M 248                                            SPECIFICATIONS FOR MATERIALS
Standard Specification for
                                     Ready-Mixed White and Yellow Traffic Paints
                                                  AASHTO DESIGNATION: M 248-91
1. SCOPE                                             D 740 Specification for Methyl              of soya oil having an iodine number of
                                                             Ethyl Keotone                       115 to 130. No recovered oil, marine or
                                                     D 1199 Specification for Calcium            soya food fatty acid derivatives shall be
1.1 This specification covers alkyd resin                                                        used. The resin shall comply with the
type, ready-mixed white and yellow                           Carbonate Pigments
                                                                                                 requirements in Table 1.
traffic paints for use on bituminous and         2.2 Federal Standards:
portland cement concrete pavements.                                                              4.1.7 Alkyd Resin Type N-The resin
                                                     TT N-95 Naptha, Aliphatic Federal           shall be supplied as a 60-mass-percent
1.2 Intended use of the traffic paint.                       Standard Number 595 Colors          solution in toluene. The resin solids shall
1.2.1 These paints may be reflectorized              Federal Test Method Nº 141                  be a medium oil soya-modified pen-
for night visibility by adding reflective        2.3 Military Standards:                         taetythritol resin. No rosin shall be per-
spheres before the paint film dries or sets,                                                     mitted. The oil fatty acids shall be either
using the drop-on or pressurized meth-               MIL C 429 Chlorinated      Paraffin,
                                                                                                 alkali refined soya oil or the fatty acids of
ods. Generally, the reflective spheres are                   Technical
                                                                                                 soya oil having an iodine number of 115
evenly dispersed to a wet film of 0.38                                                           to 130. No recovered oil, marine or soya
mm (15 mils) at a rate of 600 to 720 kg/m        3. CLASSIFICATION                               food fatty acid derivatives shall be used.
(5 to 6 lbs/gal) of paint. The amount may                                                        The resin shall comply with the require-
be altered by the purchaser.                                                                     ments in Table 1.
                                                 3.1 Types-Ready-mixed alkyd resin type
1.3 Types:                                                                                       4.1.8 Alkyd Resin Type F-The resin
                                                 paint covered by this specification shall
1.3.1 Type S Traffic Paint-This type is          be furnished in the following types, as         shall be supplied at 60-mass-percent
a slow drying paint which shall be used          specified in the invitation for bids, con-      solids in VM & P naphtha. The resin
in areas where coning is acceptable for 1        tracts or order.                                solids shall be either alkali refined soya
hour or more.                                                                                    oil or linseed oil or mixture of the two,
                                                     S - Medium oil soya modified alkyd          having an iodine number of 115 mini-
1.3.2 Type N Traffic Paint-This type                      resin. Primary solvent is V M and      mum.
has immediate drying properties and shall                 P Naphtha.
be used in areas where coning of road-                                                           4.1.8.1 The solution must tolerate a 500-
                                                     N - Medium oil soya-modified pen-           mass-percent dilution with VM & P
way is acceptable for 15 to 30 minutes.
                                                          taerythritol alkyd resin; chlorin-     naphtha. A solution containing 100 g of
1.3.3 Type F Traffic Paint-This type                      ated rubber, 4 to 1-primary sol-       20 MPa•s (20 centipoise) chlorinated
shall be used where faster drying time is                 vent is toluene.                       rubber, 130 g of resin solution, and 290 g
required with a minimum of coning. With
                                                     F - Medium oil soyallinseed alkyd           of methyl ethyl ketone shall be clear,
good drying conditions, this paint should
                                                          resin; chlorinated rubber; chlorin-    transparent, and show no separation after
dry in 3 to 6 minutes if heated to 51.5 :t
                                                          ated paraffin; 1.03 to 1.30 to         24 hours of storage at 27 ± 3°C (80 ±
2.5°C (125 -±- 5°F) in the applicator.
                                                          1.00-primary solvent is MEK.           5°F) in a ¾ full test tube.
1.4 The values stated in SI units are to be
                                                                                                 4.1.8.2 The alkyd resin, reduced to 45-
regarded as the standard.
                                                 4. MATERIALS                                    percent solids with VM & P and Naph-
NOTE-It is advisable to consult local air                                                        tha, shall have a viscosity of D to G. The
pollution regulations regarding solvents prior                                                   resin shall comply with the requirements
to selecting type paint to be used.              4.1 The materials used in manufacture           in Table 1.
