Cotton Contamination
Cotton Contamination
Cotton contamination
To cite this article: M. H. J. van der Sluijs & L. Hunter (2017) Cotton contamination, Textile
Progress, 49:3, 137-171, DOI: 10.1080/00405167.2018.1437008
                   Cotton contamination
                   M. H. J. van der Sluijsa and L. Hunterb,c
                   a
                     Commonwealth Scientific and Industrial Research Organization (CSIRO), Manufacturing, Waurn Ponds,
                   Geelong, Victoria, Australia; bCouncil for Scientific and Industrial Research (CSIR), Port Elizabeth, South Africa;
                   c
                     Nelson Mandela Metropolitan University, Port Elizabeth, South Africa
                       ABSTRACT                                                                          KEYWORDS
                       This review focusses on physical forms of contaminant including the               Cotton; contamination;
                       presence, prevention and/or removal of foreign bodies, stickiness and             foreign fibres; seed-coat
                       seed-coat fragments rather than the type and quantity of chemical                 fragments; harvesting;
                       residues that might be present in cotton. Contamination in cotton,                ginning; spinning; quality
                       even if it is a single foreign fibre, can lead to the downgrading of
                       yarn, fabric or garments, or even to the total rejection of an entire
                       batch and can cause irreparable harm to the relationship between
                       growers, ginners, merchants and textile and clothing mills.
                       Contamination thus continues to be a very important cotton fibre
                       quality parameter in the production pipeline, with countries and
                       cotton that are perceived to be contaminated heavily discounted. At
                       the same time, spinners are implementing various methods to detect
                       and eliminate contamination. Given the adverse effect on processing
                       and product quality arising from contamination, it was considered
                       important to compile a review of published work and knowledge
                       relating to the incidence, detection, measurement, consequences and
                       reduction of contamination.
                   1. Contamination
                   1.1. Introduction
                   Due to the increasing demands of modern spinning, in terms of speed, automation and
                   raw material cost and the increasingly competitive global textile market, cotton fibre qual-
                   ity, in terms of length and uniformity, strength, micronaire value, trash content, colour
                   grade and the presence of extraneous matter (any substance in the cotton, other than
                   plant material such as bark, grass, seed-coat fragments, dust and oil), is of the utmost
                   importance to the spinner. In addition, the presence of contaminants in the cotton, partic-
                   ularly foreign fibre, can greatly affect its perceived quality and value. Various contami-
                   nants, such as paper, plastic, feathers, etc., as described in Table 1, can be inadvertently
                   incorporated into the cotton bale often as a result of human interaction during harvesting,
                   ginning and baling, and even in the spinning mill itself [1,2]. Such contamination, even if it
                   is a single foreign fibre, can lead to the downgrading of yarn, fabric or garments, and/or
                   even to the total rejection of an entire batch, resulting in large financial claims and losses,
                   which can cause irreparable harm to the relationship between growers, ginners, mer-
                   chants and textile and clothing manufacturers. Depending upon its nature, the spinning
                   and fabric processing method and route as well as the end use, contamination can
                   adversely affect textile processing efficiencies due to end breakages during yarn and fab-
                   ric formation, cause damage to processing equipment (such as beaters and wire) and
                   even cause fire in the mill. More generally, in terms of the textile being produced, contam-
                   ination can adversely affect the appearance of the yarn, fabric and final product [3–5],
                   especially in fine count yarns [6], resulting in such products having to be sold as seconds.
                       It has been stated that even though the levels of foreign-fibre contamination in cotton
                   have been drastically reduced due to the routine application of various corrective actions,
                   it still represented the number one problem for manufacturers of high-quality cotton
                   products [7,8]. Figures 1 and 2 show some examples of contaminated yarns and fabrics.
                   Contaminants have also even been found in classing samples which are collected at the
                   gin after bale formation – see Figure 3. It is also worth mentioning, that contamination
Figure 2. Examples of contaminants in cotton knitted fabrics (Cotton Incorporated and CSIRO).
                   can occur, and present a serious problem, in most other natural fibres, such as wool and
                   mohair, but seldom in man-made fibres.
