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Textiles - Monoaxially Oriented High Density Polyethylene (HDPE)

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0% found this document useful (0 votes)
154 views20 pages

Textiles - Monoaxially Oriented High Density Polyethylene (HDPE)

Uploaded by

Shaheen Mave
Copyright
© © All Rights Reserved
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भारतीय मानक IS 6192 : 2023

Indian Standard (Amalgamating IS 6193 : 1971


and IS 11197 : 1985)

वस्त्रादि — एकाक्षीय उन्मुख उच्च घनत्व


पोलीइथाइलीन (एच डी पी ई)/
पोलीप्रोपाइलीन (पी पी) टे प — दवदिदि
( तीसरा पनु रीक्षण )

Textiles — Monoaxially Oriented


High Density Polyethylene
(HDPE)/Polypropylene (PP) Tapes
— Specification
( Third Revision )

ICS 59.080.01

 BIS 2023

भारतीय मानक ब्यरू ो


BUREAU OF INDIAN STANDARDS
मानक भवन, 9 बहादरु शाह ज़फर मार्ग, नई ददल्ली - 110002
MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG
NEW DELHI - 110002
www.bis.gov.in www.standardsbis.in

December 2023 Price Group 8


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Textile Materials Made from Polyolefins (Excluding Cordage) Sectional Committee, TXD 23

FOREWORD

This Indian Standard (Third Revision) was adopted by the Bureau of Indian Standards, after the draft finalized by
the Textile Materials Made from Polyolefins (Excluding Cordage) Sectional Committee had been approved by
the Textiles Division Council.

This standard was first published in 1971 and subsequently revised in 1984 and 1994. It has been revised again
on the basis of experience gained since its last revision and to amalgamate IS 6193 ‘Methods of tests for
monoaxially oriented high density polyethylene tapes’ and IS 11197 ‘Specification for monoaxially oriented
polypropylene tapes’ and also incorporate the following major changes:
a) The requirement for ash content and its test method has been specified;
b) All amendments have been incorporated;
c) Marking requirements have been modified to include the environment friendly recycling logo on the tape
package; and
d) Sampling and criteria for conformity have been modified.

The monoaxially oriented flat tapes are manufactured using thin film extrusion technology in which wide width
film is slit into narrow tapes which are subsequently stretched at elevated temperature. By doing so, the polymer
molecules are oriented in a longitudinal direction resulting in considerably improved tensile strength in that
direction combined with the reduction in linear density of tapes. Monoaxially oriented flat tapes are commonly
used in the manufacture of woven fabrics.

In the last two decades, several technological developments have taken place in polymer materials and their
performance, tape yarn manufacturing technology, tape yarn testing and analysis procedures and, the market
requirements. This has called for the revision of the existing standards on the subject to make it in line with present
requirements.

The composition of the Committee responsible for the formulation of this standard is given in Annex H.

For the purpose of deciding whether a particular requirement of this standard is complied with, the final values,
observed or calculated, expressing the results of tests, shall be rounded off in accordance with IS 2 : 2022 ‘Rules
for rounding off numerical values (second revision)’. The number of significant places retained in the rounded off
values should be the same as that of the specified values in this standard.
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IS 6192 : 2023

Indian Standard
TEXTILES — MONOAXIALLY ORIENTED HIGH DENSITY
POLYETHYLENE (HDPE) AND POLYPROPYLENE (PP)
TAPES — SPECIFICATION
( Third Revision )

1 SCOPE 3.6 Melt Flow Index (MFI) — This is a measure of


the ease of flow of the melt of a
This standard specifies requirements and test thermoplastic polymer. It is defined as the weight
methods for monoaxially oriented high density of the polymer in grams flowing in 10 min through
polyethylene (HDPE) and polypropylene (PP) tapes a capillary die of specific diameter and length by a
suitable for weaving into fabric. pressure applied by a given weight at a given
temperature. The applied pressure and the capillary
2 REFERENCES die temperature vary with polymer type and are
specified for various polymers.
The standards listed in Annex A contain provisions
which, through reference in this text, constitute 3.7 Nominal Gauge Length — The length of a tape
provisions of this standard. At the time of specimen under specified pre-tension, measured
publication, the editions indicated were valid. All from nip to nip of the jaws of the holding clamps of
standards are subject to revision and parties to the tensile tester in their starting position.
agreements based on this standard are encouraged to
investigate the possibility of applying the most 3.8 Polypropylene Tape — A flat tape made from
recent editions of these standards. polypropylene homopolymer, with a high width and
thickness ratio.
3 TERMS AND DEFINITIONS
3.9 Tape — A flat strip of thermoplastic polymer,
For the purpose of this standard, the following extruded, stretched, monoaxially oriented, with high
definitions shall apply. tensile strength and a high width and thickness ratio.
NOTES
3.1 Accelerated Weathering Test — A type of
short term, fast laboratory testing which is used to 1 The method of production of monoaxially oriented tapes
consists of manufacturing a film by circular die tubular
measure long term possibilities of material’s blown film process or by flat die cast film process. Slitting
durability under certain outdoor environmental of film into narrow width tapes and uniaxial stretching of
conditions. slit tapes in hot air oven at 130 °C to 170 °C at a stretch ratio
of 1 : 5 to 1 : 8. The oriented tapes subsequently pass over
3.2 Breaking Strength — The maximum load (or hot rolls or through a heat-set stabilizing oven at 125 °C to
135 °C to attain a longitudinal shrinkage of 4 percent to 8
force), supported by a specimen in a tensile test percent followed by cooling and winding of tapes over a
carried to rupture. It is usually expressed in Newton package under uniform tension. The hot stretching process
or kilogram (1 kgf = 9.81 N). confers monoaxial molecular orientation, imparting high
longitudinal strength to tapes.
3.3 Elongation at Break — In a tensile test, the 2 Circular die tubular blown film process is occasionally
difference between the length of an elongated used for manufacturing HDPE tapes, whereas, flat die cast
specimen at breaking load and its initial length, film process is most commonly used for manufacturing of
HDPE and PP tapes.
usually expressed as a percentage of the latter. It is
measured in percentage. Higher elongation 3 The temperatures used for extrusion, stretching and for
means higher ductility or higher plastic deformation. heat-set stabilization are polymer dependent and vary for
HDPE and PP tape production process.
NOTE — The result of elongation obtained in the test may
have slight errors because of the possibility of tape slippage 3.10 Tape Denier — A unit of measure for the linear
during testing. mass density of tape. Tape denier is the mass in
grams per 9 000 metres of the tape. Tapes with high
3.4 High Density Polyethylene Tape — A flat tape denier tend to be thick, strong, and durable.
made from high density polyethylene having a high
ratio of width to thickness. NOTE — Tex is also one of the units of measure of tape
linear density and is calculated by dividing tape denier value
by 9.
3.5 Linear Density — It is the measure of the
amount of mass per unit length and is usually 3.11 Tape Shrinkage — A measure of the reduction
denoted by denier or tex. in length of monoaxially oriented tape after it is

