www.perkinelmer.

com/supplies

Chromatography
Consumables and Supplies
Genuine PerkinElmer Products — Genuine Value

VOLUME 3 2008 – 2009 PerkinElmer—The Clear Choice in Chromatography

NEW PROMOTIONS NEW! SERIES 275 HRES LC

SAVE up to 20% Hydrogen Generators!

on all Brownlee Cartridge and The newest membrane
Conventional Columns! technology for safe
production of pure
See pages 10-19 for details.
hydrogen gas.

Portable Gas Leak Detector!

See page 56
Compact handheld detector for details.

with audible alarm.

See page 36 for details.
SAVE up to 25%
on Elite Series
Capillary Columns!
SAVE up to 25% See page 43 for details.

on Crimp Top
Headspace Vials!
See page 51 for details.

AU 1800033391 IN912225701101
KR 8228685350 SG 6567799555
ordering information

Genuine PerkinElmer Ordering Information

Products – Genuine Value Order Online
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2 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

 table of contents
Table of Contents
Liquid Chromatography
Rewards
Programs NEW Series 275 HRes LC System . . . . . . . . . . . . . . . . . 4–7

See page 55 for details. NEW Series 225 Autosampler and Accessories. . . . . . 8–9 6

DELIVERING enhanced VALUE Conventional Columns . . . . . . . . . . . . . . . . . . . . . . . 10–13

and outstanding SAVINGS on
Cartridge Columns . . . . . . . . . . . . . . . . . . . . . . . . . . 14–19
the products you use most!
Sample Loops Tubing . . . . . . . . . . . . . . . . . . . . . . . . . . . 20
Volume Purchase Program
Take advantage of the PerkinElmer® Volume Fingertight® Fittings . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
14
Purchase Agreement (VPA)
■ Our consumables and supplies business HPLC Pump Accessories. . . . . . . . . . . . . . . . . . . . . . 22–23
program is designed to help you reduce your
administrative and operating costs, while Flow Cells . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
earning your company volume based
discounts on the products you use every day Autosampler Supplies. . . . . . . . . . . . . . . . . . . . . . . . . . . 26
Standing Order Discount 20
Detector Lamps . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
For single orders with multiple scheduled shipments,
PerkinElmer offers an incremental 10% discount.

University Program Discount Gas Chromatography

PerkinElmer offers a 10% University discount on
consumables and supplies. Clarus 600 GC and GC/MS . . . . . . . . . . . . . . . . . . . . 30–31
27
GC Organic Standards. . . . . . . . . . . . . . . . . . . . . . . . 32–33

Save 20% Filters. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 34–35

Leak Detector and IR Temperature Gun. . . . . . . . . . . . . 36

on Consumables
Ferrules, Syringes and Liners. . . . . . . . . . . . . . . . . . 37–39 32
and Supplies
Vials, Caps and Septa . . . . . . . . . . . . . . . . . . . . . . . . 40–41
when purchased with
an Instrument!* Elite Series Capillary Columns . . . . . . . . . . . . . . . . . 42–44
* Consumables order must be placed within 60 days of new instrument
installation or may be included on instrument order. Some supplies Applications Kits . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45
must be included on instrument order. Ask your sales representative
for details.
Applicate Note – OVIs in Pharma . . . . . . . . . . . . . . . 46–47 38

Headspace Vials and Caps . . . . . . . . . . . . . . . . . . . . 48–51

Series 275 Packed Traps . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52

HRes ™ LC System Air Monitoring . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53
49
Expand your Separation Thermal Desorption. . . . . . . . . . . . . . . . . . . . . . . . . . 54–55
Capability while
Generators . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 56–57
Increasing Throughput
Improved resolution and throughput with
higher pressure operating range to 10,000 psi. EcoAnalytix
55
See pages 4-7 for more information.
EcoAnalytix . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58–59

See page 2 for a complete listing of local offices and for ordering information. 3
New Series 275 HRes™ LC System from

Expand your Separation

Capability while increasing throughput

Preconfigured Series 275 HRes System

Part No.
N2980935

Includes:
Series 275 Autosampler with Peltier cooling/heating option, Vacuum Degasser, Series
275 Binary Micro Pumps, Series 200 Column Oven, and Series 200 UV/Vis Detector
with high efficiency 2.4 μL flow cell and dotLink interface. Communication Cables, Static
Mixer and all Low Dead-volume Fittings, Pre-cut Tubing and connections necessary to
configure system included. TotalChrom Software and HRes columns sold separately.

Preconfigured Series 275 HRes System

Isn’t it time you considered HRes™ Fast-LC to expand your
Part No.
separation capabilities while increasing your sample throughput?
The flexible PerkinElmer Series 275 HRes™ LC System leverages N2980915
small particle-size column technology at ultra-high pressures, Includes:
giving you greater flexibility to develop methods across a wider
Series 275 Autosampler, Vacuum Degasser, Series 275 Binary Micro Pumps, Series 200
operating range. Column Oven, and Series 200 UV/Vis Detector with high efficiency 2.4 μL flow cell and
dotLink interface. Communication Cables, Static Mixer and all Low Dead-volume Fittings,
The Series 275 HRes HPLC System: Pre-cut Tubing and connections necessary to configure system included. TotalChrom
Software and HRes columns sold separately.
Versatile flexibility to expand your
separation capabilities Series 275 HRes Micro Binary Pump Package
Improve your efficiency, easily. The Series 275 HRes LC System Part No.
enables today’s LC laboratories to achieve higher levels of
performance and throughput to meet escalating scientific and business N2910601
challenges. Your lab is on the line to do it better, and do it faster.
Whether you are evaluating candidate compounds, controlling product Includes:
quality, assuring consumer safety or assessing environmental impact, Series 275 Binary Micro Pumps, High Pressure Static Mixer, and all necessary Pre-cut
the Series 275 HRes System has the power and the flexibility to 0.007”-i.d. SS Tubing to connect pump package to an injection valve. Ideal as a
accelerate your productivity. front-end to a mass spec. TotalChrom Software and HRes columns sold separately.

4 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

PerkinElmer

Features and Benefits Preconfigured Integrated System

■ Greater operating flexibility to optimize method development Flexible Enough for HRes Fast-LC
■ Improved resolution and throughput with higher pressure
operating range (500-10,000 psi) and Conventional Applications
■ Outstanding linearity and repeatability even at small injection Even though your method development options are greatly increased
volumes and high operating pressures with the Series 275 HRes System, you don’t have to convert your
■ “Best-in-class” cycle time with exceptionally low carry-over valuable tried-and-true methods developed over all these years. Our
drives increased throughput Brownlee™ HRes LC columns, available in a wide variety of stationary
■ Extremely low dispersion for maximum resolving power and phases and dimensions, can be operated over a wide range of flow
peak capacity rates and operating pressures. This allows you to select the throughput
and resolution best suited for your specific application needs.
■ High speed data capture assures excellent peak fidelity at
high sample throughput The flexibility of the Series 275 HRes System allows you to run all your
■ 21 CFR Part 11 architecture allows operation in a regulated HRes and your existing conventional methods on a single LC system!
environment

See page 2 for a complete listing of local offices and for ordering information. 5
series 275 LC autosampler and accessories

Expanded
Capabilities with
high throughput
performance

Brownlee Columns for HRes™ Fast-LC

Recent developments in LC column technology have now made the
use of sub 3 μm particle packing materials practical. These smaller
particle size materials allow higher mobile phase linear velocities to be
used, without the decrease in separation efficiency experienced with
conventional larger particle size packings. This translates into higher
throughput and higher productivity. To conserve mobile phase, these
Series 275 Autosampler sub 3 μm column materials are typically packed into 2.1 mm i.d.
The NEW Series 275 Autosampler sets the bar for automated, high columns so that flow rates (mobile phase volume) are kept low.
throughput Fast-LC sample management. However, smaller sized packings result in elevated operating pressures.
Technological advances in pump and injector designs have also kept
Features and Benefits pace, and these columns can be used at pressures as high as 10,000
psi with the PerkinElmer Series 275 HRes LC Systems.
■ High pressure operation: Designed and tested to 15,000 psi (1,034
bar) – capable of HRes Fast-LC and conventional applications The rugged construction of this new line of small particle columns for
■ Multiple Injection Modes: Supports full loop and partial fill injection high pressure application yield excellent longevity and reproducibility.
modes, and new microliter pickup mode for efficient injection as low These packings exhibit an exceptionally tight particle size distribution
as 1 μL without sample waste for excellent resolving power and are packed at elevated pressures
to assure column stability even at high pressure applications. Each
■ Short Cycle Times: Best-in-class sample throughput with a cycle column is tested to ensure the highest level of quality and efficiency in
time of 8 seconds in partial fill mode
high pressure LC testing.
■ Low Carryover: Low cross contamination typically ≤0.01% (using
caffeine). Best-in-class at protecting against cross contamination
■ Exceptional Injection Repeatability: Typically <0.3% RSD Features and Benefits
■ Available with Peltier Cooling/Heating: Exceptional cooling ■ Sub 3 μm particle technology and 2.1 μm i.d. for higher
capacity allows the air temperature in the sample compartment separation efficiency
to reach 4 °C ± 2 °C, even when the ambient temperature of lab ■ Packed to withstand higher operating pressures
is as high as 25 °C. Heating and cooling options also available as
field upgrades ■ Wide choice of stationary phases
■ Automated Derivatization, Standard Additions and Serial Dilution
functions: Automated sample preparation for unattended operation Particle
Description Length i.d. Size Part No.
Brownlee HRes Biphenyl 50 mm 2.1 mm 1.9 μm N9303912
Autosamplers and Upgrade Kits Brownlee HRes Biphenyl 100 mm 2.1 mm 1.9 μm N9303913
Brownlee HRes PFP Propyl 30 mm 2.1 mm 1.9 μm N9303914
Series 275 Autosamplers Brownlee HRes PFP Propyl 50 mm 2.1 mm 1.9 μm N9303915
Description Part No. Brownlee HRes PFP Propyl 100 mm 2.1 mm 1.9 μm N9303916
Brownlee HRes Aqueous C18 30 mm 2.1 mm 1.9 μm N9303917
Series 275 Autosampler (standard) N2930653 Brownlee HRes Aqueous C18 50 mm 2.1 mm 1.9 μm N9303918
Series 275 Autosampler with cool/heat N2930655 Brownlee HRes Aqueous C18 100 mm 2.1 mm 1.9 μm N9303919
Brownlee HRes IBD 30 mm 2.1 mm 1.9 μm N9303920
Series 275 Autosamplers Upgrade Kits Brownlee HRes IBD 50 mm 2.1 mm 1.9 μm N9303921
Description Part No. Brownlee HRes IBD 100 mm 2.1 mm 1.9 μm N9303922
Series 275 Autosampler Upgrade Kit N2930672 Brownlee Analytical 30 mm 2.1 mm 1.9 μm N9303852
(from standard to cooling) Brownlee Analytical 50 mm 2.1 mm 1.9 μm N9303853
Series 275 Autosampler Upgrade Kit N2930673 Brownlee Analytical 100 mm 2.1 mm 1.9 μm N9303854
(from standard to cool/heat)
Series 275 Autosampler Upgrade Kit N2930669
(from cool to cool/heat)

6 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

 Series 275 HRes Flowcell
HRes™ LC System
Series 275 HRes Flowcell Accessories
This 2.4 μL flowcell with 0.005" ID tubing connections is ideally suited for
the Series 275 HRes systems, requiring the absolute lowest dispersion
with exceptional performance.
High Pressure Static Mixers
Description Part No.
Static Mixers are important in facilitating complete mobile phase
S275 HRes Flowcell assembly, 2.4 μL 6 mm path length, N2920070 blending, resulting in improved retention performance. These mixers
w/fittings should be used as part of a Series 275 binary pump system, where
high pressure blending of the two pump outputs required. Mixers
incorporate a highly efficient cross-flow shearing mechanism which
produces vortex sheer mixing over a wide range of volumes. They
Syringes and Kits are now offered in both 6,000 and 15,000 psi pressure max flavors
PerkinElmer syringe kits for high pressure applications are manufactured and should be the same as or no less than half the flow rate volume.
for precise liquid delivery. All of these glass syringes come with precision For example, when pumping at a 0.5 mL/min flow rate, a 500 μL mixer
stainless steel plungers. They are used for sampling and flushing and are is ideally suited.
available in a large variety of sizes. The 250 μL syringe comes standard
with both the Series 225 and Series 275 Autosamplers.
Interferene
High Pressure
Check
Static
Standards
Mixers
Interferene
Syringe KitsCheck Standards Description Part No.
50 μL In-Line High Pressure Mixer Assembly, SS N2911200
Description Part No. 150 μL In-Line High Pressure Mixer Assembly, SS N2911201
100 μL w/200 μL Buffer Tubing N2936051 250 μL In-Line High Pressure Mixer Assembly, SS N2911202
250 μL w/500 μL Buffer Tubing N2936052 350 μL In-Line High Pressure Mixer Assembly, SS N2911205
500 μL w/1,000 μL Buffer Tubing N2936053 500 μL In-Line High Pressure Mixer Assembly, SS N2911203
1000 μL w/2,000 μL Buffer Tubing N2936054
2500 μL w/2,000 μL Buffer Tubing N2936055

Interferene
Binary Mixing-T
CheckMixers
Standards
Interferene Check Standards
Syringes Description Part No.
150 μL HP Binary High Pressure Mixing-T, SS N2911206
Description Part No. 10 μL Binary Mixing-T, SS N2911170
Sample Needle w/fittings N2936009
Air Guide Needle (62 mm) N2936000
Bio Compatible Sample Needle w/tubing Connector N2936010
High Pressure Stainless Steel
Sample Loops
Solvent and Sample Filtration The high integrity 3/16 stainless steel loops are ideal for both High Pressure
and general LC applications and ferrules come in a full range of sizes.
Syringe filters are important for high pressure applications of effectively
filter samples to prevent premature column performance loss and These loops are required for the Series 275 Autosampler, especially for
possible flow restriction of the narrow tubing that is typically required applications requiring ≥ 6,000 psi back pressure.
for high pressure LC applications.

Interferene
High Pressure
Check
Static
Standards
Mixers
Interferene
Syringe Filters
Check Standards
Description Part No.
Description Pore Size Part No.
2 μL Sample Loop, SS N2936071
PVDR 13 mm Filter (pkg. 100) 0.45 μm 02542783 5 μL Sample Loop, SS N2936056
PTFE 13 mm Filter (pkg. 100) 0.45 μm 02542782 10 μL Sample Loop, SS N2936057
20 μL Sample Loop, SS N2936058
Nylon 17 mm Filter (pkg. 100) 0.45 μm 02542880 50 μL Sample Loop, SS N2936059
Nylon 17 mm Filter (pkg. 100) 0.20 μm 02542881 100 μL Sample Loop, SS N2936060
Nylon 30 mm Filter (pkg. 100) 0.45 μm 02542882 200 μL Sample Loop, SS N2936061
Nylon 30 mm Filter (pkg. 100) 0.20 μm 02542883 500 μL Sample Loop, SS N2936062
PTFE 17 mm Filter (pkg. 100) 0.20 μm 02542884 1 mL Sample Loop, SS N2936063
2 mL Sample Loop, SS N2936064
PTFE 30 mm Filter (pkg. 100) 0.45 μm 02542885 5 mL Sample Loop, SS N2936065
PTFE 30 mm Filter (pkg. 100) 0.20 μm 02542886

See page 2 for a complete listing of local offices and for ordering information. 7
Series 225 LC Autosampler and

Performance beyond
Expectations – always

Features and Benefits

■ Short Cycle Times: Best-in-class sample throughput with a cycle
time of 8 seconds in partial fill mode
■ Low Carryover: Low cross contamination typically ≤0.01%.
Best-in-class at protecting against cross contamination
■ Multiple Injection Modes: Supports full loop and partial fill injection
modes, and new microliter pickup mode for efficient injection as low
as 1μL without sample waste
■ Exceptional Injection Repeatability: Typically <0.3% RSD
■ Available with Peltier Cooling/Heating tray compartment:
Exceptional cooling capacity allows the air temperature in the
sample compartment to reach 4 °C ± 2 °C, even when the ambient
temperature of lab is as high as 25 °C. Heating option allows tray to
reach 40 °C
■ Automated Derivatization, Standard Additions and Serial Dilution
functions: Automated sample preparation for unattended operation

Upgrade Kits and Trays

Series 225/275 Autosamplers Upgrade Kits
Description Part No.
Series 225 Autosampler Upgrade Kit N2930672
The Series 225 LC Autosampler (from standard to cooling)
The Series 225 LC Autosampler sets the bar for speed and Series 225 Autosampler Upgrade Kit N2930673
performance. A new member of the Series 200 family of liquid (from standard to cool/heat)
chromatography (LC) products, it is the ultimate sampling tool Series 225 Autosampler Upgrade Kit N2930669
designed to address your growing need for automation, quantitation (from cool to cool/heat)
and throughput. It automates key operations with built-in derivatization
and dilution, as well as automatic internal standard addition and Series 225/275 Autosampler Trays
micro-volume pick-up. With best-in-class cycle time and protection Description Part No.
against cross contamination, the Series 225 LC Autosampler is 25-Position 6 mL Vial Sample Tray N2936045
compatible with a wide range of temperature-controlled trays for 80-Position 2 mL Vial plus (5) 6 mL Vial Tray N2936046
a variety of applications and is designed for easy serviceability (for derivatization)
and maintenance. 80-Position 2 mL Vial Tray with Dilution Tray N2930676
96-well Microtiter N9302562
96-well ‘Deep-well’ Microtiter N9302560
Series 225 Autosamplers 96-well 7 mm Pre-slit Silicone Plate Mat/Seal N9302555
Description Part No. 96-well ‘Shallow’ Microtiter Plate Adaptor N2936048
Series 225 Autosampler (standard) N2930650 (supports dual microtiter plates)
Series 225 Autosampler with Peltier Cooling Option N2930651 96-well ‘Deep’ Microtiter Plate Adaptor N2936049
(supports dual microtiter plates)
100-Position 2 mL Vial Sample Tray N2936042
(200) 0.2 mL Microvial plus (5) 2 mL Vial Tray N2936043

8 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

Accessories

0.2 mL Micro Vials, Caps, and Septa 2.0 mL Vials, Caps and Septa
Description Part No. PerkinElmer Autosampler Vials are guaranteed for fit and compatibility with the
Series 200 Autosampler. Both vials and caps are totally inert to samples ordinarily
Caps/Septa analyzed by Liquid Chromatography.
Polyethylene Press-on Cross-slit Cap for 8 mm o.d. Vials N9302141
(pkg. 1,000) Crimp-on Caps
Aluminum Crimp-top Cap with Teflon-lined Butyl 03300806 Description Size Part No.
Rubber Septa for 8 mm Vials (pkg. 1,000) Crimp Green (pkg. 100) 11 mm N9302684
Crimp Top Vials Aluminum cap with Teflon®/rubber
Glass MicroVials, Tapered, 0.2 mL, 8 mm o.d. Top N9302136 Crimp Red (pkg. 100) 11 mm N9302685
(pkg. 500) Aluminum cap with Teflon/rubber
Crimp Blue (pkg. 100) 11 mm N9302686
Autosampler Vial Sleeve Aluminum cap with Teflon/rubber
Glass N9307027 Crimp Silver (pkg. 100) 11 mm N9306015
Micro Vial Kit Aluminum cap with Teflon/rubber
Polyethylene N9306080
Includes 300 μL tapered vial, blue Crimp Top Vials
polypropylene cap with bonded Type 1 borosilicate standard glass vials, 2.0 mL, 11 mm o.d. top.
silicone/PTFE septa. (pkg. 500)
Description Size Part No.
Amber Glass Vials (pkg. 100) 11 mm N9302680
Clear Glass Vials (pkg. 100) 11 mm N9301385

6 mL Vials and Caps Screw Top Vials and Caps – Wide Mouth
Description Part No. Type 1 borosilicate standard glass vials, 2.0 mL, 12 x 32 mm.
Caps/Septa Description Size Part No.
Polyethylene Press-on Slit Cap for 20 mm o.d. Vials N2936083 Amber Glass Vials (pkg. 100) 12 mm N9306057
(pkg. 25) Clear Glass Vials (pkg. 100) 12 mm N9306053
Crimp Top Vials Screw-top Vial Caps, black (pkg. 100) 10 mm N9306052
Polypropylene with PTFE/slit
Glass Large-volume Vials, 6.0 mL, 20 mm o.d. Top N9302134
white silicone
(pkg. 125)

Compatibility Table for Vials and Caps in Sample Trays

Series 225/275 Autosamplers
Tray Vials Caps
Volume Series 225/275 Tray Part No. Part No. Part No.
0.2 mL* 205-Position (200 micro vial sample plus 5 calibration vial tray) N2936043 N9302136 N9302141
03300806
2.0 mL - Crimp Top 80-Position (80-Position Sample Tray plus tank, for serial dilution) N2936047 N9302680 N9302684
85-Position (80-Position 2 mL vial sample plus 5 reagent vial tray, for derivatization) N2936046 N9301385 N9302685
100-Position N2936042 N9302686
205-Position (200 micro vial sample plus 5 calibration vial tray) N2936043 N9306015
2.0 mL - Screw Top 80-Position (80-Position Sample Tray plus tank, for serial dilution) N2936047 N9306053 N9306052
85-Position (80-Position 2 mL vial sample plus 5 reagent vial tray, for derivatization) N2936046 N9306057
100-Position N2936042
205-Position (200 micro vial sample plus 5 calibration vial tray) N2936043
6.0 mL - Snap Top 25-Position N2936045 N9302134 N2936083
85-Position (80-Position 2 mL vial sample plus 5 reagent vial tray, for derivatization) N2936046

See page 2 for a complete listing of local offices and for ordering information. 9
 Brownlee Conventional Columns from

Which Column Do I Need? Brownlee Bio

Brownlee Analytical Brownlee pH-ex C18 Wide-pore silica that is excellent for peptide and protein separation.
Brownlee Aquapore® Brownlee Spheri-5® Columns are available in 5 μ, and lengths ranging from 30–250 mm,
in 2.1 mm and 4.6 mm i.d.
Brownlee Bio Brownlee Validated™
Brownlee CHOICE™
Brownlee CHOICE ™
This line of columns is made of 60 Å silica which results in large
Having the right stationary phase for your separation is the first
surface area, high carbon loads and high retention compounds.
step in selecting the appropriate column. This should be based Columns are available in 3 or 5 μ, and lengths ranging from
on sample solubility and on chemical differences among the 30–250 mm, in 2.1 mm and 4.6 mm i.d.
sample compounds.
Depending on the mode of separation you will use, PerkinElmer Brownlee pH-ex C18
has the right column for you. In reversed-phase separations, the
Brownlee pH-ex C18, HPLC columns utilize a patented polycarbosilane
mobile phase is more polar than the stationary phase. Sample barrier layer that protects the silica particles from extremely basic
hydrophobicity also is a major determinant of the separation conditions. This layer uses multiple attachment points to the silica
mode. In reversed-phase separations, the mobile phase is more particle which yields a modified surface with enhanced stability.
polar than the stationary phase, which is traditionally a straight A second layer is then attached, providing the functional group (C18).
alkyl chain, most often C18. Using this approach to shield the silica surface, a highly durable
stationary phase is created. These columns are designed to be used in
The majority of HPLC analyses are performed in reversed-phase a pH range of 1–12 and have shown no loss of efficiency after 50 hours
mode, due to the fact that the analytes of interest can be in a pH of 12 at 60 °C.
dissolved in water, or mixtures of water and a polar organic
solvent such as methanol or acetonitrile.
Brownlee Spheri-5 ®
In normal phase separations, the mobile phase is less polar This is small-pore silica-based sorbent for separating small molecules.
than the stationary phase. Cyano phases are commonly used Both monofunctional (comb-pre) and polyfunctional (polymerized
in either reversed-phase or normal-phase mode. A stationary loop-type) C8 and C18 sorbents available.
phase incorporating both polar and nonpolar functionality can
be used in either reversed-phase or normal-phase mode. Brownlee Validated ™
These columns are made on high-purity Type B silica with inherent low
Brownlee Analytical silanophilic activity. They exhibit excellent peak shape for a wide range
PerkinElmer’s all-purpose HPLC column line for conventional as well as of compounds, while also having a wide number of phases. Columns
high-speed LC separations. The Brownlee Analytical family is available are available in 3 or 5 μ, and lengths ranging from 30–250 mm, in
in 3 or 5 μ, and lengths ranging from 30–250 mm, in 2.1 mm and 2.1 mm or 4.6 mm i.d.
4.6 mm i.d.

