at the surface of the
UHMWPE insert. In a total knee replacement, the polymer insert is compressed by the
metal component and results in compressive stresses perpendicular to the articulating
surface (Bartel, Bicknell & Wright, 1986). The delamination and pitting of the tibial insert
6.4 Case study: Compression fatigue in total knee replacements 215
A + 1.9 MPa
A —- + 0.6 MPa B + 3.4 MPa
B —- -f LBMPa C +5.5 MPo
C — — + 3.2MPO D +7.6 MPo
0 - — • 4.9 MPo
(a) (*)
A —
+ 6.7 MPq
+ 2 9 MPo
L, 0.3mm
B -- + 5.4 MPo
C — + 7.4 MPo
0 — + 9.1 MPQ
Fig. 6.10. In-situ photoelastic and laser interferometric measurements of the evolution of tensile
residual stresses in a photoelastic resin during different stages of unloading from a maximum
far-field compressive stress of-16.5 MPa. Far-field compressive stress magnitudes: (a) -2.75
MPa, (b) -0.92 MPa, and (c) -0.55 MPa. (After Pruitt & Suresh, 1993.)
also produces polymer debris which is known to cause osteolysis, infection and loosening
of the implants (Mirra, Marder & Amstuz, 1982).
Bartel, Bicknell & Wright (1986) have used a three-dimensionalfinite-elementmodel
(FEM) to analyze the stresses in condylar-type knee replacements, Fig. 6.12. This
model comprises a metal-backed UHMWPE with a uniform concave surface and the
arrangement is loaded by a metal component with a convex surface. The contact
surfaces are defined by two radii of curvature as the knee prosthesis has distinct radii
for extension and flexion. For the analysis, the contact forces were chosen to simulate
in-vivo conditions with femoral-tibial contact forces ranging from 4.3-4.9 times the
216 Cyclic deformation and crack initiation in noncrystalline solids
Fig. 6.11. A schematic representation of the geometry of interest in total knee replacement.
body weight of a typical patient. For the total knee replacement, it was found that the
maximum principal stress occurred at the surface of the UHMWPE and along the
tangent to the articulating surface. The greatest magnitudes of stresses were found to be
compressive and located at the center of contact. Further, the stresses were found to be
cyclic in nature through the natural action of flexion and extension. The model
demonstrated that the maximum principal stress at a point near the surface of a total
condylar type tibial knee component can range from 10 MPa of tension to more than
20 MPa of compression as the contact area sweeps across the surface in the action of knee
flexion, Fig. 6.12. From this work, it was established that the primary damage mechan-
isms in the total knee replacement are driven by compressive or compression-dominated
cyclic loading.
In an attempt to simulate the potentially deleterious effects of cyclic compressive
loads in nucleating fatigue cracks at corners and stress concentrations in knee
prosthesis, Pruitt & Suresh (1993) and Pruitt et al. (1995) carried out systematic
experiments of compression fatigue cracking at notches in sterilized and unsterilized
UHMWPE. On the basis of these laboratory experiments and from the information
available from knee replacement components, it was concluded that the inception and
growth of sharp fatigue cracks which have initiated under cyclic compressive loading
can be further extended by subsequent action of cyclic tensile stresses to such a critical
crack length that pitting, delamination and fatigue failure can occur at the UHMWPE
surface.
Exercises 217
articulating
surfaces
region
analyzed by
finite elements
{a)
A.I mm
anterior
10.9 mm
- edge of
contact area
Fig. 6.12. (a) A schematic of the condylar-type tibial insert made of UHMWPE. The finite
element mesh is also superimposed in this figure to illustrate the geometry analyzed, (b)
Magnitudes of the maximum principal stress (in units of MPa) at the surface of the knee
replacement during extension, (c) Magnitudes of the maximum principal stress (in units
of MPa) at the surface of the knee replacement during flexion. (After Bartel, Bicknell &
Wright, 1986.)
Exercises
6.1 A mechanical test is conducted on three different materials. In this experi-
ment, a constant tensile stress is applied instantly to a specimen. The first
material, a rubber, deforms rapidly during the application of the stress, with
218 Cyclic deformation and crack initiation in noncrystalline solids
TOTAL-LIFE APPROACHES
CHAPTER 7
Stress-life approach
' A case study of the HCF fatigue problem in aircraft gas turbine engines is presented in Section 7.6.
221
222 Stress-life approach
Fig. 7.1. Typical S-N diagram showing the variation of the stress amplitude for fully reversed
fatigue loading of nominally smooth specimens as a function of the number of cycles to failure
for ferrous and nonferrous alloys.
7.1 The fatigue limit 223
a
Endurance limit based on 5 x 108 cycles. Source: Aluminum Standards and Data, The
Aluminum Association, New York, 1976.
b
Endurance limit based on 107 cycles. Source: Structural Alloys Handbook, Mechanical
Properties Data Center, Traverse City, Michigan, 1977.
'Refers to quenched and tempered condition; the data within parentheses refer to tempering
temperature.
Many high strength steels, aluminum alloys and other materials do not generally
exhibit a fatigue limit (see dashed line in Fig. 7.1). For these materials, cra (or ACT)
continues to decrease with increasing number of cycles. An endurance limit for such
cases is defined as the stress amplitude which the specimen can support for at least
107 fatigue cycles. Table 7.1 lists the fatigue endurance limits for a variety of engi-
neering alloys along with crTS and the monotonic yield strength, cry.
If Fig. 7.1 is redrawn on a log-log scale, with the (true) stress amplitude plotted as
a function of the number of cycles or load reversals! to failure, a linear relationship
is commonly observed. The resulting expression relating the stress amplitude,
o-a = Acr/2, in a fully-reversed, constant-amplitude fatigue test to the number of
load reversals to failure, 27Vf, is (Basquin, 1910)
-— = aa = crf(2Nf) , (7.1)
' A constant amplitude cycle is composed of two load reversals. As shown later in this chapter and the
next one, the use of the number of load reversals, instead of the number of fatigue cycles, is helpful in
analyzing variable amplitude fatigue.
224 Stress-life approach
crack initiation
Nf (log scale)
Fig. 7.2. Contributions of crack initiation and crack propagation processes to total fatigue life
in a nominally smooth specimen.
which, for most metals, is in the range of —0.05 to —0.12. Typical values of o\ for
many engineering alloys are tabulated in the next chapter.
The S-N curve schematically shown in Fig. 7.1 strictly pertains to the total
fatigue life of a nominally smooth-surfaced, 'defect-free' material. Here total life
implies the number of cycles to initiate fatigue cracks in the smooth specimen plus
the number of cycles to propagate the dominant fatigue crack to final failure. This
two-stage process involving initiation and propagation is represented in the S-N
curve shown in Fig. 7.2. The fraction of the fatigue life which is expended in nucle-
ating a dominant fatigue crack of engineering size (typically a fraction of a mm) may
vary from essentially 0%, for specimens containing severe stress concentrations,
rough surfaces or other surface defects, to as high as 80% in very carefully prepared,
nominally defect-free, smooth specimens of high purity materials.
Fig. 7.3. Nomenclature for stress parameters which affect fatigue life. The variation of stress a
with time t is shown.
The mean stress is also characterized in terms of the load ratio, R = <rr^n/crmax. With
this definition, R = — 1 for fully reversed loading, R = 0 for zero-tension fatigue, and
R = 1 for a static load.
When the stress amplitude from a uniaxial fatigue test is plotted as a function of
the number of cycles to failure, the resultant S-N curve is generally a strong function
of the applied mean stress level. Figure 1.4(a) shows the typical S-N plots for
metallic materials as a function of four different mean stress levels, crml, am2, a m3
and <rm4. One observes a decreasing fatigue life with increasing mean stress value.
Mean stress effects in fatigue can also be represented in terms of constant-life
diagrams, as shown in Fig. lA(b). Here, different combinations of the stress ampli-
tude and mean stress providing a constant fatigue life are plotted. Most well known
among these models are those due to Gerber (1874), Goodman (1899),f and
Soderberg (1939). The life plots, represented in Fig. 7.4(Z>), are described by the
following expressions:
where a a is the stress amplitude denoting the fatigue strength for a nonzero mean
stress, cra\am=0 is the stress amplitude (for a fixed life) for fully-reversed loading
(am = 0 and R = — 1), and <ry and <rTS are the yield strength and tensile strength of
the material, respectively.
' The modified Goodman equation, Eq. 7.4, is generally considered to be a modification of methods
originally proposed by a number of different engineers.
226 Stress-life approach
(b)
Fig. 7.4. (a) Typical stress amplitude-life plots for different mean stress values, (b) Constant life
curves for fatigue loading with a nonzero mean stress.
(1) Equation 7.3 provides a conservative estimate of fatigue life for most engi-
neering alloys.
(2) Equation 7.4 matches experimental observations quite closely for brittle
metals, but is conservative for ductile alloys. For compressive mean stresses,
however, it is generally nonconservative. To circumvent this problem, one
may assume that compressive mean stresses provide no beneficial effect on
fatigue life.
(3) Equation 7.5 is generally good for ductile alloys for tensile mean stresses. It
clearly does not distinguish, however, between the differences in fatigue life
due to tensile and compressive mean stresses.
The constant life diagram for different mean stress levels, also commonly referred
to as the Haigh diagram (Haigh, 1915, 1917), is schematically represented as shown
in Fig. 7.5. In this figure, the maximum and minimum stresses of the fatigue cycle,
both normalized by the tensile strength, are plotted. The dashed lines denote experi-
mentally determined values of combinations of maximum and minimum stress levels
(representing different mean stresses) which represent constant fatigue lives for the
indicated number of cycles. This figure affords a convenient graphical representation
of the effects of mean stress on S-N fatigue response, although considerable experi-
mental effort is needed to determine empirically the information needed for this plot.
Similar diagrams are also developed for notched members where the net-section
stresses are used.
While the Basquin relation, given by Eq. 7.1, is valid only for zero mean stress,
Morrow (1968) has presented a modification of the Basquin relation which accounts
for mean stress effects (for any am) in the following form:
f (7.6)
7.3 Cumulative damage 227
Fig. 7.5. A schematic representation of the Haigh diagram showing constant life curves for
different mean stress levels in terms of the maximum and minimum stresses of the fatigue cycle.
The number of cycles to fatigue failure for any nonzero mean stress, iVf, can then be
written as
\/b
Nf = 1 - (7.7)
where TVf 1^ = 0 *s the number of cycles to failure for zero mean stress.
(3) Failure occurs when the linear sum of the damage from each load level
reaches a critical value.
If nt is the number of cycles corresponding to the /th block of constant stress
amplitude aai in a sequence of m blocks, and if Nfi is the number of cycles to failure
at aai, then the Palmgren-Miner damage rule states that failure would occur when
It will be shown in later chapters that damage accumulation and failure under
variable amplitude loading conditions are dictated by several concurrent mechan-
isms and that the linear damage rule may lead to erroneous predictions of variable
amplitude fatigue behavior in many situations. For example, the Palmgren-Miner
damage rule predicts a greater degree of fatigue damage due to a higher amplitude of
cyclic stresses. However, it is well established that tensile overloads applied to
notched and cracked metallic materials reduce the rate of fatigue crack growth
and that the application of compressive overloads generally has the opposite trend
(see Chapter 14).
Even for smooth specimens, the linear damage rule may provide incorrect results
because of its omission of load sequence effects. Consider a smooth fatigue specimen
which is subjected to nx and n2 cycles of two different amplitudes of cyclic stresses,
a al and a a2 , respectively, which have the same R ratio. As shown in Fig. 7.6,
a
ai > aa2- Let the fatigue life (number of cycles to failure) at cr^ and a a2 be Nn
and JVf2, respectively.
Case 1:
First consider the loading sequence in which cra2 is applied after oral. The
extent of damage induced by this lower stress level may be in excess of the damage
rule prediction of n2/Nf2, if the preceding application of <ral for n\ cycles had
nucleated cracks or significantly contributed to the number of cycles necessary at
the lower stress level to nucleate cracks. Consequently, one may observe for this case
that ]T ni/Nfi < 1. In this case, damage may occur even if cra2 is below the endurance
limit.
Case 2:
Now consider the reverse situation where the application of a a2 precedes
that of <jal. If the material strain-ages, the application of aa2 prior to <xal may
enhance the fatigue limit even if a a2 is lower than the fatigue limit. This phenomenon
is known as coaxing. For this case, J2
Case 1 Case 2
n2 cycles
(a) (b)
Fig. 7.6. Block loading sequence for (a) case 1 and (b) case 2. (c) Fractional life expended as
estimated by the Palmgren-Miner rule.
ufacturing of the component has a decisive role in dictating the initiation life for
fatigue cracks.
There exists a variety of surface treatments, such as carburizing, nitriding, flame
hardening, induction hardening and shot-peening, which are designed to impart high
strength, wear resistance or corrosion resistance locally in the near-surface regions of
the material. Furthermore, common machining operations such as grinding, polish-
ing and milling cause different degrees of surface roughness to develop. The valleys
on the rough surface serve as stress concentrations, which, in turn, induce different
levels of resistance to fatigue crack nucleation (see Chapters 4 and 15 for further
discussions on this issue).
In addition to the roughness of the surfaces, the residual stresses that are induced
by the surface treatments have an important effect on the fatigue life. Residual
stresses are generated in a component as a consequence of thermal, chemical or
mechanical treatments:
vessels are some examples. Deleterious residual stress patterns may also
arise from mechanical working, as, for example, in the undesirable devel-
opment of tensile stresses due to cold straightening (e.g., Osgood, 1982).
(2) Local volume changes associated with precipitation, chemical reactions, or
phase transformations induce residual stresses in a component. Case hard-
ening of a surface by nitriding produces compressive stresses in the diffusion
region.
(3) Each fabrication technique, such as grinding, milling, polishing, rolling, and
welding, produces its own characteristic residual stress patterns.
(4) Even in the absence of phase changes, nonuniform thermal expansion or
contraction produces residual stresses. An example of the development of
thermal residual stresses can be found in processes involving rapid quench-
ing and in thermal fatigue.
Residual stresses arising from fabrication or surface and heat treatments, when
superimposed with the applied fatigue loads, alter the mean level of the fatigue cycle
and the fatigue life for crack nucleation. In general, residual stresses affect the fatigue
behavior of materials in the same way as the static mechanical stresses superimposed
on a cyclic stress amplitude. Therefore, residual stresses are favorable, if compressive,
and detrimental, if tensile; this is especially true for high strength materials. The ben-
eficial effect of residual stresses introduced by surface treatments becomes less signifi-
cant at larger applied stresses (at lower fatigue lives) because a large amplitude of the
pulsating stress easily 'relaxes' the residual stress, particularly in softer materials.