                      In the light of the above, it is not surprising that there are serious penalties imposed on
                   the vendors for contamination in cotton [9]. In 2002, the International Textile Manufac-
                   turers Federation (ITMF) reported that claims, due to contamination in cotton, amounted
                   to between 1.4% and 3.2% of total cotton and blended yarn sales. Recognizing the slim
                   margins on which spinning mills operate, these figures illustrate the serious effect which
                   contamination can have on spinning mill profit margins [10]. In fact, it was reported in
                   2015 that contamination related losses amounted to US$200 million per year worldwide
                   [11]. A study conducted by Ahmedabad Textile Industry’s Research Association (ATIRA)
                   showed that 70% of knitted fabric complaints produced from 20 tex combed yarns were
                   due to contamination, with 80% of the contamination due to human hair and jute and
                   14% due to coloured cotton fibre [12]. It has also been stated that the presence of col-
                   oured fibres in fabrics can result in bleeding during bleaching, requiring the now larger
                   affected sections of the finished fabric to be removed or the finished fabric to be replaced
                   or redyed with other colours [13]. It has also been reported that contamination-related
                   complaints and claims amount to approximately 15% of all yarn complaints [14]. It has
                   been stated that the more steps there are in the spinning process, the more difficult it is
                   for any foreign fibre to be detected as the distance between any such foreign fibres
                   increases with the number of stages, due to increased drafting ratios. For example, the
                   distance between foreign fibres is longer in combed ring-spun yarns than in rotor-spun
                   yarns [15].
                      The issue of contamination is nothing new, and spinning mills have for a long time
                   lodged complaints and produced evidence of contamination found in cotton bales they
                   have purchased, with the first recorded official complaint raised as far back as 1909 [16].
                   Indeed, there is a feeling amongst mills, which is borne out by the ITMF Contamination
                   Surveys, that contamination is increasing and that the cotton trade (growers through to
                   merchants) has not done enough to eliminate or reduce the incidence of contamination
                   [17,18]. There are, however, no established international or universal standards relating to
                   contamination size and frequency. As a consequence, the more quality-conscious spinners
                   have defined their own allowable levels of contamination, and developed a range of
                   screening protocols in order to assess the contamination risk associated with the various
                   sources or origins of cotton [19–21]. Most end-users even go so far as to demand a zero
                   level of contamination.
                      Levels of contamination are classifiable: the weight of contaminants in cotton bales can
                   range from 1 to 100 g/tonne with contamination rates of 1–4 g/tonne considered low, 5–
                   15 g/tonne moderate and above 20 g/tonne as high [9,22]. It has been suggested that, if
                   the level of contamination is <1 g/tonne, and all other remediation controls are in place,
                   the contamination in fabric and garment would be minimal. Although, at 0.001% by
                   weight, such level of contamination appears to be extremely small, it must be remem-
                   bered that contamination is quantified by the number and frequency of incidents, rather
                   than by their weight, and 0.001% by weight can equate to as many as 15,000 foreign
                   fibres [23–25].
                      To illustrate the serious losses which can be suffered as a result of contamination, it has
                   been calculated that, during processing, a 5-g piece of polypropylene twine in a cotton
                   bale could be fragmented into some 10,000 fibres and lead to financial losses exceeding
                   US$25,000 in the case of quality apparel and US$53,000 in the case of high-quality down-
                   proof covers [3,26]. Another case showed that a spinner, who purchased a bale of cotton
                   for US$600, made it into yarn and sold the yarn with foreign fibres that were only detected
                   after bleaching and dyeing, was required to pay US$7,320 in damages [27]. From the
                   above examples it is clear that contaminants remaining undetected until found in sewn
                   and finished goods result in the most costly penalties because of the number of process-
                   ing steps that have been undertaken and the value that is expected to have been added
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                   to the fibres by that stage. It has been stated that losses can be at least 1000 times greater
                   at the later stage than if the contaminants were detected and removed from the bale prior
                   to processing [28].