Brownlee Aquapore ® For a full listing of Brownlee

This is a wide-pore silica-based support suitable for the separation of conventional columns, please visit:
large biopolymers. www.perkinelmer.com/lcsupplies

Save up to 20%
on your next Brownlee Cartridge
or Conventional Columns order!*
To qualify, use promotion code: LCBLC408
Save 15% when you buy any 2 Brownlee Cartridge or Conventional Columns!
Save 20% when you buy any 3 Brownlee Cartridge or Conventional Columns!
*Use of the LCBLC408 promotion code is required to receive your discount. Discount cannot be combined with volume purchase agreement discounts, university program discounts,
standing order discounts or other contract pricing. Discounts cannot be combined with promotion available at time of instrument purchase. Offer expires 3/31/09.

10 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

PerkinElmer

Brownlee Columns
Choose only genuine PerkinElmer BrownleeTM columns
for the best separation results. Six different column
types to meet all your analytical needs.

Features and Benefits

■ Each column individually tested and certificate provided
■ End fittings compatible with a variety of HPLC systems
■ Do not require MPLC holders

Conventional columns do not require MPLC holders.

Conventional Columns
Column Functionality Pore Diameter Å % Carbon End Cap Applications
Analytical Amino 110 2 No Excellent for carbohydrate analysis
Analytical C18 & C8 110 13 Yes Superior for non-basic analytes
Analytical Cyano 110 4 Yes General purpose for normal or reversed-phase
Analytical Biphenyl 110 – Yes U.S. EPA Method 8330
Analytical Phenyl 110 6 Yes General purpose for neutral analytes
Analytical Silica 110 – – Ideal for polar analytes
Analytical PAH 110 – Yes Maximum resolution of polynuclear aromatic hydrocarbons
Aquapore® AX-300 300 – – Used for ion exchange chromatography
Aquapore Octyl C8 300 – – Used for reversed-phase chromatography
Aquapore ODS C18 300 – – Silica based support used for the separation of large biopolymers
Bio C18 300 6 Yes High molecular weight compounds and proteins
Bio C8 300 – – High molecular weight compounds and proteins
CHOICE™ Basix 60 12 Yes Ideal for LC/MS. Excellent for amine-containing compounds
and basic pharmaceuticals
CHOICE C18 60 27 Yes Excellent for explosives or steroids
CHOICE Biphenyl 60 23 Yes Highly retentive and selective phase for aromatic compounds
CHOICE Organic acids 60 – No Used for challenging organic acids
CHOICE PFP propyl 60 17 Yes Ideal for MS, ELSD, or NPD detection of nucleosides, nucleotides,
purines, pyrimidines or halogenated compounds
Spheri-5® C8, C18, C18 ODS and Silica 80 – – Excellent for separating small molecules both
non-functional and polyfunctional
Validated™ Amino 100 2 No Ideal for carbohydrates
Validated C1 100 5 – Least retentive reversed-phase hydrocarbon packing
Validated C4 100 9 Yes High bonding coverage and base deactivation
Validated Aqueous C18 100 15 No Excellent for highly water-soluble or poorly organic-soluble compounds
Validated C18 100 20 Yes Used for the detection of anilines, barbiturates, carbonyls, fat-soluble
vitamins, fatty acids, glycerides, phthalates
Validated C8 100 12 Yes Less hydrophobic retention than C18
Validated Carbamate 100 – – Fast analysis of carbamates
Validated Cyano 100 8 Yes Basic pharmaceuticals and steroids
Validated IBD 100 12 No Unique separation for acids, bases, zwitterions and other polar compounds
Validated PFP 100 7 Yes Ideal for taxors and precursors or halogenated compounds
Validated Phenyl 100 10 Yes Separation of fatty acids, polynuclear aromatic hydrocarbons,
purines and pyrimidines
Validated Quat 100 – – High purity, base deactivated reversed-phase packing

See page 2 for a complete listing of local offices and for ordering information. 11
 Conventional Columns for all HPLC

Extensive column selection

meets all your analytical needs

Brownlee Analytical pH Range: 2.5 to 7.5 Brownlee Bio pH Range: 2.5 to 7.5

Particle Temp. Pore Carb. End Particle Temp. Pore Carb. End
Length i.d. Size Limit Size Load Cap Part No. Length i.d. Size Limit Size Load Cap Part No.
Brownlee Analytical Amino Brownlee Bio C8
Ideal for mono and disaccharide analyses. Most popular amino-based stationary Wide-bore HPLC column. High proportion of pore/surface
phase. Routine analysis of simple sugars, using isocratic elution and a refractive area available for large molecule separations.
index detector or an evaporative light scattering detector. 150 mm 2.1 mm 5 μm 300 Å 6% Yes N9303658
100 mm 4.6 mm 5 μm 80 °C 110 Å 2% No N9303503 150 mm 4.6 mm 5 μm 300 Å 6% Yes N9303659
150 mm 4.6 mm 5 μm 80 °C 110 Å 2% No N9303504
Brownlee Bio C18
Brownlee Analytical C8 Excellent for separating peptides or proteins. Wide-pore HPLC column.
Shorter retention times for hydrophobic compounds. Reliable performance 150 mm 2.1 mm 5 μm 300 Å 5% Yes N9303648
with symmetrical peak shapes for neutral to acidic compounds. 150 mm 4.6 mm 5 μm 300 Å 6% Yes N9303649
100 mm 4.6 mm 5 μm 80 °C 110 Å 7% Yes N9303515
150 mm 4.6 mm 5 μm 80 °C 110 Å 7% Yes N9303517

Brownlee Analytical C18

Suitable for a wide range of acidic to neutral hydrophobic compounds. Brownlee Choice pH Range: 2.5 to 7.5
Excellent all purpose column.
Particle Temp. Pore Carb. End
100 mm 4.6 mm 3 μm 80 °C 110 Å 13% Yes N9303507
Length i.d. Size Limit Size Load Cap Part No.
100 mm 4.6 mm 5 μm 80 °C 110 Å 13% Yes N9303512
150 mm 4.6 mm 5 μm 80 °C 110 Å 13% Yes N9303513 Brownlee CHOICE Basix
Excellent choice for analytes containing amine group functionality.
Brownlee Analytical Cyano
150 mm 4.6 mm 5 μm 80 °C 60 Å 12% Yes N9303618
Suitable for analyses of a wide range of compounds from acidic through
slightly basic. Highly-base-deactivated spherical silica. Brownlee CHOICE C18
150 mm 4.6 mm 5 μm 80 °C 110 Å 4% Yes N9303522 Excellent choice for LC/MS. Highly retentive phase
for hydrophobic and slightly polar analytes.
Brownlee Analytical PAH
100 mm 4.6 mm 3 μm 80 °C 60 Å 27% Yes N9303621
Specifically designed for challenging analyses
150 mm 2.1 mm 5 μm 80 °C 60 Å 27% Yes N9303627
of polynuclear aromatic hydrocarbons.
150 mm 4.6 mm 5 μm 80 °C 60 Å 12% Yes N9303628
150 mm 3.2 mm 5 μm 80 °C 110 Å Yes N9303430
250 mm 2.1 mm 5 μm 80 °C 110 Å Yes N9303530 Brownlee CHOICE Organic Acids
Enhanced retention and selectivity for polar organic acids. Retention is stable and
Brownlee Analytical Phenyl reproducible even with 100% aqueous mobile phase specified in the AOAC method.
Unique selectivity especially for aromatic compounds.
150 mm 4.6 mm 5 μm 80 °C 60 Å N9303631
150 mm 4.6 mm 5 μm 80 °C 110 Å 6% Yes N9303524 250 mm 2.1 mm 5 μm 80 °C 60 Å N9303632
Brownlee Analytical Silica Brownlee CHOICE Propyl
Good general purpose packing for normal phase separations. Highly retentive for basic analytes. Excellent separation of nucleosides,
150 mm 4.6 mm 5 μm 80 °C 110 Å Yes N9303525 nucleotides, purines, pyrimidines, halogenated compounds, beta blockers
and tricyclic antidepressants.
150 mm 4.6 mm 5 μm 80 °C 60 Å 17% Yes N9303644

For a full listing of Brownlee

conventional columns, please visit:
www.perkinelmer.com/lcsupplies

12 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

Instruments
Brownlee Spheri-5® pH Range: 2.5 to 7.5
Brownlee Validated pH Range: 2.5 to 7.5
Particle Temp. Pore Carb. End
Particle Temp. Pore Carb. End Length i.d. Size Limit Size Load Cap Part No.
Length i.d. Size Limit Size Load Cap Part No.
Brownlee Spheri-5 C8
Brownlee Validated Amino Small pore silica-based sorbent for separating small
Good for normal phase analytes of mono-and disaccharides or similar compounds. molecules both non-functional and polyfunctional.
150 mm 4.6 mm 5 μm 80 °C 100 Å 2% N9303534 250 mm 4.6 mm 5 μm 07120012

Brownlee Validated Aqueous C18 Brownlee Spheri-5 C18

Highly base deactivated. Compatible with highly aqueous mobile phases. Small pore silica-based sorbent for separating small
150 mm 4.6 mm 5 μm 80 °C 100 Å 15% N9303546 molecules both non-functional and polyfunctional.
250 mm 4.6 mm 10 μm 07120001
Brownlee Validated C1
Least retentive reversed phase hydrocarbon packing.
150 mm 4.6 mm 5 μm 80 °C 100 Å 5% N9303718
pH Range:
Brownlee Validated C4 Brownlee pH-ex C18 1.0 to 12.0
High bonding coverage and base deactivation. Especially useful for applications requiring high/low pH
Less retention that C18 or C8 phases. ranges (1–12). A silica based C18 column with exceptional stability.
150 mm 4.6 mm 5 μm 80 °C 100 Å 9% Yes N9303720 Particle Temp. Pore Carb. End
Length i.d. Size Limit Size Load Cap Part No.
Brownlee Validated C8
Retentive, high purity-base deactivated reversed phase packing. 30 mm 4.6 mm 3 μm 80 °C 140 Å N9303855
50 mm 4.6 mm 3 μm 80 °C 140 Å N9303856
150 mm 2.1 mm 5 μm 80 °C 80 Å 12% Yes N9303566 100 mm 4.6 mm 3 μm 80 °C 140 Å N9303857
150 mm 4.6 mm 5 μm 80 °C 80 Å 12% Yes N9303567 150 mm 4.6 mm 3 μm 80 °C 140 Å N9303858
Brownlee Validated C18
Excellent general purpose phase column. Retentive high purity packing.
150 mm 2.1 mm 5 μm 80 °C 100 Å 20% Yes N9303556
150 mm 4.6 mm 5 μm 80 °C 100 Å 20% Yes N9303558 Conventional Column Kits
Brownlee Validated Carbamate Particle Temp. Pore Carb. End
Length i.d. Size Limit Size Load Cap Part No.
A unique stationary phase specifically designed for carbamate analysis.
This column is compatible with fluorescence or LC/MS detection, and is Method Validation Column Kit
designed for fast analysis times, reducing solvent usage. Includes set of three identical Brownlee Validated C18 columns from different lots.
100 mm 4.6 mm 3 μm 80 °C 100 Å N9303569 Ideal to check robustness in the method validation process. Packing materials of
varying lot #’s.
Brownlee Validated Cyano 150 mm 4.6 mm 5 μm N9303950
High purity Cyano phase with few silanol sites. Less sensitive
to small amounts of water present in the mobile phase. C18 Lot Specific Column Kit
150 mm 4.6 mm 5 μm 80 °C 100 Å 10% Yes N9303575 Includes 3 Brownlee Validated C18 columns. Ideal tool for the R & D and Contract
Lab applications working on specific projects and studies. Identical lot# specific
Brownlee Validated IBD packing material guaranteed. Absolute minimal variability and one convenient kit
Unique selectivity and a high level of base-deactivation. for long-term use.
Reduces or eliminates the need for mobile phase additives. 150 mm 4.6 mm 5 μm N9303951
150 mm 4.6 mm 3 μm 80 °C 100 Å 12% N9303593
150 mm 4.6 mm 5 μm 80 °C 100 Å 12% N9303582

Brownlee Validated PFP

Unique selectivity for compounds containing organohalogens
or other basic functional groups.
Save up to 15% on
150 mm 4.6 mm 5 μm 80 °C 100 Å 7% Yes N9303599 Column Kits!*
Brownlee Validated Phenyl
To qualify, use promotion code: LCBLC408
High purity, highly retentive base-deactivated phase,
especially designed for aromatic analytes. *Use of the LCBLC408 promotion code is required to receive your discount. Discount
cannot be combined with volume purchase agreement discounts, university program
150 mm 4.6 mm 5 μm 80 °C 100 Å 10% Yes N9303606 discounts, standing order discounts or other contract pricing. Discounts cannot be
combined with promotion available at time of instrument purchase. Offer expires 3/31/09.

See page 2 for a complete listing of local offices and for ordering information. 13
 Brownlee Cartridge Columns for Quality

Brownlee Sorbents
PerkinElmer Brownlee™ cartridge columns are offered in a wide range of
sorbent material. Choose the right sorbent for the analysis and mode of
separation being used.

Aquapore® – is a wide-pore, silica-based support suitable for the

separation of large biopolymers.

Spheri-5® – is a small-pore, silica-based solvent for separating small

molecules. Both monofunctional (comb-type) and polyfunctional
(polymerized loop-type) C8 and C18 sorbents are available.

Polypore® – is a polymer-based (microporous, 10 μm) sorbent for the

analysis of organic acids and sugars.

Validated™ – is a small-pore, silica-based C18 sorbent for small

molecules, specifically for consistent pharmaceutical assays.

Pecosphere™ – is a small-pore, silica-based sorbent for HPLC

of small molecules.

Reduced Activity – is a small-pore, base deactivated silica-based,

reversed-phase sorbent (C18 or C8) developed for HPLC of basic
analytes and pharmaceuticals.

CHOICE™ – is a small-pore, base deactivated silica-based,

reversed-phase sorbent (C18) developed for LC/MS separations.

Peco HCODS – is especially suited for reversed-phase separation of

proteins and peptides.

Brownlee Cartridge Columns

Column Functionality Pore Diameter Å % Carbon End Cap Applications
Aquapore AX-300 (anion exchange) 300 - - Silica-based support for larger anionic compounds
Aquapore OD-300 (C18) 300 10 Yes Silica-based support for larger compounds by reversed-phase
Aquapore RP-300 (C8) 300 5 Yes Same as above, but for slightly more polar compounds
Aquapore BU-300 (C4) 300 3 Yes Same as above, but for even somewhat more polar compounds
Choice C18 100 12 Yes For high speed/efficiency separation of basic compounds/pharmaceuticals
Choice C8 100 7 Yes For high speed/efficiency separation of basic compounds/pharmaceuticals
Choice PFPP (Pentafluorophenylpropyl) 100 5 Yes For high speed/efficiency separation of basic drugs, especially for LC/MS
Pecosphere C18, monofunctional 80 11 Yes Reversed-phase column for fast separation of smaller compounds
Pecosphere CR C18 80 11 Yes Same as above, but for more basic compounds
Pecosphere CR C8 80 11 Yes Same as above, but, also, for slightly more polar compounds
Peco HCODS C18, polyfunctional 300 9 No Especially suited for reversed-phase separation of proteins and peptides
Polypore CA (calcium form), Mixed Mode Microporous - - Especially suited for separation of organic acids, as well as sugars
Polypore H (hydrogen form), Mixed Mode Microporous - - Especially suited for separation of sugars, as well as organic acids
Reduced Activity C18 80 12 Yes Reversed-phase sorbent geared for fast separation of basic
compounds/pharmaceuticals
Reduced Activity C8 80 5 Yes Same as above, but for slightly more polar compounds
Spheri-5 RP-18 (monofunctional C18) 80 11 Yes Reversed-phase separation of smaller compounds
Spheri-5 ODS (polyfunctional C18) 80 14 Yes Same as above, but with somewhat different selectivity
Spheri-5 RP-8 (monofunctional C8) 80 6 Yes Reversed-phase separation of more basic smaller compounds
Spheri-5 Phenyl (C5) 80 6 Yes Especially suited for hydrophobic interaction separation of biomolecules,
where the activity of the compound must be preserved
Spheri-5 Amino 80 3 No Normal-phase separation of smaller, relatively more polar compounds
Spheri-5 Cyano 80 4 No Same as above, but with somewhat different selectivity
Spheri-5 Silica 80 - - Same as above, but with different selectivity
Validated C18 100 18 Yes Reversed-phase separations in which very little variation in both
lot-to-lot and column-to-column variability can be tolerated
VeloSep RP-18 (C18) 100 14 Yes Reversed-phase column for high through-put and minimal solvent usage
VeloSep RP-8 (C8) 100 7 Yes Same as above, but for slightly more polar compounds

14 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

and Flexibility

Brownlee ™ Analytical Cartridge Columns

for conventional and narrowbore HPLC
Analytical cartridges from the Brownlee line are available in three
lengths (30, 100 and 220 mm) and two internal diameters (4.6 and 2.1
mm). The MPLC cartridge system allows direct coupling of a cartridge
to a guard without any dead-volume. Changing cartridges is easy with
the finger-tight cartridge design, which does not require any wrench
tightening of the holder or disconnecting of tubing from the LC system.
Peco MPLC holders (83 and 33 mm).

Features and Benefits Brownlee VeloSep ®

VeloSep columns are 3.2 mm i.d. cartridges packed with 3 μm
■ Quality – manufactured under ISO-9001 certified quality
reversed-phase support for high throughput analysis and reduced
control procedures
solvent consumption. VeloSep is packed with 3 μm C8 or C18 sorbents
■ Quick and easy cartridge change with the finger-tight design and available in 40 or 100 mm lengths.
■ Flexible – same reusable holder for 2.1 and 4.6 mm cartridges
■ Economical – less expensive than conventional columns Brownlee Validated
Brownlee Validated sorbent is derived from a neutral “Type B” silica
Brownlee CHOICE ™ with inherent low silanophobic activity. Each sorbent is tested to meet
The CHOICE™ columns provide the speed and efficiency appropriate stringent specifications for the separation of basic, neutral and acidic
for LC/MS. Each column’s separation requirements vary depending on test probes. A high-temperature bonding technique is coupled with an
the system, sample and mass spectrometer. exhaustive end-capping procedure to ensure maximum coverage of the
silica surface. A proprietary treatment step is used to further eliminate
any trace residual metals in the silica that create active absorptive
Brownlee PECO sites. This is a highly deactivated column which yields excellent peak
PerkinElmer pioneered the development of Fast HPLC and introduced shape for difficult base analytes, pharmaceuticals and small peptides.
the popular 3 x 3 column. This column is capable of rapid analysis, as
short as one to two minutes. The 83 mm long 3 x 8 column with >
10,000 plates can separate many complex mixtures in less than 10
NewGuard Columns
minutes. Peco cartridges are available with MPLC® holders. Three NewGuard cartridges are small guard cartridges (15 mm x 3.2 mm i.d.)
cartridge lengths (33, 83 and 150 mm) are available in 4.6 mm i.d. packed with 5 or 7 μm sorbents. NewGuard columns prolong column
life 2 to 5 times by eliminating particulates, contaminants and strongly
bound sample components. They act as disposable, replaceable heads
Brownlee Preparative of your analytical columns. NewGuard columns are easily coupled to
Preparative columns are 10 mm i.d. cartridges, packed with Aquapore® MPLC cartridges or conventional columns.
20 μm, 300 Å sorbents. Save time with high-pressure preparative runs
up to 3000 psi and achieve high performance with the 20 μm, 300 Å
sorbents. Typical sample capacity of the 250 mm cartridge is 50 mg to
Brownlee MPLC/Peco Holders
1 g of material; the typical flow rate is 4 – 10 mL/min. MPLC cartridge system ensures leak-free operation up to 7000 psi,
with only finger-tightening. The high-pressure seal in each end
assembly actually seals tighter as pressure increases. No wrenches are
For a full listing of Brownlee required and there is no need to disconnect any tubing to your LC
cartridge columns, please visit: system when changing a cartridge. MPLC cartridges can be directly
www.perkinelmer.com/lcsupplies coupled to another using a union.