Consider, for example, the case of shot-peening, which is widely used to improve
the fatigue life of many engineering structural parts. Examples of shot-peened com-
ponents include chassis, valve springs, gears and shafts for automobiles, and exhaust
stack for aircraft engines. In the shot-peening process, a stream of small, hard
spheres (typically 0.1 to 1 mm in diameter) is shot at a surface which is to be treated.
Depending on the diameter of the shots, the velocity of their impingement on the
surface and the duration of the process, the maximum (long range) compressive
residual stress generated by the localized plastic deformation of the surface layer
can reach about one-half the yield strength of the material. The compressive residual
stress zone spans a depth of about one-quarter to one-half the diameter of the shots.
As the shot-peened surface layer has a compressive mean stress, it acts to enhance
significantly the total fatigue life by reducing the damaging effect of the tensile
portion of fully reversed cyclic loads. Figure 7.7 shows an example of the beneficial
effect of shot-peening on the endurance limit of steels with different levels of surface
finish. A worked example quantifying the benefits of shot-peening in contact fatigue
applications is presented in Chapter 13, where the combined effects of surface rough-
ness, peening and lubrication on S-N fatigue behavior and the endurance limit are
also examined.
Caution should be exercised in designing the parameters for shot-peening. If shot-
peening is done for a longer time span than necessary, it may induce cracks along slip
7.5 Statistical considerations 231
1000
. as-fabricated
* shot-peened after fabrication
750
polished or ground
500
250
2000
Fig. 7.7. Beneficial effect of shot-peening on the fatigue life of steels of different strength levels.
The endurance limit cre (defined at 2 x 106 stress cycles) is plotted against the tensile strength,
flrjs. (After Mann, 1967.)
Here, Ns denotes the number of samples of a random variable xrv (such as the stress
amplitude in an S-N fatigue test), and mx rv and ax rv denote the mean and the
standard deviation, respectively.
A distribution in the value of the random variable is usually characterized in terms
of normal distribution, log-normal distribution, or Weibull distribution. For exam-
ple, the probability density function for normal distribution is defined as
(7.10)
where the mean mx rv and the standard deviation ax rv are as defined previously.
Usually, the fatigue strength or the endurance limit values listed from experiments
represent the arithmetic mean derived from multiple experiments. In brittle solids,
such as ceramics and polymers, and in metallic alloys with considerable microstruc-
tural variability arising from processing, the extent of scatter in fatigue data may be
large as a result of a large scatter in microscopic flaw size distribution. Consequently,
7.5 Statistical considerations 233
different sets of experiments conducted on the same material may not give the same
arithmetic mean of the critical strength parameter. To address this issue, Weibull
(1939) proposed the concept of a probability of failure, P, at a given failure strength,
crf normalized by an average value of a critical stress <rcr ave (which may be identified
with the average value of tensile fracture strength cru for a brittle solid or with the
fatigue endurance limit, a e for a metallic alloy). At low values of <xf, P -> 0, and at
very high values of a f , P -> 1. Weibull defined the failure probability as follows:
-( — I ' (7-H)
Wo/ J
where raw is known as the Weibull modulus, and af 0 is a reference strength. Note
that P in Eq. 7.11 represents the fraction of the total number Ns of identical test
specimens in a batch for which the failure strength falls below <rf. Similarly, Ps, the
probability of survival, represents the fraction of the total number Ns of identical test
specimens in a batch for which the failure strength exceeds <jf. When crf/<7f 0 = 1,
P = 1 — e x p ( - l ) = 0.633. In other words, the reference stress Of0 represents the
stress level for which the cumulative probability of failure of all specimens in the
same batch at a stress level af or lower, is 63.3%. Equation 7.11 can be rearranged to
give
1.0
0.0
(a)
-wwln(af0)
(b) ln(af)
Fig. 7.8. (a) A Weibull plot of failure probability against the normalized failure strength, (b) The
Weibull diagram, based on Eq. 7.13, whose slope is the Weibull modulus, raw.
amplitude at a fixed life) to cause failure. In practical design involving the stress-
based approach to total fatigue life, however, an endurance limit is first established
on the basis of experiments conducted on carefully prepared smooth test speci-
mens. This limit is then lowered by applying modifying factors (commonly known
as the 'knock-down factors') to account for such effects as surface finish, size
effects and constraints, temperature, stress corrosion, fretting, and numerous
unknown effects. The damaging effects of repeated contact and corrosion at sur-
faces (arising, for example, from fretting fatigue), and the mitigation, at least in
part, of such deleterious effects by recourse to shot-peening and lubrication are
addressed in Chapter 13.
7.6 Practical applications 235
Solution:
The endurance limit of the product with a rough surface finish is 40%
lower than the value measured in the laboratory. The design endurance limit
then is: 400 x 0.6 = 240 MPa. This value pertains to fully reversed cyclic stres-
sing, i.e. for R = -1 or om = 0.
The applied loading involves R = 0 and a stress amplitude, a a . From Eq. 7.2,
it is seen that a a = a m = Aa/2 for R = 0. The compressive surface stress arising
from shot-peening lowers the mean stress in surface to a new value: am = (am -
550) = (a a - 550) MPa. Assuming that the modified Goodman approximation,
Eq. 7.4, provides a reasonably accurate measure of the high-cycle fatigue life
under nonzero mean stress, we see that
? + ^=L (7 14)
'
Substituting the appropriate values,
—-—I— =1 (1 15^
v
240 1500 ' ' J
This equation gives: <ra = 283 MPa. Thus, the leaf spring could be subjected
to an applied stress amplitude of up to 283 MPa for infinite life. (Note that the
possible beneficial effect of shot-peening in enhancing the fatigue endurance
limit has not been taken into account in the numerical calculations. Thus, the
stress amplitude estimate is likely to be very conservative.)
236 Stress-life approach
(a) (b)
Fig. 7.9. (a) Distribution of different failure modes in jet engines, (b) Susceptibility of
different components to HCF problems. (After Cowles, 1996.)
7.7 Stress-life response of polymers 237
(1) Foreign object damage (FOD), which usually occurs in compressor and fan
blades: FOD can induce micronotches, tears, dents and gouges that may vary in
dimensions from tens of micrometers to tens of millimeters, depending on the
size, nature and severity of impact of the foreign object. Sources of FOD are as
diverse as sand particles and birds. As noted earlier, the leading edge of the fan
blade, which is susceptible to FOD, is laser shock peened for improved fatigue
resistance.
(2) Domestic object damage (DOD), which arises from a dislodged debris or
component from another location of the engine.
(3) Fretting fatigue, which occurs at blade and disc attachment surfaces (dove-tail or
fir-tree section), bolt flanges, and shrink-fit areas. See Chapter 13 for terminology
definitions and detailed discussions pertaining to fretting fatigue.
(4) Galling, which occurs in the same regions as fretting, except that it involves greater
displacements due to major engine throttle and speed changes.
(5) HCF-LCF interactions, where HCF is exacerbated by LCF as, for example, when
creep and thermo-mechanical fatigue in hot sections (such as turbine blades) cause
further reductions in fatigue life, over and above that due to vibrations.
Current methods to assess the HCF life of critical components in aircraft gas
turbine engines entail the following general steps, (i) Appropriate stress analysis
(largely based on the finite-element method) are performed to determine the mean
stress level, (ii) Structural dynamics simulations are carried out to determine resonant
frequencies and excitation modes, (iii) The design of the component is then carried
out in such a way that (a) it meets the criteria for safe life for HCF with the
appropriate mean stress level (using the modified Goodman diagram), and (b) no
resonance-related problems arise. The parameters that serve as input to design are
gathered from specimen testing and component testing, and the stress-life approach is
empirically modified to allow for reductions in life due to FOD, DOD, fretting and
galling.
Fig. 7.10. Schematic representation of the typical variation of stress amplitude <xa with the
number of cycles to failure 7Vf for polymeric materials.
sufficiently large to form crazes, a distinct region I may not exist and the slope
of the Aa-Nf curve at the high Aa end will be a mere extrapolation of that in
region II.
The dependence of total fatigue life on the stress amplitude in region II is a
manifestation of the enhanced role of microscopic crack growth on fatigue fracture.
At the higher aa end of region II, slow growth of crazes and their transformation into
cracks are dominant mechanisms of failure. A slope of 14MPa per decade of iVf
seems to be characteristic of region II in a variety of polymeric materials fatigued at
room temperature. As the test temperature is raised, there is a competition between
shear banding and crazing in this region, as in the case of tensile deformation.
The high-cycle fatigue region represented in region III essentially forms the
endurance limit for the polymer. The fatigue life here is controlled by the incuba-
tion time for the nucleation of microscopic flaws. The relative dominance of
nucleation and growth of crazes and cracks constitutes the main distinction
between regions II and III.
7.7.2 Mechanisms
The mechanisms controlling the total fatigue life of polymers also vary with
many morphological, thermal, mechanical and environmental factors.
(1) When the cyclic loading involves high strain rates, the material is prone to
hysteretic heating and to thermal softening. Consequently, increasing the
test frequency (typically beyond 10 Hz for experiments conducted in the
laboratory environment) results in a reduction in fatigue life. In an attempt
to address these issues, the American Society for Testing and Materials
(Philadelphia) developed standard methods in 1971 for the fatigue testing
of polymers. These procedures are spelled out in Specification D-671-71.
The standard calls for the measurement of temperature at fatigue failure
unless it can be demonstrated that the heat rise is not significant.
Furthermore, when thermal softening controls fatigue fracture, this stan-
dard defines the fatigue failure life operationally as the number of loading
7.8 Fatigue of organic composites 239
as matrices for organic composites include polyesters, epoxies, Nylon 66, PC,
polyphenylenesulphide, polyamideimide, PSF, PVC, and polyetherimide.
200
I, • PSF
V PSF+10% glass
O PSF+ 20% glass
A P S F + 40% glass
O PSF+ 40% carbon
Fig. 7.11. A stress-life plot showing the variation of maximum tensile stress <jmax as a function
of the number of fatigue cycles to failure 7Vf for injection-molded PSF which is reinforced
with different amounts of short glass fibers and with 40% short carbon fibers. The results
are based on room temperature fatigue tests conducted at R = 0.1, and vc = 5-20 Hz. The
small arrows denote that no failure occurred at the indicated number of cycles. (After Mandell
et ai, 1983.)
matrix playing an increasingly dominant role in the fatigue process. Similar char-
acterizations of fatigue failure have also been developed using strain-based
approaches (e.g., Dharan, 1975; Talreja, 1987).
Nondestructive test methods based on acoustic emission, radiography, and mod-
ulus and damping measurements of fiber composites subjected to fatigue loads show
fiber breakage, debonding, or matrix cracking fairly early in the fatigue process. The
growth of such microscopic degradations continues to result in the lowering of the
stress at which failure occurs with increasing numbers of fatigue cycles. In view of this
progressive degradation, the useful fatigue life of many continuous-fiber composites is
often defined as the number of cycles needed to cause a certain reduction in the elastic
modulus. It is also common to characterize the distributed (microscopic) fatigue
damage using Weibull statistics (see, for example, Talreja, 1987). At high cyclic fre-
quencies, hysteretic heating also becomes an important factor. Furthermore, anom-
alous improvements in fatigue life may result in some cases due to the realignment of
fibers, crack blunting, periodic overloads or frequency fluctuations.
242 Stress-life approach
1200
1000
800
\ 600
200
100
.^ = 60°
Fig. 7.12. Stress-life plots showing the variation of maximum tensile stress a max as a function
of the number of fatigue cycles to failure N? for an epoxy resin matrix reinforced with 60
volume % unidirectional glass fibers. 4> denotes the angle between the fiber direction and the
tensile axis. The tests were conducted at room temperature at R = 0.1 and vc = 19 Hz. (After
Hashin & Rotem, 1973.)
<717)
The parameter q varies from zero for no notch effect to unity for the full effect
predicted by the elasticity theory. Kt is a function only of the component geometry
and loading mode and is available in many handbooks (e.g., Peterson, 1959).
However, Kf is determined from experimental measurements or empirical, engineer-
ing 'rules-of-thumb'. An example of such a measure of Kf is the well known Peterson
equation for ferrous wrought alloys (Peterson, 1959):
where An is a constant whose value depends on the strength and ductility of the
material (An ~ 0.25 mm for annealed steels and An ~ 0.025 mm for steels of very
high strength) and p is the notch-root radius.
The stress-life approach is employed for high-cycle fatigue failures ahead of stress
concentrations by appropriately modifying the smooth specimen (unnotched) endur-
ance limit ae. This involves either dividing the stress range A a for all fatigue lives by
the factor Kf (which often leads to very conservative results) or merely reducing the
fatigue limit ae by a factor of Kf. This method is unsuitable for situations where
considerable plastic deformation occurs ahead of the stress concentration.
where the peak value of K^S is always smaller than the yield strength of the material
cry in both tension and compression. In order to assess the effect of the mean stress
on fatigue life, the modified Goodman equation, Eq. 7.4, or some other approach
discussed in Section 7.2 may be employed. Using the modified Goodman diagram
for the notched member, we see that
max y
K{ \ aTS j
Figure 7.13 schematically shows the modified Goodman diagram for smooth and
notched specimens which are subjected to cyclic loading under a nonzero mean
stress. These specimens are subjected to an applied stress amplitude of *Sa and
KfSz, respectively, as indicated in the figure. Note that for the elastically deforming
notched member, the intercepts in both the ordinate and the abscissa are reduced by
a factor of Kf as compared to the unnotched fatigue specimen.
244 Stress-life approach
Kf
Fig. 7.13. The effect of mean stress on fatigue life as determined from the modified Goodman
diagram for notched and unnotched fatigue specimens.
complete failure
I
A\T\\\\T\\\
nonpropagating cracks
no cracks
— Aae/Kt
Fig. 7.14. Threshold stress range (fatigue limit) for crack initiation at a notch tip, characterized
by the unnotched fatigue limit Acre divided by Kf or Kt and plotted as a function of Kt.
(After Frost, Marsh & Pook, 1974.)
Sa = 200 MPa, and a mean stress, Sm = 250 MPa. For the notch geometry of
the rod, the elastic stress concentration factor, Kt9 and the notch sensitivity
index, q, are found from appropriate handbooks to be 2.3 and 0.92, respectively.