                       As blending of cotton lint from various parts of the world is a standard practice for spin-
                   ning mills, it is often difficult for a mill to pinpoint the origin of the contaminants, once an
                   incident has occurred or complaint has been received. Nevertheless, through the practical
                   experience of mill staff and from industry hearsay, cotton purchases from origins that are
                   known, or perceived, to be contaminated, are either avoided or the use of those growths
                   by the mill minimized. This is not always easy because the majority of cotton is produced
                   in Asia from which the most heavily-contaminated cottons originate [5]. Once an origin
                   has achieved a reputation for contamination, the likelihood of it achieving base world
                   market prices is slim, and cottons from that origin are usually heavily discounted, with dis-
                   counts ranging from 5% to 30%, even if the fibre quality is acceptable [19,22,23,29]. For
                   example, it has been stated that contamination is the biggest issue facing Indian cotton
                   [30,31] and that India and Pakistan are losing 10%–15% of the export value of their raw
                   cotton, totalling over US$500 million per year, due to contamination [20]. Another report
                   by the State Bank of Pakistan, estimated that contamination in the Pakistani cotton crop is
                   responsible for an annual loss of between US$1.4 and US$3 billion in export earnings, due
                   to discounted fibre, yarn, fabric and garments [32]. In order to minimize the effect of con-
                   tamination, the Pakistani government in 2002 introduced a ‘contamination-free cotton ini-
                   tiative’ which required textile mills to pay a premium of 63% for zero-contaminated fibre
                   [33]. Similarly, a large Indian vertically integrated textile and clothing manufacturer offers
                   Indian suppliers premiums of US$5 and US$2.4 per bale ‘for good and fair’ contaminated
                   cotton respectively, as judged by their contamination index [19]. Another large Indian
                   spinning company employs contract farming both to ensure supply and to reduce con-
                   taminants, resulting in a drop in the amount of contamination from a level of 18-20 g per
                   bale to <1g per bale [34]. Also, some mills will not, unless heavily discounted, purchase
                   hand-picked cotton due to the typically high incidence of contamination [9,13,22,35]
                   despite the fact that hand-picked cotton generally has fewer neps, fewer short fibres
                   and better length uniformity. This type of experience in India and Pakistan is in
                   contrast to that of Australia and the US, which continue to achieve premiums for their cot-
                   ton due to their reputation for having low contamination levels [1,2,35–38]. A survey con-
                   ducted in 2011 found that mills using such low-contamination cotton could demand a
                   premium of between 2 and 20 US cents/kg for their yarn due to the guarantee of being
                   able to deliver contaminant-free yarn for use in high-quality garments and light/pale
                   shades [37].
                   unfortunate as it has been stated that the type of contaminants have changed from the
                   late 1970s to 1990 [28].
                       The ITMF defines 16 categories of contamination, which are listed in Table 1. In the
                   ITMF survey, mills are asked to indicate the sources of contamination according to the 16
                   categories and to indicate in each category whether the contamination level was non-
                   existent/insignificant, moderate or serious. Essentially therefore, the survey records the
                   perception of spinners and should be regarded as akin to an ‘opinion poll’; whilst not
                   based on scientific evidence, even so it can still be considered a valuable source of infor-
                   mation and data for the industry [39,40]. It must be borne in mind that there are contami-
                   nants such as rocks, stones, human hair and other types of material that may be present
                   in bales of cotton that are not covered by the ITMF categories.
                       Across all growths, the incidence of contamination labelled ‘moderate’ or ‘serious’ (see
                   Table 2 and Figure 4) increased steadily from 14% of all bales surveyed in 1989 to 26% in
                   2003, followed by a decrease to 22%, stabilizing at this level between 2005 to 2009. This
                   was followed by a slight increase to 23% in 2011, a further increase to 26% in 2013 and
                   then a reduction to 23% again in 2016 – see Figure 4. What is notable in Figure 4 is the
                   steady increase in reported contamination worldwide after 1993, which is largely attrib-
                   uted to spinners becoming more aware of contamination as the number of complaints
                   received from fabric and garment manufacturers increased, as well as consumers becom-
                   ing more quality conscious [18]. Within this context, it is important to note that the instal-
                   lation of automatic detection systems in the spinning mills also began to provide more
                   accurate information on the type and frequency of contamination. A contributing factor
                   to the rise could also be that increasing automation and the subsequent reduction in
30
25
% contaminated coon 20
15
10
Year
                   labour (i.e. human intervention) led to reduced human vigilance and fewer opportunities
                   for operatives to detect and eliminate contaminants, specifically in the ginning and spin-
                   ning mills [3,28,41,42].