Save up to 20%
on your next Brownlee Cartridge
or Conventional Columns order!*
To qualify, use promotion code: LCBLC408
Save 15% when you buy any 2 Brownlee Cartridge or Conventional Columns!
Save 20% when you buy any 3 Brownlee Cartridge or Conventional Columns!
*Use of the LCBLC408 promotion code is required to receive your discount. Discount cannot be combined with volume purchase agreement discounts, university program discounts,
standing order discounts or other contract pricing. Discounts cannot be combined with promotion available at time of instrument purchase. Offer expires 3/31/09.

See page 2 for a complete listing of local offices and for ordering information. 15
Brownlee MPLC Cartridge Columns for

Brownlee cartridge columns

offer an extensive range of
phases and column lengths

Ion Exchange
30 mm x 4.6 mm i.d.* 30 mm x 2.1 mm i.d.* 100 mm x 4.6 mm i.d.**
2 per package 2 per package 1 per package
Column Description Part No. Part No. Part No.

AX-300, Aquapore® 7 μm, 300 Å, weak anion 07110073 07110074 07110075

Polypore CA
®
10 μm, polymeric, calcium form 07110091 07110093
Polypore H 10 μm, polymeric, hydrogen form 07110085 07110087

Polar Phase
30 mm x 4.6 mm i.d.* 30 mm x 2.1 mm i.d.* 100 mm x 4.6 mm i.d.**
2 per package 2 per package 1 per package
Column Description Part No. Part No. Part No.

Amino, Spheri-5 ®
Aminopropyl, 5 μm, 80 Å 07110037 07110039
Cyano, Spheri-5 Cyanopropyl, 5 μm, 80 Å 07110043 07110045
Silica, Spheri-5 5 μm, 80 Å 07110031 07110032 07110033
Silica, Spheri-10 10 μm, 80 Å 07110145

Reversed Phase
30 mm x 4.6 mm i.d.* 30 mm x 2.1 mm i.d.* 100 mm x 4.6 mm i.d.**
2 per package 2 per package 1 per package
Column Description Part No. Part No. Part No.

BU-300, Aquapore Butyl C-4 7 μm, 300 Å 07110061 07110062

Cyano, Spheri-5 Cyanopropyl, 5 μm, 80 Å 07110043 07110045
OD-300, Aquapore ODS C-18, 7 μm, 300 Å 07110235 07110234 07110232
ODS, Spheri-5 C-18, polyfunctional, 5 μm, 80 Å 07110019 07110020 07110021
Phenyl, Spheri-5 Phenyl, 5 μm, 80 Å 07110025 07110027
RP-8, Spheri-5 C-8, monofunctional, 5 μm, 80 Å 07110001 07110002 07110003
Pecosphere 3CR C-18, Base Deactivated, 3 μm 02580195
RP-18, Spheri-5 C-18, monofunctional, 5 μm, 80 Å 07110013 07110014 07110015
Pecosphere 3CR C-8, Base Deactivated, 3 μm 02580191
RP-300, Aquapore Octyl C-8 7 μm, 300 Å 07110055 07110056 07110057

* Requires Holder (07150013) ** Requires Holder (07150014)

16 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

Choice and Variety

Scavenger Columns
33 mm x 4.6 mm i.d.*
5 per package
Column Description Part No.

Silica Scavenger 10 μm 02580203

C18 Scavenger Monofunctional, 10 μm, 80A 02580202

Ion Exchange
100 mm x 2.1 mm i.d.** 220 mm x 4.6 mm i.d.*** 220 mm x 2.1 mm i.d.***
1 per package 1 per package 1 per package
Column Description Part No. Part No. Part No.

AX-300, Aquapore 7 μm, 300 Å, weak anion 07110077

Polypore® CA 10 μm, polymeric, calcium form 07110095
Polypore H 10 μm, polymeric, hydrogen form 07110089

Polar Phase
100 mm x 2.1 mm i.d.** 220 mm x 4.6 mm i.d.*** 220 mm x 2.1 mm i.d.***
1 per package 1 per package 1 per package
Column Description Part No. Part No. Part No.

Amino, Spheri-5 Aminopropyl, 5 μm, 80 Å 07110041

Cyano, Spheri-5 Cyanopropyl, 5 μm, 80 Å 07110047
Silica, Spheri-5 5 μm, 80 Å 07110035

Reversed Phase
100 mm x 2.1 mm i.d.** 220 mm x 4.6 mm i.d.*** 220 mm x 2.1 mm i.d.***
1 per package 1 per package 1 per package
Column Description Part No. Part No. Part No.

BU-300, Aquapore Butyl C-4 7 μm, 300 Å 07110064

Cyano, Spheri-5 Cyanopropyl, 5 μm, 80 Å 07110047
OD-300, Aquapore ODS C-18, 7 μm, 300 Å 07110233 07110231 07110236
ODS, Spheri-5 C-18, polyfunctional, 5 μm, 80 Å 07110022 07110023 07110024
Phenyl, Spheri-5 Phenyl, 5 μm, 80 Å 07110029
RP-8, Spheri-5 C-8, monofunctional, 5 μm, 80 Å 07110004 07110005 07110006
Pecosphere 3CR C-18, Base Deactivated, 3 μm
RP-18, Spheri-5 C-18, monofunctional, 5 μm, 80 Å 07110016 07110017 07110018
Pecosphere 3CR C-8, Base Deactivated, 3 μm
RP-300, Aquapore Octyl C-8 7 μm, 300 Å 07110058 07110059 07110060

* Requires Holder (07150028) ** Requires Holder (07150014) *** Requires Holder (07150015)

See page 2 for a complete listing of local offices and for ordering information. 17
Brownlee NewGuard Cartridge Columns

Guard Cartridge Columns and

Accessories
NewGuard Columns
NewGuard cartridges are small guard cartridges (15 mm x 3.2 mm i.d.)
packed with 5 or 7 μm sorbents. NewGuard cartridges prolong column
life by eliminating particulates, contaminant's, and strongly bound
sample components. They act as replaceable, disposable heads of NewGuard cartridges directly coupled to a 220 mm MPLC
your analytical columns. There is negligible loss of efficiency and cartridge and connected externally to a 250 mm conventional column.
little effect on retention or resolution. NewGuards are available in a
convenient 3-pack and can be coupled directly to any MPLC cartridge
with a union (07150018).

Features and Benefits

■ Prolong column life by 2 to 5 times
■ Protect your column from particulates and strongly bound
sample components
■ Optimized dimensions to prevent loss of resolution
■ Easy coupling to MPLC cartridges or conventional columns View of the NewGuard holder
■ Finger-tight seal to 7000 psi using NewGuard holders and a NewGuard 3/pack.
■ Can be used for sample preconcentration
(connected to sample injection loop)

15 mm cartridge*, 3.2 mm i.d., 3 per pkg. Standards Solutions

Description Part No. Test Mix
Amino, Aquapore® Amino, 7 μm spherical 07110098 Description Part No.
Anion, Aquapore Anion, 7 μm spherical 07110102 Universal test mix for reversed-phase (5 mL/pkg.) 00890893
Cyano, Aquapore Cyano, 7 μm spherical 07110100
Diol, Aquapore Diol, 7 μm spherical 07110105
Standards
Phenyl, Aquapore Phenyl, 7 μm spherical 07110096
RP-2, Aquapore Dimethyl, 7 μm spherical 07110086 Description Part No.
RP-4, Aquapore Butyl, 7 μm spherical 07110088 HPLC SV Calibration Mix #5/610 PAH 00891542
RP-8, Aquapore Octyl, 7 μm spherical 07110090 HPLC 610 Calibration Mix A 00891543
RP-18, Aquapore ODS, 7 μm spherical 07110092 HPLC 610 Calibration Mix B 00891544
Silica, Aquapore Silica, 7 μm spherical 07110106
Validated®, C18, 5 μm spherical 00402237
* Requires holder (07150001)
Note: Actual bed length of NewGuard is about 13 mm

Replacement Seals for MPLC and Prep-10 Holders

Item Description Part No.
Prep-10 Inlet Seal One each (Prep-10 Seal Replacement Kit tools required) 07150012
Prep-10 Outlet Seal One each (Prep-10 Seal Replacement Kit tools required) 07150026
Seals for MPLC Holders Two 7000 psi seals (Seal Replacement Kit tools required) 07150024
Seal Replacement Kit for MPLC Holders Tools and two 7000 psi seals 07150023

18 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

and Holders for choice and variety

MPLC/Peco™ Holders
The patented MPLC cartridge system ensures leak-free operation up to 7000 psi, with only finger-tightening. The high-pressure seal in each end assembly actually seals
tighter as pressure increases. No wrenches are required, and there is no need to disconnect any tubing to your LC system when changing a cartridge. Each MPLC cartridge
can be directly coupled to another using a union.
Name Description Part No.
Universal Holder Kit Includes 100 and 220 mm holder bodies, 07150025
2 end assemblies, 1 union, 1 NewGuard end assembly.
NewGuard® Holder Holds a single NewGuard cartridge or a single 20 mm 07150001
CHOICE™ cartridge.
30 mm Holder Holds a single MPLC and CHOICE 30 mm cartridge. 07150013

33 mm Peco Holder Holds 33 mm Fast LC Peco cartridge only. 07150028

50 mm Holder Holds a single 50 mm CHOICE cartridge only. N2580030

83 mm Peco Holder Holds 83 mm Fast LC Peco cartridge only. 07150029

100 mm Holder Holds a single MPLC 100 mm cartridge. 07150014

150 mm Holder Holds a single MPLC 150 mm cartridge. 07150030

220 mm Holder Holds a single MPLC 220 mm cartridge. 07150015

250 mm Holder Holds a single MPLC 250 mm cartridge. 07150031

100 mm NewGuard Holder for a NewGuard and a 100 mm coupled cartridge. 07150016
System Holder
220 mm NewGuard Holder for a NewGuard 07150017
System Holder and a 220 mm coupled cartridge.
130 mm MPLC Holder for a 30 and 100 mm coupled cartridge. 07150032
System Holder
Union For direct coupling of 2 cartridge holders. 07150018
(Two holder bodies and 2 end assemblies also required.)
NewGuard Upgrades a 30 mm holder to a NewGuard holder. 07150002
End Assembly
End Assembly Holder component. 07150019

30 mm Holder Body Holder component. 07150020

100 mm Holder Body Holder component. 07150021

220 mm Holder Body Holder component. 07150022

Prep-10 Cartridge Holders

Name Description Part No.
100 mm Prep-10 Holder Holds a single 100 mm Prep-10 cartridge. 07150005

250 mm Prep-10 Holder Holds a single 250 mm Prep-10 cartridge. 07150006

See page 2 for a complete listing of local offices and for ordering information. 19
sample loops

Chemically-inert and mechanically

strong PEEK sample loops and
tubing for HPLC applications

Clean-Cut Tubing Tool

Clean-Cut™ tubing tool is designed to cut Teflon®, Tefzel® and polymers
in general but, in particular, PEEK tubing. The compact design enables
every chromatographer to carry it in his pocket. A unique safety locking
mechanism secures the blade when not in use.

Tubing Accessories
Description Part No.
Clean-Cut Tubing ED020015
Clean-Cut Tubing Replacement Blade ED020016

PEEK Tubing
PEEK tubing has the strength
required to withstand continuous
use at HPLC pressure without
PEEK Sample Loops swelling or bursting. The
dense polymer structure of
Sample loops are made from PEEK tubing and fittings. PEEK PEEK tubing eliminates the
(poly-ether-ether-ketone) is a mechanically-strong, chemically-inert permeability to organic solvents
polymer, ideal for HPLC applications where metal surfaces may that causes other polymer tubing,
interact with the mobile phase or sample component. Each sample Tubing and Connectors
such as Tefzel ®, to sweat.
loop is supplied with two PEEK hex-head nuts and ferrules. These
fittings grip the tubing in two locations for a more reliable connection. Use PEEK with virtually any organic or inorganic liquid. PEEK tubing is
not affected by halide salts, high-strength buffers or other aggressive
Description Size Part No. mobile phases that degrade stainless steel.
PEEK Sample Loop 20 μL N9306035
PEEK Sample Loop 50 μL N9306036
PEEK Sample Loop
Internal Loop (PEEK and Ceramic)
200 μL
2 μL
N9306038
N9306022
PEEK Tubing
Description Length Part No.
1
⁄16 in o.d. x 0.007 in i.d. 5 ft N9302678
Stainless Steel Sample Loops ⁄16 in o.d. x 0.010 in i.d. 5 ft N9302650
1

Model Model Model

7125/7010 7725 8125
Size Part No. Part No. Part No. Stainless Steel Tubing
10 μL 09904938 N9306024 ■ Pre-cut and mirror-polished in 316 stainless steel
50 μL 09904940 N9306026
100 μL 09904942 N9306027 41000013 Description Length Part No.
200 μL 09904818 N9306028 09904818 1
⁄16 in o.d. x 0.015 in i.d. 6 ft 00873036
5 mL N9306032 1
⁄16 in o.d. x 0.007 in i.d. 3 ft 02540838

20 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

 supplies and accessories
One-piece, easy-to-use
Fingertight® fittings

PEEK Fingertight ® Fittings

High-performance Fingertight® fittings for the
most demanding applications.
This PEEK Fingertight® fitting is the toughest with regard to chemical
resistance and pressure. This high-performance Fingertight® fitting is
recommended for the most demanding applications and will resist
pressures up to 6,000 psi (400 bar). Made from a single piece of
PEEK, the size permits tightening without tools.
Description Part No.
PEEK One-Piece Fingertight® Fitting ED020005

Fittings Kits
Biocompatible Column Fittings for LC. Recommended for users of a
PerkinElmer Biocompatible LC system. Contains nuts, ferrules
and unions.
Stainless Steel Fittings
Stainless steel nuts are available in both Parker-Hannifin and Part No.
Rheodyne™ formats. The nuts are used to connect 1⁄16 inch o.d. N9301001
stainless steel tubing and feature a 10-32 thread size. PerkinElmer
also offers select SSI fittings for 1⁄16 inch o.d. tubing in 1⁄4 -28 thread size. Fittings Kit for LC
All-in-one fittings kit. The kit contains Rheodyne™ and SSI nuts
and ferrules as well as Fingertight ® II nuts and ferrules for toolless
Stainless Steel Fittings installation. Zero-dead-volume unions are also included. In addition
you receive varying lengths of stainless steel tubing in 0.007 and
Description Part No. 0.010 inch i.d.s, as well as 0.30 inch i.d Tefzel® tubing.
Parker-Hannifin Ferrule, ⁄16 inch
1
00873032 Part No.
Parker-Hannifin Nut, 1⁄16 inch 09903980
Parker-Hannifin Nut & Ferrule Kit, 1⁄16 inch 00890945 N9301002
Includes: 6 nuts and 6 ferrules
Parker-Hannifin Zero-Dead-Volume Union 09903289
Operation Kit
with nuts and ferrules Recommended for purchasers of their first LC. Includes tubing, union,
Rheodyne™ Ferrule, 1⁄16 inch 09904947 fittings, syringe, basic LC book and test mix.
Rheodyne™ Nut, 1⁄16 inch long body 09904974
Part No.
Rheodyne™ Nut, 1⁄16 inch short body 09904956
Rheodyne™ Nut and Ferrule Kit, 1⁄16 inch 02540274 00890873
Includes: 6 ferrules, 3 short nuts and 3 long nuts

See page 2 for a complete listing of local offices and for ordering information. 21
 Enhance the Performance of your HPLC

Vacuum kits for all your

degassing requirements
Check Valves
HPLC check valves allow solvent to flow in only the desired direction.
Check valves are easy to install with the torque wrench kit. For all
PerkinElmer pumps an intermediate check valve is required. The input
check valve, which is identical, should be ordered. The check valves of
the biocompatible pumps differ from those of the stainless steel pumps
in that all portions that contact fluid are composed of titanium.

Check Valves
Inlet/Intermediate Outlet
Check valve Check valve
Type Part No. Part No.
Standard Stainless Steel 02540177 02540197
Micropump 02540177 02540197
Biocompatible Titanium N2600226 N2600192

Maintenance Kits and Tools

Degassing Kits Description Part No.
Using a solvent degassing system will extend the performance of your Biocompatible Piston Seal Replacement Kit N2910385
pump. PerkinElmer offers both vacuum degassing systems that can Includes: Four Seals, Backup Rings, and O-rings
handle all your degassing requirements. Check Valve Torque Wrench 02540871
Diaphragm for Pulse Compensator N2601316
High Pressure Piston Seal Replacement Kit N2910383
Series 200 On-Line Vacuum Degasser Kit Includes: Four Seals, Backup Rings, and O-rings
This is a low-volume, high efficiency, on-line module for the removal of Insertion Tool N2601503
dissolved gasses from HPLC solvents. The vacuum degasser is Micropump Piston Seal Replacement Kit N2910384
available in 3 and 5 channel models to support isocratic, binary and Pulse Compensator Repair Kit N2600313
quaternary pumps as well as degassing of autosampler flush solvent. Includes: Diaphragm, Elastomer Plug, and Seal
Seal Removal Tool N2601295
Description Part No. Series 200 Bio LC Pump Maintenance Kit N2910346
3-channel Vacuum Degassing Package N2600571 Includes: Fuses, Seals, O-rings, and Seal Tools
Includes: a Vacuum Degasser, one 1 L Bottle with Cap, Series 200 Pump Maintenance Kit N2910345
one 2 L Bottle with Cap, one Organizer Tray and Accessory Includes: Fuses, Seals, O-rings, and Seal Tools
5-channel Vacuum Degassing Package N2600570
Includes: a Vacuum Degasser, two 1 L Bottle with Caps,
two 2 L Bottles with Caps, Solvent Tray and Organizer
Binary Bottle Cap Kit N2600522
Replacement Vacuum Degasser Bottles
Includes: two Caps, Tubing, Fittings and Labels required Description Part No.
for two Solvent Bottles
Quatenary Bottle Cap Kit N2600523 1 L Glass Bottle N2600497
Includes: four Caps, Tubing, Fittings and Labels required 2 L Glass Bottle N2600498
for four Solvent Bottles

22 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

Pump

Solvent Sparger and Solvent Filters Static Mixers

Solvent filters remove unwanted particulate matter from the LC The Series 200 static mixer accessory (100-240 V) is used to facilitate
instrument. Spargers connect directly to the solvent delivery line and complete mobile phase blending, resulting in improved retention
are easily removed for cleaning. The scavenger column is ideal for performance. The mixer will most typically be used as part of a Series
eliminating particulate material from solvents. 200 Pump package — where high-pressure blending of two pump
outputs is required. Mixers incorporate a highly efficient crossflow
shearing mechanism which produces vortex sheer mixing over a wide
flow range.
Solvent Sparger and Solvent Filters
Solvent Reservoir Sparger
Description Size Part No. Series 200 Static Mixers
Stainless Steel 10 μm 09903610 ■ Improve gradient accuracy and increase sensitivity
Titanium 10 μm N2600070 ■ Reduce baseline noise
Stainless Steel 40 μm 09903615
Titanium 40 μm N2600089 ■ In-line binary format

Solvent Filters Description Size Part No.

Description Part No. Binary T Mixer 10 μL N2911170
Binary T Mixer 25 μL N2911171
In-Line Solvent Filter System 09903606
In-Line Mixer Assembly 150 μL N2911173
In-Line Solvent Filter Replacement Kit 02540311
In-Line Mixer Assembly 500 μL N2911172
In-Line Solvent Filter System, Titanium N2600259
Binary T Mixer Cartridge 10 μL N2911174
Replacement 2 μm Titanium Filter Element N2601477
Binary T Mixer Cartridge 25 μL N2911175
Replacement Seal for In-Line Solvent Filter N2601262
Binary T Mixer Cartridge 50 μL N2911176
Binary T Mixer Cartridge 150 μL N2911177
Binary T Mixer Cartridge 250 μL N2911178

Series 200 Dynamic Mixer

Series 200 Dynamic Mixer Accessory (100-240 V) – Used to facilitate
complete mobile phase blending, resulting in improved retention
performance. The mixer will most typically be used as part of a Series
200 Micro pump package – where high-pressure blending of 2 pump
outputs is required. Three different volume mixing heads (75, 200 and
400 μL) are available.

Kit includes: Mixer Accessory, Stainless Steel “Tee” Fitting (N2911127),

U.S. style AC Line Cord and 0.1 A Type T Fuse.

Part No.
N2910520

Mixing Heads
Size Part No.
75 μL N2910521
Mixing Head
200 μL N2910522
400 μL N2910523

See page 2 for a complete listing of local offices and for ordering information. 23
supplies and accessories

Injection valves and rotor seals

for analytical HPLC

Rheodyne ™ 9725 PEEK

Bio Injection Valve
Model 9725 is inert and well-suited to the chromatography of biological
molecules, including applications with aggressive mobile phases. This
Flom Analytical Injection Valve valve is useful in all applications in which metal contact with the mobile
The Flom Analytical Injection Valve is a very reliable manual HPLC phase and or sample should be avoided. This valve uses PEEK vent lines
injection valve. It comes with a built in “Inject” contact closure and a Teflon® rotor seal and can be operated in a pH range from 0–14.
connection output. A PEEK rotor seal is provided for excellent
Description Part No.
solvent/sample resistance and the fluid path is designed for minimal
dispersion. This valve is available in either stainless steel or PEEK, 9725 Injection Valve for Series 200 Autosampler N9306020
depending on the application or need.
Rheodyne ™ 8125 Low-Dispersion
Description Part No.
Stainless Steel Injection Valve
Flom Injection Valve Stainless Steel N9306073
Ideal for use in an LC/MS system, the model 8125 is designed for
Flom Injection Valve PEEK N9306072
1 and 2 mm microbore columns and can also be used with
conventional analytical (3 to 5 mm) columns. Small flow passages
Injector Valve Rotor Seals produce low dispersion, maintaining the high mass sensitivity inherent
For both Series 200 Autosampler and manual injectors. in micro columns.