Fully reversed cyclic stress tests conducted on smooth (unnotched) laboratory
specimens give the following material parameters for the Basquin equation, Eq.
7.1: Of = 1000 MPa and b = -0.12. The endurance limit was estimated from
these tests to be 280 MPa. The yield and tensile strengths of the steel are
ay = 600 MPa and a TS = 1050 MPa. Estimate the high-cycle fatigue life of
the notched rod.
Solution:
From Eq. 7.17, we find that the fatigue notch factor, Kf = 1.2. For the
given loading conditions, i.e. Sm = 250 MPa, 5 a = 200 MPa, we thenfindan
equivalent value of fully reversed cyclic stress, SaLm=(b f ° r a n unnotched speci-
men using Eq. 7.20. For this purpose, we rewrite Eq. 7.20 as:
i - i
Here X\ and X2 are scalar constants which may vary from point to point, but are
constants for a given material point in the solid.
As an example, an increase in the internal pressure of a close-ended, thin-walled
cylindrical tube causes the hoop stress <rhoop and the axial stress aaxial to vary in
proportion to each other so that at all times,tfhoop/^axiai= 2. If the thin-walled
cylinder is subjected to an axial tension P and a torque about the axis T, propor-
tional loading occurs only if P oc T. Any other mutual variation of P and T gives
rise to nonproportional loading. Further discussions of nonproportional and out-
of-phase loading are considered in the next chapter in the context of strain-life
fatigue.
7.10 Multiaxial cyclic stresses 247
= "W
(7.24)
Another measure of the intensity of the multiaxial stress state (and used in the Tresca
yield criterion which was discussed in Section 1.4.3) is the maximum shear stress,
r max , which acts on at most three mutually perpendicular sets of planes that intersect
the principal stress axes at 45°:
ox -
= max (7.25)
For fluctuating multiaxial stresses, Eq. 7.24 is written in terms of the amplitudes of
principal stresses aza (/ = 1, 2, 3) and the amplitude of the effective stress a a e as
In the most elementary stress-life analysis for multiaxial fatigue involving a zero
mean stress, the Basquin exponent b and the fatigue strength coefficient a[ in Eq. 7.1,
which are determined from experiments conducted on smooth specimens subjected
to fully reversed uniaxial cyclic loads, are used in conjunction with the following
stress-life equation for multiaxial stresses to determine the fatigue life, JVf:
(7.27)
In some cases, a steady, nonfluctuating load in one mode (such as bending) may be
superimposed on cyclic stresses in another mode (such as cyclic torsion). Here, the
effects of mean stress on fatigue failure should be considered. If it is assumed that the
controlling mean stress is related to the steady value of the hydrostatic stress, an
effective value of this mean stress, a m , may be defined in terms of the mean values of
the principal stresses, crim (i = 1, 2, 3), as
+ °zm- (7.28)
' Recall from Chapter 1 that the octahedral shear stress is the resolved shear stress on the n-plane, which
is the plane oriented at equal angles to the three principal stress directions.
248 Stress-life approach
Alternatively, an effective mean stress may be defined based on the octahedral shear
stress as
With this equation, the generalization of the modified Goodman equation to multi-
axial fatigue then involves an equivalent fully-reversed uniaxial cyclic stress. The
fatigue life under multiaxial cyclic stresses involving nonzero mean stresses is next
determined using Eq. 7.27.
One of the major drawbacks of such effective stress approaches is that the differ-
ing effects of axial tension and compression mean stresses in a multiaxial fatigue test
may not be accurately captured. In addition, the orientation of fatigue cracks with
respect to the loading axes is not quantitatively determined from such criteria.
Furthermore, a wide variety of experimental observations (to be discussed next)
reveal that the normal stress also plays a critical role in influencing fatigue lives in
multiaxial loading.
regime B
10 10 10° 10'
Nf (cycles)
regime A regime B
1.0
0.8
0.6
0-4
0.2
maximum shear through the fatigue life. The fraction of life, N/Nf, expended in
initiating a dominant shear crack is less than 0.1; the remaining 90% of life is spent
in propagating this shear crack. For Nf > 106 cycles, the local mode of failure occurs
on planes oriented normal to the local principal tensile stress, with the microscopic
tensile cracks oriented at 45° to the shear cracks. This failure process is categorized
as regime B in Fig. 7A5(a). The fraction of life expended in initiating the dominant
crack rises to 0.2 at N/Nf ~ 107 cycles.
When the Inconel 718 alloy is subjected to axial tension fatigue, Fig. 7.15(6), a
different failure pattern emerges throughout the life. In both the low-cycle and high-
250 Stress-life approach
cycle fatigue failure regimes, the macroscopic crack plane is approximately normal to
the tensile loading axis. For JVf < 105 cycles, regime A, the local mode of micro-
scopic cracking is along planes of maximum shear stress. As discussed in detail in
Chapter 10, this microscopic mode of initial crack advance in tension fatigue is
commonly referred to as Stage I, where single-slip failure along planes of local
maximum shear induces a serrated or faceted fracture morphology. Such features
are clearly evident in the micrograph shown in Fig. l.\5(b). Within regime A, the
fraction of life expended in nucleating a dominant fatigue crack gradually rises from
approximately 0.1 at JVf ~ 103 cycles to about 0.4 at Nf ~ 105 cycles. For N{ > 106
cycles, regime B, a tensile mode of failure emerges under imposed tension fatigue,
with the fraction of total life expended in nucleating a dominant fatigue flaw (1 mm
in size) gradually rising to as high as 0.9 at JVf ~ 107 cycles. Such a mode of failure is
commonly referred to as Stage II, whose microscopic mechanisms are examined in
detail in Chapter 10.
The extent to which regimes A and B individually dominate the total fatigue life,
and the fraction of total life expended in creating a dominant flaw within each of
these regimes is a strong function of the composition and micro structure of the
material, and of the test environment. Locally tensile failure patterns can also be
induced in some alloys subjected to cyclic torsion, especially in the high-cycle fatigue
regime.
some other approach to account of the effect of mean stresses; see later discussion in
this chapter).
Figure 1 A6(a) schematically shows a fatigue specimen subjected to bending-tor-
sion cyclic loads. The reference coordinate axes, x, y and z, are marked on the figure.
Let the orientation of a critical plane be defined with reference to this original
coordinate system with the aid of two angles: the angle, y, between the axis of the
specimen (the x axis) and the line of intersection of the critical plane with the surface,
and the angle, cp, between the normal to the critical plane, which is along the z
direction in Fig. 7.16(&), and the z axis. A new set of coordinate axes, x\ y and
zr, is defined in Fig. 7.16(7?) to facilitate the visualization of the critical plane orienta-
tion. Using straightforward methods for coordinate transformation, the components
of the stress and strain tensor in the x\ y and z1 coordinate system are written as
cos^siny — sin^sinyX
cos cp cosy sin cp cosy I. (7.32)
—sincp — cos<p /
Then the important components of the stress acting on the potentially critical plane
are identified as: the normal stress (o^vX t n e (in-plane) shear stress (cry^) which
produces a mode II type crack opening, and the (out-of-plane) shear stress which
produces a mode III type crack opening (see Chapter 9 for further discussions of
mode II and mode III).
(a) (b)
Fig. 7.16. Schematic of a fatigue specimen subjected to bending-torsion cyclic loads (a) and the
definition of the critical plane and the associate nomenclature (b).
252 Stress-life approach
In general, the identification of the orientations of the critical planes for general
multiaxial loading with nonproportional stress fluctuations can become very cum-
bersome. However, as reviewed by Chu, Conley & Bonnen (1993), some simplifica-
tions can be extracted by noting that most fatigue cracking initiates at the surface.
Given the state of plane stress at the surface elements of the specimen, criteria based
on mode I (tensile failure) and mode III (torsional or out-of-plane shear failure) type
damage lead to cp = 90° as the critical orientation, whereas mode II type failure
based on in-plane shear stresses lead to <p = 45° as the critical orientation. With this
fixed orientation of cp, only variations in the angle y need to be calculated. If such
approximations cannot be applied to a given material or loading situation, detailed
computations based on the critical plane approach need to be undertaken.
Here, a and f$ are material parameters determined experimentally, which are con-
stants for a given life. An increase in the maximum normal stress an max acting on the
plane of the critical alternating shear stress causes a corresponding reduction in the
permissible cyclic shear stress ra as per Eq. 7.33, for a fixed fatigue life. McDiarmid
has proposed several variations of the Findley criterion, the most recent of which
attempts to account for different types of cracking patterns observed during multi-
axial fatigue (McDiarmid, 1994).
The justification for the incorporation of a normal stress component, in the form
of either a maximum normal stress or a hydrostatic stress, in Eq. 7.33 and in other
critical plane criteria presented in subsequent sections and in the next chapter, stems
from the differing effects on crack growth from tensile and compressive mean
stresses.f From a mechanistic viewpoint, one possible rationale for such an effect
is that interlocking and closure of the microscopic irregularities of the crack faces
seen, for example, in the Stage I transgranular crack growth process seen in Fig.
7.15(6), can influence the transmission of shear tractions. The magnitude of tensile or
compressive normal stresses can consequently determine how effectively such con-
tact between crack faces and the attendant transmission of shear loads occurs. One
may then envision the possibility of a minimization or elimination of such contact,
and a resultant increase in the rate of advance of the crack, due to tensile mean
stresses. Such a situation is demonstrated in the case study on multiaxial fatigue
' Historically, criteria for multiaxial fatigue failure on the basis of both shear and normal stresses have
also been considered in the earlier works of Gough, Pollard & Clenshaw (1951) and Stulen & Cummings
(1954). A survey of historical developments in the area of multiaxial fatigue is given by Garud (1981).
7.10 Multiaxial cyclic stresses 253
presented in Chapter 8. A number of criteria have also been put forth to identify
critical planes of failure on the basis of different combinations of normal and shear
strains for proportional and nonproportional loading. These approaches are also
discussed in Chapter 8.
(Zenner, Heidenreich & Richter, 1985; Froustey & Lasserre, 1989). For a phase
difference of 0° between torsional and bending stress cycles, all of the foregoing
theories give essentially the same result. For 90° out-of-phase loading, larger differ-
ences are seen among the different criteria. A quantitative comparison of the pre-
dictions of the foregoing theories with experimental results for in-phase and out-of-
phase loading of high-strength metals is given in Papadopoulos et al. (1997).
Exercises
7.1 The S-N curve for an elastic material is characterized by the Basquin rela-
tionship, o^ — C • Nf, where C is a material constant, <ra is the stress ampli-
tude, Nf is the number of fully reversed stress cycles to failure and b is the
Basquin exponent approximately equal to -0.09. When the stress amplitude
is equal to the ultimate tensile strength of the material in this alloy, the
fatigue life is 1/4 cycle. If a specimen spends 70% of its life subject to
alternating stress levels equal to its fatigue endurance limit ae , 20% at
l.l<re and 10% at 1.2<re, estimate its fatigue life using the Palmgren-Miner
linear damage rule.
7.2 Explain why the modified Goodman diagram can be rewritten in terms of
the endurance limit, cre, as
where cre\am=o is the endurance limit for zero mean stress cyclic loading.
7.3 A circular cylindrical rod with a uniform cross-sectional area of 20 cm is
subjected to a mean axial force of 120 kN. The fatigue strength of the
material, a a = 0%, is 250 MPa after 106 cycles of fully reversed loading
and <rTS = 500 MPa. Using the different procedures discussed in this chap-
ter, estimate the allowable amplitude of force for which the shaft should be
designed to withstand at least one million fatigue cycles. State all your
assumptions clearly.
7.4 A rotating bending machine produces a pure bending moment uniformly
over the gage length of a fatigue specimen. Show that, in a bending specimen
rotating at an angular velocity &>, the cyclic stress will be of the form
Aa = A sin&tf, where A is the peak stress amplitude and t is the time.
7.5 Why is tempered glass more resistant to tensile fracture than ordinary glass?
7.6 A cylindrical shaft of circular cross section is subjected to a bending moment
of constant amplitude over its entire length. The deformation of the shaft
material can be approximated by an elastic-perfectly plastic constitutive
model and the yield strength in tension can be considered equal to that in
compression. If the outer fibers of the shaft yield plastically over a depth of
1/4 of the diameter during the application of the bending moment, qualita-
Exercises 255
Strain-life approach
^Wf(2tff)c, (8.1)
where ef is the fatigue ductility coefficient and c is the fatigue ductility exponent. In
general, ef is approximately equal to the true fracture ductility ef in monotonic
tension, and c is in the range of —0.5 to —0.7 for most metals. Typical values of
€f and c for a number of engineering alloys are listed in Table 8.1.
f =f + ^, (8.2)
256
8.1 Strain-based approach to total life 257
Table 8.1. Cyclic strain-life data for some engineering metals and alloys.
(8.4)
Combining Eqs. 8.1, 8.2 and 8.4, one obtains
(8.5)
The first and second terms on the right hand side of Eq. 8.5 are the elastic and plastic
components, respectively, of the total strain amplitude. Equation 8.5 forms the basis
for the strain-life approach to fatigue design and has found widespread application
in industrial practice. Table 8.1 provides a list of representative data for the stress-
life and strain-life characterization of some commonly used engineering alloys.
8.1, and 8.5, respectively. In order to examine the implications of Fig. 8.1 for 'short'
and 'long' fatigue lives, it is useful to consider a transition life, which is defined as the
number of reversals to failure (27Vf ) t at which the elastic and plastic strain amplitudes
are equal. From Eqs. 8.1 and 8.4,
At short fatigue lives, i.e. when 2Nf < (2JVf)t, plastic strain amplitude is more
dominant than the elastic strain amplitude and the fatigue life of the material is
controlled by ductility. At long fatigue lives, i.e. when 27Vf ^> (27Vf)t, the elastic
strain amplitude is more significant than the plastic strain amplitude and the
fatigue life is dictated by the rupture strength. Optimizing the overall fatigue
properties thus inevitably requires a judicious balance between strength and duc-
tility (e.g., Mitchell, 1978).
Mean stress effects have also been incorporated into the uniaxial strain-based
characterization of fatigue life in a simple manner (Morrow, 1968). Assuming that
a tensile mean stress reduces fatigue strength o\, such that (see Eq. 7.6):
the strain-life relationship, Eq. 8.5, can be rewritten (see Section 7.2) as
(8.8)
A C
Fig. 8.2. Mean stress relaxation in a cyclically softening material subjected to strain-controlled
fatigue.
imposed strain level C is expected to be lower than that at A. With a tensile mean
strain level, the tendency for similar behavior in compression is not significant, and
consequently, the shape of the hysteresis loop for the portion C to D will be
roughly the same as that from A to B. This process results in a progressive
reduction in the mean stress with increasing strain cycling, as shown in Fig.