1
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IS 6192 : 2023

subjected to elevated temperatures, the heating agents, anti-rodent agents, pigments, carbon black,
medium may be hot air, hot oil or heat inducing light fillers (calcium carbonate) and reinforcement agents
source. Tapes showing high shrinkage are may be added to HDPE or PP raw materials for
considered dimensionally unstable and can cause improved tape properties.
deforming of the fabrics made out of these tapes.
5 REQUIREMENTS
3.12 Tape Tenacity — A measure of the tape
breaking strength in gram divided by the linear 5.1 The high density polyethylene and
density of tape, usually in denier. Tape tenacity is polypropylene tapes shall conform to the
commonly denoted by unit, gram per denier or gpd. requirements as specified in 5.1.1 to 5.1.8.
3.13 Time-to-Break — The time interval, measured
5.1.1 The finished tape width shall be as agreed to
in suitable units during tensile testing, such as
between the buyer and the seller. The finished width,
seconds, during which the tape specimen is under a
however, shall be more than 2 mm but not exceeding
(generally increasing) tension, that is, absorbing the
5 mm and shall be subjected to a tolerance of
energy supplied before the breaking strength is ± 5 percent on agreed or declared width, when tested
reached. as per method given in Annex B.
NOTE — Time-to-break does not include the time required
to remove slack from the specimen. On machines supplied 5.1.2 The thickness of the tape shall correspond to
with an autographic recorder the time to break is indicated
by the time elapsing after the pen registers the initial force the linear density and width. The tape thickness shall
sustained by the specimen until the pen registers the be subjected to a tolerance of ± 10 percent on agreed
maximum force. The commonly accepted time to break the or declared thickness, when tested as per method
sample during tensile testing of tapes is 20 s ± 3 s. given in Annex B.
4 MATERIAL AND MANUFACTURE 5.1.3 The linear density of tape shall be as agreed to
between the buyer and the seller. The linear density
4.1 High Density Polyethylene Tapes of the tape shall be minimum 380 denier (42.22 tex)
when tested as per method given in Annex C. The
The tape shall be made from high density denier of tape shall be subjected to the tolerances
polyethylene having a density 0.940 g/ml to ± 10 percent on individual value, and ± 5 percent on
0.965 g/ml at 27 °C (see also IS 7328) and melt flow average value.
index of 0.4 g/10 min to 1.5 g/10 min for blown film
process and 0.8 g/10 min to 2.0 g/10 min for the cast 5.1.4 The average tenacity shall be minimum
film process when measured at 190 °C under a load 36 g/tex (4 g/denier) for high density polyethylene
of 2.16 kg when determined in accordance with tapes and 45 g/tex (5 g/denier) for polypropylene
IS 13360 (Part 4/Sec 1). The grade of polyethylene tapes when tested as per method given in Annex D.
used for the manufacture of tapes shall be selected The average tenacity shall not be less than the value
taking into consideration the film extrusion process specified and none of the individual value shall not
used. Polyethylene used for the manufacturing of be less than 10 percent of the specified tenacity
tapes shall conform to the requirements as specified value.
in IS 10146, excluding overall migration.
5.1.5 The average value of the elongation at break of
4.2 Polypropylene Tapes tape shall not be less than 15 percent but shall not
exceed 25 percent and none of the values shall fall
The tape shall be made from polypropylene outside the range specified when tested as per the
homopolymer having a density 0.900 g/ml at 27 °C method specified in Annex D.
(see also IS 10951) and melt flow index of 1.5 g/
10 min to 7.0 g/10 min for cast film process when 5.1.6 If agreed to between the buyer and seller, the
measured at 230 °C under a load of 2.16 kg when tapes may be manufactured from UV stabilized
determined in accordance with IS 13360 (Part 4/ HDPE and PP resins. The UV stabilized tapes shall
Sec 1). The grade of polypropylene chosen shall be have at least 50 percent retention of the original
the one suitable for the manufacture of film by the breaking strength when tested after the same has
cast film process. Polypropylene used for the been exposed to UV radiation and accelerated
manufacturing of tapes shall conform to the weathering in accordance with the test method given
requirements as specified in IS 10910, excluding in Annex E. The average tape tenacity before and
overall migration. after UV radiation exposure shall be determined as
per the test procedure given in Annex D.
4.3 Additives and Masterbatches
5.1.7 The average heat shrinkage of HDPE tapes at
As agreed between buyer and seller, functional 60 °C shall not exceed 5 percent and at 100 °C shall
additives like antioxidants, UV stabilizers, antistatic