                       Table 2 gives the worldwide averages per contamination category recorded during the
                   various surveys [18]. As can be seen in Table 2, the major type of contamination in all cot-
                   ton bales continues to be organic matter such as leaves, feathers, paper and leather,
                   whose contribution has steadily increased as a proportion of total contamination from
                   30% in 1989 to a high of 55% in 2013, then decreasing to 47% in 2016. The next most
                   prevalent contaminants are pieces of fabric and string made from woven plastic and plas-
                   tic film, followed by jute/hessian, which originate from bale covers and picking bags and
                   cotton both natural and coloured, mainly from bale covers but also from apparel, cleaning
                   rags and module ropes. The next highest contributor is inorganic matter such as sand/
                   dust, rust and metal wires, which is followed by oily chemical substances such as grease
                   and oil, contamination by which is mainly due to excess lubrication, worn seals and
                   hydraulic oil leaks during harvesting and ginning, stamp colour (mainly due to using per-
                   manent markers to identify modules or bales) rubber and tar. The incidence of oily chemi-
                   cal substances and inorganic matter, such as rust and metal, has remained fairly constant
                   since 1989.
                       Fabric and string contaminants mainly originate from module covers for both conven-
                   tional and round modules, plastic shopping bags and fertilizer bags, agricultural mulch
                   film, plastic twine, irrigation tubing and to a large extent from bale covers damaged dur-
                   ing warehousing and shipping [41,43–45]. The incidence of plastic contaminants has
                   become a major problem in the US as well as in other countries that have adopted the
                   new John Deere spindle and stripper harvesters; such equipment produces round mod-
                   ules covered with plastic wrap [46–48] with the potential to act as a contaminant source.
                       To improve bale covers and reduce potential contamination, certain countries such as the
                   US and Australia have changed their industry practices, with the US initiating the Joint Cotton
                   Industry Bale Packaging Committee to draw up specifications for bale covers and ties. Only
                   four types of bale covers are approved, namely 100% cotton (both woven and knitted),
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                   having contamination levels of around 4%–5%. According to the results of the ITMF surveys,
                   the most contaminated cottons continue to originate from India, Turkey and certain coun-
                   tries in Africa and Central Asia, with the least contaminated cotton continuing to originate
                   from the US, Israel, Australia and from certain countries in West Africa. The ITMF survey
                   results are very similar to the results of a survey conducted by the National Cotton Council
                   of America in 2008, which showed that cotton originating from the US, Australia, Israel, Bra-
                   zil and certain countries in Africa were perceived to be the least contaminated by US and
                   international mills [53]. Changes in contamination status have also occurred over time. For
                   example, cotton from Zimbabwe was once considered to be one of the least contaminated,
                   whereas it is now perceived as contaminated, demonstrating that continued industry vigi-
                   lance is required to maintain favourable perceptions by potential customers. It is also nota-
                   ble that mechanically-harvested cotton is generally less contaminated, probably due to the
                   lower level of interaction between humans and the cotton during mechanical harvesting
                   and the subsequent ginning processes; hand pickers, for example, use plastic bags to hold
                   the cotton, which can be a serious source of contaminants [6].
                   1.2.1. Limitations
                   It is important to note that there are a number of limitations associated with the ITMF Con-
                   tamination Survey, including the following:
                      (1) The number of companies participating in the ITMF Contamination Survey and the
                          number of evaluations have declined steadily since 2005, with only a small number
                          of spinning mills from Asia participating, despite the fact that when considered on a
                          worldwide basis, this is where the majority of cotton is consumed.
                      (2) Participating mills make a largely subjective assessment of the contamination found
                          in the cotton from a particular source, and this applies also as to whether they
                          regard the occurrence of the contamination as insignificant, moderate or serious.
                          The ITMF methodology states that the ‘basic statistical unit (the sample) of this sur-
                          vey is a spinners assessment of a given description of cotton which it had consumed
                          during the last 12 months’.
                      (3) The Survey is unable to quantify the number or proportion of bales actually affected
                          by contamination.
                      (4) Low overall levels of contamination can conceal the presence of higher levels of
                          particular contaminants, as each category is given equal weighting in determining
                          the average contamination level.