8.2(6). The rate of decrease in mean stress progressively diminishes as the mean
stress level approaches zero.
Mean stress relaxation can also occur in cyclically hardening materials (e.g.,
Sandor, 1972), although the mechanisms here are less obvious. Cyclic hardening
reduces the plastic strain range and increases the stress range for a fixed total strain
amplitude. With reference to Fig. 8.2(a), the material develops a higher flow stress at
C than at A. However, with a tensile mean stress, the material yields more in tension
than in compression. This preferential plastic straining alters the shape of the hyster-
esis loops in such a way that the stress at point D is lower than that at B, although C
is at a higher stress level than at A. The net result is that a relaxation of mean stress
occurs in a cyclically hardening material as well.
We conclude this section by noting that the low-cycle fatigue behavior of poly-
meric materials is also often characterized empirically using strain-based approaches.
Figure 8.3 shows the variation of total strain amplitude Ae (log scale) as a function
of the number of load reversals to failure 27Vf (log scale) for polycarbonate at 298 K.
Note the similarity of this curve with the corresponding one for metals presented in
Fig. 8.1.
260 Strain-life approach
0.2
0.1
0.08
0.06
Ae
0.04
0.02
0.01
0.008
10° 102 104 106
2N{
Fig. 8.3. Total strain amplitude Ae plotted against the number of load reversals to failure 2Nf
(log-log scale) for polycarbonate at 298 K. (After Beardmore and Rabinowitz, 1975.)
(iii) If the fatigue ductility coefficient, e[ = 0.22, and the fatigue ductility
exponent, c = -0.59 (in Eq. 8.1), find the number of temperature rever-
sals to failure. Identify the location at which failure initiates on the basis
of Coffin-Manson criterion.
(iv) The results obtained in the above three parts are an oversimplification
in that they do not account for the temperature-dependence of material
properties. If the properties vary with temperature in the same manner
as in part (iv) of the example problem in Section 3.10.5, discuss the
effects of such temperature-dependence on your results in items (i)-(iii).
Solution:
It is given that:/ p = (r-Jrof = 0.25, and Tini = 400 °C, r room = 25 °C,
and the applied temperature amplitude (see Fig. 3.16(Z?)),
|AT a | = r ini — r room = 375 °C. It is noted that creep effects are less dominant
compared to plasticity effects. Denoting the properties of the matrix by the
subscript T and those of the particle by the subscript '2' and substituting the
appropriate values in Eq. 3.26, it is found that the elastic mismatch parameter
Mel = 0.35. Substituting the numerical values of the various terms in Eq. 3.28,
we find that the temperature change, from the initial stress-free temperature
(400°C) at which plastic yielding begins is: lAT^I = 174°C, i.e. at 400 -
174 = 226 °C. The temperature change beyond which any reversal in tempera-
ture induces a reversed plastic zone is \AT2\ =2\ATl\ = 348°C, i.e. at 400 -
174 = 52 °C. Since the first cooling is down to 25 °C, subsequent thermal
cycling would induce a reversed yield zone.
(i) Substituting the numerical values of geometrical and material parameters
into Eq. 3.31, and solving iteratively for the reversed plastic zone rc, we
see that that (rc/r{f « 1.06.
(ii) It can easily be shown, from the information provided in Section 3.10.3,
that the maximum plastic strains develop at the particle-matrix interface,
i.e. at r = rx. The second term on the right hand side of Eq. 3.37 can be
used to estimate the rate of plastic strain acumulation per cycle.
Substituting r = rx into this term, we note that the rate of plastic strain
accumulation per cycle (for the given thermal amplitude ATa), is
-1 (8.9)
Substituting the appropriate material properties and the result for rc from
part (i), it is seen that A6pl = 4.4 x 10"4.
(iii) The interface between the particle and the matrix develops the maximum
plastic strain which fully reverses during one complete thermal cycle.
From Eq. 8.1,
262 Strain-life approach
for elastic deformation. In Eq. 8.13, Aa00, Aa and Ae are the amplitudes of the fully
reversed nominal stress, notch tip stress and notch tip strain, respectively. For fixed
values of the imposed stress range Aa°°, Eq. 8.13 is an equation of a rectangular
hyperbola,
AaAe = (KfAa°°)2/E = constant. (8.14)
There is a family of curves, with different combinations of Aa and Ae, which satisfies
this equation. Kf can be uniquely determined by simultaneously solving Eq. 8.13
with the cyclic stress-strain constitutive equation, Eq. 3.5, for the material.
Multiplying both sides of Eq. 3.5 by Aa, one obtains
K,< • (8-15)
- AcrAe = constant
Fig. 8.4. Schematic illustration of the procedure used to determine the local stresses and strains
at a notch tip.
with the characteristic cyclic stress-strain behavior of the material, the local stress ax
and the local strain €{ at the notch tip corresponding to a far-field tensile stress o™ is
determined by the intersection of two curves: (i) the Neuber hyperbola represented
by the condition that ae = (K{a°°)2/E = constant, and (ii) the cyclic stress-strain
curve given by e = a/E + (a/Kf)l/rl{. Point Q in Fig. 8.4 represents the local stress-
strain coordinates at the notch tip corresponding to a far-field tensile stress crf°.
If the far-field stress is now reversed to a (compressive) value af°, the stress range
causing this reversal is Aa°° = of0 — a™. The corresponding local stress range and
strain range values for the notch tip are Aa and Ae, respectively. To determine these
values, the origin of the stress-strain coordinate system is now located at point Q.
The stress-strain hysteresis curve obtained from the cyclic deformation tests is now
used in conjunction with the Neuber rule, AaAe = (KfAa°°)2/E = constant, to
locate the stress-strain coordinates for the notch tip for a far-field stress value of
erf0. This is represented by Eq. 8.16 and by the point R in Fig. 8.4.
All subsequent reversals of loading employ Eqs. 8.14—8.16 to determine the local
fields at the notch tip. This local strain approach can easily be implemented in a
computer code.
In practical situations, particular attention has to be paid to the relationship
between accumulated damage under variable amplitude loading and that measurable
in a laboratory specimen under constant amplitude loading conditions. Cycle count-
ing techniques have been developed to reduce complex fatigue loading histories to a
series of discrete events so that cyclic damage could be properly accounted for. A
number of counting techniques have been proposed to accomplish these goals: these
include the so-called rainflow counting, range pair, level crossing and peak counting
methods.
8.3 Variable amplitude cyclic strains and cycle counting 265
The extent to which any of the aforementioned methods for local strain analysis
will provide successful predictions of fatigue life in a material depends on the frac-
tion of fatigue life expended to initiate small flaws ahead of the notch and on the
remaining fraction to propagate this flaw to failure. In addition to the local stress
and strain calculations, fracture mechanics-based analyses of the stress and deforma-
tion fields ahead of notches are of considerable interest in developing a rational
approach to this notch fatigue problem.
4 4' 2 4 4'
time
(a) (b)
2, 2' 4, 4'
Fig. 8.5. (a) A random strain-time history imposed on a ductile solid, (b) The corresponding
stress-time history, (c) Fig. (a) replotted with the time axis pointing downward, to illustrate
the rainflow technique, (d) Stress-strain hysteresis loops extracted from the rainflow counting
method. (After Landgraf & LaPointe, 1974.)
downward, as shown in Fig. 8.5(c). Imagine now that the lines connecting the
strain peaks are a series of 'pagoda roofs' and that rain is dripping down these
roofs (hence the name 'rainflow counting method'). Several rules are imposed on
rain dripping down the roofs so that equivalent hysteresis loops can be extracted
from the strain history (e.g., Dowling, 1972; Anzai & Endo, 1979). The follow-
ing rules are imposed to define the flow of rain on the roofs: (i) The strain
history is plotted such that the first and last peaks or valleys have the largest
magnitude of strain. This ordering eliminates counting half cycles, (ii) Rainflow
initiates at each peak (such as point 1) and is allowed to drip down continuously.
However, the flow of rain from a peak must stop whenever it drips down a point
which has a more positive strain value than the one from which it drips. For
example, rain dripping down peak 2 must stop opposite peak 4 because the
latter location has a more positive strain value than the former location.
Similarly, the flow must stop when it comes opposite a minimum more negative
than the minimum from which it is initiated. For example, flow from valley 5
must stop opposite valley 6 because the latter location is more negative than the
former, (iii) Rainflow must stop if it encounters rain from the roof above. For
example, during flow from points 3 to 4, rain dripping down from point 2 is
8.3 Variable amplitude cyclic strains and cycle counting 267
encountered and hence flow must stop at point 2'. Note that every part of the
strain-time history is counted once and only once.
Now apply the above rules to the strain history in Fig. 8.5(c). Rainflow begins
on the outside at the highest peak strain and follows the pagoda roof down to
the peak at 2. At this point, the flow drips down to location 2' and continues
down to point 4. From 4, rainflow continues down to location 4' (which has the
same strain magnitude as that at 4). From there, the flow path is along 4' to 6, 6
to 7, and 7 to V. The stress-strain path from this sequence of events corresponds
to the hysteresis loop defined by the circuit 1 —> 4, 4r —> l r , i.e. the outermost
loop in Fig. 8.5(d).
Three additional hysteresis loops can be defined from the rainflow analysis of
the remaining paths. These include paths 2 -> 3 -» 2\ 5 ->> 4' - • 5', and
6 —• 7 -> 6/ in Fig. 5(c). Note that these hysteresis loops are not symmetrical
about the origin of the strain axis.
If the random strain history shown in Fig. %.5(a) were to be repeated m
times, the rainflow method would characterize all of these random loading
events in terms of the four hysteresis loops shown in Fig. 8.5(d), with each
loop repeated m times. Constant amplitude, uniaxial fatigue data can now be
generated on smooth laboratory test specimens using these hysteresis loops
and the material constants b, c, cr'f and ef are determined experimentally.
Mean stress effects on fatigue life are accounted for by recourse to Eq.
8.8, for example, where Ae and a m appropriate for a particular strain cycle
are substituted along with the foregoing material properties to obtain the
number of cycles to failure, 7Vf, representative of that strain cycle. These
results could be used in conjunction with the Palmgren-Miner rule to sum
the fatigue damage. Specifically, this entails the summation of damage for
each strain cycle to obtain
(8-17)
where M ( = 4 in the example shown in Fig. 8.5) is the total number of key
events (in the form of strain cycles) identified from the rainflow counting
method and d is the accumulated fractional damage. Alternatively, the
cycle counting method can be used in conjunction with the life prediction
methods employing variable amplitude crack growth, which are discussed in
Chapter 14.
Computer algorithms for cycle counting are available in the ASTM Annual
Book of Standards section 3, vol. 03.01, 1986 (American Society for Testing and
Materials, Philadelphia). Some simple algorithms have also been published by
Downing & Socie (1982).
268 Strain-life approach
where for the fully plastic state, the Poisson's ratio, v = 0.5 and for the elastic state,
v = 0.33 for most metals and alloys. In Eq. 8.18, e1? e2 and e3 are the three principal
strains, with ex > e2 > €3- The effective plastic strain based on the distortional energy
theory is written as
where the superscript 'p' denotes plastic strains. The corresponding effective strain
measures based on the maximum shear strain values are
6
_ /max _ 1 ~ 63 i p _ 2 p 2 , p px
a n a 6
^e - Y ^ - j + y » e - j /max ~ 3 V61 ~ €3)' ^.ZUj
The objective of the theories of multiaxial fatigue is to predict fatigue life under
complex loading conditions in terms of laboratory data of strain-life curves gathered
from uniaxial fatigue tests using simple criteria for failure. If the amplitude of the
maximum principal strain, A^/2, determines failure, Eq. 8.5 may be rewritten to
obtain
In terms of the von Mises criterion, the strain-based expression for multiaxial fatigue
life becomes
8.4 Multiaxial fatigue 269
where the effective strain is denned in Eq. 8.18. Similarly, with the Tresca criterion, it
is useful to note the correlation between axial strain and shear strain,
Combining Eqs. 8.22 and 8.23 and taking v = 0.3 for elastic deformation and v = 0.5
for plastic deformation, it is seen that
(8.24)
The main drawback of these effective strain measures is that they do not adequately
capture the effects of mean stress on multiaxial fatigue life. In an attempt to over-
come this limitation, Smith, Watson & Topper (1970) suggested a simple 'energy-
based approach' to account for mean stress effects. In their approach, multiplying
both sides of Eq. 8.5 by the maximum stress (crmax = crm + {Aa}/2) results in
f ^f2b b
c. (8.25)
This model is predicated on the premise that no fatigue damage occurs when
<jmax < 0, which can be at variance with experimental observations.
These rather strong limitations of the foregoing theories led to considerations of
other approaches, such as the critical plane approach to multiaxial fatigue failure
(Section 7.10), which is taken up in the following subsections specifically in the
context of low-cycle fatigue.
shear
strain
-70°
Fig. 8.6. (a)—(c) Three different proportional loading paths for the multiaxial straining
experiments which have the same maximum shear strain amplitudes, but different normal
stresses and strains across the planes of maximum shear strain, (d) Mohr's circle construction
showing the orientations of the planes of maximum shear strain, (e) A schematic illustration
of the orientations of the two planes of maximum shear strain. (After Socie, 1993.)
different. Figure 8.6(d) is the Mohr's circle of strain for these cases, where it is seen that
two mutually perpendicular planes are subjected to the same maximum shear strain
amplitudes. The orientations of these planes are schematically sketched in Fig. 8.6(e).
Since the sign of the shear strain has no physical significance, these two planes would be
expected to undergo the same extent of damage if shear strain amplitude alone
determined the evolution of damage. Figures 8.7(a)-(c) show the orientations of the
cracks formed for the three different loading paths sketched in Figs. 8.6(a)-(c),
respectively. It is apparent that the cracking angles seen in Figs. S.l(a)-(c) closely match
the orientations of maximum shear strain planes predicted by the Mohr circle in Figs.
8.6(d) and (e). This also implies in this case that the maximum shear strain plane controls
the evolution of damage and cracking in the Inconel 718 alloy. The loading paths shown
in Figs. 8.6(a) and (c) give rise to crack planes oriented at -70° and + 20°, respectively, as
seen from the angles of cracks in Figs. SJ(a) and (c), respectively. The loading history
shown in Fig. 8.6(6) promotes a crack angle of -20°, as seen in Fig. 8.7(6), because its
loading direction is the reverse of that in the other two cases.