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IS 6192 : 2023

not exceed 8 percent. On the other hand, the heat of this standard may be certified as per the
shrinkage of PP tapes at 100 °C shall not exceed conformity assessment schemes under the
5 percent and at 125 °C shall not exceed 8 percent. provisions of the Bureau of Indian Standards Act,
For heat shrinkage testing, the tapes shall be 2016 and the Rules and Regulations framed
subjected to the specified temperatures for a period thereunder, and the tape packages may be marked
of 10 min in hot air circulating oven in accordance with the Standard Mark.
with the test method given in Annex F.
6.4 Storage
5.1.8 The tapes when tested for ash content in
accordance with the test procedure given in The tape packages shall be stored in cool and dry
Annex G, shall not be more than 6 percent for non- place, covered warehouse at temperature below
UV stabilized tapes and 2.2 percent for UV 50 °C and shall be protected from direct sunlight,
stabilized tapes. smoke, fumes, open flame and radiation.

6 MARKING, PACKING AND STORAGE 7 ATMOSPHERIC CONDITIONS FOR


SAMPLE CONDITIONING AND TESTING
6.1 Marking
Prior to the test, specimens shall be conditioned to
Each tape package shall be tagged with a moisture equilibrium from dry side in standard
label/sticker containing the following information: atmosphere of (65 ± 2) percent relative humidity and
27 °C ± 2 °C temperature as laid down in IS 6359.
a) Manufacturer’s name and identification
mark; NOTE — Prior to the test, the test specimens preferably be
conditioned in the atmosphere as specified in 7, for at least
b) Polymer type (HDPE/PP) 24 h.
c) Lot number;
8 SAMPLING AND CRITERIA FOR
d) Tape denier/Tape width in mm; CONFORMITY
e) Net mass (when packed);
f) Recycling logo (see Note 1); 8.1 All tape packages of the same polymer material,
tape width, tape denier, colour and produced under
g) Swachh Bharat logo (see Note 2); and similar conditions of production and delivered to a
h) Any other information as required by the buyer shall be grouped together to constitute a lot.
law in force.
8.2 Unless otherwise agreed to between the buyer
NOTES
and the seller, the number of tape packages to be
1 Each tape package shall be marked with a recycling selected from a lot shall be in accordance with the
logo as shown below. While marking the symbol, the
respective basic raw material name corresponding to
sampling data given in Table 1. These packages
polymer identification number shall be indicated shall be selected at random and to ensure the
below the symbol in accordance with IS 14534. randomness of selection, IS 4905 may be followed.

8.3 Conformity of lot to the requirements of standard


shall be determined based on the tests carried out on
samples selected from it.

8.4 The number of samples to be selected depends


on the size of the lot and the number of tape
2 Each tape package shall also be marked with a packages to be sampled, shall be in accordance with
Swachh Bharat logo, clearly visible on the label, either col (2) and col (3) of Table 1. At least 10 test
compatible with the art work of the buyer or in black
colour. specimens are to be taken from randomly sampled
tape packages for testing tape width, tape thickness,
6.2 Packing tape denier, tape tenacity, elongation at break,
tenacity of UV stabilized tape for strength retention,
Unless otherwise agreed to between the buyer and tape shrinkage and ash content analysis.
the seller, each tape package shall be suitably packed
in a film pouch and about 100 of such tape packages 8.5 Criteria for Conformity
shall further be packed into a larger secondary
The lot shall be considered in conformity with the
package and secured from soiling and damage
requirements of the relevant specification if the
during storage and transportation.
specimens drawn from all the packages satisfy the
6.3 BIS Certification Marking relevant requirements as specified in 5.1.1 to 5.1.8.

The tape packages conforming to the requirements

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IS 6192 : 2023

Table 1 Sample Size and Criteria for Conformity


(Clauses 8.2, 8.4 and C-3)
Sl No. No. of Tape Packages in a Lot No. of Tape Packages to be
Sampled
(1) (2) (3)
i) Up to 150 5
ii) 151 to 500 8
iii) 501 to 3 000 13
iv) 3 001 and above 20

ANNEX A
(Clause 2)
LIST OF REFERRED STANDARDS

IS No. Title IS No. Title


IS 4905 : 2015/ Random sampling and pharmaceuticals and
ISO 24153 : randomization procedures drinking water
2009 (first revision)
IS 10951 : 2020 Specification for
IS 6359 : 2023 Methods for conditioning polypropylene (PP)
of textiles (first revision) materials for moulding and
extrusion (second revision)
IS 7328 : 2020 Specification for
polyethylene material for IS 13360 (Part 4/ Plastics — Methods of
moulding and extrusion Sec 1) : 2000 testing: Part 4 Rheological
(second revision) properties, Section 1
Determination of the melt
IS 10146 : 1982 Specification polyethylene
mass flow rate (MFR) and
for its safe use in contact
the melt volume flow rate
with foodstuffs,
(MVR) of thermoplastics
pharmaceuticals and
(first revision)
drinking water
IS 14534 : 2023 Plastics — Recovery and
IS 10910 : 1984 Specification for
recycling of plastics waste
polypropylene and its
— Guidelines (second
copolymers for its safe use
revision)
in contact with foodstuffs,

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IS 6192 : 2023

ANNEX B
(Clauses 5.1.1 and 5.1.2)
METHOD OF TEST FOR MEASUREMENT OF TAPE WIDTH AND TAPE THICKNESS

B-1 PRINCIPLE of suitably calibrated spring-loaded dial micrometre.