                                                 shall conform to the requirements of the
                                                                                                 4.1.9 Chlorinated Rubber-The rubber
                                                 following specifications:
2. REFERENCED DOCUMENTS                                                                          shall have a fixed chlorine content of
                                                 4.1.1 Lead Chromate-ASTM D 211                  65.0-percent minimum when previously
                                                 Type III.                                       dried at 100 ± 5°C (212 ± 9°F) for 24
2.1 ASTM Standards:                                                                              hours.
                                                 4.1.2 Titanium Dioxide-ASTM D 476
    D 79 Specification for Zinc Oxide            Type III Rutile (T102 80-percent purity,        4.1.9.1 A 20-mass-percent solution in
    D 211 Specification for Chrome               minimum).                                       toluene shall have a maximum color of 4
          Yellow and Chrome Orange               4.1.3 Calcium Carbonate-ASTM D                  (Gardner) and a Brookfield viscosity of 9
    D 476 Specification for Titanium             1199 Type GC-II.                                to 25 MPa•s (9 to 25 centipoises).
          Dioxide Pigments                       4.1.4 Magnesium Silicate-ASTM D                 4.1.10 Chlorinated            Paraffin-MIL
    D 362 Specification for Industrial           605.                                            C429A.
          Grade Toluene                          4.1.5 Zinc Oxide-ASTM D 79.                     4.1.11 VM & P Naphtha-T7-N-95.
    D 600 Specification for Liquid Paint         4.1.6 Alkyd Resin Solution Type S-The           4.1.12 Toluene-ASTM D 362.
          Driers                                 resin shall be supplied as a 60-                4.1.13 Methyl Ethyl Ketone-ASTM D
    D 605 Specification for Magnesium            masspercent solution in VM & P naph-            740.
          Silicate Pigment                       tha. The resin solids shall be a medium
                                                                                                 4.1.14 Driers-ASTM D 600 Class B.
    D 711 Test Method for NoPick-Up              oil soya modified resin. No rosin shall be
                                                 permitted. The oil fatty acids shall be         4.1.15 Suspending             Agent-Organo
          Time of Traffic Paint
                                                 either alkali refined soya oil or fatty acids   Montmorillonite.
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M 248                                          SPECIFICATIONS FOR MATERIALS
4.1.16 Chlorinated Rubber Stabilizer for                            TABLE 1 Characteristics of Alkyd Resin Solutions
Type N and F paint, epichlorohydrin or                                                Alkyd Resin        Alkyd Resin       Alkyd Resin
                                                            Characteristics
propylene oxide.                                                                          Type S           Type N            Type F
                                              Solids, mass percent                        60 ± 1            60 ± 1            60 ± 1
                                              Phthalic acid, mass percent                 30 min            30 min            33-37
5. REQUIREMENTS                               Oil acids, mass percent                     50 min            54 min            48-55
                                              Iodine Nº                                  115-130           115-130           115 min
                                              Color, gardner (max)                           9                 9                9
5.1 Color-The yellow paint shall match        Acid number (max)                              8                 8                8
color chip Nº 33538 of Federal Standard-      Viscosity:
595a.                                         Reduced to 45-mass-percent solids           D to H            D to H             D to G
5.2 Pigment-The pigment used in the
formulation of the paint shall conform to
Table H for the respective types and                             TABLE 2A Composition of Pigment White Traffic Paint
color.                                                                                         Mass Percent
5.2.1 The extracted pigment upon                                           Type S                Type N                   Type F
                                              Pigment Ingredients      Min        Max        Min         Max         Min         Max
analysis shall conform to the quantitative
                                              Titanium dioxide          29        31          29         31          34.0        36.0
requirements of Tables 2-A and 2-B, for       Calcium carbonate         34        36          34         36          25.0        27.0
the respective types.                         Magnesium silicate        34        36          34         36          30.0        32.0
5.3 Vehicles-All vehicles shall be free       Zinc oxide                 -         -           -          -          8.0         10.0
from rosin and rosin derivatives. The
component parts of the vehicle used shall
be as indicated in Table 3 for the respec-
                                                                TABLE 2B Composition of Pigment Yellow Traffic Paint
tive types.                                                                                   Mass Percent
5.3.1 Types N and F shall contain 2-                                       Type S                Type N                   Type F
percent stabilizer based on the mass of       Pigment Ingredients     Min         Max       Min         Max          Min         Max
chlorinated rubber.                           Lead chromate           33.0        36.0      34.0        36.0         34.0        36.0
                                              Magnesium silicate      30.0        33.0      11.0        13.0         11.0        13.0
5.4 Quantitative Requirements for the         Calcium carbonate       35.0        38.0      53.0        55.0         53.0        55.0
Paint-The paint shall meet the require-
ments specified in Tables 4-A and 4-B
for the respective type and color.