For both the Rheodyne and Flom valves, rotor seals should be periodically Description Part No.
replaced every 6 months to a year and are available in PEEK. For the
8125 Low-Dispersion Stainless Steel Injection Valve N9306021
Rheodyne valve, they are also available in Vespel. PEEK is more inert
towards amines and other basic biomolecules/pharmaceuticals,
exhibiting less sample carryover. However, Vespel is somewhat Rheodyne ™ 7725 Analytical Injection Valve
more resilient than PEEK, providing somewhat better wear life. Inject from 1 μL to 5 mL with high accuracy and precision,
Description Part No. with the Rheodyne™ 7725 and 7725i valves.
Flom Rotor Seal PEEK N9306068 Rheodyne™ 7725 and 7725i valves are versatile injectors and can use
Rheodyne 7725 Vespel Rotor Seal 09904802 both partial-filling and complete-filling methods for loading the sample
Rheodyne 8125 Vespel Rotor Seal 10070900 loop. Wide port angles of the 7725/7725i valve provide improved
Rheodyne 7725/9725 PEEK Rotor Seal N9306044 access to fittings. Sample loop with a 2 μL internal capacity is also
available. In a clean system, the 7725/7725i typically can make more
than 30,000 injections before requiring replacement of the rotor seal.
For a full listing of Rheodyne ™ Description Part No.
injection valves, please visit:
www.perkinelmer.com/lcsupplies 7725 Injection Valve for Series 200 Autosampler N9306019
7725i Injection Valve with Internal Switch N9306017

24 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

 supplies and accessories
Interchangeable flowcells
and pump accessory kits

Bio Conversion Kits

There are two kits available; one that contains all of the parts necessary
to convert the Series 200 pump and Series 200 autosampler for Bio
applications. The other contains all of the parts necessary to convert
only the Series 200 Pump for Bio applications.

Description Part No.

S200 Pump and S200 Autosampler Conversion Kit N2910035
S200 Pump Conversion Kit N2910036

Series 200/785A UV/VIS and Series 200 EP

Pump Seal Kits PDA Detector Flow Cells
The standard 10 mm pathlength used with conventional 4.6 mm i.d.
Description Part No. columns provides the highest detection limits possible for your sample.
The 6 mm pathlength flowcell has been optimized for lower-dispersion
High Pressure Piston Seal Replacement Kit N2910383
LC analysis and is the perfect choice when using narrowbore, 2.1 mm
Includes: Seals (4), Backup Rings and O-Rings
or microbore, 1 mm columns (see Figure 1). The 3 mm pathlength
Micropump Piston Seal Replacement Kit N2910384
is the choice for semiprep LC to avoid detector saturation at high-
Includes: Seals and O-Rings
solute concentrations.
Series 200 Pump Maintenance Kit N2910345
Includes: Fuses, Seals, O-Rings and Seal Tools Description Size Part No.
Series 200 Standard Flowcell 15 μL, 10 mm N2920124
785A Standard Flowcell 12 μL, 8 mm N2920117
Flowcell Bulkhead Union 25000323
Flowcell Assembly Microbore 2.4 μL, 6 mm 29000544
Flowcell Assembly Prep 1.7 μL, 3 mm 29000545

Photo Diode Array Detector Flowcells

Series 200 EP
Description Size Part No.
Series 200 Standard Flowcell 15 μL, 10 mm N2920124
Flowcell Assembly Microbore 2.4 μL, 6 mm 29000544
Flowcell Assembly Prep 1.7 μL, 3 mm 29000545

Series 200
Description Material Size Part No.
Detector Backpressure Regulator Standard Flowcell Assembly Stain. Steel 12 μL, 10 mm N2922028
The detector backpressure regulator is a device that is attached Flowcell Assembly PEEK 12 μL, 10 mm N2922029
to the outlet of the detector to prevent outgassing in the flowcell, Low-volume Flowcell Assembly Stain. Steel 5 μL, 4.5 mm N2922030
eliminating variations to the detector baseline. LC-135C/235
Description Material Part No. Description Material Size Part No.
Backpressure Regulator Stainless Steel 09907126 Flowcell Assembly Titanium 8 μL N2350211
Adjustable from 15 – 59 psi

See page 2 for a complete listing of local offices and for ordering information. 25
autosampler vials

Vials, caps and septa are inert to samples

ordinarily analyzed by liquid chromatography
and guaranteed for fit and compatibility
Microsyringes (For Manual Injection)
Syringes are used for accurate and precise liquid delivery. Each
syringe is hand-fitted to assure maximum accuracy. Our syringes are
composed of glass barrels and precision stainless steel needles. The
needle features a blunt tip, required for use with a Rheodyne injector.
Description Part No.
10 μL Syringe 09904937
25 μL Syringe 09904823
50 μL Syringe 09904941
100 μL Syringe 09904822

Solvent and Sample Filtration

Description Part No.
All-Glass Filter Apparatus N9301063
For Solvent Filtration
FP Vericel Hydrophilic Filters N9301067
For Aqueous Mobile Phase, 47 mm, 0.45 μm (pkg. 100)
PTFE Hydrophobic Filters N9301068
Autosampler Vials and Caps For Nonaqueous Mobile Phase, 47 mm, 0.45 μm (pkg. 100)

with the unique Inter-Seal ®

Autosampler Vial Starter Kits
bonded Septa and Cap Complete and convenient starter kits for your volatile and
PerkinElmer screw thread vial caps use the revolutionary Inter-Seal® standard applications. Each kit contains everything you
Bonding System. Using a process that bonds silicone/PTFE and other will need to run your LC instruments under two convenient
elastomeric compounds directly into thermoplastic closures eliminates part numbers. Each kit contains syringes, vials,caps and vial rack.
liner fallout whilst still providing the excellent resealability and multiple
injection capability. No adhesives are used in this process, bonding Description Qty. Part No.
the cap and septa at the molecular level of plastic and rubber. This LC Screw Top Starter Kit N2930366
septa has a very broad chemical resistance and can be used in many Includes:
markets including; the environmental market, diagnostic packaging, 30 mL pump priming syringes 3
pharmaceutical packaging, cosmetic and food packaging. Racks for 50 vials-12 mm 2
PTFE/SILICONE screw caps (pkg. 100) 4
2 mL screw top vials w/label &
Vials, Caps and Septa Fill lines (pkg. 100) 2
Vials 12x32 mm amber vials (pkg. 100) 2
Description Pkg. Part No. 25 μL blunt syringes 2
1/16 union tubes 2
200 μL Clear Glass Micro Vial 500 N9302136 Nut and ferrules (pkg. 6) 1
To be used with Glass Vial Sleeve (N9307027)
Glass Support Sleeve 25 N9307027 LC Crimp Top Starter Kit N2930365
Includes:
300 μL Polypropylene Vial Kit 500 N9306080
Crimper tool (manual) 1
Includes: tapered polyethylene vial, blue cap
Racks for 50 vials-12 mm 2
with bonded silicone/PTFE septa
2 mL 11 mm crimp top vials (pkg. 100) 3
2 mL Clear Glass Crimp Vial 100 N9301385
2.0 mL crimp top amber vials (pkg. 100) 1
2 mL Amber Glass Crimp Vial 100 N9302680
25 μL blunt syringes 1
2 mL Clear Glass Screw Top Vial 100 N9306053
11 mm decappers tool (manual) 1
2 mL Amber Glass Screw Top Vial 100 N9306057
11 mm Silver Crimp top caps
w/Septa (pkg. 100) 4
Caps
Description Pkg. Part No.
8 mm Silver Aluminum Crimp Cap 1,000 03300806 Save 10% on New
PTFE/Rubber
11 mm Snap Cap 1,000 04978532 Starter Kits for your
11 mm Silver Aluminum Crimp 100 N9306015
Cap PTFE/Rubber 10 mm Black 100 N9306052 Autosampler!
Polypropylene Screw Cap with PTFE/Pre-Slit White Silicone To qualify, use promotion code: LCSK1208
Offer may not be used in conjunction with other discounts or promotions. Offer expires 3/31/09.

26 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

 detector supplies
For outstanding performance, use only
PerkinElmer deuterium, tungsten
or xenon HPLC lamps

UV/VIS Deuterium Series 200/200 EP

Detector Lamp Photo Diode Array Detector Lamp

Photo Diode Array Detector Lamps

UV/VIS Detector Lamps
The Series 200/200 EP Photo Diode Array Detector provides true UV/VIS detection
Our extensive quality control and inspection process demands and high resolution spectral data. The excellent signal-to-noise characteristics
the very best quality sources. Choosing a PerkinElmer deuterium, make it ideally suited for low-volume or low concentration samples.
tungsten or xenon source provides outstanding ultraviolet and
Series 200 EP
true visible performance.
Components Part No.
■ Exceptional performance anywhere in the Deuterium Lamp N2925030
detector’s 190–700 nm wavelength range Tungsten Lamp N2922011
■ Lamp changes are quick and easy due to
a unique self-aligning lamp mount Series 200
Components Part No.
Series 200/785A UV/VIS Detector Lamps
Deuterium Lamp (Phase 2) N2922046
Components Part No.
Tungsten Lamp N2922011
Deuterium Lamp N2920149
Tungsten Lamp N2920146 LC-135C/235
Components Part No.
LC-295 UV/VIS Detector Lamps
Detector Lamp N2351285
Components Part No.
Deuterium Lamp 02712266

Fluorescence Detector Lamps

Refractive Index Detector Lamps The major benefit afforded by fluorescence detection is the inherent high
The Series 200/200a Refractive Index, with its deflection-type design, allows sensitivity of the technique coupled with outstanding specificity. The Series 200a
sensitive detection of these compounds with low noise and drift characteristics. Fluorescence Detector provides signal to noise ratio of >700:1 from trace
analysis using a 150 W xenon source.
Series 200/200a
Series 200/200a
Components Part No.
Components Part No.
Tungsten Lamps 02712273
Xenon Lamp N2922082

LC-240
For our complete listing of Components Part No.
HPLC detector lamps, please visit:
www.perkinelmer.com/lcsupplies
Xenon Lamp L2251157
Festoon Lamp 04969486

See page 2 for a complete listing of local offices and for ordering information. 27
software

IRIS spectral
processing software

Spectral Library Matching

Spectral library matching is another valuable feature available in
IRIS software. You can use PDA spectra to confirm the identity of
chromatographic peaks. IRIS contains a spectral library function,
allowing users to construct libraries of standard spectra taken under
specific analytical conditions. These libraries can be used for
automated spectral matching. A chromatogram, when collected
or reprocessed, can be compared against the library — and each
component’s spectral profile analyzed to find the best match. The
matching algorithm gives a “Hit Quality” rating indicating the quality or
confidence level in the match. This value can be used to automatically
update the chromatographic method and can be included in the
final analytical report, an ideal tool for laboratories working in
method development.

Introduction
With the continued need to increase productivity and enhance the
quality of analytical results, the use of photo diode array (PDA)
detectors continues to grow rapidly. However, in order to truly utilize the
power, performance and wealth of data generated by a PDA detector,
an equally powerful software package is essential.

The IRIS™ spectral processing software from PerkinElmer offers a full

suite of functionality and an intuitive user interface, all protected under
a fully 21 CFR Part 11-compliant architecture. Used in conjunction with
the award-winning TotalChrom® Chromatography Data Systems (CDS),
IRIS spectral processing software brings spectral handling to a new
level of efficiency and ease-of-use.

User Interaction
IRIS features an Outlook™-like graphical user interface that facilitates
a short learning curve and allows an easy navigation into information.
A hierarchical relationship and a tree-like structure of data are available Compliance for FDA-Regulated Industries
on screen for a convenient sample tracking. A single environment for
IRIS software provides a complete range of features and functionality
all software functions is available, as well as specific views for certain
to ensure FDA 21 CFR Part 11 compliance and similar regulatory
functions. User-specific customizable views can be prepared for
agencies’ requirements. IRIS software provides multi-level user
needed tasks.
permissions, password-protected access control and full audit-trailing,
as well as configurable e-signature points.
Confirmation of Peak Identity and Purity
One of the most important benefits a PDA detector delivers is the
IRIS Spectral processing Software
confirmation of the identity and/or purity of a chromatographic peak. IRIS is an optional software program for spectral processing of data
IRIS spectral processing software performs automated mathematical acquired from the PerkinElmer S200 Diode Array Detectors. Requires
processing, determining the similarity of spectra within every peak in IPM for PerkinElmer LC Modules (N5150162) for control of S200.
the run. This is a necessary tool to calculate spectral peak purity, Also requires TotalChrom or TurboChrom 6.3.1 or higher.
providing critical information on the efficiency of the separation. This
Part No.
resulting purity value is then automatically inserted into the final
TotalChrom chromatography report and available for the Review N5150130
& Approve process. Also available in the report is the maximum
absorbance wavelength of each peak. This “Lambda Max” value
is useful in confirming the proper identity of the component.

28 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

 reference tools
LC Separation Notes CD
and Technical Tips Poster

Valuable LC Technical Tips Guide

at your fingertips, including:
■ Commonly used formulas applied in
chromatographic separation (USP/EP)
■ Tips to improve sensitivity for specific detectors
■ Care and maintenance of your HPLC
■ Solvent miscibility
■ HPLC pump pressure conversion factors
■ Column void volume and optimum flow rates
■ Wall poster measures 24" x 36"

Order your FREE copy today! Visit:

www.perkinelmer.com/LCtechtips

PerkinElmer LC
Separation Notes CD
Enjoy the convenience of:
■ References to separations conducted on 516 compounds
or class of compounds
■ References point to over 230 LC applications – just one click away
■ Information on the column used in the application
■ Analytical conditions such as flow, gradient and solvents
■ A labeled chromatogram with information on the compounds,
matrix and sample preparation
■ Application by industry
■ Applications presented in a one page template for easy printing
■ CD also contains a full electronic copy of the Consumables and
Supplies reference catalog

Order your FREE copy today! Visit:

www.perkinelmer.com/LCseparations

See page 2 for a complete listing of local offices and for ordering information. 29
clarus 600 gas chromatograph

The fastest injection-to-injection

time in conventional
gas chromatography

Every fast-paced, high-volume laboratory

shares a common goal: to speed up
analytical cycle times. Now, PerkinElmer
delivers with its latest innovation in GC,
the high-performance Clarus ® 600
Gas Chromatograph.

Clarus 600 Gas Chromatograph –

the innovation is simply its speed
Powered by the fastest available heat-up QUICK GLANCE
and cool-down conventional oven ■ Oven cool-down from 450 °C to 50 °C in less than 2 minutes
■ Integrated autosampler adds flexibility and automation
PerkinElmer has always led the way with innovations in gas
chromatography and the Clarus 600 Gas Chromatograph (GC) ■ Temperature programmable inlets deliver performance and
is no exception. It features a unique, high-performance oven with flexibility for more demanding applications
the fastest combined heat-up and cool-down rate in a conventional ■ Programmable pneumatic control (PPC) adds automation efficiencies
GC oven design. ■ Exclusive optional PreVent pressure-balanced system enhances
Autosampler pre-rinse performs time-consuming syringe rinse with performance and productivity
sample before the GC becomes ready, saving time in between runs. ■ Innovative, intuitive touch-screen interface makes operation easy–
The resulting shorter injection-to-injection time will significantly no training required
increase your throughput and productivity by speeding up your ■ Scalable TotalChrom CDS make data management and reporting
analytical cycle time. And higher productivity means a fast return easier than ever
on your investment (ROI).
■ PerkinElmer’s complete offering allows easy integration of
best-in-class mass spectrometer, headspace, headspace
trap or thermal desorption

See for yourself how

the NEW Clarus 600 GC will
increase your productivity!

Try our ROI Calculator at

www.perkinelmer.com/GC

30 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

 clarus 600/560 gas chromatograph/mass spectrometer
Get results better
and faster with
the NEW Clarus
600/560
Family of GC/MS

Take your GC/MS to the limit with the A model for every lab’s needs:
Clarus ® 600 Gas Chromatograph/
Mass Spectrometers (GC/MS). Clarus 600 C GC/MS:
■ Electron ionization and chemical ionization with 255 L/sec turbomolecular pump
It provides the performance and
throughput you require with the Clarus 600 T GC/MS:
ruggedness you demand. ■ Electron ionization with 255 L/sec turbomolecular pump

Clarus 600/560 S GC/MS:

Whatever you need it for the ■ Electron ionization with 75 L/sec turbomolecular pump
Clarus 600 GC/MS family delivers Clarus 600/560 D GC/MS:
■ Electron ionization with air-cooled oil diffusion pump
The compact Clarus 600 GC/MS, with its advanced electronics,
features the widest mass range and best-in-class detection limits
of any quadrupole MS. Our high-speed scanning delivers far better
peak integrity and accuracy. Its gas chromatograph has the fastest Convenient GC/MS Consumable Kits
heat-up and cool-down oven in a conventional GC. Multiple pumping
options offer an instrument for every lab’s needs. Plus, the system is GC/MS PSS Injector Starter Kit
driven by our sample-centric TurboMass™ software for ease-of-use
Part No.
from data collection to evaluation and reporting.
N6100447
Whether you do routine “workhorse” applications or challenging
research requiring more capabilities, the Clarus 600 GC/MS is an Contents: Pkg. Qty. Part No.
extremely robust, precise and accurate system that can handle all
5.0 μL Autosampler Syringe 1 N6101390
your demands.
Vial Locator (dongle) 2 N6101182
PSS Injector Viton o-rings (250 deg) 10 1 N6101747
PSS Injector Kelrez o-rings (350 deg) 1 10 09921004
PSS split/splitless Injector, 2 mm, no wool 2 N6121004
Graphite/Vespel ferrules, for 0.25 mm columns 10 2 09920104
QUICK GLANCE Thermogreen Speta (50 pieces) 1 N6621028
■ El and CI: best-in-class signal/noise specifications offer new Rhenium Filament 1 N6470012
possibilities for analysis Aluminum oxide powder (3 oz) 1 4190197
■ Plug-and-play ion source: loosen two screws and easily change
when needed GC/MS CAP Injector Starter Kit
■ Three pumping systems: provide the right performance to fit your Part No.
needs and budget
N6100448
■ Smaller footprint: for economical space use
■ Fastest scan rates (12,500 amu/sec): for the most accurate Contents: Pkg. Qty. Part No.
determination of peaks 5.0 μL Autosampler Syringe 1 N6101390
■ Widest mass range (1–1,200 u): encompasses a variety of Vial Locator (dongle) 2 N6101182
applications, such as brominated flame retardants CAP Injector Viton o-rings (250 deg) 10 N9302783
■ SIFI™ simultaneous collection of selected ion and full ion CAP Injector Kelrez o-rings (350 deg) 10 N9302782
scanning data for the most productive analytical work CAP split/splitless Injector, 4 mm, no wool 2 N6121001
■
Graphite/Vespel ferrules, for 0.25 mm columns 10 2 09920104
UltraTune™ automated tuning for BFB/DFTTP or custom
tuning on any compound for faster setup Thermogreen Speta (50 pieces) 1 N6621028
Rhenium Filament 1 N6470012
Aluminum oxide powder (3 oz) 1 4190197

See page 2 for a complete listing of local offices and for ordering information. 31
Organic Standards from PerkinElmer GC

Organic Calibration Standards

for 8000 series
U.S. EPA Methods
Method 8260B for Water
and Solid Waste Matrices
Method 8260B is an analytical method that uses a GC/MS equipped
with a capillary column to perform the separation of the volatile organic
compounds found in water and a variety of solid waste matrices.

Method 524.2 is an analytical method that uses a purge and trap device
for sample preparation and a GC/MS equipped with a capillary column
to perform the separation of volatile organic compounds.

Interferene
Volatile Organics
CheckCombination
Standards Blend
Contains all analytes in Mixes A, C and D.
Method SW-846 is an analytical method which utilizes a Clarus 600 GC to
perform the separation of the volatile organic components found in a variety
PerkinElmer offers a wide selection of GC and GC/MS standards. of solid waste matrices. To detect the GC eluant a Clarus 600 GC/MS is used.
Each solution is supplied with a comprehensive Certificate of
Analysis that documents quality and assurance to the highest level Description Part No.
obtainable by a Calibration Standard. 1.2 mL @ 2,000 μg/mL in P & T Methanol N9331047

Organic Certified Reference Materials from PerkinElmer are a new

addition to an already extensive organic product line, designed to
enhance your one-stop shopping experience. Each new standard is
provided in convenient 1.2 mL ampules to minimize waste and comes
Interferene
Method 8260B
Check
Standards
Standards
with a pre-labeled amber glass storage vial with cap for easy use. Description Part No.

To ensure customer satisfaction, our Organic Mixes are prepared Alternate Four-Component Surrogate Standard for Method 8260B
at concentration levels that take into consideration a number of 1.2 mL @ 2,000 μg/mL in P & T Methanol N9331042
factors including: vapor pressure, evaporation, breakdown rates and
dilution schemes. PerkinElmer goes the extra step by analyzing each Internal Standard for Method 8260B
organic standard on the Clarus 600 GC and GC/MS state-of-the-art 1.2 mL @ 2,000 μg/mL in P & T Methanol N9331041
instrumentation, to ensure that the standard conforms to the
customer’s exact needs.