The thickness shall be measured to an accuracy of
Physical measurement of tape specimen to quantify 2 micrometre. The pressure applied by the contact
the size, such as width, thickness or length using foot of the dial micrometre shall be not less than
suitable measuring devices with high accuracy 140 kN/m2 (1.428 kgf/cm2).
levels.
B-3.2 Test Procedure
B-2 TAPE WIDTH
Dry and clean the surface of the anvil and spindle
B-2.1 Apparatus head, and of the specimen. Place the specimen on the
anvil and lower the spindle head on to it slowly. The
The width of the tape shall be determined by
total load applied by the spindle shall be 110 g. Ten
measuring with a steel rule having 0.1 mm divisions.
readings shall be taken over a length of not less than
B-2.2 Test Procedure and Results 2 m at regular intervals and between 15 s and 2 min
after the load is applied and the average value to be
The width shall be measured to the nearest 0.1 mm. reported as the thickness of the tape.
The average of 10 readings shall be taken over a
length of not less than 2 m and reported as the B-4 TEST RESULTS
average width of the tape. A tolerance of ± 5 percent
Take average of the measurements of all the
on the average value shall be permissible.
specimens of a sample to obtain the average
B-3 TAPE THICKNESS thickness value. This method can produce
measurements with a maximum error of
B-3.1 Apparatus + 0.002 5 mm. A tolerance of ± 10 percent on the
average value shall be permissible.
The thickness of tape shall be determined by means

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IS 6192 : 2023

ANNEX C
(Clauses 5.1.3, D-4.1 and F-3.2)
METHOD OF TEST FOR MEASUREMENT OF LINEAR DENSITY (DENIER) OF TAPE

C-1 PRINCIPLE between the two marks. Measure at least 10 tape


specimens.
The linear density is determined from the mass of a
specified length of tape and expressed in denier or C-4 TEST PROCEDURE
tex. The specimen is first conditioned free from
tension for predetermined time duration and then the For determination of mass of the test specimen (M),
length is measured under standard pretension. The take at least 9 m and 10 m length of tape specimen
specimen is then weighed, and the mass is used in (L) for Denier and Tex measurement, respectively.
calculating the linear density (denier) of the Measure the specimen length to an accuracy of 1 mm
specimen. and correspondingly weigh each test specimen
correctly to 1 mg.
C-2 APPARATUS
C-5 CALCULATIONS
C-2.1 Digital Balance with Pan — Digital balance
with sample holding pan, capable of weighing test Calculate the linear density for each test specimen
specimen to an accuracy of 1 mg. by one of the following formulae:
C-2.2 Length Measuring Scale — A metallic ruler 100 ×90 × 𝑀
or a suitable length measuring instrument graduated a) Denier =
𝐿
in millimetres, and capable of measuring dimensions
up to 10 m with an accuracy of 1 mm. 100 ×10 × 𝑀
b) Tex =
𝐿
C-3 PREPARATION OF TEST SPECIMENS
where
Select at least five tape packages as given in Table 1 M = Mass of the test specimen in grams; and
and before initiating tape specimen sampling,
L = length of test specimen in metre.
discard the initial few metres of tape from the sample
package. From each tape package, draw enough
length of tape specimen and keep on a flat horizontal C-6 TEST RESULTS
table with markings at both ends, having specified Calculate denier for at least 5 samples and obtain the
dimension between the two marks, preferably 9 m average denier value. This method allows denier
for denier and 10 m for tex measurement. Render the measurements with a maximum error of
tape yarn flat on a table and free from any twist or + 0.5 percent. A tolerance of ± 5 percent on the
wrinkles and apply fixed pretension of 0.5 cN/tex
average value shall be permissible.
± 0.1 cN/tex. Measure and cut the tape specimen

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IS 6192 : 2023

ANNEX D
(Clauses 5.1.4, 5.1.5, 5.1.6 and E-4.1)
METHOD OF TEST FOR MEASUREMENT OF BREAKING STRENGTH, ELONGATION AT
BREAK AND TENACITY

D-1 PRINCIPLE the test. Also, the edge of the surface


of each jaw shall be such test it would
D-1.1 Conditioned tape specimen is gripped not cut or damage the specimen during
between the two clamps of the tensile testing testing;
machine and a continual increasing load is axially
NOTE — The faces of the jaws are generally,
applied by moving one of the clamps until the flat, engraved or corrugated. To avoid the
specimen breaks. Values of elongation chances of slippage or damage to the specimen,
corresponding to a predetermined load, maximum packing materials like paper, felt, leather, plastic
breaking strength and elongation at break of the test or rubber sheet may be used.
specimen are noted. Tenacity is determined by
dividing the breaking strength in grams by the linear A schematic diagram of the above type of
density in denier, whereas, the elongation at break clamp is shown in Fig. 1. The length of
(percent) is determined by dividing the elongation specimen between points A and A1 is the
by the initial gauge length. test length or the gauge length.