5.5 Qualitative Requirements:                        TABLE 3 Composition of Non-Volatile Vehicle White and Yellow Traffic Paint
                                                                                                Mass Percent
5.5.1 Condition in Container-The                                           Type S                 Type N                  Type F
respective types of paint shall not show      Vehicle Ingredients     Min         Max         Min         Max       Min          Max
excessive settling, gelling or curdling and   Alkyd resin solids      100          -           79         81         30          32
shall be easily redispersed with a hand       Chlorinated rubber       -                       19         21         38          40
paddle to a smooth, homogeneous state.        Chlorinated paraffin     -                        -                    29          31
After storage for periods up to 6 months
from date of packaging, the pigment shall
be readily dispersed and viscosity of the
                                                                    TABLE 4A Quantitative Requirements of White Paint
paint shall not have changed more than 5                                                            Requirements
KU from that of the freshly delivered                                              Type S              Type N                  Type F
paint.                                        Characteristics                 Min         Max      Min       Max        Min             Max
5.5.2 Spraying Properties-The paint as        Pigment, percent                61.0        63.0     57.0      59.0       48.0            50.0
received shall have satisfactory spraying     Total solids, percent           77.0          -      75.0        -        69.5             -
and hiding properties when applied            Nonvolatile vehicle,                          -      41.0        -        41.0             -
                                              percent by mass of vehicle      42.0
through a nozzle on a conventional traf-      Density, kg/m3 (lbs/gal)        1510          -      1582        -         1426            -
fic striper to a metal plate at a wet film                                   (12.6)               (13.2)                (11.9)
thickness of 0.38 mm (15 mils).               Viscosity, Krebs units           70          80       70        80          70            80
5.5.3 Appearance-The sprayed film             Fineness, Hegman                  3           -        3         -           4             -
shall dry to a smooth uniform finish free     Drying time, minutesa             -          60        -        15           -            5
                                              a
from roughness, unevenness, and other           ASTM D 711.
surface imperfections.
5.5.4 Skinning-The paint shall not skin                            TABLE 4B Quantitative Requirements of Yellow Paint
within 48 hours in a three-quartersfilled,                                                         Requirements
tightly closed container.                                                          Type S             Type N                Type F
                                              Characteristics                 Min         Max     Min        Max       Min         Max
                                              Pigment, percent                61.0        63.0    60.0        62.0     50.0        52.0
6. PACKING AND MARKING                        Total solids, percent           77.0          -     76.5          -      70.5          -
                                              Nonvolatile vehicle, per-                     -     42.0          -      40.5          -
                                              cent by mass of vehicle         42.0
6.1 The paint shall be delivered in such      Density. kg/m3 (lbs/gal)        1510                1678                 1486
                                                                                            -                   -                    -
containers as may be specified in the                                        (12.6)              (14.0)               (12.4)
contract. Each container shall bear a label   Viscosity, Krebs units           70          80      70          80       70          80
with the following information shown          Fineness. Hegman                  3           -       3           -        4           -
thereon: name and address of manufac-         Drying time. minutesa             -          69       -          15        -          5
                                              a
                                                ASTM D 711.
turer and contractor, shipping point, trade
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M 248                                        SPECIFICATIONS FOR MATERIALS
mark or trade name, kind of paint, for-     accordance with the appropriate method            for pigments and solids can be expected if
mula, number of liters (gallons), date of   in Federal Test Method Standard No.               weighing precautions are not taken.
manufacture and lot number, title and       141. If no method exists in the Federal           7.2 The purchaser tray utilize X-ray
number of this specification, and type of   Test Method, the appropriate ASTM                 analysis, gas chromatography, infra-red,
paint.                                      Method shall be used.                             or ultra violet spectral analysis of the
                                            NOTE 2-Because of the volatility of the           paint or its components to determine
7. METHODS OF SAMPLING AND                  solvents used, extreme care must be taken         whether specified ingredients were used.
   TESTING                                  when testing Type F paint for pigment and         Evidence of adulteration or improper
                                            solids. It is recommended that closed contain-    formulation shall be cause for rejection.
                                            ers, weighing bottles and transfer devices such
7.1 Except as shown in Section 6.2 the      as syringes or pipettes be used. High results
paint shall be sampled and tested in
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