For customer ease, all Organic Standards are prepared with a precision
of +/- 0.5% and accompanied with a comprehensive Certificate of
Analysis (lot specified by part number). Data packs are also available
Interferene
Ketones for Check
MethodStandards
8260B
upon request. These include a chromatogram of the standard and Description Part No.
quantitative report listing the values for each analyte.
1.2 mL @ 2,000 μg/mL in P & T Methanol N9331043

For a full product listing of NEW

Mix B Purgeable
Interferene CheckGases
Standards
PerkinElmer GC Standards please visit:
www.perkinelmer.com/gcsupplies for Methods 8260B/524.2
Description Part No.
1.2 mL @ 2,000 μg/mL in P & T Methanol N9331048

32 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

and GC/MS
Interferene
Method 8270C
Check
Surrogates
Standards
Description Part No.
Acid Surrogate for Method 8270C
1.2 mL @ 2,000 μg/mL in Methanol N9331037
8000 Series Solid and Base Neutral Surrogate for Method 8270C
Hazardous Waste Methods 1.2 mL @ 2,000 μg/mL in Methylene Chloride/Acetone N9331038
Resource Conservation and Recover Act (RCRA) under SW-846,
“Test Methods for Evaluating Solid Waste”
■ Method 8080A contains detailed operating procedures to be followed
by laboratories analyzing solid and liquid matrices. It is a method that
600 Series Wastewater Methods
uses a GC/ECD to perform the separation of the selected pesticides
following concentration and clean up of an extract for aqueous or
Clean Water Act “Wastewaters”
solid samples
Method 624 Standards Kit for Volatile Organic Compounds
■ Method 8082 is used to determine the concentrations of PCB’s,
Contains: N9331060, N9331061, N9331062, 9331063.
either as individual congeners or Aroclors by GC/ECD.
The U.S. EPA Method 624 is an analytical method which utilizes a TurboMatrix
Headspace Purge and Trap instrument for sample prep and a Clarus 600 GC
equipped with a packed column to perform the separation of the volatile organic
Method 8082
Interferene Check
PCB’sStandards
(polychlorinated compounds found in a 5 mL sample of municipal or industrial wastewater. To
detect the eluant a Clarus 60 GC/MS is used.
biphenyls) Standards Kit
Description Part No.
Method 8082 is used to determine the concentration of PCB’s either as individual
congeners or Aroclors. A Clarus 600 GC with a capillary column is used to perform 1.2 mL @ 2,000 μg/mL in P & T Methanol N9331064
the separation and to detect the eluent and ECD (electron capture detector) or
ELCD (electrolytic conductivity detector) is used. Mix A for Method 624
1.2 mL @ 2,000 μg/mL in P & T Methanol N9331060
Description Part No.
1.2 mL @ 1,000 μg/mL in Hexane N9331028 Purgeable Gases Mix B for Method 624
1.2 mL @ 2,000 μg/mL in P & T Methanol N9331061

Mix C for Method 624

1.2 mL @ 2,000 μg/mL in P & T Methanol N9331062
Interferene
Method 8270C
Check
Standards
Standards
Mix D for Method 624
Method 8270C is an analytical method which utilizes a Methylene Chloride
extraction of aqueous sample or Methylene Chloride:Acetone extraction of solid 1.2 mL @ 2,000 μg/mL in P & T Methanol N9331063
sample and a Clarus 600 GC equipped with a capillary column to perform the
separation of the compounds. To detect the GC eluant a Clarus 600 GC/MS is used.
Description Part No.
Semi-Volatile Calibration Standard for Method 8270C Interferene
Method 8100/625
Check Standards
1.2 mL @ 2,000 μg/mL in Methylene Chloride/Benzene N9331030 Method 8100
Method 8100 is a method for the analysis of polynuclear aromatic hydrocarbons.
Internal Standard for Method 8270C
A Clarus 600 GC is used to perform the separation of compounds with an FID
1.2 mL @ 2,000 μg/mL in Methylene Chloride/Benzene N9331036 (flame ionization detector) to detect the eluent.
Method 625
Method 625 is an analytical method that uses a methylene chloride extraction of
municipal or industrial wastewater, concentrated to 1 mL and a GC/MS equipped
Interferene
Method 8270C
Check
Mixes
Standards to perform the separation of acid and base neutral extractable fractions.
Description Part No. Description Part No.
HICAL-Acids Mix for Method 8270C Polynuclear Aromatic Hydrocarbons for Method 8100/625
1.2 mL @ 2,000 μg/mL in Methylene Chloride N9331031 1.2 mL @ 2,000 μg/mL in Methylene Chloride/Benzene N9331044

Analyte Mix for Method 8270C Polynuclear Aromatic Hydrocarbons Mix B for Method 8100
1.2 mL @ 2,000 μg/mL in Methanol N9331032 1.2 mL @ 1,000 μg/mL in Methylene Chloride/Benzene N9331045

Balance Mix for Method 8270C Surrogate Standard for Method 8100
1.2 mL @ 2,000 μg/mL in Methylene Chloride N9331033 1.2 mL @ 2,000 μg/mL in Methylene Chloride N9331046

See page 2 for a complete listing of local offices and for ordering information. 33
Inline Gas Purifiers for Clarus GC and

Fast and easy to use Click-On

Inline Super Clean™ Gas Purifiers
save you time and money
PerkinElmer Click-On Inline Super
Clean ™ Purifiers reduce your
maintenance system downtime
Using the Click-On Connectors lets you change the trap without
introducing contaminant’s into your system. Click-On connectors
can replace a trap, without introducing impurities into the system.
This in turn eliminates the need to flush the system.
The unique Click-On Connector fitting has a spring-loaded needle
valve, which seals when a trap is removed and only opens when a
new trap is connected and locked into position. When the Click-On
connectors are installed into the gas line, there is no need to loosen
or tighten any fittings, simply click on the new trap in seconds.
The ability to add a Click-On Inline Super Clean™ Indicator after the
stainless steel trap gives the user a clear visual indication of when to
change the filter. This indicator may also be used as a standalone trap.

Click-On Inline Purifier Compatibility Chart

Moisture Oxygen Hydrocarbons Combination Triple
Type of Gas Filter Filter Filter Filter Filter
Acetylene √ √
Air √ √ √
Carbon Dioxide √ √
Helium √ √ √ √ √
Hydrogen √ √ √ √ √
Features and Benefits Methane √ √
■ Reduce system downtime with Click-On fast connectors Nitrogen √ √ √ √ √
■ High purity ensures 99.9999% pure gas Nitrous Oxide √ √ √ √ √
■ No open gas line when changing the trap Oxygen √ √ √
Propane √ √
■ Helium Specific Glass Indicating Triple Trap is ideal for GC/MS
P5 √ √
■ No tools necessary to replace trap (5% Methane in Argon)
P10 √ √
(10% Methane in Argon)
Product Specifications
Purifier Type Gas Quality* Max. Pressure Max. Flow Use For H20 Capacity O2 Hydrocarbons Est. Lifetime
Moisture 99.9999% 11 bar, 160 psi 25 L/min Inert carrier gas 21 g NA NA > 3 years
He, Air, H2
Oxygen 99.9999% 11 bar, 160 psi 25 L/min Inert carrier gas NA 3,000 mL NA > 3 years
Hydrocarbons 99.9999% 11 bar, 160 psi 25 L/min Inert carrier gas NA NA 36 g (as n-butane) > 3 years
Air, H2
Combination Moisture/ 99.9999% 11 bar, 160 psi 25 L/min Inert carrier gas 10 g NA 18 g (as n-butane) > 2 years
Hydrocarbons He, Air, H2
Indicating Triple Moisture/ 99.9999% 11 bar, 160 psi 25 L/min Inert carrier gas 3g 400 mL 5 g (as n-butane) > 1 year
Oxygen/Hydrocarbons He
Triple Moisture/ 99.9999% 11 bar, 160 psi 25 L/min Inert carrier gas 6g 1,000 mL 12 g (as n-butane) > 2 years
Oxygen/Hydrocarbons
*Results @ 2 L/min

34 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

GC/MS
3-Cartridge Gas
Purification System

Stainless Steel Trap Kits

Description Connector (Qty) Part No.
Combination: Oxygen/Moisture Trap 1
⁄8" Brass (2) N9306108
Combination: Oxygen/Moisture Trap 1
⁄8" SS (2) N9306109 AFS Manifold
Combination: Moisture/Hydrocarbons Trap 1
⁄8" Brass (2) N9306117 and Mounting Hardware
Combination: Moisture/Hydrocarbons Trap 1
⁄8" SS (2) N9306118
Triple: Oxygen/Moisture/Hydrocarbons Trap 1
⁄8" Brass (2) N9306110
Triple: Oxygen/Moisture/Hydrocarbons Trap 1
⁄8" SS (2) N9306111 Advanced Filter System
Triple Gas Specific (He): 1
⁄8" Brass (2) N9306112 The Advanced Filter System has high capacity and
Oxygen/Moisture/Hydrocarbons efficiency levels for oxygen, water and hydrocarbons.
Triple Gas Specific (He): ⁄8" SS (2)
1
N9306113 The recommended maximum flow rate is 2.0 L/min
Oxygen/Moisture/Hydrocarbons and 200 psi maximum operating pressure.

Stainless Steel Traps Features and Benefits Advanced

Description Part No. Filter System
■ Two indicators, for oxygen and moisture
Moisture Trap N9306100
■ Easy cartridge replacement with on/off knob
Oxygen Trap N9306101
Hydrocarbons Trap N9306102 ■ Double seal construction for safety
Combination: Oxygen/Moisture Trap N9306103 ■ Check valves protect gas lines during cartridge replacement
Combination: Moisture/Hydrocarbons Trap N9306105
Triple: Oxygen/Moisture/Hydrocarbons Trap N9306104 System Capacity Efficiency
Triple Gas Specific (He): Oxygen/Moisture/Hydrocarbons N9306106
Oxygen 850 cc < 1 ppb
Water 12 g < 10 ppb
Helium Specific Glass Indicating Triple Hydrocarbns 8g < 1 ppb
Trap for your PerkinElmer Clarus GC/MS A polycarbonate shield surrounds the glass indicator section of the filter
PerkinElmer recommends the use of the Helium Specific Glass is sealed, unlike other gas filters, the gas flow is secure even if the glass
Indicating Triple Trap for your GC/MS system. This trap contains should break. This redundant sealing system and robust construction
oxygen, moisture and hydrocarbons adsorbents in one trap and is provides a new level of security in gas filtration. Maximum flow rate is
packed and purged under helium. 2.0 L/min with 200 psi max operating pressure.
The glass indicating trap clearly shows when the filter needs to be Description Part No.
replaced with the use of color changes. The packing material is a
Advanced Filter System N9303963
silica-based environmentally friendly substitute for cobalt dioxide (blue)
Replacement Cartridge N9303964
in the moisture indicator.
Manifold and Mounting Hardware N9306139
Available as a kit with the necessary 1⁄8" brass connectors, and as a
replacement trap, this system is easy to install. 3-Cartridge Gas Purification System
Description Connector (Qty) Part No. This system provides for high capacity contaminant removal for GC
Indicating Glass Triple Gas Specific (He): N9306107 supply gasses, and allows for individual cartridge replacement.
Oxygen/Moisture/Hydrocarbons Cartridge replacement is recommended after processing 19 cylinders
Indicating Glass Triple Gas Specific (He): ⁄8" Brass (2)*
1
N9306114 of 8 m3 high purity gas (99.997%).
Oxygen/Moisture/Hydrocarbons
Indicating Glass Triple Gas Specific (He): ⁄8" SS (2)
1
N9306116 Features and Benefits
Oxygen/Moisture/Hydrocarbons
■ All stainless steel cartridges are easy to replace
■ High capacity
■ Wall bracket gets the system up and out of the way

System Capacity Efficiency

Save 10% on Oxygen
Water
1,000 cc
25 g
< 1 ppb
< 30 ppb
Click-on Gas Hydrocarbons (C5 and higher) 19 g < 1 ppb

Purifier Kits!* Description

Purification System, 3 Head All Steel System
Part No.
N9306135
Cartridge Set, Gas Purification All System Cart (Replacement) N9306136
Including the Helium Specific Cartridge, Gas Purification Moisture N9306137
Glass Indicating Trap Kit Cartridge, Gas Purification Hydrocarbon N9306138
Cartridge, High Capacity O2 Replacement N9306004
*Savings off list price.
Hardware, Gas Purification Manifold/Mtg N9306140
Hardware, Gas Purification Manifold/Mtg for bench or wall N9306140

See page 2 for a complete listing of local offices and for ordering information. 35
gc supplies

Essential GC lab
supplies from PerkinElmer
MiniTemp MT4 Non-contact
Temperature Measurement
with Laser Sighting
Features and Benefits
■ Displays thermal measurement readings
in °C or °F
■ Easy point and shot infrared technology
in a pocket size configuration
■ Great for instrument thermal test
confirmation, including GC injector
port and detector measurements,
Portable Gas Leak Detector thermostatted LC vials, and
enzymatic hydrolysis baths
The new PerkinElmer compact handheld electronic gas leak detector is
the ideal solution for detecting gas leaks in your Gas Chromatography
Non-contact Surface Temperature
systems. Leaks in your system waste gas and can cause detector
Measurement with Laser Sighting
noise, baseline instability, and shorter column life. This portable unit
detects minute leaks of any gas with thermal conductivity different from
air. The reference gas inlet draws in ambient air for comparison to air
drawn into the sample probe. A leak is detected by both LED bar graph Specifications
display and audible alarm.
Model MiniTemp MT4
Temperature Range -18 to 400 °C
Detectable Gases (0 to 750 °F)
Distance to Spot Size (D:S) 8:1
Gas Minimum Detectable Indicating LED
Type Leak Rate (atm cc / sec) Light Color Response time 500 m/sec
Emissivity Pre-set at 0.95
Helium 1.0 x 10-5 Red
Hydrogen** 1.0 x 10-5 Red Accuracy ±2%, or ±2°C (±3 °F)
Nitrogen 1.4 x 10-3 Yellow whichever is greater
Argon 1.0 x 10-4 Yellow Typical Distance to Target (Spot) Up to 1.5 m (4 ft)
Carbon Dioxide 1.0 x 10-4 Yellow Laser Sighting Yes

The popular MiniTemp MT4 also includes single dot laser sighting to assist with aiming.
Battery: Rechargeable Ni-MH internal battery pack (6 hours normal 9 volt battery included. Recalibration is not available.
operation)
Universal Power Adapter Set: US, UK, European, Australian plugs
included Description Part No.
Operating Temperature Range: 32-120 °F (0-48 °C) MiniTemp MT4 N9306074
Humidity Range: 0 – 97%
Warranty: 1 Year Basic Tool Kit
Certifications: CE, Japan
Compliance: WEEE, ROHS Description Part No.
Tools come in a tool box for easy storage and use N9301327
Features and Benefits
Kit Includes:
■ Sleek ergonomic, hand-held design with rugged side grips
Open-end Wrench Set (6 pc), Screwdriver Set (6 pc.), Adjustable Wrench (6 in), Chain
■ Automatic shut-off capabilities Nose Pliers (narrow), Wire Cutters, and Wire Strippers
■ Optimized sample flow path
■ LED readout and audible alarm Deluxe Tool Kit
Description Part No.
Description Part No.
Shipped in a plastic tool box for convenient storage N9301328
Portable Electronic Leak Detector N9306089
Soft Carrying Case N9306142 Kit Includes:
Probe (fine tip) N9306063 Open-end Wrench Set (6 pc.), Screwdriver Set (6 pc.), Adjustable Wrench (6 in), Chain
**Caution: The PerkinElmer leak detector is not designed for determining leaks in a combustible Nose Pliers (narrow), Wire Cutters, Wire Strippers, Slip-joint Pliers (6 in), Long Nose
environment. This unit may be used for determining trace amounts of hydrogen in a GC No. 5 Stainless Steel Tweezers (43⁄8 inches), Needle File Set (6 pc.), Allen Key Set (11 pc.
environment only. imperial sizes), and Allen Key Set (9 pc. metric sizes)

36 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

 septa and ferrules
Merlin MicroSeal™
and SilTite™ ferrules

SilTite™ metal ferrules provide a continuous leak-free connection

and are perfect for connecting your column to a GC/MS. Merlin MicroSeal ™ Septum
The SilTite metal ferrule and nut are manufactured from the same
™

material and therefore expand and contract at the same rate, eliminating The Merlin MicroSeal™ septa is a unique replacement
the need to retighten, even after temperature cycling. The base of the septa employing a two-step sealing system and an advanced
SilTite™ ferrule forms a perfect seal with the MS interface, ensuring a elastomer material.
leak-free connection. SilTite™ metal ferrules have a temperature limit well Because the syringe needle does not pierce the septa, there is no
above the temperature capacity of the injector, MS interface or GC oven. debris and ghost peaks are greatly reduced. The MicroSeal™ septa also
reduces the incidence of bent syringe needles and liner contamination.
Description Hole Size Part No. Usable in either manual or autosampler applications, this septa can
improve your productivity and run reliability. Designed to be used with
SilTite Ferrules Starter Kit (pkg. 10)
™
0.4 mm N9306090
23 gauge straight needle syringes. Pressure ranges from 4 to 100 psi
SilTite™ Ferrules Starter Kit (pkg. 10) 0.5 mm N9306091
and injection port temperatures up to 325 °C.
SilTite™ Ferrules Starter Kit (pkg. 10) 0.8 mm N9306092
SilTite™ Ferrules (pkg. 10) 0.4 mm N9306093
SilTite™ Ferrules (pkg. 10) 0.5 mm N9306094 Features and Benefits
SilTite™ Ferrules (pkg. 10) 0.8 mm N9306095
SilTite™ Nuts (pkg. 5) N9306096 ■ Thousands of injections before septa change
■ 2-step sealing system
Capillary Column Ferrules ■ No debris — no ghost peaks
■ Temperatures up to 325 °C
Graphite
■ Pressure ranges 4 to 100 psi
Ferrule of choice for high-temperature applications up to 450 °C.
Graphite seals easily and does not stick to glass columns. ■ Easy installation
®
Graphite/Vespel
15% graphite/85% polyimide ferrule recommended for use with GC/MS Description Pkg. Part No.
systems. Temperature limit 350 °C. Merlin MicroSeal™ Septum Kit N9303344
® Includes: Injector Port Adapter,
Vespel
2 Septa and 1 Nut
Not reusable. Not recommended for fused silica capillary columns. Merlin MicroSeal™ Septum 1 N9303345
Use these ferrules on 1⁄16 inch metal tubing and glass-lined receivers.
Temperature limit 350 °C.

Injector Septa
Capillary Column Ferrules ■ Thermogreen® LB-2 septum, extremely low bleed over a wide range of inlet
temperatures — 100 to 350 °C. Easier needle penetration and high puncture
Nut Graphite Graphite/Vespel® tolerance make this septum ideal for autosamplers. This septum is already
Size Column i.d. / Ferrule i.d. Part No. Part No. conditioned and ready to use
1
⁄16 in 0.18 – 0.25 mm / 0.4 mm 09920104 ■ BTO™ (Bleed Temperature Optimized) injector septa, 11 mm diameter.
1
⁄16 in 0.18 – 0.32 mm / 0.5 mm 09903700 09920105 Maximum recommended operating temperature 300 °C
1
⁄16 in 0.18 – 0.32 mm / 0.5 mm* N9306001 N9306000 ■ PTFE/Silicone injector septa, 11 mm diameter
1
⁄16 in 0.18 – 0.53 mm / 0.8 mm 09920141 09920107
1
⁄8 in 0.18 – 0.53 mm / 1.0 mm 09903394 Description Pkg. Part No.
1
⁄8 in 0.18 – 0.32 mm / 0.5 mm* 09903395 Thermogreen Injector Septa
®
50 N6621028
1
⁄8 in 0.18 – 0.32 mm / 0.5 mm 09903981 Low Bleed Injector Septa 25 N9303343
*2-hole PTFE/Silicone Injector Septa 50 00090652

See page 2 for a complete listing of local offices and for ordering information. 37
syringes

GC injector and
autosampler syringes

Point Style 2
This is a general purpose point style
designed for septum penetration in all
chromatographic techniques. The needle
has a 22° bevel to minimize coring and
needle plugging.

Point Style 3
Needle has a 90° bevel. Point style is
recommended when the syringe is used
for accurate pipetting of liquids. Excellent
Autosampler Syringes for mixing standards of very small volume.
Syringes from PerkinElmer are individually inspected for accuracy
and performance.

Recommended autosampler syringes are available in 0.5, 5 and 50 μL GC Injector Syringes

capacities. For routine analyses, the metal plunger in barrel with
PTFE-tipped seal is the standard syringe as shipped with each Clarus® ■ All PerkinElmer injectors have been tested and optimized for use with a
GC instrument. Alternative syringes to use are the metal plunger in 7 cm needle
barrel or the 0.53 mm on-column injection. ■ A 7 cm needle is critical to be sure your sample is deposited in the optimal zone
Description Part No. Removable Needle Syringes (RN)
50 μL Syringe, Metal Plunger 0.63 mm o.d. needle N6101760 Syringe Pack Point
5 μL Syringe, Metal Plunger PTFE-tipped Seal N6101390 Capacity Gauge Length Size Style Part No.
0.63 mm o.d. needle
5 μL Syringe, Metal Plunger 0.63 mm o.d needle N6101251 10 μL 1 #2 N9302210
5 μL On-column Syringe Metal Plunger N6101380 25 μL 1 #2 N9302211
0.47 mm o.d needle 50 μL 1 #2 N9302212
0.5 μL Low Injection Volume Syringe, N6101252 100 μL 1 #2 N9302213
Metal Plunger 0.63 mm o.d. needle Replacement Needles for RN Syringes
0.5 μL Low Injection Volume Syringe, N6101253
Syringe Pack Point
Metal Plunger 0.47 mm o.d. needle
Capacity Gauge Length Size Style Part No.
10 μL 26S 2 in 3 #2 N9302222
Ultramicro Volume Syringes 25/50/100 μL 22S
250 μL 22S
2 in
2 in
3
3
#2
#2
N9302224
N9302226
■ Recommended for liquid sample injections of less than 5 μL for
gas chromatography Fixed Needle Syringes
■ Syringes come standard with needle length of 7 cm — optimum for Syringe Pack Point
PerkinElmer injectors Capacity Gauge Length Size Style Part No.

Syringe Pack Point 10 μL** 1 #2 00230523

Capacity Gauge Length Size Style Part No. 10 μL* 6 #2 N9302230
25 μL 1 #2 N9302202
0.5 μL 25 1 N9302231 25 μL 1 #3 09904823
1.0 μL 22 1 00230177 50 μL 1 #2 N9302203
1.0 μL 26† 1 00230111 50 μL 1 #3 09904941
2.0 μL 25 1 N9302235
*Savings based on one-piece price. Savings of 20% reflected in price shown.
†
Recommended for PerkinElmer wide-bore capillary adapter **Standard fitted with 7 cm needle.