                   and eliminate contaminants. Contamination in cotton occurs in many types, shapes and
                   sizes and, while larger pieces of contaminants are more likely to be removed during proc-
                   essing, each mechanical process to which the cotton is subjected in opening, cleaning
                   carding and combing has the potential to reduce the size of the contaminants. The even-
                   tual result is a large number of fragments, particles or fibres, depending on the original
                   form of contamination, the latter being particularly problematic. Foreign fibres, when
                   present, tend not to be distributed uniformly across the contents of a bale or across bales;
                   generally, or initially at least, they form clusters which are very much dependent on the
                   particular process and machinery used, the type of raw material and the machine settings
                   [6]. It is worth noting that the vast majority of contaminants remain intact during the
                   opening and cleaning stages in the blowroom, but then become fragmented later. Fur-
                   thermore, although some contaminants are removed during the carding and combing
                   processes [55,56], the large majority are severely fragmented during carding, mainly due
                   to the action of the revolving flats [8,57–59]. The resulting smaller pieces and fragments
                   are difficult to remove and can remain largely undetected, only becoming noticeable in
                   subsequent processing stages and quite late in the conversion process. This type of con-
                   tamination can lead to drafting issues during drawing, roving and spinning, resulting in
                   end-breakages during the roving and spinning processes, or more costly and in the worst
                   case, it may only be detected once the finished fabric or garment is inspected before sale.
                   It has also been stated that some 20% of machine stops during sectional warping are
                   caused by foreign fibres [60].
                   The actual principles and techniques applied for the detection of contaminants in cotton
                   often differ according to the nature of the contaminants to be detected (e.g. dyed or
                   undyed polypropylene) and at what stage(s) in the processing pipeline detection and
                   removal are to take place. Some examples are as follows:
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                   true for hand-picked cotton and in countries where labour costs are comparatively low,
                   with gins employing large numbers of people to feed and operate the gin [12,77,78].
                      Contamination detection-and-removal systems, developed originally for spinning mills,
                   have been applied in gins since the early 2000s. Nevertheless, despite their successful
                   application in Greece [79], the systems, or the sensors they employ, have not performed
                   well to date in high-volume and physically-harsh ginning environments (in terms of dust
                   and heat) [80]. Moreover, there is no immediate incentive, financial or otherwise, to the
                   grower or ginner, to cause them to take more precautions to avoid and minimize contami-
                   nation in baled cotton, despite the poor reputation and subsequent problems it causes in
                   the longer term [57,81]. Furthermore, there is a large cost associated with adapting the
                   particular systems originally designed for application in a spinning mill environment to
                   cope with the conditions that exist in a gin [80]. It has however been stated that cleaning
                   equipment installed in modern gins can potentially remove large contaminants that are
                   mixed in with seed-cotton [24,79] and this seems to be the case in India where a number
                   of gins have installed such systems with a 40–45% cleaning efficiency [82]; a typical layout
                   of such a modern saw gin is shown in Figure 7.
                      A number of studies were conducted in the US during 2015 and 2016, to determine the
                   efficiency of the ginning process in removing plastic sheet material of different types and
                   sizes. These studies showed that cylinder-type cleaners (rotating cylinders with spikes to
                   convey seed cotton across grid bars) removed some 10% of plastic contaminants, while
                   extractor-type cleaners (mainly the stick machine, where rotating saws hold the cotton
                   while centrifugal force removes larger foreign matter such as burrs and sticks), removed
                   56% of plastic with 17% found in the lint, the level of removal depending upon the type
                   and size of the plastic as well as on airflow and processing rates [47,83–85].
                      From the above, it is clear that it is preferable if not imperative to avoid contaminants
                   entering the ginning process in the first place, one solution being to install a camera in
                   the module feeder that automatically detects and alerts gin operators to the presence of
                   large pieces of contamination caught on the module beaters. The CSIRO Module Hood
                   Contamination Sensor, which alerts ginners and also provides a time stamp on
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                   contamination as it enters the gin, has been installed in 27% of Australian gins since the
                   2012 ginning season [47], with a similar camera-based system being trialled in the US dur-
                   ing 2016 [46]. Further research in this area is continuing with various systems for the
                   detection of plastic in seed-cotton being investigated including using ion mobility, UV
                   fluorescence, visible and near-infrared and short-wave infrared [46,86–89]. The detection
                   of contamination is obviously an important part of the solution, but the question remains
                   as to whether the ginners would be willing to stop production to remove the contami-
                   nants once they have been detected.
                   Figure 9. Operators patrol a bale laydown to remove contamination from bales (CSIRO).
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Figure 10. Manual removal of contaminants from cotton prior to processing (CSIRO).
                   yarn. It was estimated that up to 2004, the installation of foreign matter detectors in spin-
                   ning mills cost the industry in excess of US$150 [10,19,21,44,92]. It has been stated that
                   excluding yarn clearers, spinning mills had, since 1990, invested over US$500 million on
                   systems to detect and remove contaminants in cotton [93]. At an average cost of
                   US$250,000 to US$500,000 per unit, such outlays would increase the cost per bale of cot-
                   ton by between US$5 and US$10 [5,11].