D-2 APPARATUS b) Means for adjusting the distance between


the clamps such that the tape specimens can
D-2.1 Tensile Testing Equipment — A tensile be tested at 200 mm nominal gauge length;
testing machine is provided with two crossheads; NOTE — For undrawn tapes having very high
one is adjusted for the length of the specimen and potential of extension during test, it is recommended
to test the tape specimens at 50 mm nominal gauge
the other is driven to apply tension to the test length.
specimen till it breaks. The crosshead driving
mechanisms used are Constant Rate of Traverse c) Means for driving by power, one of the pair
(CRT), Constant Rate of Loading (CRL) and, of clamps at a specified constant-rate-of-
Constant Rate of Extension (CRE). However, the traverse (CRT) so that the test specimen
most commonly used driving mechanism is the breaks in 20 s ± 3 s (average time to break).
CRT. Test shall be carried out at the rate of
traverse of 300 mm/min ± 15 mm/min; and
D-2.2 Clamps d) A scale or dial or autographic recording
chart graduated to give load in newtons
a) Two clamps with the following provisions (kilograms) and elongation in millimetres.
to grip the tape specimens: The load cell of the testing shall be selected
1) Each clamp of the machine shall such that all the observed values would lie
consist of two metallic jaws and each between 20 percent and 80 percent of the
jaw face shall be in line both with full-scale load. The permissible error in the
respect to its mate in the same clamp machine at any point in this range shall not
and to the corresponding jaws of the exceed ± 1 percent.
other clamp; and
D-2.3 Other Requirements
2) Each clamp of the machine shall be of
curved type in which the tape is a) Means for applying pre-tension of
gripped between the plain-faced jaws (0.05 ± 0.01) g/denier to the specimen
and this makes a half turn around a when clamped (tension device may be a
cylindrical extension of one of the dead weight, a spring or an air-actuated
jaws before passing on to the other mechanism);
similar clamp. The cylindrical friction b) An analogue or digital scale and dial or
surface shall be between 10 mm to autographic chart recorder graduated to
20 mm in diameter. Each clamp shall give load and elongation at predetermined
be provided with a mechanical or load and at break; and
pneumatic device so constructed that
through its means a specimen can be c) A pair of scissors or a sharp blade,
secured firmly between the jaws of the measuring scale, stopwatch, etc.
clamps so that it does not slip during

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IS 6192 : 2023

FIG. 1 SCHEMATIC DIAGRAM OF GRIPPING CLAMPS

D-3 TEST PROCEDURE at random several metres of tape between two


successive tests. Perform minimum 10 tests or as
D-3.1 Test on Conditioned Specimens for agreed to between the buyer and the seller.
Tenacity and Elongation
D-3.2 Repeat the procedures laid down in D-3.1.1 to
D-3.1.1 Set the clamps of the testing machine so that D-3.1.3 for all the specimens to be tested.
the distance between the clamps is 200 mm ± 2 mm
or as agreed to between the buyer and the seller. D-4 CALCULATIONS
Take the tape from the conditioned sample and
discard a first few metres of tape. Fix one end of the Determine the tape tenacity in grams per denier
specimen in jaw of top clamp and apply the required (gpd) and elongation at break in percentage for each
pre-tension from the free end and secure the other test specimen.
end in jaw of bottom clamp.
D-4.1 Tenacity
D-3.1.2 Operate the tensile testing machine and
continue the test to rupture and record the breaking Calculate the tape tenacity as per the formulae given
load and elongation at break from the load below and compute the average tape tenacity from
elongation curve of the autographic chart recorder all the observed values.
provided.
Tenacity, gpd =
NOTES Average breaking strength in newton
× 100
Average linear density in denier
1 For determining breaking strength of tapes having
elongation at break greater than 75 percent, the nominal NOTE — The linear density of tape shall be determined
gauge lengths may be reduced to 100 mm. For testing from the same package in accordance with Annex C of this
undrawn tapes, the nominal gauge lengths may be reduced standard.
to 50 mm.
2 Even if a test value is isolated because of a break near the D-4.2 Elongation at break
jaw, the value shall be noted but not considered in
calculations. If such breaks exceed 10 percent of the number Calculate the elongation at break as per the formulae
of test specimens analysed, suitable corrective action should given below and compute the average elongation at
be taken on jaws and clamps of the machine.
break from all the observed values.
D-3.1.3 Open both the clamps and remove the Elongation at break, percent =
broken specimen. Test another test specimen in a gauge length at break − initial gauge length
similar manner as in D-3.1.1 and D-3.1.2 discarding × 100
Initial gauge length

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IS 6192 : 2023

D-5 TEST RESULTS confirm to the requirements given in 5.1.4 and 5.1.5.