38 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

 glass inlet liners
Glass Inlet Liners
for PerkinElmer Injector Systems
Programmed Temperature Split/Splitless (PSS) Injector Liners
Dimensions (mm)
Description i.d. x o.d. x length Pkg. Part No.
Quartz Split Liner 2 x 4 x 86.2 1 N6121004
PerkinElmer Standard (ships in instrument)
Quartz Splitless Liner 1 x 4 x 86.2 1 N6121006
Excellent for low-volume analysis (ships with instrument)
On-Column Glass Liner 2.4 x 4 x 86.2 1 N6101539

Borosilicate Glass Split Liner 2 x 4 x 86.2 5 N9302949

This liner is loosely packed with wool for the specific use of analyzing fuel in oil
Glass PSS Drilled Uniliner (hole at the top) NEW! 2 x 4 x 86.2 5 N9303424
Glass liner with siloxane deactivation
Glass PSS Drilled Uniliner (hole on the bottom) NEW! 2 x 4 x 86.2 5 N9303425
Glass liner with siloxane deactivation

Capillary Split/Splitless Injector Liners

Dimensions (mm)
Description i.d. x o.d. x length Pkg. Part No.
Quartz Liner for Split Operation 4 x 6.2 x 92.1 1 N6121001
Good for large volume injections
Quartz Liner for Splitless Operation 2 x 6.2 x 92.1 1 N6121002
Standard Injector Liner (ships with instrument)
Glass Liner for Split Operation 4 x 6.2 x 92.1 1 N6101052
Universal liner for general purpose analysis
Glass Liner for Splitless Operation 2 x 6.2 x 92.1 1 N6101372
Universal liner for general purpose analysis
Precision Split Glass Liner Deactivated Surface with wool 4 x 6.2 x 92.1 5 N6121020
Wool can be adsorptive if fibers are broken
Zero Dilution Glass Outer Liner 2.7 x 6.3 x 69 1 N1011445
Ideal for trace headspace work
Zero Dilution Inner Liner 1 x 2 x 73 1 N1011446
Use with Outer Liner (N1011445)

Packed Column Injector Liners

Dimensions (mm)
Description i.d. x o.d. x length Pkg. Part No.
Wide-Bore Column On/Off Quartz Liner 6 x 4 x 92.1 1 N6121003
Wide-Bore Column Glass Liner 6 x 4 x 92.1 1 N6101375
Drilled Uniliner (hole on bottom) NEW! 4 x 6.2 x 92.1 5 N6502013
Good for PPC equipped GCs. Recommended for analysis in which
compounds of interest could be affected by a tailing solvent peak.
Gooseneck Drilled Uniliner (hole on top) NEW! 4 x 6.2 x 92.1 5 N6502014
Use for trace, active samples. Gives high recovery and linearity.

Purchase 5 packs of inlet liners on the same order and receive 5% off!
Purchase 10 packs of inlet liners on the same order and receive 10% off!
Offer may not be used in conjunction with other discounts or promotions. Offer expires 3/31/09.

See page 2 for a complete listing of local offices and for ordering information. 39
autosampler vials, caps and septa

Low prices on autosampler

vials and caps
Always have enough vials and
caps readily available
for your analysis

Autosampler Vial Convenience Kits

The screw top convenience pack provides 100 vials and 100 pre-
assembled caps and septa together in an environmentally clean,
resealable clamshell pack. Clear crimp top vials and silver crimp caps
with PTFE/rubber septa are also packed in a 100 piece clamshell pack.

1 Pack 10 Packs
Description Pkg. Part No.
Clear Crimp Top Vials and Silver 100 N9300654
Caps with PTFE/Rubber Septa
Clear Screw Top Vials and Black 100 N9301945
Caps with PTFE/Butyl Rubber Septa
Prices shown are per pack price.

Autosampler Starter Kit

Autosampler crimp and screw top vials,
The PerkinElmer Autosampler Starter Kit contains everything you need
to run the Clarus® GC autosampler under one convenient part number. guaranteed for fit and compatibility.
Screw thread vials are custom designed for the PerkinElmer Clarus GC.
Part No. Manufactured from Type 33 borosilicate glass, the vials have high-
N6120105 temperature tolerance and are chemically inert. Color variety crimp
caps offer easy identification within the laboratory on 2 mL crimp top
Contents: vials. Microsampling with a maximum capacity of 200 μL can be
accomplished with the use of a low-volume insert and support foot.
5 μL x 0.63 mm o.d. syringe, 2 mL clear sample vials (100), 2 mL amber sample
vials (100), blue crimp caps with septa (100), green crimp caps with septa (100),
red crimp caps with septa (100), septa for waste/wash vials (100), crimper 11 mm,
decapper 11 mm, 2 mL vial rack.
Autosampler Vials and Caps
GC Educational Consumable Kit - Description Size Pkg. Part No.
Electronic Crimper
Crimp Top Vials
Part No. Clear Glass 11 mm 100 N9301385
N6500570 Amber Glass 11 mm 100 N9302680

Contents: Crimp Caps

Blue with Teflon®/Rubber 11 mm 100 N9302686
Crimper 11 mm Electronic with Universal battery pack (1), N6101390 syringe-9000 Green with Teflon®/Rubber 11 mm 100 N9302684
5.0 μL .63 NDL DYNA (2), 12 mm 50 holder vial rack (2), 11 mm (2 mL) crimp top Red with Teflon®/Rubber 11 mm 100 N9302685
vials (100), 11 mm cap and septa (100), N9316076 col-Elite-5-30M-2.5UM-.25MM Silver with Teflon®/Rubber 11 mm 100 N9306015
column (1).
Screw Top Vials
GC Educational Consumable Kit - Clear Glass 8 mm 100 N9302945
Manual Crimper Screw Caps
Part No. Screw Caps 9 mm 100 N9303441
Septa for Black Screw Caps 100 N9303442
N6500571
PTFE-Coated Butyl Rubber
Contents: Inserts
Crimper 11 mm manual hand crimper (1), N6101390 syringe-9000 5.0 μL .63 NDL Low Volume, Clear Glass 200 μL 1,000 N9302681
DYNA (2), 12 mm 50 holder vial rack (2), 11 mm (2 mL) crimp top vials (100), 11 mm Vial Support for insert 500 N9302682
cap and septa (100), N9316076 col-Elite-5-30M-2.5UM-.25MM column (1).

40 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

 software
TotalChrom — a proven solution
with leading-edge productivity

Streamlining your laboratory workflow, the entire process from Report templates can perform calculations between different peaks
setting up an analytical method to the final approval of reports in the same sample or even between samples, as well as automate
statistical determination to replicate injections, with full control over
is a streamlined series of operations in TotalChrom.
the output format.
PerkinElmer’s TotalChrom Chromatography Data System (CDS) is
designed to provide laboratories with the total answer to
chromatography data-handling needs. Unsurpassed 21 CFR Part 11 Compliance
for Regulated labs
Introduction The TotalChrom system features Enhanced Security™, a proprietary
protocol for supporting United States FDA 21 CFR Part 11 compliance.
Acquiring, processing, reporting, reviewing and approving data is a
Audit trails and electronic signatures recorded during data acquisition,
streamlined series of operations in PerkinElmer’s TotalChrom CDS, soft-
instrument control and data analysis processes ensure that data
ware designed to fit your laboratory workflow and maximize
integrity is always maintained. System features fully document all
productivity. With its scalable architecture, 21 CFR Part 11 compliance
methods, sequences, and reports, including instrument run logs, and
features and proven algorithms, TotalChrom offers a computing
provide a complete and unambiguous link from the initial experiment to
strategy to manage your chromatography data quickly and securely in
the final results. Multiple TotalChrom “JobTypes” can be created to
both regulated and non-regulated environments.
control who can perform what functions in the system.
When configured with a PerkinElmer Clarus GC or a PerkinElmer Series
200 HPLC system, TotalChrom CDS is the controller and data manager
for the overall system. TotalChrom CDS can also control selected Quickly and Easily Navigate, Review
instruments from other vendors and can acquire data from any chro- and Approve Your Data
matographic system through A/D interface. In the “paper world,” reports need to be reviewed and signed. The
The TotalChrom client/server (TC C/S) data system is the solution in TotalChrom Review & Approve (R&A) feature is a graphical reviewing
multi-user environments. TC C/S systems can easily integrate all environment that allows intuitive navigation into data and reports and
existing chromatographs into a single networked system supporting an provides for the implementation of a data-approval cycle. With TC R&A,
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compared at a glance.

Reviewing and approving reports can be done electronically, with

User Interaction multiple levels of authority and secure electronic signatures.
TotalChrom features TC Publisher, a powerful application that extends High-throughput applications have dramatically increased the amount
report capabilities beyond the standard templates by providing a of information produced every day in a laboratory. This feature
sophisticated laboratory report generator using standardized tools. streamlines tedious data review by using a single environment to
Unique features let you graphically format the exact report as needed navigate into data, just like we, every day, navigate into e-mail.
without extensive training or special commands. It ensures that the
stages of chromatographic analysis, report generation and distribution
are quick, easy and complete.

See page 2 for a complete listing of local offices and for ordering information. 41
elite columns

Elite Series capillary columns

use only the finest quality
high-strength fused silica

Top 10 reasons to buy PerkinElmer Phase Cross Reference Chart

Elite Series Capillary Columns
Phase/Description Equivalent Capillary Phase
1. Finest quality of high-strength fused silica
Elite-1, Elite-1ht DB-1, DB-1ht, HP-1, HP-101, Ultra-1, SPB-1,
2. Each column individually inspected and tested 100% Dimethyl CP-Sil 5CB, CI-Sil5CBMS. RSL-150, RSL-160, Rtx-1,
3. Reproducible results BP-1, CB-1, OV-1, 007-1MS, SP-2100, SE-30
4. Crosslinked and bonded stationary phase Elite-200 Trifluoropropylmethyl DB-210, AT-210, VF-200MS, 007-210, Rtx-200
5. Robust column cage Elite-5, Elite 5ms, Elite -5ht DB-5, DB-5ms, DB-5ht, Ultra-2, SPB-5, CP-Sil8CB,
6. Superior resolution 5% Diphenyl – 95% Dimethyl RSL-200. Rtx-5, BP-5, CB-5, OV-5, 007-2(MPS-5),
SE-52, SE-54, XTI-5. Rtx-5ms, PTE-5, HP-5ms
7. Wide selection of stationary phases available
8. Reduced baseline bleed Elite-5Amine PTA-5
5% Diphenyl –
9. Lower baseline noise 95% Dimethyl Polysiloxane
10. Column lengths from 5 to 105 M
Elite-35, Elite-35ms DB-35, DB-35ms, Rtx-35, SPB-35, AT-35, Sup-Herb
35% Phenyl – 65% Methyl
Elite-17, Elite-17ms, Elite-17ht DB-17, DB-17ht, HP-17, RSL-300, Rtx-50,
Why choose fused silica? 50% Phenyl – 50% Methyl 007-17(MPS-50), SP-2250, HP-50+
Many factors influence the quality of a column. Fused silica is considered
Elite-1301 DB-1301, Rtx-1301, CP-624
to be the purest form of glass, with fewer metal oxides (Lewis acid sites)
6% Cyanopropylphenyl
and hydrogen bonding (surface silanol) groups. The stationary phase is
cross linked (polymerized) and also bonded to the surface of the column Elite-1701 DB-1701, SPB-7, CP-Sil 19CB, Rtx-1701,BP-10,
to provide a high degree of stability, resulting in lower bleeding of the 14% Cyanopropylphenyl – CB-1701, OV-1701, 007-1701
stationary phase at elevated temperatures. The superior inertness of 86% Dimethyl
the column means that acidic and basic compounds can be analyzed
Elite-225 DB-225, HP-225, SP-2330, CP-Sil 43CB, RSL-500,
on the same column.
50% Cyanopropylphenyl – Rtx-225, BP-225, CB-225, OV-225, 007-225
50% Phenyl methyl
Selecting the right Stationary Phase Elite-WAX DB-FFAP, HP-20M, SUPELCOWAX 10, CP-WAX 52CB,
The inherent efficiency (large number of theoretical plates) of capillary Polyethylene Glycol SUPEROX II, CB-WAX, STABILWAX, BP-20,
columns allows you to choose from relatively few types of phases, Elite-CW 007-CW, Carbowax, HP-Innowax
compared to the many varieties of packed columns previously required.
Elite-FFAP DB-WAX, HP-FFAP, Nukol, SUPEROX FA,
Perhaps more importantly, because capillary columns are more efficient,
Polyethylene Glycol – STABILWAX-DA, 007-FFAP, OV-351, DB-FFAP
you will see superior resolution resulting in narrower, taller peaks that
Acid Modified
allow easier integration from your data system. Identification of small
peaks are facilitated by a reduced baseline bleed and lower baseline Elite-608 SPB-608, NON_PAKD Pesticide, DB-608,
noise. Non-polar Elite-1 columns from PerkinElmer will preferentially Specialty phase for semi- 007-608, HP-608
retain non-polar compounds, whereas the PerkinElmer Elite-200 column volatile pesticides (EPA 608)
phase provides high selectivity for analytes containing lone pair electrons,
Elite-624, Elite-Volatiles DB-624, DB_VRX, VOCOL, NONPAKD AT-624, Rtx-Volatiles,
such as nitro and carbonyl groups. Elite-WAX polyethylene glycol
Specialty phase for volatiles Rtx-502.2, 007-624, HP-624, CP-624, Rtx-624
columns are highly selective toward polar compounds such as alcohols.
Elite-CLPesticides Rtx-CLPesticides
Specialty Phase for
What length do I need? Chlorinated Pesticides
Typically capillary columns are available in lengths from 15 to 105 meters.
The longer the column the more resolving power, but this also increases Elite-VMS Rtx-VMS
the analysis time. Doubling a column length only increases resolution Specialty Phase for Volatile
by approximately 40% but, under isothermal conditions, will double Organics on GC/MS
the analysis time. If using a temperature programmed analysis retention Elite-PONA DB-Petro100, Petrocol DH, HP-PONA,
times are more dependent on the temperature than on the column Dimethyl polysiloxane SPB-1, 007-1, RTx-1PONA
length. PerkinElmer provides columns in the most popular lengths processed for detailed
of 5, 10, 12, 15, 25, 30, 50, 60, 75, 100 and 105 meters depending analysis of petroleum naphtha
upon the column i.d.

42 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

 elite columns
Elite-200, Elite-5Amine
and Elite-CLPesticides
Elite-5Amine 5% Diphenyl Elite-200 Trifluoropropylmethyl
and 95% Dimethyl Polysiloxane Polysiloxane Capillary Column
The tubing surface of the Elite-5Amine is chemically altered to reduce Elite-200 is considered to be one of the best capillary columns in the
tailing of basic compounds. Thorough testing on each column ensures market today, solving many difficult separation problems not possible
that every column exceeds the requirements for analyzing ppm levels of on any other bonded stationary phase. Due to the electrophilic nature
amines, without priming. The temperature program/bleed profile is of the fluorine-containing polymer, Elite-200 trifluoropropyl stationary
measured to ensure low bleed at maximum operating temperature. phase has a unique selectivity creating interactions with compounds
This column is ideal for analyzing a wide variety of basic compounds that contain groups displaying lone-pair electrons, or with
such as alkylamines, diamines, triamines, ethanoloamines electron-rich molecules.
nitrogen-containing heterocycles.
Primary Applications
Primary Applications Ideal for solvents, Freon®, fluorocarbons, alcohols, ketones, silanes
Specifically designed for amines and other basic compounds. and glycols, environmental analytes and CFCs.

Features and Benefits Features and Benefits

■ Thermally stable to 315 °C ■ Low bleed
■ Reduced tailing ■ Superior inertness
■ Low bleed at maximum operating temperature ■ Equivalent to USP G6 phase
■ Eliminates column priming ■ Thermally stable to 340 °C
Description Dimensions Part No. Description Dimensions Part No.
Elite-5Amine 15 M x 0.32 mm x 1.00 μm N9316676 Elite-200 15 M x 0.25 mm x 0.10 μm N9316616
Elite-5Amine 15 M x 0.53 mm x 3.00 μm N9316681 Elite-200 15 M x 0.32 mm x 1.50 μm N9316632
Elite-5Amine 30 M x 0.25 mm x 0.50 μm N9316673 Elite-200 30 M x 0.25 mm x 0.25 μm N9316619
Elite-5Amine 30 M x 0.25 mm x 1.00 μm N9316675 Elite-200 30 M x 0.53 mm x 1.00 μm N9316642
Elite-5Amine 30 M x 0.32 mm x 1.50 μm N9316679 Elite-200 60 M x 0.53 mm x 0.25 μm N9316637
Elite-200 60 M x 0.53 mm x 1.00 μm N9316643

Elite-CLPesticides
Elite-CLPesticides is specially designed to overcome the coelutions
and analyte breakdown typically encountered in chlorinated pesticide For a full listing of
Elite ® capillary columns, please visit:
analyses for U.S. EPA methods 8081, 608 and CLP. Column bleed www.perkinelmer.com/gcsupplies
measured by ECD is extremely low at temperatures greater than
300 °C, which is critical for baking out the column to remove
high-boiling compounds commonly found in pesticide/PCB extracts.

Primary Applications
Chlorinated pesticides and herbicides. U.S. EPA Methods 504, 608,
619, 8081, 8151 and CLP.

Features and Benefits

■ Thermally stable to 340 °C
■

■
Low column bleed — ideal for ECD or GC/MS analysis
Exceeds performance criteria for U.S. EPA Methods 8081, 608, CLP
Save on your next
■ Baseline separation in less than 15 minutes Elite Column purchase!*
Description Dimensions Part No. To qualify, use promotion code: GCELC408
Elite-CLPesticides 15 M x 0.25 mm x 0.25 μm N9316661
Elite-CLPesticides 15 M x 0.53 mm x 0.50 μm N9316665
Elite-CLPesticides 15 M x 0.25 mm x 0.20 μm N9316667 Save 15% when you buy any 2 Elite Columns!
Elite-CLPesticides 30 M x 0.32 mm x 0.50 μm N9316664 Save 25% when you buy any 3 Elite Columns!
Elite-CLPesticides 30 M x 0.32 mm x 0.25 μm N9316670
Elite-CLPesticides 30 M x 0.53 mm x 0.42 μm N9316672
*Use of the GCELC408 promotion code is required to receive your discount. Discount cannot be
combined with volume purchase agreement discounts, university program discounts, standing
order discounts or other contract pricing. Discounts cannot be combined with promotion available
at time of instrument purchase. Offer expires 3/31/09.

See page 2 for a complete listing of local offices and for ordering information. 43
elite columns

Elite-Guard and Elite-Siltek®

guard columns

Maintain the integrity of your

capillary column with a fused
silica guard column
Using the Elite-Guard or Elite-Siltek® guard column lengthens the life
of the capillary column and improves the analyte focusing. The 5 M
length of deactivated uncoated fused silica is connected to the inlet
end of the capillary column and traps nonvolatile residues, preventing
them from collecting at the head of the analytical column. This length
of fused silica does not contain stationary phase adding only a minimal
amount of time to the analysis.

PerkinElmer offers both the intermediate-polarity deactivated guard

column and the Siltek® deactivated guard column as it is important to
match the polarity of the solvent and the polarity of the surface
deactivation. Elite-Guard intermediate-polarity deactivated column
has an operating temperature up to 325 °C. Siltek® deactivation creates
a highly inert surface for very active compounds such as chlorinated
pesticides with a maximum temperature range up to 380 °C.

Features and Benefits

■ Increase the life of the capillary column
■ Maintain retention time and resolution on capillary column
■ Traps nonvolatile particles
■ Increases column performance
■ Elite-Guard temperature range to 325 °C
■ Elite-Siltek® guard temperature range to 380 °C
Wide-Bore Adapter Kit
Description Dimensions Part No.
Contains all the parts necessary to adapt packed column injectors
quickly and easily for use with wide-bore capillary columns. Includes Elite-Guard 5 M x 0.10 mm N9316601
0-20 mL/min flow controller element, wide-bore adapter with 1⁄16 inch Elite-Guard 5 M x 0.18 mm N9316602
fitting, wide-bore glass liner and column support hanger. Elite-Guard 5 M x 0.25 mm N9301356
Elite-Guard 5 M x 0.32 mm N9301357
Description Part No. Elite-Guard 5 M x 0.45 mm N9316605
Wide-Bore Adapter Kit N6120001 Elite-Guard 5 M x 0.53 mm N9301358
Elite-Siltek® Guard 5 M x 0.25 mm N9316607
Elite-Siltek® Guard 5 M x 0.32 mm N9316608
Elite-Siltek® Guard 5 M x 0.53 mm N9316609

Universal Connectors
■ Allows for fast, leak-free connections of fused-silica columns
Wafer Scribes
■ The new fused-silica tapered design allows connection of any size column
and is easy to use. (Suitable for 0.1 to 0.53 mm columns) The PerkinElmer ceramic wafer scribe is inexpensive and ideal for
cutting polyimide fused silica capillary columns and guard columns.
Description Part No. The scribe is easy to hold and simple to use. All four sides can be
Universal Connector (pkg. 5) N9302149 used as a cutting tool. (pkg. 10)
Universal Y Splitter (pkg. 1) N9303448
Description Part No.
Polyimide Sealing Resin (5 g) N9301343
Undeactivated Presstight Column Connectors (pkg. 5) N9303962 Wafer Scribes (pkg. 10) N9301376

44 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

 application kits
Convenient Consumable Kits
for a Variety of Applications

NEW from PerkinElmer! Environmental Application Kit

Complete Consumable Application Kits for U.S. EPA Method 8260B
All your consumable needs in one convenient kit, designed specifically Part No.
to be used within the application requirements for OVI, Environmental, Promo Code: GC020804 (see details below) N9300658
Blood Alcohol and Biodiesel Materials Testing application notes*.
Contents: Pkg. Qty. Part No.

Biodiesel Application Kit ASTM 6584 20 mm Headspace Crimp Vials 1,000 1 B0104236
19 mm PTFE-Coated/Silicone Caps, Springs & Septa 1,000 1 B4000022
Part No.
20 mm Electronic Crimper, 110 V 1 N9302571
N9300670 20 mm Electronic Crimper 1 N9302594
Application Notes NEW! 1 09936885
Contents: Pkg. Qty. Part No. Polyimide Deactivated 1 N9301357
Autosampler Syringe 5.0 μL (0.47 mm) 1 2 N6101380 Uncoated Tubing / 5 m x 0.32 mm
Elite-5ht Column 15 M x 0.32 mm x .10 μm 1 1 N9316274 Elite-Volatiles / 30 m x 0.25 mm x 1.4 μm 1 N9316388
Elite Guard Column (ht) 5 M x 0.53 mm 1 1 N9316609 Universal Connector 5 1 N9302149
Mini Union Connector Kit – Includes Mini Union and 5 1 N9306128
Nuts, 0.32 mm Ferrules and 0.53 mm Ferrules
11 mm Electronic Crimper 1 1 N9302592 OVI (Organic Volatile Impurities)
Crimp Vials 2 mL 100 5 N9301385
Aluminum Crimp Caps 11 mm Rubber/PTFE 100 5 N9306015
Application Kit for Pharmaceuticals
GC Septa 50 1 N6621028 Part No.
Injector Liner, Hour Glass 1 2 N6101703 Promo Code: GC020801 (see details below) N9300655

Contents: Pkg. Qty. Part No.