8.4 Multiaxial fatigue 271
am*
Fig. 8.7. (a)-(c) Observations of crack paths for the proportional straining histories shown in
Figs. 8.6.(a)-(c), respectively. (From Socie (1993). Copyright the American Society for
Testing and Materials. Reproduced with Permission.)
It is also apparent from Fig. 8.6(e), however, that the maximum normal strains on the
two critical planes with the highest shear strain amplitude are different. Although the
loading paths followed in the experiments entail proportional straining, the principal axes
of stress and strain are not coincident, and consequently, the maximum normal stresses
on the two planes of maximum shear strain amplitude are not the same. Observations of
subcritical crack growth on the different planes clearly reveal that the maximum shear
strain planes which have the highest tensile normal stress across them exhibit the highest
crack propagation rates and the lowest fatigue lives. Compressive normal stresses inhibit
the advance of cracks, while the tensile normal stresses facilitate crack growth.
The results discussed in this section thus clearly show how maximum shear strain
amplitudes govern the initiation of fatigue cracking and how mean stresses on the planes
of maximum shear influence fatigue crack growth and overall fatigue life. It is thus
evident that the critical plane theories for multiaxial fatigue should incorporate the effects
of both shear and normal components of multiaxial stresses/strains for life prediction.
This case study also serves to provide a mechanistic justification for the various stress-life
criteria described in Section 7.10 and for the additional criteria based on cyclic strains to
be presented in the following sections.
Case A
el>€2>€3
surface ^
plane
mmm
id)
CaseB
€l>e2>e:
surface
plane
planes of maximum shear strain amplitude lie on the specimen surface plane. Under
these circumstances, the cracks advance more in a direction parallel to the surface
than normal to the surface, thereby increasing the aspect ratio of the crack. This
pattern of cracking has been termed 'case A' by Brown & Miller. When the case A
cracks become longer, i.e. when their critical dimensions span several grain dia-
meters, stage II crack growth occurs as a result of simultaneous or alternating slip
involving more than one slip system. At this time, the direction of crack advance and
the plane on which it occurs are as shown in Fig. 8.8(<f).
Now consider the possibility shown in Fig. 8.8(^) where the magnitudes of princi-
pal strains are such that the planes of maximum shear strain amplitude occur on the
planes schematically sketched in Figs. 8.8(/) and (g). Here, the stage I cracks initiate
at the surface and advance at 45° angles into the material, and this mode of cracking
has been termed 'case B\ (The fatigue crack growth process along persistent slip
bands (Chapter 4) for ductile single crystals represents case B cracks.) The direction
of stage II crack growth for case B is also from the free surface into the material, as
sketched in Fig. 8.8(A). Uniaxial tension fatigue leads to the same shear stress for
case A and case B and hence it can facilitate either mode of failure. Mixed tension-
torsion fatigue loading, however, invariably promotes case A cracks.
Brown & Miller (1973) postulate that the criterion for cracking for case A and case
B follows the general relationships:
A ymax ,
"=/a (8.26)
8.4 Multiaxial fatigue 273
where Aymax/2 and Aen/2 are maximum shear strain amplitude and normal strain
amplitude, respectively, during the low-cycle fatigue loading, and / a and / b are
different nonlinear functions of their arguments for case A and case B, respectively.
The examples shown in the preceding subsection on Inconel 718 and the work of
Fatemi & Socie (1988) demonstrate that the peak normal stress to the plane of
maximum shear strain amplitude influences the propagation of stage I cracks
under a variety of multiaxial loading conditions that induce case A and case B
cracking.
along which stage I, shear cracks (see Sections 7.10.3 and 7.10.4) are
likely to form. The planes on which the tensile normal strains are max-
imum are oriented at 45° to the axis of the tube. Tensile cracking would
be expected to occur on these planes. These results are schematically
sketched in Fig. 8.9.
(ii) Case 2: For torsional cyclic loading with superimposed axial tension,
there develops a superimposed tensile stress on only one of the two
shear planes (i.e. the added tensile stress acts only parallel to the axial
direction). Shear cracking due to stage I would then preferentially occur
only on this plane (see Fig. 8.10), and the overall fatigue life would be
expected to be smaller than that in part (i). Superimposed tension is not
expected to alter the stresses on the vertical shear plane. The superim-
posed static tension would, however, raise the stresses equally on both the
tension planes oriented at 45° to the tube axis. The resulting possibilities
for failure are schematically shown in Fig. 8.10. Thus, the addition of an
axial tensile load to a cyclically twisted cylindrical tube is expected to be
detrimental to fatigue life, irrespective of whether the failure occurs by a
shear mode or a tensile mode.
(iii) Case 3: For torsional loading with superimposed axial compression, one
of the two shear planes (i.e. the plane normal to the applied compression
axis) develops a normal compressive stress and hence is not expected to
develop any cracks. On the other hand, the other shear plane which is
parallel to the applied compression axis can easily develop a shear crack,
and hence the overall fatigue life may not be higher compared to the
shear failure for Case 1 or Case 2. The two 45° planes on which tensile
stresses develop would both exhibit a reduced propensity for cracking as
AT
|
"T
I
\
Fig. 8.9. A schematic illustration of the evolution of cyclic shear strains, normal strains, shear
damage and tensile damage for cyclic torsional loading of the cylindrical tube, Case 1.
8.4 Multiaxial fatigue 275
f % /
\
/ \
/
cyclic shear strain (•*—») cyclic tensile strain (•*—•>)
static tensile stress (—•) static tensile stress (—••)
Fig. 8.10. A schematic illustration of the evolution of cyclic shear strains, normal strains,
shear damage and tensile damage for cyclic torsional loading of the cylindrical tube with a
superimposed axial tensile load, Case 2.
AT
Fig. 8.11. A schematic illustration of the evolution of cyclic shear strains, normal strains,
shear damage and tensile damage for cyclic torsional loading of the cylindrical tube with a
superimposed axial compressive load, Case 3.
276 Strain-life approach
AT
\J time
•3 +
r\
\j time
(a)
(b)
time proportional
loading path
normal strain
'S +
/
90° out-of-phase
\j time
loading path
(c) (d)
Fig. 8.13. (a) A cylindrical specimen subjected to combined axial and torsional fatigue loads, (b)
Strain-time history for proportional loading where the axial and torsional strains are in phase.
(c) Strain—time history for nonproportional loading where the axial and torsional strains are 90°
out of phase, (d) The loading path for in-phase and 90° out-of-phase loading in strain space, for
the strain histories considered here.
in constant proportion to each other and the phase angle between them is zero.
Multiaxial fatigue involving 90° out-of-phase variation between the axial and
shear strains is shown in Fig. 8.13(c). The loading path for proportional loading
corresponds to a straight line in strain space, Fig. 8.13(d), where the axial strain is
plotted against the shear strain. The 90° out-of-phase loading path is a circle in
normalized strain space.
There exists experimental evidence which appears to suggest that in-phase cyclic
straining is more damaging to fatigue life at low strain amplitudes, while out-of-
phase cyclic straining is more damaging at high strain amplitudes, when the ampli-
tudes of the applied tension (or bending) or torsion for proportional and nonpro-
portional loading are comparable. It should, however, be noted that to obtain the
same strain range, the applied normal and shear strains for nonproportional loading
must be increased compared to those for proportional loading. This is because for
27S Strain-life approach
comparable applied strains, the maximum strains are smaller for nonproportional
loading than for proportional loading. When the maximum strains are held compar-
able for the two cases, it is almost always seen that nonproportional loading is at
least as damaging, and generally more damaging, than proportional loading.
Available approaches to handle nonproportional fatigue loading can be broadly
classified into two groups. The first group regards effective values of cyclic stress or
strain without regard to their variations along specific planes or crack growth direc-
tions. For example, Taira, Inoue & Yoshida (1968) integrated the octahedral shear
strains throughout a cycle, in order to circumvent the problem of changes in the
direction of stresses. The second group of methods used to characterize nonpropor-
tional loading considers the conditions on a critical plane, which were discussed in
detail in the preceding subsections.
It is of interest to consider here the multiaxial fatigue experiments of Lamba &
Sidebottom (1978) on tubular specimens of OFHC copper. Their results show that a
plot of the maximum Mises equivalent plastic stress range with the maximum plastic
strain range provides a unique (stable) hysteresis loop for symmetric strain-con-
trolled loading in tension-compression, cyclic torsion or in-phase tension-torsion.
Here the cyclic deformation is independent of the loading direction as long as the
loading direction remains unaltered during the fatigue test (i.e. for proportional
loading).
A completely different picture emerges when the tension and torsion cyclic loads
are 90° out of phase with each other. For a fixed value of maximum plastic strain
range, the out-of-phase fatigue test results in a 40% higher stress level (in the stabi-
lized hysteresis loop) than the proportional or in-phase multiaxial test. Similar trends
have also been seen by Kanazawa, Miller & Brown (1979). This additional hardening
occurs for out-of-phase loading as well as for any changes in cycling direction. These
differences do not depend on whether the fatigue specimen is initially subjected to
uniaxial loading or not. However, this additional hardening obtained in out-of-phase
cyclic loading can be erased if uniaxial fatigue having the same maximum strain
range is imposed after the multiaxial test.
Exercises
A metallic material is shot-peened \n an attempt to improve its fatigue life.
The shot-peening process results in a compressive residual stress of 250 MPa
at the surface of the material. The material has the following monotonic and
fatigue characteristics in the as-fabricated condition (before shot-peening):
E = 210 GPa, ^ = 1000 MPa, o{ = 1100 MPa, 4 = 1.0, n{ = 0.13,* =
-0.08, and c = -0.63. (See the discussions related to Eqs. 3.5, 7.1 and 8.5 for
the definition of these variables.) On a log-log plot, show the variation of the
total strain amplitude Ae/2 with the number of reversals to failure 27Vf for the
material in both the as-fabricated and shot-peened conditions.
Exercises 279
DAMAGE-TOLERANT
APPROACH
CHAPTER 9
WV = -?*£». (9.1)
where, for plane strain and plane stress, respectively,
283
284 Fracture mechanics and its implications for fatigue
8a—*\
mi in
Fig. 9.1. A large plate of an elastic material containing a crack of length 2a.
Here E is Young's modulus and v is Poisson's ratio. The surface energy of the crack
system in Fig. 9.1 is
Ws = 4aBYs, (9.3)
where ys is the free surface energy per unit surface area. The total system energy is
then given by
na2a2B A n
u =wP =T- + 4aBYs. (9.4)
Griffith noted that the critical condition for the onset of crack growth is:
2
dU dJ¥j> dWs
+ 2ys = 0, (9.5)
U^i UwH UvH IL
where A = 2aB is the crack area and dA denotes an incremental increase in the crack
area. Note that the total surface area of the two crack faces is 2A. The resulting
critical stress for fracture initiation is
orf = (9.6)
As the second derivative d2 U/da2 is negative, the above equilibrium condition, Eq.
9.6, gives rise to unstable crack propagation.
Griffith's idealized model for brittle fracture considers a sharp crack for which the
near-tip stresses exceed the cohesive strength of the material. In common engineering
materials, nonlinear deformation processes are induced near the crack tip under the
influence of the applied stress. Thus, although the Griffith concept laid the founda-
tion for the physics of fracture, its energy balance considerations cannot be directly
9.2 Energy release rate and crack driving force 285
applied to most engineering solids. Orowan (1952) extended Griffith's brittle fracture
concept to metals by simply supplementing the surface energy term in Eq. 9.6 with
plastic energy dissipation. The resultant expression for fracture initiation is
_ \2Ejy, + yv)
(9.7)
na
where yp is the plastic work per unit area of surface created. Note that yp is generally
much larger than ys.
u + du
displacement
(b)
Fig. 9.2. (a) An elastic plate containing an edge crack subjected to dead weight loading.
(b) Changes in the force-displacement curve and components of mechanical energy during
incremental crack growth.
286 Fracture mechanics and its implications for fatigue
displacement
(a) (b)
Fig. 9.3. (a) An elastic plate containing an edge crack subjected to displacement controlled
loading, (b) Changes in the force-displacement curve and components of mechanical energy
during incremental crack growth.
where O is the stored elastic strain energy and WF is the work done by the external
forces.
Irwin (1956) proposed an approach for the characterization of the driving force
for fracture in cracked elastic bodies, which is conceptually equivalent to that of the
Griffith model. Irwin introduced, for this purpose, the energy release rate Q which is
defined as
(9.9)
Consider the estimation of Q for the following two loading situations.
Case (1): Load-control or dead-weight loading
The cracked plate is subjected to afixedforce F by the application of a dead
weight as shown in Fig. 92{a). In this load-controlled case, the components of
mechanical energy (for a fixed crack length a) are written as
Fu
and W¥ = Fu, (9.10)
where T, in general, is the applied load (which equals a fixed value, F, for the
particular case of dead-weight loading). Combining Eqs. 9.8 and 9.10, it is seen that
Wp = - * = - y . (9.11)
Now consider an increase in crack length from a to a + 8a. This causes a correspond-
ing increase in displacement from u to u + 8u under the fixed force F, as shown in
Fig. 9.2(b). From Eqs. 9.9 and 9.11, the energy release rate for dead-weight loading is
written as
'du\
(9.12)
, IB \% F fixed
9.2 Energy release rate and crack driving force 287
As shown in Fig. 9.2(6), the advance of the crack by an increment 8a (with F fixed)
leads to a net increase in the stored strain energy by the amount
Z Z
F fixed
Case (2): Displacement-controlled loading
Now consider the situation shown in Fig. 9.3, where the displacement u is
controlled and the force F varies accordingly. When the crack advances by an
increment 8a under a fixed displacement w, the change in W? is zero, and hence
= <5O. From Eq. 9.9,
=
or <?=-- — ~y~ — ' (9*14)
u fixed •" L ° ^ J u fixed L ®a J M fixed
As shown in Fig. 9.3(6), the advance of the crack by an increment 8a (with u fixed)
leads to a net decrease in the stored strain energy by the amount
=-f. Z
(9.15,
u fixed
The compliance, C, of a cracked plate, which is the inverse of the stiffness, is
defined as
u
(9.16)
Combining Eq. 9.16 with Eqs. 9.12 and 9.14, it is seen that
&£
IB da
Equation 9.17 holds for both load control and displacement control, i.e. the energy
release rate Q is independent of the type of loading.! This result can also be ratio-
nalized by noting that the magnitudes of the change in stored energy under load
control (Eq. 9.13) and displacement control (Eq. 9.15) differ only by (8F • Su)/2,
which is a negligible quantity. For crack advance by an increment 8a with a given
F and w, therefore,
(9.18)
F fixed u fixed
It is noted that the definition of Q given in Eq. 9.9 is valid for both linear and
nonlinear elastic deformation of the body (see the Section 9.7.1). Q is a function of
the load (or displacement) and crack length, and is independent of the boundary
conditions (i.e. type of loading) for the cracked body. The Griffith criterion for
fracture initiation in an ideally brittle solid can be re-phrased in terms of Q such that
^ 2 y s . (9.19)
' This is to be expected since, as shown later, the critical value of the energy release rate is related to the
fracture toughness, which is a property of a material.