Calculate the average tape tenacity and elongation at NOTE — If required, the test results for tape tenacity may
be provided in tex based measuring units. The typical unit
break for at least 10 samples. The minimum tape
conversion chart is provided below (g = gram, den = denier,
tenacity (gpd) and the elongation at break shall dtex = decitex, and cN = centi Newton):

Sl No. Unit g/den g/tex g/dtex cN/tex

(1) (2) (3) (4) (5) (6)


i) g/den 1 (g/tex)/9 (g/dtex) × 10/9 (cN/tex) × 0.113
ii) g/tex (g/den) × 9 1 (g/dtex) x 10 (cN/tex) × 1.02
iii) g/dtex (g/den) × 0.9 (g/tex)/10 1 (cN/tex) × 0.102
iv) cN/tex (g/den) / 0.113 (g/tex)/1.02 (g/dtex)/0.102 1

ANNEX E
(Clause 5.1.6)
UV RESISTANCE TEST

E-1 PRINCIPLE d) Pre-set timer functions incorporated for


accuracy and time cycle repeatability.
UV light resistance of HDPE/PP monoaxially
oriented tapes is analysed using accelerated E-3 TEST CONDITIONS
weathering test. UV exposure testing uses
fluorescent UV light, rain, dew and in special case The test shall be carried out with fluorescent UV-
wind to simulate long term outdoor exposure to lamp Type B (313 nm or its equivalent). The test
natural sunlight. This test measures the effect of duration shall be 192 h (about eight days) in
ultraviolet light on the mechanical properties of a continuous mode.
product.
The test cycle shall be 8 h at 60 °C ± 3 °C with UV-
To determine the effects of UV radiation and radiation alternating with 4 h at 50 °C ± 3 °C with
weathering on HDPE/PP tape samples, the tapes are condensation. Irradiance level throughout the test
exposed to UV radiation under accelerated + 0.04
shall be maintained at 0.63 W/m2.
weathering test as given in E-3 and E-4. The UV − 0.00
exposed tapes are then tested for tape tenacity and
the extent of tape tenacity retained vis a vis E-4 TEST PROCEDURE
unexposed tape sample is determined.
E-4.1 Determine the average initial tape tenacity
E-2 APPARATUS (before UV exposure) as per the test method
specified in Annex D.
UV accelerated weathering tester is an instrument
that reproduces outdoor environmental effects like The sample holder for tapes shall ensure
sunlight, rain and dew with alternating cycles of unobstructed exposure to UV light and other
fluorescent UV light exposure and moisture at weathering conditions. The exposed tape sample
controlled, elevated temperatures. size shall be appropriate in length suitable for tensile
testing.
This instrument essentially has the following
accessories and systems: E-4.2 Expose the specimen alternately to ultraviolet
light and condensation in respective test cycle in
a) Fluorescent UV lamps to simulate short- continuous mode for total 192 h.
wave ultraviolet part of sunlight;
b) Water spaying and humidity control system E-4.3 The type of fluorescent UV lamp, the timing
during the condensation cycle; of the UV and condensation exposure and the
temperature of UV exposure and condensation shall
c) Temperature setting, temperature cycle be as specified in E-3.
repeatability and monitoring system; and

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E-5 TEST RESULTS as obtained in E-4.1; and


E-5.1 Determine the average tape tenacity b = Average tape tenacity after UV exposure as
separately after UV exposure as mentioned in D-4.3. obtained in E-5.1.

E-5.2 Determine the percent retention of original NOTES


tape tenacity as follows: 1 The UV source is an array of fluorescent lamps (with
lamp emission concentrated in the UV range).
Retention of original tape tenacity, percent =
2 Condensation is produced by exposing the test
𝑏 surface to a heated, saturated mixture of air and water
× 100 vapour, while the reverse side of test specimen is
𝑎
where exposed to the cooling influence of ambient room air.

a = Average tape tenacity before UV exposure

ANNEX F
(Clause 5.1.7)
METHOD OF TEST FOR MEASUREMENT OF HEAT SHRINKAGE

F-1 PRINCIPLE F-3 TEST PROCEDURE

F-1.1 Physical measurement of dimensional changes F-3.1 Test specimens


in the length of monoaxially oriented tape specimen
before and after exposure to elevated temperatures. Ten test specimens each about 150 mm long are
The shrinkage is determined by the ratio of the required.
contraction in length of the tape sample after test and
the initial sample length before the test. F-3.2 The linear density of tape is first determined
according to Annex C. Dead weights are prepared,
F-1.2 Shrinkage is an important quality control each having a mass in grams equal to 0.05 times the
parameter to ensure the dimensional stability of linear density value in denier. Top end of each
monoaxially oriented tapes and the products made specimen is tied to the specimen mounting frame
thereof. and the bottom end of the specimen is attached with
dead weight. Two marks are made on each tape such
F-2 APPARATUS that:
a) The distance between the marks shall be
F-2.1 Hot Air Circulating Oven — A hot air
100 mm ± 0.5 mm;
circulating oven made of heat insulating walls and
having enough size to hold at least twenty b) The distance from the top mark to the
specimens, freely hanging from the top without specimen holder shall be minimum 10 mm;
touching the bottom. The oven shall have suitable and
temperature control and monitoring device, capable
c) The distance from the bottom mark to the
of maintaining air temperature in the range of 50 °C
to 150 °C with an accuracy of ± 1 °C. The oven shall point of attachment of the weight shall be
also be equipped with a forced air circulation and minimum 10 mm (see Fig. 2).
monitoring system.
F-3.3 Specimens shall be exposed to the following
specified temperatures for 10 min;
F-2.2 Specimen Mounting Frame — The
specimen mounting frame shall be such that test For HDPE tapes — at (60 ± 2) °C and at (100 ± 2) °C
specimens of at least 150 mm in length can be
vertically mounted on it with one of its ends is fixed For PP tapes — at (100 ± 2) °C and at (125 ± 2) °C
to the top clamp and the other end hanging
downwards and attached with dead weight for On completion of the test period for 10 min, the oven
applying pre-tension. The dead weights shall have temperature is brought down to room temperature.
suitable grip or fastening arrangement to attach to The specimens are then removed from the mounting
the tape. The oven height shall be such that the frame and the distance between the two marks is re-
weights are supported only by the tape, that is, the measured to an accuracy of 1 mm.
weights shall not be allowed to rest on the bottom of
the oven (see Fig. 2). F-3.4 Take at least 10 readings for each sample.