                      Careful control of waste recycling and of machine maintenance in the spinning mill are
                   also paramount to avoid the accidental introduction of contaminants into the process
                   [35,82]. Furthermore, spinning mills that produce yarns from various fibre types, blends
                   and even dyed material, either sequentially or simultaneously, need to have procedures in
                   place to ensure that all the machines are adequately cleaned prior to starting up a new
                   run, as well as to ensure that the different fibres are segregated to minimize contamina-
                   tion due to loose fly [82]. UV lights installed in the packing and inspection departments
                   can assist in detecting chemical/oily substances and foreign fibres, including synthetic
                   (man-made) fibres that fluoresce [35] – see Figure 11.
                      Contamination detection and removal systems installed in the blowroom prior to card-
                   ing are common and form a critical component of the blowroom, with these systems nor-
                   mally installed at the beginning of the blowroom line, after coarse cleaning and initial
                   opening of the fibre and before the final cleaning stage; however, a number of spinning
                   mills have also installed a second machine at the end of the blowroom line [74,92,94]. The
                   first contamination detection and removal system became available on the market in the
                   early 1990s and was based on the CSIRO Dark Lock Sorter patent, originally developed for
                   the wool industry. Current systems, such as those manufactured by UsterÒ Technologies
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Figure 11. Inspecting cones of yarn for contaminants under UV lights (CSIRO).
                   AG (Uster, Switzerland), Tr€ utsczhler GmbH & Co. Kg (Mo€nchengladbach, Germany), Vetal
                   Textiles And Electronics Private Limited (Coimbatore, India), Loptex Italia S.r.L. (Montano
                   Lucino, Italy) and Barco NV (Kortrijk, Belgium), detect contaminants by means of using
                   acoustic, optical and colour sensors. These sensors can, depending on the particular sys-
                   tem, detect coloured, white, colourless and even transparent fibres as the material passes
                   through a viewing chamber after initial opening and before the final cleaning stage before
                   carding. When a contaminant is detected, it is measured (registered) and then pneumati-
                   cally removed via an alternative material-flow outlet [92]. Despite the fact that there are
                   estimated to be over 5000 contamination detection and removal systems installed world-
                   wide [35,57,59], they continue to be rather expensive and require highly-skilled techni-
                   cians for their operation. There are also issues with their capacity as well as with the
                   amount of good fibre that is extracted together with the contaminants being ejected
                   [5,9,41,91], with older systems removing 100–120 kg and newer systems 30–40 kg per day
                   of good fibre [95].
                      In 2004, it was reported that the equivalent of 25% of the global cotton consumption
                   was processed through contamination detection and removal systems installed in the
                   blowroom [21], with the present authors estimating that up to 80% of all cotton currently
                   consumed globally is processed through these systems. It has, however, been stated that
                   these systems remove only around 60%–75% of contaminants, their degree of effective-
                   ness being dependent on the positioning of the system (at the beginning or end of blow-
                   room line), the degree to which the fibre is opened prior to the attempt at detection, the
                   size and colour of the contaminants, the production rate and the possible number of air
                   blasts per hour (by pneumatic valves) that are able to be delivered by the equipment to
                   remove the contaminants [4,5,8,9,17,25,41,43,61,73,90,92].
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Figure 12. Blowroom equipped with UsterÒ Jossi Vision Shield (UsterÒ Technologies AG).
                      In addition to the foreign-matter detectors installed in the blowroom, there are devices
                   on the market that can be added to the creels of drawing and lapping machines, which
                   detect foreign fibres (of a different colour) and stop the machine for removal of the con-
                   taminant by the operator [42,48,76,82,96]. Figure 12 shows an example of a modern blow-
                   room contamination detection and removal system.
                   material ranging from 1 cm2 down to 0.001 cm2 in size and are therefore considered to be
                   the most reliable for contamination detection and removal [8,76]. In 2006, 75% of yarn
                   clearers installed on winding machines worldwide (excluding China) had foreign-fibre
                   detectors fitted [91]. The actual number of such installations will be greater today, given
                   the modernization of the Chinese spinning industry. The types of contamination removed
                   and the efficiency of their removal depend on the sensors employed and also the specific
                   yarns they monitor. The disadvantage of these systems is their cost and sensitivity to a
                   large number of contaminants which, in extreme cases, can result in loss of production,
                   increased waste and increased processing and labour costs, as well as in a reduction in
                   yarn quality due to increases in the number of splices and in some instances, knots, due
                   to clearer cuts in spinning [5,8,17,41,42,55]. Clearers may also be installed on modern,
                   high-production spinning machines, such as air-jet and rotor (open-end) spinning
                   machines, but to avoid a dramatic drop in efficiency and yarn strength due to splicing
                   and piecings, these clearers need to be set to remove only the major contaminants [8,91].