288 Fracture mechanics and its implications for fatigue
Fig. 9.4. The three basic modes of fracture, (a) Tensile opening (mode I), (b) In-plane sliding
(mode II). (c) Anti-plane shear (mode III).
9.3 Linear elastic fracture mechanics 289
(9.20)
where r and 0 are the polar coordinates shown in Fig. 9.5. The in-plane strain
components are related to the in-plane radial and angular displacements according
to
dur
€„ —•
ur 1 due
= +
7 7 Ho'
= /T\ H dur due _ M
(9.21)
Fig. 9.5. Coordinate system and stresses in the near-tip region of a crack in a plate.
290 Fracture mechanics and its implications for fatigue
= (1 - v)aee - varr,
= or9. (9.24)
For the plane problem, the equations of equilibrium, Eqs. 9.20, are satisfied when the
stress components are expressed by the Airy stress function x through
The compatibility condition, Eq. 9.22, when expressed in terms of the Airy stress
function, satisfies the biharmonic equation,
V ^ Z ) = O, V > = £ + I A+ - L | 1 . (9.26)
The boundary conditions for the plane problem of the plate containing a traction-
free crack are
aee = ar0 = 0 for 0 = ±n. (9.27)
The choice of the Airy stress function for the present crack problem should be such
that x n a s a singularity at the crack tip and is single-valued. A possible form of /
which satisfies this requirement is
x = ftp(rj0) + q(r,0), (9.28)
where p and q are harmonic functions of r and 6 which satisfy the Laplace equations
V2p = 0 and V2q = 0.
Following the approach of Williams (1957), we consider solutions of separable
form for the Airy stress function, x — ^(r)©(#)? based on
p = Air* coskO + A2rx sinkO,
q = Blr{x+2)cos(k + 2)6 + B2r{x+2) sin (k + 2)0, (9.29)
which lead to
X = r(x+2) [Ax cos kO + Bx cos (k + 2)0]
+ r{M)[A2 sin kO + B2 sin (A + 2)0]. (9.30)
This equation consists of a symmetric part (the term within the first set of brackets
on the right of the equality sign) and an anti-symmetric part (the term within the
second set of brackets on the right of the equality sign). The symmetric part, which is
an even function of 0, provides the mode I solution for crack tip fields and the
antisymmetric part, which is an odd function of 0, provides the mode II solution.
Taking only the first term here to obtain the mode I fields,
9.3 Linear elastic fracture mechanics 291
d2v
-± z = (X + 2) (X + 1) rk[Ax cosXO + Bx cos (X + 2)6>],
dr
d (\ dX
X = ^ l . (9.33)
where Z is an integer including zero, and
B A (9 34)
'
or (ii) sin Xn = 0 and hence
A, = Z and ^ = -Ax. (9.35)
Since the governing equations 9.20-9.24 are linear, any linear combination of the
admissible solutions also provides a solution. Hence, from Eqs. 9.33-9.35,
*=f, (9.36)
where Z is a positive or negative integer, including zero. Although, from a purely
mathematical standpoint, there is no basis to reject any value of A, the solution can
be chosen to be of the lowest order singularity which is consistent with physical
arguments. From Eqs. 9.31, it is seen that otj ~ / and e(j ~ / . Therefore, the strain
energy density is given by
X = [cos^ + I c o s f ] + o ( r 2 ) + O 0 - 5 / 2 ) + "--,
(9.40)
The second term on the right hand side of Eq. 9.40, with an exponent of 0 for r, is a
nonsingular, but nonvanishing, term. The higher order terms, with exponents greater
than zero, vanish as r —• 0. Rewriting Ax =
TSix8Jx
K5\M alyy(e)/
+ (terms which vanish at crack tip), (9.42)
where the first term is the leading singular term for linear elastic mode I crack
problems. The second term, generally referred to as the 'T term', contains the non-
singular stress GXX — T (Williams, 1957; Irwin, 1960; Larsson & Carlsson, 1973; Rice,
1974). For example, a brittle crack of length 2a lying on the x-z plane under
remotely uniform biaxial stresses a^x and a™, is subjected to
Kl = ay^y^Ka' and T = axxx-cr^r (9.43)
Although the leading singular term of the asymptotic solution, Eqs. 9.41-9.43, is
adequate for characterizing most linear elastic fatigue crack growth problems, the
omission of the T-stress can introduce significant errors in certain fatigue situations.
Examples of such situations include: (i) short fatigue cracks, (ii) cracks subjected to
mixed-mode loading where the in-plane shear stresses are substantially larger than
the tensile stresses, and (iii) small cracks inclined at a small angle to the far-field
tensile axis. Furthermore, different geometries of cracked specimens can influence
the near-tip yield behavior in different ways because of the differences in the T-stress
term. This effect and the attendant influence on fatigue crack closure are considered
in Chapter 14.
For the plane problem, the leading terms for mode I stress fields in cartesian
coordinates are
. 0 . 30
1 — s i n - sin —
. 0 . 30
cos- 1 + sin- sin — (9.44a)
. 0 30
sin- cos —
9.3 Linear elastic fracture mechanics 293
When written in cylindrical coordinates, the stressfieldsfor mode I have the follow-
ing leading terms:
1 + sin 2 -
0
cos- 2o
2 cos -
Ore .00
sin- cos-
= vx(prr
9z = 0- (9 Mb)
The corresponding displacements are
0 30
(2K- l)C0S--C0Sy
IE
(2K + 1) s i n - - s i n —
0 30
(2K — 1) cos - — cos —
IE n , fi . 30
(1+v) -(2K- 1) sin-+ sin —
Uz = (9.45)
"
For plane stress,
(3-v)
K = vx = 0 , v2 = v,
"(1+v)'
and, for plane strain,
K = (3- 4v), vi = v, v2 = 0. (9.46)
The term KY in Eqs. 9.44 and 9.45 is the mode I stress intensity factor which incor-
porates the boundary conditions of the cracked body and is a function of loading,
crack length and geometry. For plane problems, it is independent of the elastic
constants.
The near-tip fields for mode II can be derived in a similar fashion by applying the
boundary conditions, Eq. 9.27, to the antisymmetric part of the Airy stress function,
Eq. 9.30. The resulting asymptotic solutions for mode II are:
.Of 0 30
— sin- 12 + cos- cos —
. 0 0 . 30
sin- cos- sin — (9.47a)
2nr
0 (. . 0 . 30\
cos- I I - sin- s m y l
sin- I 1 — 3 sin2-J
— 3 s i n - cos -
\f2nr
cos- 1 — 3sm -
2 V 2
Gzz = VX{GXX + cryy) = VX((7rr
a
xz — ayz — arz ~ °Qz =
0. (9.476)
0 30
(l+v) I (2*:+ 3)sin- + sin —
0 30
—(1+v) |(2/c —3)cos- + cos—-
0 36"]
(l + v) i 0 i
36
ur (2/c—l)sin- + 3sin —
ue IE V2n 9 39~\
(l + v) -(2/c+l)cos- + 3cos
(9.48)
— sin-
^ «!
sin-
cos-j
xx yy ff 00 zz '
ux = uy = ur = ue = 0. (9.50)
The above singular solutions for all three modes of fracture indicate that the
stresses and displacements, respectively, are of the form
(9.51)
9.3 Linear elastic fracture mechanics 295
where the subscript M refers to the modes of failure, I, II, and III. The appropriate
stress intensity factor for each mode is denned as
= lim <V2Jtrcryy
r-»0 0=0
= lim <
0=0
^-dominance over which the asymptotic results, Eqs. 9.44-9.50, provide a reason-
able approximation to the full solution. As alluded to earlier, an understanding of
the conditions of ^-dominance is essential for the characterization of fatigue fracture
involving highly crystallographic crack growth, mixed-mode loading conditions or
small fatigue flaws. A detailed discussion of each of these cases will be taken up in
later chapters.
^ = CAKm, (9.53)
where da/dN is the change in the length of the fatigue crack per load cycle (a is the
crack length and N is the number of fatigue cycles) and AK is the stress intensity
factor range denned as
= Kmax-Kmm. (9.54)
9.4 Equivalence of Q and K 297
KmzLx a n d ^min? respectively, are the maximum and minimum stress intensity factors
corresponding to the maximum load, P m a x (or maximum nominal stress, crmSiX) and
the minimum load, Pmin (or minimum nominal stress, crmin). Recall that
I m a x = YcrmSLxy/na and Kmin = Ycrmin^/na for a center-cracked plate containing a
crack of length 2a which is subjected to tensile fatigue with a far-field stress range,
ACT = crmax — <rmjn. Y is the finite size correction factor for the plate. The terms C and
m in Eq. 9.53 are empirical constants which are functions of the material properties
and microstructure, fatigue frequency, mean stress or load ratio, environment, load-
ing mode, stress state and test temperature. The empirical crack growth law, Eq.
9.53, due to Paris et al. is the most widely used form of characterizing fatigue crack
growth rates for a vast spectrum of materials and test conditions. Equation 9.53 also
represents one of the most useful applications of the theory of linear elastic fracture
mechanics. Further details of the fracture mechanics-based approach to characteriz-
ing fatigue will be considered in subsequent chapters.
r +8a i
^{cfyyUy ~\~ O%yU% ~\~ O,yU ^ AX.
The factor 2 before the integral sign appears because of the displacement of the two
(9.55)
opposing crack surfaces, and the factor 1/2 after the integral sign is introduced
following the assumption of proportionality between the stresses and displacements.
Substituting the appropriate stresses atj- forr = x — a and 0 = 0 and displacements ut
for r = a + da — x and 6 = 0 from the previous section into Eq. 9.55, it is readily
seen, in the limit of 8a -> 0, that
= Gi + Gn + Gin. (9.56)
da
The energy release rate G and the stress intensity factors Kh Ku and Km in the three
modes of fracture are uniquely related. For the general three-dimensional case
involving plane strain and anti-plane strain loading,
2
(1 - V2)) , 2 , K2\ , (1+V) K2 rQ c?x
y —— ^ — \Ki +AII) H ^ — ^III K7-5/)
and, for plane stress,
G = ± {Kl + K%). (9.58)
298 Fracture mechanics and its implications for fatigue
Note that, when the crack advances in its own plane, i.e. for self-similar, coplanar
crack growth, the energy release rates for the different modes of fracture are simply
additive. This relationship also provides a means for developing mode-invariant
criteria for the onset of failure under multiaxial loading conditions.
2 3£7' 12 '
From Eq. 9.17 and Fig. 9.6(c),
2h
±
Y
\IC{d)
displacement, u
(b)
da
Fig. 9.6. (a) The double cantilever beam specimen, (b) A plot of the load versus the
displacement showing the compliance, (c) Compliance change as a function of crack length.
300 Fracture mechanics and its implications for fatigue
where /cf(a) is the stress intensity factor per unit applied load and
c(a) = C(a)/B.
In order to calibrate the stress intensity factor for a DCB specimen, prepare a
number of specimens with different crack lengths, a. Use a clip gage to measure
the opening displacement u at the loading point, shown in Fig. 9.6(#), as a
function of F. For each specimen with a known crack length, plot F versus u
as in Fig. 9.6(c) and the slope C(a). Control the load such that no crack exten-
sion occurs during this experiment. From similar results on multiple DCB speci-
mens, plot c(a) versus a. Find kf(a) and Ki(a) using Eqs. 9.63 and 9.64.
*y2.
(ii) A measure of compliance c(l) may be defined as q = c(l)Q, where Q is the
force acting on the piston per unit thickness as shown in the figure.
9.4 Equivalence of Q and K 301
Fig. 9.7. A schematic of the pressurized bulge or blister test and the associated nomenclature.
I w(x)dx = qH.
known that
(9.67)
* - % * •
Solution:
The compliance of the system is defined as
q = c(l)Q. (9.68)
Observe that (i) the pressurized liquid is incompressible, (ii) the pressure under
the blister is equal to the pressure in the piston, and (iii) the pressure in the
piston is directly related to Q by
(9.69)
Substituting Eq. 9.65 in Eq. 9.66, we obtain
_ 15 EqHh3
P (9.70)
~T~~J~~'
Now substitute Eq. 9.69 into Eq. 9.70 to get
8 1 /5 ^
(9.71)
Arranging this equation into the form of Eq. 9.68, we note that
302 Fracture mechanics and its implications for fatigue
(9 72)
-
The compliance interpretation of Q is given by Eq. 9.67. Noting that there are
two crack tips at the blister in Fig. 9.7 and taking the result from Eq. 9.72,
For plane stress, we take this equation with the link between KY and Q to get
I 32^ f> V
Young's modulus E appears in this equation because KY has been written in
terms of the displacement q. Instead, if use is made of Eq. 9.71, the stress
intensity factor becomes
[2 I2
(976)
1 (K \
rnp = — (— 1 , for plane strain,
3TC \ayj
1 / jr \ 2
rp = - ( — ) , for plane stress. (9.77)
n\ayj
Precise analyses of the plastic zone size and shape in modes I and II in strain-
hardening solids are discussed in Section 9.10 for plane strain and plane stress.
Following similar arguments, the plastic zone size ahead of a mode III crack is
found to be
9.5 Plastic zone size in monotonic loading 303
(9.78)
(9.79)
The requirement of bounded stresses at the point x = a-\- rp provides the condition
that Ki + Ki =0. Solving for r p , one finds that
r /ncr°°\
-^p = sec - — - 11. (9.80)
a \2ayJ
For cr°° <3C oy and hence for rp <^C a, this equation asymptotically leads to a plastic
zone size
t t t t
i i i i i
Fig. 9.8. A schematic representation of the Dugdale plastic zone model.