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FIG. 2 SPECIMEN MOUNTING FRAME

F-4 TEST RESULTS where


Express the shrinkage as a percentage shrinkage at a = Initial length of the specimen; and
the temperature at which the test was carried out.
Calculate the heat shrinkage percentage from the b = Final length of the specimen after heat
initial and the final lengths of test specimen. treatment.

𝑎−𝑏
Heat shrinkage, percent = × 100
𝑎

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ANNEX G
(Clause 5.1.8)
DETERMINATION OF ASH CONTENT

G-1 PRINCIPLE G-3 TEST PROCEDURE

The procedure is used to find the inorganic residue G-3.1 Clean the crucible and heat it at 590 °C
in the HDPE/PP tape sample by ashing it in a muffle ± 10 °C for 10 min to 15 min and cool it in a
furnace. A weighed amount of tape sample is heated desiccator.
to 590 °C. The polymer sample (organic portion) is
burnt at 590 °C until the constant mass of inorganic G-3.2 Weigh the empty crucible to nearest 0.001 g.
matter is obtained. The residue (inorganic matter) is
reported in terms of percentage ash content in a G-3.3 Weigh 3 g of tape sample in the crucible
given sample. (nearest to 0.001 g).

G-2 APPARATUS G-3.4 Heat the crucible directly on burner so that the
sample burns slowly, and loss of ash is avoided.
G-2.1 Weighing Balance — accurate to 0.001 g Continue burning until no more smoke is evolved.

G-2.2 Silica Crucibles — sufficient volume to G-3.5 Transfer the crucible in the muffle furnace,
accommodate 3 g of sample in such a way that the which is already maintained at approx. 590 °C and
level of the sample after filling the crucible does not keep inside for about 2 h.
cross half the height of the crucible.
G-3.6 Remove the crucible from the furnace and
G-2.3 Bunsen burner cool it to room temperature in a desiccator and weigh
it and record the weight to an accuracy of 0.001 g.
G-2.4 Silica triangle and tripod
G-3.7 Keep the crucible in the muffle furnace for
G-2.5 Muffle Furnace — capable of being another 30 min, cool in a desiccator and weigh again.
controlled thermostatically at 590 °C ± 10 °C Repeat the procedure until the constant mass is
obtained.
G-2.6 Desiccator — containing an effective drying
agent (for example silica gel) that does not react G-4 TEST REPORTING
chemically with ash components
Weight of ash
Ash content, percent = × 100
G-2.7 Gloves and crucible holder Weight of tape sample

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IS 6192 : 2023

ANNEX H
(Foreword)
COMMITTEE COMPOSITION
Textile Materials Made from Polyolefins (Excluding Cordage) Sectional Committee, TXD 23

Organization Representative(s)

Indian Institute of Packaging (IIP), Mumbai DR TANWEER ALAM (Chairperson)

ACC Limited, Mumbai SHRI ANURAG TYAGI


DR MANISH KARANDIKAR (Alternate)

All India Flat Tape Manufacturers Association (AIFTMA), SHRIMATI PADMAJA REDDY
New Delhi SHRI SAJJAN RANASARIA (Alternate)

All India HDPE/PP Woven Fabric Manufacturing SHRI NARESH BHANDIA


Association, Bangalore

Cement Manufacturers Association (CMA), Noida DR S. K. SAXENA


SHRI VISHAL MOHITE (Alternate)

Central Institute of Petrochemicals Engineering & DR SANDESH KUMAR JAIN


Technology (CIPET), Lucknow SHRI VIVEK KUMAR (Alternate)

Central Pollution Control Board (CPCB), New Delhi SHRI KAMLESH SINGH
SHRI RISHABH SRIVASTAV (Alternate)

Chemicals and Petrochemicals Manufacturers Association SHRI AJAY SARDANA


(CPMA), New Delhi SHRI UDAY CHAND (Alternate)

Consumer Guidance Society of India, Mumbai DR SITARAM DIXIT


DR M. S. KAMATH (Alternate)

Federation of Indian Chambers of Commerce & Industry SHRI MANOJ MEHTA


(FICCI), New Delhi SHRI AMIT KAKKAR (Alternate)

Food Corporation of India (FCI), New Delhi SHRI RAJAGOPAL A.