                   It was estimated that in 2008, only 20% of the yarns spun on the rotor spinning machine
                   were cleared using yarn clearers designed to detect and remove foreign fibres [35], a
                   number that will be greater today given the modernization and installation of new rotor
                   spinning machines worldwide, an assertion highlighted by the fact that Schlafhorst
                   (Ubach-Palenberg, Germany) have sold >1 million Corolab clearers that can detect and
                   remove foreign fibres since 2005 [97]. A study conducted on rotor spinning showed that
                   high rotor speeds (>100, 000 rpm), smaller rotors (<36 mm) and low yarn counts (<25
                   tex) are more susceptible to being adversely affected by foreign fibres [98]. Figure 13
                   shows an example of a rotor spinning machine equipped with yarn clearers.
                      Spinners have also stated that yarn clearing systems only remove some 70%–85% of
                   contaminants [9,17,25,55,90]. From a commercial study, conducted by UsterÒ
                   Figure 13. Rotor spinning machine with Loepfe YarnMaster 1NI yarn clearers (Loepfe).
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Figure 14. Winding machine equipped with Loepfe Yarnmaster Zenit yarn clearers (Loepfe).
                   the fabric depends upon a number of factors such as fabric structure and compactness
                   and yarn twist. For example, contaminants cannot easily be removed from knitted cotton
                   fabrics, as this is likely to cause holes, while in a woven cotton fabric it is generally very dif-
                   ficult to remove contaminants present in the warp direction, due to the presence of size
                   [35].
                       UV lights can be installed in the yarn packing and inspection departments for the
                   detection of chemical/oily substances and foreign fibres such as polyester that fluoresce
                   [35]. Chemical treatments, such as bleaching/scouring in preparation for dyeing can some-
                   times reduce the problem of contamination, but that depends on the nature of the con-
                   taminants and adds further costs which are not always acceptable. The ‘chemical-
                   treatment’ option may, however, have to be phased out due to environmental legislation
                   prohibiting aggressive bleaching, for example with chlorine [17].
                       There is no doubt that all of the methods and approaches discussed above reduce the
                   risk of a yarn/fabric manufacturer receiving contamination-related claims but do not guar-
                   antee that the yarn or fabric produced will be totally free of contamination. Added to this
                   is the fact that there are no international standards for acceptable levels and sizes of con-
                   taminants in fabrics [91].
                   2. Cotton stickiness
                   Cotton stickiness, when it occurs, can present a major problem in terms of textile process-
                   ing performance, cost and product quality. The main problem related to cotton stickiness
                   is that of the sticky deposit or residue adhering to any machine part or surface encoun-
                   tered by the cotton along the processing pipeline, subsequently causing the build-up of
                   an accumulation of fibres on that part of the machine (together even with dust or grit)
                   during the ginning and spinning processes.
                       Cotton stickiness is a very wide field of investigation, with a large number of technical
                   and scientific publications; the main focus in the current review is on the various causes of
                   cotton stickiness and the consequences thereof in terms of textile processing and product
                   quality. For further detailed background information and list of references, the reader is
                   referred to the following excellent publications (also reviews) which deal in great detail
                   and depth with stickiness and also list a large number of relevant references, namely
                   Hequet and Abidi [100], Hequet, Henneberry and Nichols [101] as well as Gourlot [102]
                   and papers by Gourlot and co-workers presented at the ICCTM - ITMF Stickiness Working
                   Group meetings in 2012 [103], 2014 [104] and 2016 [105].
                   the biggest issue facing Sudanese cotton, resulting in US$15–30 million loss which equa-
                   tes to a reduction of 23%–46% in the export value of their raw cotton per year [101,109].