304 Fracture mechanics and its implications for fatigue
(9.81)
This asymptotically exact result due to Dugdale compares well with the Irwin
approximation, Eq. 9.77, for plane stress.
In the above model, one notes that an opening displacement 8 = 2v(a) at x = ±a
and y = 0 exists (which may be regarded as a consequence of necking ahead of the
crack). It can be shown that the crack tip opening displacement takes the form
sec
(^H (9-82)
or asymptotically, when a°° «(T y ,
(9.83)
CTyE
\ ^ = 2ys. (9.84)
(*,0)
-2ay
(a)
• \P-AP
, 0)
cyclic plastic zone
monotonic plastic zone
\ \\
Fig. 9.9. Schematic representation of the development of cyclic plastic zone upon unloading.
(After Rice, 1967.) (a) Monotonic plastic zone created by a far-field load P. (b) Stress
distribution due to the reduction of the load by AP which, when superimposed with (a), gives
the result in (c).
tion factor at the tip of the sharp crack leads to the formation of a reversedflowzone
which is embedded within the monotonic plastic zone.
For proportional loading, the changes in the near-tipfieldsdue to the reduction of
the load are given by the solution derived earlier for monotonic loading (Section 9.3)
with the exception that the loading parameter is replaced by the load range AP and
that the yield stress and strain are replaced by twice their values corresponding to the
load P. This modification is introduced to obtain the correct values of stresses in the
reversed flow zone after subtracting the changes due to the load reduction AP, Fig.
9.9(6). If closure of the crack faces is not encountered, the superposition of the near-
306 Fracture mechanics and its implications for fatigue
tip stresses in the fully loaded state, Fig. 9.9(<s), and in the partially unloaded state,
Fig. 9.9(&), leads to the stress distribution at the tip of the crack under the far-field
load P — AP, Fig. 9.9(c). Thus, for a crack which is only partially unloaded from a
far-field tensile load, there exists within the monotonic plastic zone a region of
reversed flow (termed the 'cyclic plastic zone') of size rc in which residual compres-
sive stresses are induced. For an elastic-perfectly plastic solid undergoing propor-
tional flow, the stress within the cyclic plastic zone is equal to the flow stress in
compression (—ay). The size of rc is derived by replacing KY by AKi and ay by —2ay
in Eq. 9.66 so that, for plane stress,
I/A*
(9.85)
n\2a
For zero-tension-zero loading, AKj = Ki and rc = r p /4. For materials which
cyclically harden or soften, ay in Eq. 9.85 should be replaced by the cyclic yield
strength, oy.
There are some interesting consequences of reversed plastic flow during unloading
from a far-field load:
(1) Even after the far-field load is fully removed, there exists a zone of residual
compressive stress ahead of the fatigue crack which has (previously) been
subjected to far-field cyclic tension. This residual stress zone can have
important implications for transient crack growth phenomena observed
under variable amplitude fatigue (see Chapter 14).
(2) Since residual stresses are self-equilibrating, the residual compressive
stresses at the crack tip must be offset by residual tensile stresses away
from the crack tip.
(3) If a nonclosing flaw (such as a sharp notch) is unloaded from a far-field
compressive load, reversed plastic flow at the notch-tip creates residual
tensile stresses. This zone of residual tension can induce stable mode I
fatigue crack growth in notched plates loaded in uniaxial cyclic compression
(see Chapter 4).
(4) A cyclic variation in the stress intensity factor A^ I ? from 0 to Kx, gives rise
to a cyclic crack tip opening displacement A<5t, which is one half of the total
opening displacement 8 under a monotonic stress intensity factor Ki9 Eq.
9.83:
\K2
A5t^—L. (9.86)
layh
(5) In the absence of crack closure, the value of rc and cyclic variations in
stresses, strains and displacements depend only on AP and are independent
of the maximum load P.
(6) When crack closure does not occur, the plastic superposition is valid up to
the point when rc = rp, that is, for complete load reversal involving equal
tension-compression fatigue.
9.7 Elastic-plastic fracture mechanics 307
Whereas the cyclic plastic zone size for a stationary fatigue crack in an elastic-
perfectly plastic solid is one-quarter the size of the monotonic plastic zone, a plane
stress analysis by Budiansky & Hutchinson (1978) shows that the reversed yield zone
for an extending fatigue crack is less than 10% of the Dugdale monotonic yield zone
size. This point is taken up for further discussion in Chapter 14. Analyses of cyclic
damage zones ahead of fatigue cracks in ceramics are discussed in Chapter 11.
Fig. 9.10. A contour around a crack tip and the nomenclature used in the definition of the /
integral.
308 Fracture mechanics and its implications for fatigue
faces are traction-free, the line integral / along any contour T which encircles the
crack tip is given by
(987)
fA -
where u is the displacement vector, y is the distance along the direction normal to the
plane of the crack, s is the arc length along the contour, T is the traction vector and w
is the strain energy density of the material. The stresses atj are related to w by the
relation a^ — dw/dey. For a material which is characterized by linear or nonlinear
elastic behavior (i.e. by deformation plasticity), / is independent of the path T taken
to compute the integral.
Rice (1968) showed that / is the rate of change of potential energy (with respect to
crack advance) for a nonlinear elastic solid and that J reduces to the energy release
rate Q for a linear elastic material:
(9.88)
da
If F is regarded as the contour which just encircles the cohesive zone in the
Barenblatt model, it is found that / is equal to the energy release rate given in Eq.
9.84: / = Qc = 2ys. Furthermore, if the line integral is applied to the Dugdale model,
the following relationship between / and the crack tip opening displacement Su Eq.
9.83, is obtained:
/ = ay8t. (9.89)
, n),
aayeylnrj
J__\ rl/(n+D Qfr ny (991)
otayeylj
The universal functions 6^.(0, «)5 ^(0, w), and ut{0, n) in Eqs. 9.91 vary with the polar
angle 0, the strain hardening exponent n and the state of stress, i.e. plane stress or
plane strain. The factor /„ depends mildly on the strain hardening exponent n.
Since / is a measure of the intensity of crack-tip fields, the onset of crack advance
under quasi-static loads can be formulated on the basis of a critical value, J = Jc.
When conditions of/-dominance (see Section 9.7.4) are satisfied in the plane strain
test specimen, the measured critical value of plane strain fracture toughness is
denoted by / I c . Detailed test procedures for the experimental measurement of / I c
are spelled out in the test standard E-813 developed by the American Society for
Testing and Materials (Philadelphia) in 1981. Under linear elastic, plane strain con-
ditions,
/ i c = — (1 - v 2 ) . (9.92)
This relation is used to infer an equivalent Kic value from / I c measurements in high
toughness ductile solids in which valid Kic testing will require unreasonably large test
specimens.
St = dn^, (9.93)
where dn is a function of a, ey, and n. dn ranges in value from about 0.3 to 0.8 as n is
varied from 3 to 13 (Shih, 1981).
The crack tip opening displacement provides a measure of the size of the region at
the crack tip where finite strain deformation is dominant. The condition for the onset
of quasi-static fracture can also be stated as 8t = 8tc, where 8tc is a critical crack tip
310 Fracture mechanics and its implications for fatigue
opening displacement for the material under consideration. This approach to deter-
mining critical conditions for fracture initiation is sometimes appealing in that 8t
provides a physical length scale for fracture which is often needed for developing the
vital link between microscopic failure processes and macroscopic fracture toughness.
The magnitude of 8t varies continuously during fatigue due to the fluctuations in
load. The effective range of 8t in a given fatigue cycle is determined by the following
factors: (i) the extent of reversed flow ahead of the crack tip, as seen in the devel-
opment of Eq. 9.86, (ii) the roughness of the fracture surfaces (which is influenced by
the microscopic fatigue mechanisms and the microstructural size scale), and (iii) the
presence of any corrosion films or residual stretch of plastically deformed or trans-
formed material on the fracture surfaces which cause premature closure of the crack
even at a far-field tensile stress (see Chapter 14).
Noting the connection between / and K from Eqs. 9.57, 9.58 and 9.88, an expres-
sion for cyclic crack tip opening displacement can be derived. It is of the form given
in Eq. 9.86.
(2) The region in which finite strain effects dominate and the region in which
microscopic failure processes occur must each be contained well within the
region of the small-strain solution dominated by the singular fields, Eqs.
9.91.
The HRR fields exactly satisfy the first requirement for the use of deformation
theory of plasticity if proportional loading occurs everywhere. Then, the singularity
fields, Eqs. 9.91, based on the deformation theory assumptions are also solutions to
the corresponding J2 flow (incremental) theory equations (Section 1.4.3). Although
this requirement for proportional loading is not exactly fulfilled in general in an
elastic-power law plastic solid, the conditions encountered during the application
of monotonic, uniaxial loads to stationary cracks do provide a reasonable justifica-
tion for the use of deformation theory.
The aforementioned second requirement for the validity of / to characterize non-
linear fracture provides the physical basis for determining the inner radius, r0, of the
annular zone of /-dominance. Let R denote the outer boundary of the zone of J-
dominance which may be taken as the maximum distance ahead of the crack tip
within which the singularity solutions, Eqs. 9.91, match (say, within 10% error) the
full solutions (estimated using techniques such as the finite-element method) for the
particular specimen geometry under consideration. Finite-element, flow theory
model calculations of the crack-tip fields by McMeeking (1977) and McMeeking
& Parks (1979), which take into account crack tip geometry changes, reveal that
the finite strain effects are significant only over a distance of at most 38t. This result
provides a measure of r0. From a microstructural standpoint, r0 should be bigger
than the size of the process zone; for example, the grain size for transgranular
cleavage or intergranular fracture, and the mean spacing of void-nucleating particles
for ductile failure by void growth. Numerical simulations of near-tip fields for small-
scale yielding conditions in power law hardening materials show that the HRR
singular solutions hold over a distance of 20-25% of the size of the plastic zone
directly ahead of a mode I crack for essentially the entire range of strain hardening
exponents found in ductile alloys.
Under large-scale yielding, however, the size of the region of / dominance is
strongly dependent on specimen configuration. For these cases, where the entire
uncracked ligament may be fully engulfed in a plastic zone, the size of the region
of J dominance, R, is as small as 1 % of the length of uncracked ligament for a
center-cracked tension specimen or 7% of the length of the uncracked ligament for a
deeply cracked bend bar or a compact tension specimen (McMeeking & Parks,
1979). This is the reason why standardized test procedures for determining the
critical value of J in quasi-static loading, / Ic , require the use of deeply cracked
bend or compact tension specimens where the initial pre-crack length to the specimen
width ratio is at least 0.5 (see ASTM Standard E-813 for / Ic testing; American
Society for Testing Materials, Philadelphia). With this requirement and the result
that the zone of finite strains at the crack tip spans a distance of 38U it can be shown
312 Fracture mechanics and its implications for fatigue
that the minimum uncracked ligament size, b, needed to obtain a valid / Ic estimate is:
b = 25/ Ic /a y .
For /-controlled crack growth, Hutchinson & Paris (1979) have suggested that the
regime of elastic unloading and nonproportional loading should be confined to well
within the zone of /-dominance. In other words,
(i) In order to carry out a 'valid' plane strain fracture initiation toughness
test, small-scale yielding should be ensured. For the compact specimen
shown in Fig. A.2(a), this implies that the length of the crack, a, the size
of the uncracked ligament, (W — a), and the specimen thickness, B,
should be larger than at least 25 times the plane strain plastic zone size
(Eq. 5.1), i.e.
For small-scale yielding, / I c and Kic are related by Eq. 9.92 so that the
above equation can be rewritten as
K2
(W-a)>25—(\ -v2). (9.97)
E(Jy
Substitution of the appropriate numerical values gives the result that
(W — d) = 9.3 mm. For materials with high fracture toughness and
low yield strength values, the measurement of / I c thus provides an appeal-
ing test procedure for the estimation of fracture toughness.
(Dowling & Begley, 1976). This procedure is schematically illustrated in Fig. 9.\2{a).
Here the rising part of the load-displacement hysteresis loops for two different crack
lengths ax and a2 are shifted to a common origin. The /-integral is then obtained
from the potential energy difference corresponding to the shaded area and from Eqs.
9.56 and 9.88.
F o r the cyclic loading of a specimen under load control, there is some ambiguity in
defining the proper limits of integration in the determination of the strain energy.
(a)
a, a0
(b)
(c)
Fig. 9.12. Determination of/-integral with stabilized cyclic hysteresis loops, (a) Hysteresis loops
for two different crack lengths in displacement-controlled fatigue and the translation of the
rising part of the stabilized hysteresis loop to a common origin, (b) Similar method for load-
controlled fatigue with the minimum load being employed as the reference point, (c)
Determination of / using a single specimen.
9.7 Elastic-plastic fracture mechanics 315
Sadananda & Shahinian (1979) have suggested use of the minimum load of the
fatigue cycle as a reference point for shifting the load-displacement curves, Fig.
9.12(&). Here the rising portions of the load-displacement curves are translated to
a common origin at the minimum load. The shaded area gives the potential energy
from which the /-integral for cyclic loading can be computed. Note that these
methods require the measurement of at least two load-displacement curves corre-
sponding to two different crack lengths. Approximate methods have been developed
in an attempt to overcome this limitation and to determine / from a single specimen.
Figure 9.\2{c) schematically illustrates this method. If Ae is the total area under the
load-displacement curve (shaded region), / for characterizing fatigue crack growth
(for an edge-cracked or compact tension specimen) is determined from
J =
Tb ^IAQ + a2P(8
™* ~ 5 ™ n) }' (9 98)
'
where B is the thickness of the specimen, b is the length of the uncracked ligament, P
is the load, <5max and 8min are the maximum and minimum displacements shown in
Fig. 9.12(c), and ax and a2 are correction coefficients which are functions of the
crack length and have been published by Merkle & Corten (1974).
The justification for the above methods apparently rests on the argument that the
phenomenological constitutive models for cyclic plasticity (Chapter 3) can be for-
mulated in terms of stable hysteresis loops and that, if such loops can be mathema-
tically translated to a common origin after each load reversal, the requirement for
the stress to be proportional to the current plastic strain can be effectively satisfied.
Although many researchers have employed the /-integral to characterize fatigue
fracture at room and elevated temperatures, it should be noted that the cyclic /
approach can seriously violate the basic assumptions leading to the development
of the /-integral. Severe nonproportional loading and the rapid advance of the
fatigue crack promote conditions where material descriptions based on the deforma-
tion theory of plasticity do not hold. At this point, experimental documentation of
a reasonably good characterization of fatigue crack growth under some elastic-
plastic conditions is the main justification that can be provided for the application
of/-integral to cyclic loading. See Chapter 15 for a further discussion of this topic.