SHRI A. K. U. B. SINGH (Alternate)

Dept. of Chemical & Petrochemical, Ministry of Chemical & SHRI O. P. SHARMA


Fertilizers, New Delhi SHRI VARUN POONIA (Alternate)

Directorate of Sugar, New Delhi Ministry of Consumer SHRI SANGEET SINGLA


Affairs, Food & Public Distribution, New Delhi SHRI D. K. JHA (Alternate)

Gas Authority of India Limited (GAIL), New Delhi SHRI MANISH KHANDELWAL

Government e Marketplace (GeM), New Delhi REPRESENTATIVE

Gujarat Narmada Valley Fertilizers Co. Ltd, Narmadanagar SHRI YOGESH N. PATEL
SHRI RAKESH S. AGRAWAL (Alternate)

Gujarat State Fertilizers and Chemicals Limited, Gujarat SHRI DILIPKUMAR BHIKHABHAI SHAH
SHRI PUJAN B. VAISHNAV (Alternate)

Haldia Petrochemical Ltd, Kolkata SHRI RAJ K. DATTA


SHRI T. R. SRIKANTH (Alternate)

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Organization Representative(s)

HPCL-Mittal Energy Limited, Noida SHRI VINEET KUMAR GUPTA


SHRI ALAKESH GHOSH (Alternate)

Indian Farmers Fertiliser Cooperative (IFFCO) Ltd, SHRI HARISH KUMAR


New Delhi SHRI OM PRAKASH KUMAR (Alternate)

Indian Flexible Intermediate Bulk Container Association SHRI MAKRAND APPALWAR


(IFIBCA), New Delhi SHRI RAVISH KAMATH (Alternate)

Indian Institute of Packaging (IIP), Mumbai DR AMIT SINGLA


SHRI TUSHAR K. BANDYOPADHYAY (Alternate)

Indian Oil Corporation Limited (IOCL), New Delhi SHRI SUMIT BASU
SHRI RAJA PODDAR (Alternate)

Indian Sugar Mills Association (ISMA), New Delhi SHRI G. K THAKUR


SHRI PANKAJ RASTOGI (Alternate)

Inspection Syndicate of India Pvt Ltd, Kolkata SHRI A. K. BASU


SHRI ARNAB BASU (Alternate)

Lamifabs & Papers (P) Ltd, Aurangabad SHRI KAMLESH DHOOT


SHRI KISHORI LAL (Alternate)

Lohia Corp Ltd, Kanpur DR UPENDER KRISHEN SAROOP


SHRI RAJEEV KUMAR DWIVEDI (Alternate)

Mangalore Refinery and Petrochemicals Limited, Mangaluru SHRI NILANJAN GUHA


SHRI NARATTAM CHAKRABORTY (Alternate)

Ministry of Consumer Affairs, Food & Public Distribution, SHRI ASHOK KUMAR
New Delhi DR SUBHASH GUPTA (Alternate)

Ministry of Environment, Forest and Climate Change DR SATYENDRA KUMAR


(MoEF&CC), New Delhi DR BHAWNA SINGH (Alternate)

National Federation of Cooperative Sugar Factories Ltd SHRI K. MURALIDHAR CHOWDARY


(NFCSF), New Delhi SHRI K. V. NAGARAJA SETTY (Alternate)

Nayara Energy Limited, Mumbai SHRI TUSHAR DONGRE

Office of the Textile Commissioner, Mumbai SHRI N. K. GUPTA


SHRI C. R. KALESAN (Alternate)

Plastindia Foundation, Mumbai SHRI SURENDER CHOUDHARY


DR E. SUNDARESAN (Alternate)

Rashtriya Chemical and Fertilizers Limited, Mumbai SHRI KAUSTUBH KOKANE


SHRIMATI DIPALI TAMMEWAR (Alternate)

Reliance Industries Limited (RIL), Mumbai SHRI RAJU VENKAT


SHRI V. RAVIKANTH (Alternate)

Texel Industries Ltd, Kalol SHRI SHAILESH R. MEHTA


SHRI VINAY TRIPATHI (Alternate)

The Fertilizer Association of India (FAI), New Delhi DR D. S. YADAV


DR NARESH PRASAD (Alternate)

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Organization Representative(s)

Ultratech Cement Limited, Mumbai DR AWADHESH K. SINGH


SHRI SANDEEP

VCPL, Vadodara SHRI V. SREENIVASAN


SHRI G. M. PATEL (Alternate)

Windmoller & Holscher India Pvt Ltd, New Delhi SHRI ANUJ SAHNI
SHRI SAURABH KUMAR SHARMA (Alternate)

BIS Directorate General SHRI J. K. GUPTA, SCIENTIST ‘E’/DIRECTOR AND


HEAD (TEXTILES) [REPRESENTING DIRECTOR
GENERAL (Ex-officio)]

Member Secretary
SHRI ASHWANI KUMAR
SCIENTIST ‘B’/ASSISTANT DIRECTOR
(TEXTILES), BIS

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Bureau of Indian Standards

BIS is a statutory institution established under the Bureau of Indian Standards Act, 2016 to promote harmonious
development of the activities of standardization, marking and quality certification of goods and attending to
connected matters in the country.

Copyright

BIS has the copyright of all its publications. No part of these publications may be reproduced in any form without
the prior permission in writing of BIS. This does not preclude the free use, in the course of implementing the
standard, of necessary details, such as symbols and sizes, type or grade designations. Enquiries relating to
copyright be addressed to the Head (Publication & Sales), BIS.

Review of Indian Standards

Amendments are issued to standards as the need arises on the basis of comments. Standards are also reviewed
periodically; a standard along with amendments is reaffirmed when such review indicates that no changes are
needed; if the review indicates that changes are needed, it is taken up for revision. Users of Indian Standards
should ascertain that they are in possession of the latest amendments or edition by referring to the website-
www.bis.gov.in or www.standardsbis.in.
This Indian Standard has been developed from Doc No.: TXD 23 (21629).

Amendments Issued Since Publication


Amend No. Date of Issue Text Affected

BUREAU OF INDIAN STANDARDS


Headquarters:
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Published by BIS, New Delhi

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