Biodiesel Application Kit Elite-130 / 130 m x 0.53 mm x 3.0 μm 1 N9316687
ASTM 6584 & D2887 SIMDIS2 Zero Dilution Glass Outer Liner 1 N1011445
Zero Dilution Glass Inner Liner 1 N1011446
Part No.
Polyimide Uncoated 1 N9301354
N9300672 Deactivated Tubing / 5 m x 0.18 mm
20 mm Headspace Crimp Vials 1,000 1 B0104236
Contents: Pkg. Qty. Part No. Assembled Headspace Caps and Septa 1,000 1 B4000022
Autosampler Syringe 5.0 μL (0.47 mm) 1 2 N6101380 20 mm Electronic Crimper 1 N9302594
Elite-5ht Column 15 M x 0.32 mm x 0.10 μm 1 1 N9316274 Application Notes NEW! 1 09936887
Elite Guard Column (ht) 5 M x 0.53 mm 1 1 N9316609
Mini Union Connector Kit – Includes Mini Union and 5 1 N9306128
Nuts, 0.32 mm Ferrules and 0.53 mm Ferrules Materials Testing or Food and Beverage
Elite-MXT2887 SIMDIS Column 1 1 N9316689
20 mm Electronic Crimper 1 1 N9302594
GC/Headspace Consumables Kit
Crimp Vials 2 mL 100 5 N9301385 Part No.
Aluminum Crimp Caps 11 mm Rubber/PTFE 100 5 N9306015 Promo Code: GC020803 (see details below) N9300657
GC Septa 50 1 N6621028
Injector Liner, Hour Glass 1 2 N6101703 Contents: Pkg. Qty. Part No.
Graphite Ferrules 10 1 09903394
20 mm Headspace Crimp Vials 1,000 1 B0104236
Assembled Headspace Caps and Septa 1,000 1 N1010070
Blood Alcohol Application Kit 20 mm Electronic Crimper 1 N9302594
Part No. Application Notes NEW! 1 09936888
Promo Code: GC020802 (see details right) N9300656

Contents: Pkg. Qty. Part No.

20 mm Headspace Crimp Vials
19 mm PTFE/Butyl Caps, Springs & Septa
1,000
1,000
1
1
B0104236
N1010070
Save 15% on your next
20 mm Electronic Crimper
Application Notes NEW!
1
1
N9302594
09936886
Application Kits
Elite-BAC-1 / 30 m x 0.32 mm x 1.8 μm 1 N9316579 Kit promo codes must be used at time of order
Elite-BAC-2 / 30 m x 0.32 mm x 1.2 μm 1 N9316577 Promotion Codes:
1
⁄16" to 0.5 mm 2-hole Graphite Ferrule 5 1 N9306001 GC020801 for N9300655, GC020802 for N9300656,
GC020803 for N9300657, GC020804 for N9300658
* For full downloadable pdf format application notes, Offer may not be used in conjunction with other discounts or promotions. Offer expires 3/31/09.
please visit: http://las.perkinelmer.com/applications

See page 2 for a complete listing of local offices and for ordering information. 45
 Determination of Residual Solvents-USP

Meeting the Updated Requirements for

the Residual Solvents in
Pharmaceutical Materials
Experimental
The instrumental platform used in these analyses, was the
PerkinElmer® TurboMatrix™ HS-40 headspace system and the
PerkinElmer Clarus® 600 Gas Chromatograph with FID. The
following instrument parameters used in this study achieved
results which exceeded the USP detection-limits method
criteria for the analysis of class 1 and class 2 solvents.
The sample vial was equilibrated at 80 ºC for 20 minutes; the
needle temperature and transfer line temperature were
maintained at 110 ºC and 140 ºC, respectively. The injection
system utilized was the pressure-balanced sampling technique.
The system first pressurizes the headspace vial for 1 minute at
18 psi. Following pressurization, the vial pressure is allowed to
decay onto the column performing a timed sample injection.
The time used was 0.1 minutes which allowed for a 1-mL
volume of headspace to be injected.
The pressure-balanced sampling technique allows for optimu
m analytical results, including enhanced precision, recoveries,
detection limits and inertness.
Within USP method 467, there are two sets of column/oven
conditions, A and B. The data presented here were acquired
utilizing the GC conditions described in procedure A.

Results
The measure of system suitability for class 1 residual solvents is
determined by the signal-to-noise value for each component.
When analyzing class 1 solvents by procedure A, the criteria of
signal to noise for benzene must be greater than 5:1 and the
signal to noise of the other components must be greater than 3:1.
The experimentally determined signal-to-noise values are
presented in figure 1; the signal to noise achieved ranged from
Introduction 11:1 for carbon tetrachloride, a poorly-responding component
The United States Pharmacopeia (USP) has implemented a when FID detection is used, to 143:1 for 1,1-Dichloroethene, with
revised method for the determination of residual solvents, benzene responding at 89:1.
chapter 467; this revision has brought the methodology of USP
467 into close alignment with European Pharmacopeia (EP) Conclusion
method 2.4.24. The USP and EP determination of class 1 and
Demonstrated here are method and data which operate under
class 2 residual solvents is performed with static headspace
the guidance of and fulfill the performance criteria of both USP
(HS) sample introduction and gas chromatography (GC) with
467 and EP 2.4.24 for the determination of residual solvents in
flame ionization detection (FID); class 3 has flexibility in the
pharmaceutical materials. Recent revisions of these methods
technique, however, it is often included in the HS analysis.
have aligned the analytical techniques to allow for a single
The purpose of this paper is to work under the guidance of the method to meet the criteria of both organizations. Within the
USP and EP to achieve the best method possible for the scope of USP chapter 621 and EP chapter 2.2.28, the injection
analysis of residual solvents, while adhering to USP 467 and volume was reduced to improve peak shape and method
EP 2.4.24 criteria. Discussed will be the analysis of class 1 performance; necessary sensitivity was maintained with the
residual solvents. modified method.

46 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

Method 467

Chromatogram
HEADSPACE CONDITIONS
Headspace Unit: TurboMatrix HS
Needle Temperature: 110 °C
Transfer Line Temperature: 130 °C
Oven Temperature: 80 °C
Thermostat Time: 20 min
Vial Pressurization Time: 1 min
Injection Time: 0.1 min
Column Pressure: 18 psig
Vial Pressure: 18 psig

GC CONDITIONS
Headspace: TurboMatrix HS
Needle Temperature: 110 °C
Transfer Line Temperature: 130 °C
Oven Temperature: 80 °C
Thermostat Time: 20 min
Vial Pressurization Time: 1 min
Injection Time: 0.1 min
Column Pressure: 18 psig
Vial Pressure: 18 psig
Gas Chromatograph: Clarus GC
Analytical Column: Elite - 1301
(30 m x 0.53 mm x 3.0 μm)
Injector temperature (or program): 140 °C
Oven Temp 1: 40 °C
Hold: 20 min
Rate: 10 °C/min
Oven Temp 2: 240 °C
Hold: 20 min
Figure 1: Chromatogram demonstrating the performance of the class 1 system-suitability solution.
Rate: End
Detector Type: FID
Detector Temperature: 250 °C

GC/HS Pharmaceutical OVI Application

Consumables Kit
Part No.

N9300655

Contents: Part No.

Save 15% on Elite-1301: 30 M x 0.53 mm x 3.0 μm

Zero Dilution Glass Outer Liner (Cap Injector)
N9316687
N1011445
Zero Dilution Glass Inner Liner (Cap Injector) N1011446
OVI Application Kits* Polyimide-Uncoated Deactivated Tubing (5m x 0.18mm)
Crimp Top Headspace Vials (pkg 1000)
N9301354
B0104236
*Use promotion Code GC020801. See page 45 for details. Offer expires 3/31/09. Assembled Headspace Caps and Septa PTFE B4000022
20 mm Electronic Crimper N9302594
Application notes (New) 09936887

See page 2 for a complete listing of local offices and for ordering information. 47
headspace and headspace trap accessories

For TurboMatrix Headspace

and Headspace Trap

Sample Trays
For use on the Mid-Range or High-Capacity headspace sampler.

Description Part No.

TurboMatrix 40 Mid-Range Sample Tray M0413592
TurboMatrix 110 High-Capacity Sample Tray M0413593

Transfer Lines
Description Tubing i.d. Length Part No.
Siltek Deactivated Fused-Silica 0.25 mm 5m N9316607
Siltek Deactivated Fused-Silica 0.32 mm 5m N9316608

Miscellaneous Accessories
Description Part No.
Gas Chromatography – Theory and Practice, N1011210
Static Headspace Book by L. Ettre and B. Kolb

TurboMatrix 40
Headspace Trap Cold Trap Options
Headspace Trap instruments only.
Sample Head Assembly Replacement Parts Description Part No.
Description Part No. TurboMatrix HS Trap Cold Trap Tube (Carbopack C) N6200150
1 Platinum/Iridium Needle, Wide-Bore B0144169 TurboMatrix HS Trap Air Monitoring Trap* M0413628
Platinum/Iridium Needle, Small-Bore B0500959 *Trap comes standard with the instrument.
Platinum/Iridium Needle, Jet B0510364
Silcosteel Needle, for Headspace Trap Only N6700130
Stainless Steel Needle, Wide-Bore B0131385
Stainless Steel Needle, Small-Bore B0500987 Headspace Sample Head
Stainless Steel Needle, Jet (ships with instrument) B4000011 Assembly Schematic
2 Needle Seal Assembly (without O-Rings) B0500833
3 O-Ring for Needle Seal Assembly (pkg. 10) B0198110
4 Vespel Ferrule 1/16 in. (pkg. 10) 09920127
5 Male Nut 1/16 in. N9302832
6 GLT Adapter Tube B0503956
GLT Adapter Tube, Silcosteel N6700113
7 Graphite/Vespel Ferrule 1/16 in. x 0.4 mm 09920104
For use with 0.25 mm i.d. Transfer Line, pkg. 10
Graphite/Vespel Ferrule 1/16 in. x 0.5 mm 09903700
For use with 0.32 mm i.d. Transfer Line, pkg. 10
1
8 Nut 1/16 in. Swagelok N9300059
9 Fused-Silica Capillary Transfer Line: 9
0.25 mm i.d. x 5 m length N9301356
8
0.32 mm i.d. x 5 m length N9301357 7
6
5
4

Solid Glass Blocking Trap 2

3
Description Part No.
2
Block for use in standard headspace mode. N6701170
3

48 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

 headspace vials/caps
One-step solution – from field sample
to lab results – NEW PerkinElmer
Headspace screw top vials and caps
Headspace Screw Top Vials
and Preassembled Caps
NEW from PerkinElmer, headspace screw top vials and preassembled
caps allows for samples to be taken in the field and directly analyzed
on the TurboMatrix Headspace Sampler* without having to transfer
the sample into another vial. Screw thread vials are designed for a
guaranteed fit.

PerkinElmer cap septa are lot tested and certified for impurities to the
level of 1 ppb benzene. Test conditions use the PerkinElmer TurboMatrix
Headspace FID for the analysis, assuring you of the highest quality to
attain reproducible results.

The cap is conveniently preassembled for ease of use and packed in

clean Mylar® bags to reduce the risk of contamination.

Features and Benefits

■ Samples from field to lab — no transfer necessary
■ No crimping or decrimping tools needed
■ No variation in correct sealing
■ Lot tested and certified septa
■ Easy disposal after use
Headspace Mini Starter Kit
Using only the PerkinElmer lot-tested, certified, approved septa, gives
the analyst the same excellent analytical results that the TurboMatrix Contains the same great consumables as the Headspace Starter Kit but with
Headspace Crimp Vials have always provided. fewer headspace vials. (200 total) 100 each 22 mL Crimp and Screw top vials.

Description Pkg. Part No. Part No.

22 mL Headspace Screw Top Vials* 100 N9306075 N6710197

22 mL Headspace Screw Top Vials* 1,000 N9306078
18 mm PTFE/Butyl Assembled Cap/Septa 100 N9306076
18 mm PTFE/Silicone Assembled Cap/Septa 100 N9306077
*Headspace vials are not compatible with TurboMatrix 40 and 110
Headspace Starter Kit
manufactured before September 1, 2006.
The Headspace Starter Kit contains a variety of headspace consumables so you
can evaluate different types of septa and vials for your sampling requirements.
Part No.

Save up to 15% N6710195

on Headspace Contents:
22 mL Headspace Crimp Vials
Pkg.
100
Qty.
5
Part No.
N9306079

Screw Top Vials** 19 mm PTFE/Butyl Septa/Cap/Springs

19 mm PTFE/Silicone Septa/Cap/Springs
100
100
1
1
B0104239
B0104241
19 mm Aluminum Silicone Septa/Cap/Springs 100 1 B0104243
when purchased in packs of 1,000! O-rings 10 1 B0198110
Needle Seal Assemblies 1 2 B0500833
To qualify, use promotion code: GCHSV408 Pressure Gauge with Needle for Vials 1 1 B0501377
Book by B. Kolb and L. S. Etre; Static Headspace 1 1 N1011210
Save 10% when you buy 5 packs of 1,000! Gas Chromatography Theory and Practice
Save 15% when you buy 10 packs of 1,000! 20 mm Hand Crimper 1 1 N9302785
22 mL Headspace Screw Top Vials* 100 5 N9306075
**Use of the GCHSV408 promotion code is required to receive your discount. Discount 18 mm PTFE/Butyl Assembled Cap and Septa* 100 1 N9306076
cannot be combined with volume purchase agreement discounts, standing order
discounts or other contract pricing. Discounts cannot be combined with promotions 18 mm PTFE/Silicone Assembled Cap and Septa* 100 1 N9306077
available at time of instrument purchase. Expiration date 3/31/09.

See page 2 for a complete listing of local offices and for ordering information. 49
 TurboMatrix Headspace Vials, Caps and

Our exclusive design ensures a safe

operation and guaranteed
fit every time

Hand and Benchtop Crimpers

Description Part No.
8mm Hand Crimper N9306127
11mm Hand Crimper 00090699
11mm Hand Decapper Tool N9301390
20mm Hand Decapper N9301270

Benchtop Vial Crimper N6621006

11mm Crimper Jaws N6621008

Electronic Crimpers
PerkinElmer’s patented vial and cap design incorporates
pressure-relief features which guarantee safe operation Features and Benefits
with the high pressure typically developed during thermostatting. ■ Universal voltage
Ordinary vials and caps without these safety features may burst. ■ Precision control crimping
■ Ergonomically-designed grip
■ Numerous reproducible crimps from a
single charge
22 mL Headspace Vials ■ Includes standard Black & Decker®
22 mL headspace vials give a maximum liquid sample volume of 15 mL. VersaPak® Gold battery and charger
These vials have a greater wall thickness and round base which enables ■ Fully rechargeable
them to withstand pressure up to 60 psig. Low-volume sampling can be
achieved by using a 6 mL crimp vial and vial adapter. The vial adapter is Description Voltage Part No.
compatible with TurboMatrix HS 16, TurboMatrix HS 40 or Headspace
40 XL instruments; however, it is not compatible with the TurboMatrix 20 mm Electronic Crimper Universal N9302594
HS 110 headspace sampler. All PerkinElmer headspace vials are with global mains plug pack
manufactured to specific tolerances that are guaranteed to fit within 20 mm Electronic Decapper Universal N9302595
PerkinElmer instruments. Other manufacturers’ vials do not meet these with global mains plug pack
exact manufacturing specifications and can damage the instrument. 11 mm Electronic Crimper Universal N9302592
Damage to the instrument under these circumstances will void the with global mains plug pack
PerkinElmer warranty agreement. 11 mm Electronic Decapper Universal N9302593
with global mains plug pack
Electronic Crimper Battery N9302585
Rechargable Battery N9302596

50 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

Septa

Choosing the Right Septa

Septa Recommended Temperature Chart
for your Analysis
Upper Temperature
Although a wide variety of septa is available, chemical compatibility and Material Limit at Vial Inertness
temperature are the most critical to the analysis. Temperature applies
not only to the vial, but also to the temperature of the instrument’s Butyl Rubber 100 °C Poor
needle used for pressurization and sample transfer, which is heated to PTFE-Coated Butyl Rubber 100 °C Good
prevent condensation. A needle temperature higher than the vial Aluminum-Coated Silicone 120 °C Good
temperature setting can decompose the septum material. PTFE-coated PTFE-Coated Silicone 210 °C Good
silicone and aluminum-coated silicone offer the highest temperature
operating limits. (See Septa Recommended Temperature Chart)

Only genuine PerkinElmer headspace septa are batch tested for

impurities to the level of 1 ppb benzene for silicone/PTFE, Save up to 25%
butyl/PTFE and aluminum/PTFE septa; the butyl septa is tested
to 20 ppb of toluene. Test conditions use the PerkinElmer on bulk quantity
TurboMatrix headspace FID for the analysis, assuring you of the
highest quality to attain reproducible results. purchases of
Features and Benefits Headspace Vials,
■

■
PerkinElmer septa designed for the patented pressure release cap
Provided in resealing Mylar® bags for cleanliness and storage
Caps and Septa!
■ Available pre-assembled into caps with starsprings Use promotion code: GCHSV408
■ Batch tested to the level of 1 ppb benzene
■ Tested for VOCs

Headspace Vials, Caps and Septa

Description Pkg. Part No.

6 mL Headspace Clear Glass Vial** 125 N9302134
(use with N6120110)
Low Volume Vial Adapter (use with N9302134) 10 N6120110
22 mL Headspace Clear Glass Vial 1,000 B0104236
Butyl Rubber 100 B0159356
Butyl Rubber
Butyl Rubber preassembled
1,000
1,000
B0159357
N1010070
Savings available
PTFE-Coated Butyl Rubber
PTFE-Coated Butyl Rubber
100
1,000
B0104239
B0104240 on packs of 1,000!
PTFE-Coated Butyl Rubber preassembled 1,000 B4000025
Aluminum-Coated Silicone 100 B0104243
Aluminum-Coated Silicone 1,000 B0104244
Aluminum-Coated Silicone preassembled 1,000 B4000028 Bulk quantity discounts are not
PTFE-Coated Silicone 100 B0104241 available on packs of 125 or less.
PTFE-Coated Silicone 1,000 B0104242
PTFE-Coated Silicone preassembled 1,000 B4000022
22 mL Headspace Crimp Top Vials 100 N9306079

Savings available on packs of 1,000. Bulk quantity discounts not available on packs of 125 or less.
Offer may not be used in conjunction with other discounts or promotions. **Not compatible with TurboMatrix Headspace 110.

See page 2 for a complete listing of local offices and for ordering information. 51
thermal desorption

Packed traps specifically

designed for PerkinElmer
Thermal Desorbers

Air Monitoring Trap

Low flow trap packed with carbonaceous sorbents suitable for
ozone precursor and air toxics monitoring.

Cold Traps
TurboMatrix Thermal Desorption Trap Supplies Cold Traps Fittings and Accessories
Trap supplies from PerkinElmer, the market leader in thermal desorption, will Description Qty. Part No.
provide exceptional analytical performance. Used for U.S. EPA Method TO17, the
PerkinElmer standard trap, packed with Tenax™, on the TurboMatrix™ Thermal Graphite Ferrule 2 L4271187
Desorber, will improve productivity and trapping capacity. The TurboMatrix air SilTite™ Ferrule (GC/MS) 0.4 mm 10 N9306093
monitoring trap is packed with carbonaceous sorbents suitable for ozone SilTite™ Ferrule (GC/MS) 0.5 mm 10 N9306094
precursor and air toxics monitoring. SilTite™ Ferrule (GC/MS) 0.8 mm 10 N9306095
SilTite™ Nuts 5 N9306096
Description Qty. Part No. PTFE Ferrule 10 L4275110
Cold Traps for TurboMatrix Graphite/Vespel® Ferrule for ATD 400 5 L1003027
Air Monitoring Trap 1 M0413628 Valco® Graphite/Vespel® Ferrule for ATD 400 5 L1003028
Empty Trap 1 M0413627 Trap Filter Disk L1003030
Tenax™ TA 60/80 Packed Trap 1 M0413535 Trap Packing Disk 20 L4271290
Carbopack® C Packed Trap 1 N6200150 Trap Packing Retaining Spring 5 N6301054
Quartz Wool (untreated) 5g N6102354
Cold Traps for ATD 400 Cold Trap Packing Tool L4271203
Air Monitoring Trap 1 L4275108 Cold Trap Removal Tool L4271205
Trap Nuts (2 required) 1 L4275009 Regulator 0–60 psig N6101474
Trap Tube Low Flow, Empty 1 L4275107 Backflush Nozzle for ATD 400 L4275072
(Narrow-bore at one end. Allows minimum Internal Standard Injection Accessory for ATD 400 L4270010
gas flow during trap desorption) Liquid Nitrogen Accessory for ATD 400 L4270009
Tenax™ TA 60/80 Packed Trap 1 L4275089 Gauze Loading Rig L4070023
Empty Trap 1 L4271106 Replacement Plastic Plunger for Gauze Loading Rig L4071151

52 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

 thermal desorption
Cost-effective,
round-the-clock air monitoring

The Model STS 25 sequential tube sampler is used for the

continuous monitoring of atmospheric concentrations of
volatile organic compounds.
The unit is housed in a compact weatherproof box and allows the
monitoring of indoor and outdoor atmospheres. This convenient
portable unit designed for pumped air sampling of up to 24 tubes,
offers cost-effective, round-the-clock monitoring for the workplace
and ambient air. It can be operated by a 12 V battery or can connect
to 120 V/24 V mains electricity, making it extremely versatile for use in
the laboratory or in the field. The sampler includes cables with jack plug
connectors (for use with the monitoring pump) and a set of diffusion
limiting caps. Maintenance kit and accessories are also available.

Features and Benefits

■ Portability – small, lightweight and compact
■ Variable sampling times – operator adjusted from minutes to hours
■ Sample integrity – diffusion limiting caps block the sample
from contaminants
■ Sampling versatility – heaters are included to prevent condensation

Description Part No.