An alternative approach for characterizing fatigue crack growth under elastic-
plastic conditions is often formulated in terms of crack opening displacements. Here,
the fatigue crack growth rate is envisioned as being proportional to the cyclic crack
tip opening displacement, A<5t, defined in Eq. 9.86 such that da/dN oc A<5t. This
type of analysis provides a size scale, A<5t, for comparisons with striation spacing,
residual crack wake stretch or fracture surface oxide thickness to correlate crack
growth and crack closure (see Chapters 10 and 14). Furthermore, the crack opening
displacement offers a convenient means for comparing the fatigue crack growth rates
in different modes of fracture on a common scale. It can be seen from Eq. 9.93 that
characterizations of crack advance based on / and on 8t are essentially equivalent for
316 Fracture mechanics and its implications for fatigue
proportional loading. The implications and limitations of the approaches for fatigue
crack growth under nonlinear fracture conditions are examined in later chapters.
(9.102)
That is, in this operational definition, Q represents the difference, normalized by the
yield strength cry, between the actual hoop stress at the crack tip and that given by the
HRR singular field at a fixed distance 2J/cry directly ahead of the crack tip. The
distance r = 2J/ay is chosen so as to lie just outside the blunting zone characterized
by the finite strains; under such conditions, Q is found to be essentially independent
of r.
Alternatively, the ^-dominated small-scale yielding field, (tf//)SSY;T=o> c a n a ^ so
serve as the reference solution. O'Dowd & Shih (1991, 1992) define Q as
at 0 = 0, r = —. (9.103)
Equations 9.102 and 9.103 can be interpreted in the following manner. Positive
(negative) values of Q raise (reduce) the level of crack-tip hydrostatic stress from
that given by the HRR solutions or the small-scale yielding solution.
The variation of hoop stress, aee, as a function of the normalized distance ahead of
the crack tip, r/(J/cry), for plane strain and for E/ay = 500 and v = 0.3 are plotted
in Fig. 9.13(a) and (b) for small strain (HRR solution) and finite strain, respectively,
for different values of n and for 6 = 0. These pertain to the reference fields: T = 0
and 2 = 0.
6.0 r 6.0
\ \
•\ \ y
\ \ n=3
5.0 . \ \ r* » 5.0 \
s/*= 3
Y
/
\ \
4.0 -
\ ^5 ^v^- 4.0 - -. 5
10 " ^ ^ *
•'•• . 2 0 ' • s
3.0- 3.0-
n = 00 "/ / n = oo '" - "
s
i | i , . , 1 , i
2.0 2.0
0.0 1.0 2.0 3.0 4.0 5.0 0.0 1.0 2.0 3.0 4.0 5.0
rl(Jlay) rl(Jlcfy)
(a) (b)
Fig. 9.13. The variation of hoop stress, ae9, as a function of the normalized distance ahead of the
crack tip, r/(J/cry), for plane strain and for E/ay = 500 and v — 0.3 for (a) small strain (HRR
solution) and (b) finite strain, respectively, for different values of n and 0 = 0 for the reference
fields: T = 0 and Q = 0. (After O'Dowd & Shih, 1991, 1992.)
318 Fracture mechanics and its implications for fatigue
O'Dowd & Shih have calculated Q and Qm for several finite width geometries and
find the difference between them to be always smaller than 0.1. Consequently, the
definition of Q given in Eq. 9.103 has been recommended as the basis upon which
crack-tip stress triaxiality is quantified.
/ = ^(l-v2). (9.105)
Also, from dimensional considerations, it can be shown that
( 9 - 106 )
r
ay oy
Making use of Eq. 9.103, we write
(1^9e9,n,v,Q). (9.109)
y \J/cry ay )
Within the J-Q annulus, the fields are adequately represented by the form of Eq.
9.107. Values of Q for a variety of specimen geometries and crack sizes (a/W) can be
found in O'Dowd & Shih (1991, 1992). Implications of the two-parameter approach
to fatigue crack growth characterization is discussed in Chapter 15.
9.9 Mixed-mode fracture mechanics 319
0.5 r—
0.0
-0.5
-1.0
-1.5
-2.0
I
-1.0 -0.5 0.0 0.5 1.0
Tidy
Fig. 9.14. The variation of Q with T/ay for different values of n (for E/ay = 500 and v = 0.3).
(After O'Dowd & Shih, 1991, 1992.)
^ .aljiO) + Ku5$
5$(0)l (9.110)
where r and 0 are the polar coordinates centered at the crack tip (see Fig. 9.5) and
ojj(0) and ojj(0) are the dimensionless universal functions described in Eqs. 9.44 and
9.47. For small-scale yielding, the /-integral is related to mixed-mode stress intensity
factors by
where E' is defined in Eq. 9.2. The relative strengths of K^ and Kn can be char-
acterized in terms of an elastic mixity parameter, Me, which is defined as (Shih,
1974)
aee(r, 0 = 0) 2 K,
Afc=-tan"1 lim = -tan- l K . (9.H2)
In this characterization, Me = 0 for pure mode II, Me = 1 for pure mode I, and
0 < M e < 1 for different mixities of modes I and II.
The near-tip fields for the mixed-mode crack problem in an elastic-plastic solid
whose constitutive response is represented by the nonlinear elastic (deformation)
theory are analogous to the HRR fields for mode I described in Eq. 9.91 and are
of the form
, it). (9.113)
9.10 Combined mode I-mode II fracture in ductile solids 321
The dimensionless functions <rzy, cre, e?, and ut depend only on the polar angle 0, the
strain hardening exponent n, and the near-tip plastic mixity parameter, M p , which is
defined similar to M e as
croo(r, 0 = 0)}
M^-tan"1 lim
n
2
-tan -1 (9.114)
71
where M p equals 0 for pure mode II, 1 for pure mode I, and 0 < M p < 1 for
different mixities of modes I and II. The strength of the singular fields given in
Eqs. 9.113 is the parameter K^. The superscript P denotes that it is a plastic stress
intensity factor and the subscript M refers to the mixed-mode condition. A definite
meaning to this parameter has been given (Shih, 1974) by setting the maximum value
of the ^-variation of the effective stress, <je = v/{(3/2),f^y}5 to unity where
stj = oij — (o'kk/^ij- The strength of the dominant mixed-mode singularity, K^,
can be related to the /-integral via Mp:
-1.5
-180 90 180
Fig. 9.15. Circumferential variations of stresses and strains shown in order of increasing load
asymmetry for small-scale yielding and plane strain loading conditions. Strain hardening
exponent, n = 13. (From Shih, 1974. Copyright American Society for Testing and Materials.
Reprinted with permission.)
short fatigue cracks where plastic zone dimensions comparable in size to the crack
length cause uncertainties in characterization.
ya;
-0.6
plane strain
Fig. 9.16. Contours of plastic zones shown for different values of the strain hardening exponent
n for mode I and mode II cracks subjected to plane stress and plane strain loading. (After Shih,
1973, 1974.)
Fig. 9.17. A schematic representation of (a) kinked and (b) forked crack geometries and the
associated nomenclature.
9.11 Crack deflection 325
kx = an{a)Kl+aX2(a)Kll,
k2 = a2i(a)Kl + a22(a)Ku, (9.116)
where KY and Ku denote the mode I and mode II stress intensity factors for the main
crack in the absence of the kink or fork. To a first order approximation in a, the
dimensionless factors for the infinitesimal kink are (Bilby, Cardew & Howard, 1977;
Cotterell & Rice, 1980)
( 3 cos - +
3/ . a 3a
-lsm- + —
Suresh & Shih (1986) have presented a summary of available stress intensity factor
solutions for kinked and forked cracks as functions of the deflection angle and the
length of the deflected part of the crack. The variations of the near-tip stress intensity
factors, kx and k2, for a line crack containing a kink of length b = 0.1 a and subjected
to a far-field tensile stress intensity factor Ki are plotted in Fig. 9.18(a) as a function
of the kink angle, a. Similar results for a symmetrically forked crack with a fork
length b = 0.1a are presented in Fig 9AS(b) as a function of the included fork angle,
2a (Kitagawa, Yuuki & Ohira, 1975; Lo, 1978). Note that k2 vanishes at 2a = 32° for
b/a = 0.1. A similar observation was made by Bilby, Cardew & Howard (1977) who
calculated the included angle 2a for k2 = 0 to be 36° for b/a = 0.025.
1.0
b
= 0.1
a
^ \
0.5 - -kJK,
0.0
; K
-0.5 -
. , i , . i ,
60 120 180
2a (degrees)
(b)
Fig. 9.18. Variation of normalized kx and k2 for b/a = 0.1 as a function of (a) kink angle a and
(b) fork angle 2a. (After Kitagawa, Yuuki & Ohira, 1975.)
326 Fracture mechanics and its implications for fatigue
The studies discussed above also show that for b/a > 0.5, kx and k2 are indepen-
dent of b/a. A similar trend is observed for symmetrically forked elastic cracks. This
is consistent with the known result that the kinked and forked crack solutions for
b/a > 0.5 approach those for a crack inclined at an angle f$ (radians) (/* = n/2 — a)
to a remote tensile stress intensity K^.
-£r = sin/* cos/?. (9.118)
z/ Sa
Fig. 9.19. Crack deflection leading to (a) tilting and (b) twisting of the crack front.
9.12 Case study: Damage-tolerant design of aircraft fuselage 327
^ k^K&t, (9.120)
where the functions a\^ and o\>^ can be found listed in Lawn (1993). Equations 9.120
provide only a crude result since the twisting of a crack plane, Fig. 9.19(Z>), causes the
formation of steps along the crack path; this may promote mode II displacements as
well. Furthermore, the near-tip stress intensity factors may deviate considerably
from the predictions of Eqs. 9.120 as a consequence of frictional sliding along the
deflected segments of the crack.
The elastic solutions for kx and k2 for kinked or forked cracks are strictly valid
only when the plastic zone size is smaller than the zone of dominance of the kx and k2
singular fields, which itself is a fraction of the kink or fork length b. From a knowl-
edge of (i) the elastic solutions for kx and k2 as a function of the deflected crack
geometry, (ii) the universal mixed-mode plastic near-tip fields, and (iii) the numeri-
cally determined relationship between Me and M p as a function of the strain hard-
ening exponent n for a given deflected crack geometry, Suresh & Shih (1986) have
determined the near-tip fields ahead of a kinked or a forked crack for plane strain
and small-scale yielding conditions. Their results show that the combined effects of
crack tip plasticity and crack deflection can promote a more beneficial crack growth
resistance than deflection alone.
cylindrical fuselage with stiffeners, however, is nearly twice that of the longitudinal stress.
Consequently, the worst situation here would be for the crack to be oriented along the
axial direction. In order to arrest the advance of such a crack, tear straps or crack
arresters are commonly introduced under the frames, midway between two neighboring
frames, and under the longerons. The thickness of the tear straps is approximately the
same as that of the fuselage skin.
The spacing between adjacent tear straps provides the basis for the maximum crack
size in design. It means that, for the medium-range passenger transport aircraft, the
fuselage has to be designed with provisions for the existence of a longitudinal crack as
long as 500 mm.
Exercises
9.1 In the compliance calibration of an edge-cracked fracture toughness test-
piece of an aluminum alloy, it was observed that a load of 100 kN produced
a displacement between the loading pins of 0.3 mm when the crack length
was 24.5 mm, and 0.3025 mm when the crack length was 25.5 mm. The
fracture load of an identical testpiece containing a crack of length
25.0 mm was 158 kN. Calculate the critical value of the mechanical potential
energy release rate Q at fracture and hence the plane strain fracture tough-
ness Kic of the alloy. All testpieces were 25 mm thick. For the alloy, Young's
modulus, E = 70 GPa and Poisson's ratio, v = 0.3.
9.2 Starting with the unsymmetric part of the Airy stress function, Eq. 9.30,
where
and assuming that x is separable, i.e. x = R(r) • ©(#), derive the leading term
of the asymptotic singular solution for mode II,
following the procedure discussed in Section 9.3.2 for Mode I. Write com-
plete expressions for the different components of the stress field and com-
pare your results with Eq. 9.47.
9.3 Use the result from the previous problem to show that the expression for the
leading terms for the displacements is of the form
y
where /x is the shear modulus. Derive complete expressions for ux and uy and
compare your results with those given in Eq. 9.48.
9.4 A piston (89 mm in diameter) is designed to increase the internal pressure in
a cylinder from 0 to 55MPa. The cylinder (closed at the other end!) is
200 mm long with internal diameter = 90 mm, outer diameter = 110 mm,
Exercises 329
9.7 For plane strain and small-scale yielding conditions, the region of /-dom-
inance spans a distance R of up to 25% of the size of the monotonic plastic
zone at the crack tip. Assuming the requirement for /-dominance to be that
R > 38t (where 8t is the crack tip opening displacement defined in Section
9.7.3) and noting that 8t & 0.6//a y for a low hardening material, prove that
the requirement for /-dominance is always satisfied for a low hardening steel
with the following properties: E/cry = 500 and Poisson's ratio, v = 0.33.
9.8 Two engineering alloys, of the same overall yield strength (300 MPa) and
elastic properties, are being considered as candidate materials for a parti-
cular structural application. Material 1 has a grain size of lOjim, while the
grain size of Material 2 is 220 jim. Both alloys fail in an intergranular
fracture mode by the nucleation, growth and coalescence of voids at grain
boundaries. The structural component, for which the alloys are being con-
sidered, is subjected to a tensile stress of 85 MPa. It contains a through-
thickness single edge crack of length a = 25 mm. The thickness of the part
containing the crack is 30 mm and its width is 100 mm. (The equations
necessary to calculate the stress intensity factor for this problem can be
found in the Appendix.)
(a) Comment on the extent and validity of /-dominance for the two mate-
rials under consideration.
(b) An examination of the ASTM standard (E813) for elastic-plastic frac-
ture toughness testing of these two materials reveals the requirement
that the depth of the initial crack (i.e. the notch length plus the length of
the fatigue pre-crack) be at least one-half of the width of the specimen
(e.g., compact tension, three-point bend specimen, or four-point bend
specimen). Why?
9.9 Derive expressions for the near-tip mode I and mode II stress intensity
factors, kx and k2, respectively, for a center-cracked plate containing a
crack which is inclined at an angle fi to the far-field tensile load and sub-
jected to a far-field mode I stress intensity factor, 7^. Check your answers
with Eq. 9.118.