Model STS 25 Sequential Tube Sampler L4280001
Model STS 25 Maintenance Kit N6609060
Includes; Rotor Tube Seals (pkg. 50), Filter Disks (pkg. 25),
Diffusion Limiting Caps (pkg. 5) and Rotor Seal (pkg. 10)
12 V Rechargeable Battery L4280002
Air Monitoring Pump (120 V) L4271275
Cable (for connecting STS 25 to a generic 12 V battery) L4285007
Diffusion Limiting Caps (pkg. 5) L4285001
Electrical Adapter L4280003 Consumable Application Kits
Allows for direct connection to wall outlet 120 V/240 V.
Also acts as a battery charger for 12 V battery. All your consumable needs in one convenient kit, designed specifically to be used
Rotor Filter Disk L4281023 within the application requirements for Air Monitoring and Ozone Precursor
Viton O-Ring (pkg. 50) L4275033 application notes*.
Air Monitoring Application Kit
Part No.
N6710187

Contents: Pkg. Qty. Part No.

Air Toxics Stainless Steel Thermal Desorber Tubes 10 1 N9307001
Air Monitoring Trap 1 1 M0413628
Methyl Silicone Column 100 m x 0.32 mm x 5 μm 1 1 N6300155

Ozone Precursor Application Kit

Personal Monitoring Pump
Part No.
This compact and lightweight sampler combines convenience
N6710186
and useful functions for accurate sampling.
The personal monitoring pump offers two modes of sampling which are Contents: Pkg. Qty. Part No.
easily activated by turning the selector dial located at the back of the
Alumina PLOT Column 50 m x 0.32 mm i.d. 1 1 N6301107
sampler. Two low-flow modes of sampling allow constant flows from
Air Monitoring Trap 1 1 M0413628
5 – 200 cc/min, as well as constant pressure for multiple
Methyl Silicone Column 50 m x 0.32 mm x 1.0 μm 1 1 N6301108
sorbent-tube sampling from 1 – 350 cc/min (combined flow rates).
* For full downloadable pdf format application notes,
Description Part No. please visit: http://las.perkinelmer.com/applications
Personal Monitoring Pump 5-100 mL/min 110 V N6102351

See page 2 for a complete listing of local offices and for ordering information. 53
thermal desorption

Thermal Desorber
kits and accessories
from PerkinElmer

Thermal Desorber Industrial

Hygiene Application Kit
All your consumable needs in one convenient kit, designed specifically
for Industrial Hygiene using Thermal Desorption*.

Thermal Desorber Starter Kit Workplace Air Monitoring Industrial

PerkinElmer’s convenient starter kit includes all products you need to Hygiene Application Kit**
run the TurboMatrix Thermal Desorber.
Part No.
N6710188
Features and Benefits
■ All items available under one part number in a convenient kit Contents: Pkg. Qty. Part No.
■ Guaranteed PerkinElmer parts Cold Trap O-Ring, 0.145 i.d./0.070 w.d. 1 1 09200091
Cold Trap Tube (Tenax TA) 1 1 L4275089
■ Improved chromatography with exceptional analytical
Empty Glass Sample Tubes – No caps 10 1 L4071594
performance using PerkinElmer parts
Graphite Ferrule 2 1 L4271187
Pen Clips for Stainless Steel Sample Tubes 10 1 L4071029
Part No. PTFE Ferrule 10 1 L4275110
M0413541 PTFE Filter Disk – Either side of the cold trap 10 1 L1003030
Tenax TA Stainless Steel Sample Tubes 10 1 N9307005
Contents: Pkg. Qty. Part No.
* For full downloadable pdf format application notes,
Glass Fiber Separator Disks 6 1 L4271290 please visit: http://las.perkinelmer.com/applications
Glass Sample Tubes 10 1 M0413598 ** Applicable to TurboMatrix 100/150/300/350 and 650 only.
Glass Wool 1 1 54120790
Graphite Ferrules 2 1 L4271187
O-Ring 1 1 L1003006
O-Ring, Viton 1 1 L1003008 Thermal Desorber Caps and Accessories
Packing Gauze 100 1 L4071034
PTFE Filter Discs 10 1 L1003030 Description Pkg. Part No.
PTFE Filter Discs – Large 10 1 L1003029
Brass Long-Term Storage Caps 1 09908851
Retaining Spring 50 1 L4071123
Recommended for long-term storage,
Sample Tube-5 mL 1 1 04970673
two required per tube. Also requires Teflon®
Stainless Steel Retaining Spring 2 1 L6301054
Ferrule (L1003015).
Stainless Steel Sample Tubes – Capped 10 1 M0413595
Combined Teflon® Ferrule 1 L1003015
Tenax TA 60/80, Mesh-15 g 1 1 04978064
For use with 1⁄4 in Brass Long-Term Storage
Trap Tube Nuts 2 1 L4275009
Caps (09908851), two required per tube.
Trap Tubes 2 1 M0410094
Diffusion Caps – Standard 10 L4070207
For passive air sampling, to ensure
correct diffusion path length.
TurboMatrix Upgrade Kit Diffusion Caps with Membrane 10 L4070208
As above, with silicone membrane inserted.
Pen Clips 10 L4071029
Internal Standard Addition/Tube Dry For Stainless Steel Thermal Desorber Tubes.
Purge Add-On Kit PFA Teflon® Ferrules 20 M0413625
This kit adds capability to introduce a known quantity of a gaseous For TurboMatrix Storage End Caps.
standard into the sample tube prior to desorption to verify analyte TurboMatrix Analytical Caps 20 N6200119
recovery. Standard gas is added to the tube in the sampling direction, PTFE caps with o-ring, required for use on
allowing use of tubes packed with multiple adsorbents. the TurboMatrix instrument during analysis.

Requires, but does not include, an options board, when added to the
entry-level thermal desorber. Installation by PerkinElmer Service is
required, but not included. For a full listing of thermal desorber
kits and supplies please visit us at:
Part No. www.perkinelmer.com/gcsupplies

M0413555

54 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

 thermal desorption
Packing material tube
identification and polarity
now on every tube!

Unconditioned Thermal Desorber Tubes

For your convenience, new low-cost thermal desorber tubes are offered
in both stainless steel and glass. Each tube maintains its unique serial
number which is etched for easy identification. Tubes are offered
with a variety of sorbent packing materials for many GC applications
including indoor and outdoor air monitoring, analysis of flavors and
fragrances and the analysis of outgassing from packaging, polymers,
Fully conditioned
pharmaceuticals and semi-conductor material. These tubes are
Thermal Desorber tubes shown
unconditioned and ship with plastic end caps for short-term storage.

Conditioned Thermal Desorber Tubes

Stainless steel and glass sample tubes are available with a wide
Packed Unconditioned Sample Tubes, variety of packing materials from single to multi-bed. PerkinElmer
Thermal Desorber tubes will now be printed with the packing material
Plastic End Caps (pkg. 10) clearly identified on each tube. In addition an arrow will also be printed,
which points to the end of the tube where sample is drawn from, and
Stainless Steel Glass also indicates the end that desorb vapors will exit.
Sorbent Part No. Part No.
Each tube is etched with a unique serial number for ease of traceability
Air Toxics N9307050 N9307058
and adsorbent identification. Stainless steel tubes may also be fitted
Carbopack® B60/80 N9307051 N9307059
Carbosieve® SIII 60/80 N9307052 N9307060 with clips that accept adhesive labels for identification. Packed tubes
Tenax™ GR 60/80 N9307053 N9307061 are shipped with long-term brass storage caps and all PerkinElmer
Tenax™ TA 60/80 N9307054 N9307062 thermal desorber tubes are thermally conditioned and tested for
Chromasorb™ 60/80 N9307055 N9307063 background and backpressure.
Carbopack® B 60/80 N9307056 N9307064
Carbopack® C 60/80 Packed Conditioned Sample Tubes,
Carbosieve® SIII 60/80
Carbotrap® C/B N9307065
Brass Long-Term Storage Caps (pkg. 10)
NIOSH N9307057 N9307066 “NOT for Analytical test applications”, USE N6200119 PTFE caps and
O-ring. (pkg. 20)
Empty Sample Tubes without Caps Stainless Steel Glass
Description Part No. Sorbent Part No. Part No.
Stainless Steel (pkg. 10) L4270128
Air Toxics N9307001 N9307008
Glass (pkg. 10) L4071594
Carbopack® B60/80 N9307002 N9307009
Stainless Steel (pkg. 100) L4270129
Carbosieve® SIII 60/80 N9307003 N9307010
Tenax™ GR 60/80 N9307004 N9307011
Empty Sample Tubes with Caps Tenax™ TA 60/80 N9307005 N9307012
Description Part No. Chromasorb™ 60/80 N9307006 N9307013
Carbopack® B 60/80 N9307000 N9307007
Stainless Steel (pkg. 10) M0413595
Carbopack® C 60/80
Glass Lined Stainless Steel (pkg. 10) M0413597
Carbosieve® SIII 60/80
Glass (pkg. 10) M0413598
Carbotrap® C/B N9307026
NIOSH 2549 N9307038 N9307037

See page 2 for a complete listing of local offices and for ordering information. 55
 Hydrogen and Air Gas Generators

New and Improved

next generation
Generators for your
application needs
No Maintenance Hydrogen Generators
A Safe Source of Hydrogen
Both the PGX-H2 and the No Maintenance Hydrogen Generators have an auto shutoff
procedure that places the units in standby in the event of an internal error and
selectable alarms allow the user to be informed whenever operating conditions vary
from the set point.
PGX-H 2 Hydrogen Generators The No Maintenance (NM-H2) Hydrogen Pure Gas Generators employ the newest
membrane technology available for electrolytic production of pure hydrogen gas,
Pure gas hydrogen generator employ the newest membrane including exclusive no maintenance auto-drying technology.
technology available for the safe production of pure hydrogen gas.
This patented design is ideal for operation with gas analyzers, as fuel
gas for flame tools, or as a source for pure hydrogen in plasma Technical Specifications for No Maintenance
chambers and other isolated environments. Electrolytic membrane
technology is preferred over alternative hydrogen generating Electrolysis cell PEM Membrane type
techniques because it is clean, requires less maintenance and there is H2 purity 99.9999%
no need to store chemicals to maintain operation. The generators offer
silent operation and require only deionized or distilled water with no Auto Drying System No maintenance of drying cartridges
caustic solutions that can affect the purity of the hydrogen. (exclusive system)
Delivery pressure 155 psig - 10 barg (max.)
H2 flow rate Adjustable, according to model
Technical Specifications for PGX-H2 (100 - 160 - 250 - 300 - 500 - 600 - 1000 mL/min)
Safety Auto shut-off
Electrolysis cell PEM Membrane type
User interface Set points, system status
H2 purity 99.9999%
Display 4 row x 34 character LCD, set points, status, alarms
Delivery pressure 100 psig - 7 barg (max)
Indicator lights Power ON, System OK, System error
H2 flow rate Adjustable, according to model
Options Remote control
(100 - 160 - 250 - 300 - 500 - 600 mL/min)
Cascading via RS-485 of up to 32 units in parallel
Safety Auto shut-off for models 250 and 500 only (patented feature)
User interface Set points, system status
Display 4 row x 34 character LCD, set points, status, Description Part No.
alarms
100 mL/min of hydrogen N9307070
Indicator lights Power ON, System OK, System error 160 mL/min of hydrogen N9307071
Outputs RS232C, bi-directional 250 mL/min of hydrogen N9307072
500 mL/min of hydrogen N9307073
Options Remote control
1000 mL/min of hydrogen N9307074
Cascading via RS-485 of up to 32 units in parallel
for models 250 and 500 only (patented feature)
Accessories
Description Part No.
Description Part No.
Cable for Cascading N9307093*
PGX-H2 100 mL/min of hydrogen N9306058 I/O Board N9307094
PGX-H2 160 mL/min of hydrogen N9306059 Remote control RS-232 N9307095*
PGX-H2 250 mL/min of hydrogen N9306060 (Includes converter, cables, software)
PGX-H2 500 mL/min of hydrogen N9306061 Auto refill N9307096*
PGX-H2 Desiccant Cartridge, Fitting and Refill Kit N9306064 Deionizer LE bag N9307097
PGX-H2 Desiccant Refill (sufficient for 3 cartridge refills) N9306065 Triangle deionizer LE bag N9307098
PGX-H2 Deionizer Bag N9306066 *Requires I/O Board

56 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

Zero and Ultra Air Generators
The Zero / Ultra Zero Air Generators produce laboratory grade purified
air for FID (flame ionization detectors) and other detectors. Designed
with safety and convenience in mind, this system will generate purified
and hydrocarbon free air from an existing in-house oil-free compressed
air supply, eliminating the need for inconvenient high-pressure gas
cylinders. Eliminating gas cylinders reduces annual operating costs
associated with materials, labor, and down-time.

The Zero / Ultra Zero Air Generator series removes HC pollutants to

less than 0.1 ppm, and all forms of particles. Operation of the WALL
generator requires low levels of electrical power consumption. This MOUNTABLE
complete turnkey system is engineered with the highest quality
components, is easy to install, and requires minimal annual
maintenance. The Ultra Zero Air Generators will remove CO and HC
pollutants to less than 0.1 ppm, and NOx contaminants to 1 ppm.
Carbon dioxide is also removed to about 1 ppm levels.
Ultra Zero Air Generators
Specifications for Zero Air Features and Benefits
Part No. N9307075 N9307076 N9307077 N9307078 N9307079 ■ Flow rate: < 0.1 ppm HC; < 0.1 ppm CO; < 1 ppm NOx; < 5 ppm CO2
Outlet 1500 3000 6000 15000 30000 ■ Produce laboratory-grade purified air for the most accurate and
Zero Air mL/min mL/min mL/min mL/min mL/min convenient calibration of testing equipment
Maximum 1.5 L/min 3.0 L/min 6.0 L/min 15.0 L/min 30.0 L/min ■ Designed with safety and convenience in mind, this system will
Continuous generate purified air from an existing in-house oil-free compressed
Output
air supply, eliminating the need for inconvenient high-pressure
Flow Rate
gas cylinders
Electrical 230/115 VAC 230/115 VAC 230/115 VAC 230/115 VAC 230/115 VAC
Requirements 250 W max 250 W max 250 W max 480 W max 480 W max ■ Eliminate gas cylinders reducing annual operating costs associated
Temperature / N/A Included Included Included Included with materials, labor and downtime, and reduces risk of injury
Pressure to workers
Control Board ■ Will remove CO and HC pollutants to less than 0.1 ppm and NOx
contaminants to 1 ppm. Carbon dioxide is also removed to about
1 ppm levels. Operation of the generator requires low levels of air
Description Part No. consumption and electrical power
■ Fully supported by PerkinElmer Service Organization
1.5 L/min of air (without compressor) N9307075
3.0 L/min of air (without compressor) N9307076
6.0 L/min of air (without compressor) N9307077
15.0 L/min of air (without compressor) N9307078 Specifications for Ultra Zero Air
30.0 L/min of air (without compressor) N9307079 Part No. N9307081 N9307082 N9307083 N9307080
Outlet Ultra Zero Air 1500 mL/min 3000 mL/min 6000 mL/min 15000 mL/min
Outlet Carbon Dioxide < 5 ppm < 10 ppm < 10 ppm < 10 ppm
Concentration
Specifications for Zero and Ultra Zero Air Outlet Nitrogen Oxides
Concentration
< 0.1 ppm < 1 ppm < 1 ppm < 1 ppm

Outlet Hydrocarbon Concentration < 0.1 ppm Outlet Dewpoint < -70 °C < -50 °C < -50 °C < -50 °C
Outlet Carbon Monoxide Concentration < 0.1 ppm Electrical 230/115 VAC 230/115 VAC 230/115 VAC 230/115 VAC
Outlet Particles < 0.5 Microns Removed 99.99% Requirements 270 W max 270 W max 270 W max 500 W max
Outlet Air Temperature Ambient +15 °C
Max Inlet Hydrocarbon Concentration 100 ppm Description Part No.
Maximum Outlet Pressure 6.5 bar
Max Inlet Carbon Monoxide Concentration 50 ppm 1.5 L/min of air (without compressor) N9307081
Max Inlet Temperature 40 °C 3.0 L/min of air (without compressor) N9307082
Inlet Pressure Range (regulated to 7 bar) 4.5–10 bar 6.0 L/min of air (without compressor) N9307083
Inlet Port 1/4" NPT 15.0 L/min of air (without compressor) N9307080
Outlet Port 1/8" NPT All models come WITHOUT a compressor.
Oil Free Compressor Required.

See page 2 for a complete listing of local offices and for ordering information. 57
 Introducing EcoAnalytix from PerkinElmer

The New Measure of Success

EcoAnalytix TM is PerkinElmer’s collaborative problem-solving initiative

that creates application-based solutions for supporting local,
regional and global projects. It is through these focused solutions
that PerkinElmer contributes to protecting and improving our world.

Application Development Centers Community Outreach

Two new PerkinElmer EcoAnalytix Application Development Centers PerkinElmer’s EcoAnalytix program encourages local and global
(ADC), in Shanghai and Mumbai, have been established and are advocacy and partnerships for ecosystemic excellence on all levels.
being resourced to help facilitate support of responsible growth
within the industry and to support rapidly growing infrastructure PerkinElmer is working with and through customers, local governments
in developing countries. and NGOs and the public to generate awareness of topics of
importance to global health and well-being to people across the world.

PerkinElmer’s EcoAnalytix PerkinElmer’s Commitment to

What is Eco? Environmental Responsibility
“Eco” is derived from the idea of an ecosystem – a defined group of interdependent PerkinElmer is dedicated to ensuring that its facilities and employees
entities existing together within the environment they inhabit or depend on. operate in a manner that is environmentally conscious and contributes
to a better world.
Why Eco?
Because we want our customers to understand that we view their businesses PerkinElmer facilities are taking an active role establishing programs to
as complete, unique and contributing ecosystems. minimize impact on the environment. Whether in the laboratory,
production facilities or other operations, the company is designing safe
What is Analytix? products and processes that prevent pollution, conserve resources and
reduce waste. Employee involvement is integral to the continuous
“Analytix” refers to the process of analyzing and providing measurement of
improvement of environmental safety and health programs.
the ecosystem – anything that we consume, breathe, see or touch.
EcoAnalytix is more than analytical solutions. It is training, SOPs,
What is EcoAnalytix? regulatory leadership, community outreach and industry collaboration,
Combined, “Eco” and “Analytix” refer to the analytical measurements of our all working together to get you to better answers faster. A new way of
entire world. viewing your world, your needs — your business ecosystem.

Why EcoAnalytix?
Because only PerkinElmer can best help our customers make a measurable difference.

58 CALL TODAY AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

EcoAnalytix Application Focus
The EcoAnalytix initiative focuses on three primary application areas
that are integral to global health and well-being: Biofuels Development,
Environmental Analysis and Food Safety.

Biofuels Development
EcoAnalytix solutions from PerkinElmer can help you achieve your business PerkinElmer knows that the right training, methods, applications,
and operations objectives, from the field through to processing, and from reporting and support are as integral to getting answers as the
fermentation to the final product, while ensuring the quality of biofuels and instrumentation. That’s why PerkinElmer has developed a novel
meeting regulatory requirements. Pre-defined analyzers and platforms support approach to meet the challenges that today’s labs face — that
both ASTM and EN methods. approach is called EcoAnalytixTM.
PerkinElmer’s Latest Biofuels Testing Analyzers include:
■ EcoAnalytix Biodiesel Glycerin and Methanol Analyzer - based on the Clarus
500 GC with an innovative dual-oven design and a TurboMatrix™ Headspace,
offering a unique solution to test for free/total glycerin and residual methanol
according to EN and ASTM standards

Environmental Analysis
EcoAnalytix analyzers and platforms for environmental analysis from PerkinElmer
provide methods, guidebooks and standard operating procedures where
necessary so that you can keep pace with regulatory change. We provide
industry leading environmental monitoring technology as well as renowned
expertise and advocacy that shape regulatory methods.
EcoAnalytix water quality platforms will provide specific analyzers and
methodologies to detect trace metal, organic, pesticide, chemical and radioactive
contaminants in water.

PerkinElmer’s Latest Environmental Analyzers include: PerkinElmer’s Melamine Analyzer

■ EcoAnalytix Polycyclic Aromatic Hydrocarbons Analyzer - based on a complete
preconfigured Series 200 UV/Vis & Fluorescence HPLC system, providing expe-
dited ramp-up and increased uptime for challenging PAH analyses that require
specific regulated methods

Food Quality and Safety

Visit us Online!
EcoAnalytix analyzers and platforms for food safety from PerkinElmer provide
methods, guidebooks and standard operating procedures where necessary to
allow you to simply and quickly meet or exceed an increasing level of scrutiny for
To find out more about
food safety standards in an ever-expanding global food supply chain. EcoAnalytix PerkinElmer’s EcoAnalytix
food safety platforms are designed to assure food quality while ensuring
regulatory compliance. Specific applications include the analysis of foods and solutions, please visit:
food stuffs for melamine, pesticide, organic, chemical and metal contaminants.

PerkinElmer’s Latest Food Quality and Safety Analyzers include: www.perkinelmer.com/

■ EcoAnalytix Melamine Analyzer - based on the Clarus 600 T GC/Mass ecoanalytix
Spectrometer, delivering the first complete solution on the market for this
application using GC/MS technology which includes everything the laboratory
needs for rapid ramp-up

See page 2 for a complete listing of local offices and for ordering information. 59
 PerkinElmer products —
proven quality, reliability
and results.

NEW PRODUCTS PerkinElmer—The Clear Choice in Chromatography

GC-HS Consumables HRes HPLC Columns!

Application Kits High-pressure operating
range up to 10,000 psi.
Save time and money with See pages 6-7 for details.
Regulatory Test Kits!

IR Temperature Gun!
Low-cost, non-contact temperature
measurement with laser sighting.
See page 36 for details.

Gas Filtration Systems!

Protect your capillary columns
with the correct high-quality
Blood Alcohol Materials Testing gas filtration system.
Environmental VOA Pharmaceutical OVI
See pages 34-35 for details.
Food and Beverage See page 45 for details.

AU 1800033391 IN 912225701101 KR 8228685350 SG 6567799555

PerkinElmer Life and Analytical Sciences, Inc.

710 Bridgeport Avenue
Shelton, CT 06484
007949_05