                   Similarly, Arizona experienced major whitefly outbreaks in the 1980s and 1990s and the
                   resulting perception regarding susceptibility to stickiness continues to lead to a
                   US$0.0563/lb discount relative to Californian cotton [108].
                      In fact, sticky cottons, where the stickiness is caused by honeydew contamination for
                   example, are virtually impossible to process on their own into yarn of acceptable quality.
                   Furthermore, the costs for controlling stickiness in the field can be extremely high, with
                   insecticide treatment costs to control aphids and whitefly costing growers in Arizona up
                   to US$145/acre in 1995 [108].
                   The most common and problematic causes of stickiness in practice, even today, are
                   those due to excess sugars related to insect secretions, notably aphids (Aphis gossypii
                   Glov.) and whitefly (Bemiesia tabaci Genn.); generally referred to as honeydew (insect
                   honeydew), these secretions are responsible for some 80%–90% of stickiness prob-
                   lems. Such stickiness caused by insects, mainly aphids, whiteflies and mealybugs, all
                   members of the insect order Homoptera, is the most problematic and common. In
                   general, a high percentage of melezitose (a tri-saccharide), along with a low percent-
                   age of trehalulose (an unusual disaccharide; an isomer of sucrose), indicates the pres-
                   ence of honeydew from aphids. Conversely, a dominance of trehalulose indicates
                   contamination by honeydew from whitefly. These insects ingest plant juices, extract
                   proteins and other nutrients from them and then expel honeydew (composed of sug-
                   ars and other carbohydrates) which falls onto the cotton plant leaves or lint after boll
                   opening, leaving a sticky, hygroscopic sugary deposit. Subequently a black sooty
                   mould can grow on the honeydew secretion on the cotton, darkening the lint and
                   adversely affecting its grade.
                      Physiological or plant-related stickiness mainly originates from highly immature cot-
                   tons (which can contain up to about 0.9% sugars) and plant sap, but can also arise from
                   crushed seeds, motes and seed fragments and fine leaf particles, as well as from the pro-
                   duction of excessive levels of cotton wax.
                   stickiness has several possible causes, no one particular test can account for all causes; a com-
                   bination of chemical and physical/mechanical (e.g. mini-card) tests generally being required.
                       Most tests for sugar content fail to detect the random spotty honeydew contamination
                   from whiteflies and aphids, since just a few large drops of honeydew, each of which con-
                   tain only a few milligrams of sugars, are sufficient to create a stickiness problem, without
                   also generating any significant effect on the overall (average) sugar levels.
                       Stickiness arising physiologically from (plant) sugars however, is rare; under normal
                   conditions, any such stickiness should disappear quickly (within a few months) as bacteria
                   and fungi present on the lint readily metabolize any glucose, fructose and sucrose present.
                       Contamination due to lubricating oils show up as brilliant blue–white fluorescence
                   under UV light, whereas alcohol extractables give a good indication of the general level of
                   non-cellulosics present in cotton [101,102].
                       There are various tests for stickiness, some of which are listed below [100,110,111]:
                         Chemical tests:
                         A. Oxidation-reduction methods
                               Potassium ferricyanide (also known as the Perkins method)
                               Fehling/Follin test
                               Benedict test
                               Bremen honeydew test
                         B. Enzymatic tests
                         C. Chromatographic
                               Gas chromatography (GC)
                               High-performance liquid chromatography (HPLC)
pH
Indicator spray
Thermo-mechanical
Mechanical
Other:
                         NIR
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                      UV Fluorescence
                      Electrical Conductivity
                      Stickiness Tester (also known as the Stanley Anthony method)
                   Despite the large range of test methods listed here there is currently no recognized com-
                   mercial standard method for measuring stickiness in cotton lint on a high volume basis
                   [101]. From the various test methods listed above, the HPLC test is the only chemical test
                   method currently recognized by the research community as providing important informa-
                   tion on the source of the stickiness; it is however not feasible for mass testing as it is time
                   consuming and costly [100]. In terms of the thermo-mechanical test methods, the High
                   Speed Stickiness Detector (H2SD) and the Lintronics Fiber Contamination Tester (FCT).
                   FCT test methods offered the potential to become high-speed laboratory test methods;
                   the FCT instrument has now been superseded by the Loepfe and Mesdan instruments
                   [100,112].
                      In terms of the mechanical test methods, the mini-card test method relates well to the
                   conditions experienced by stickiness during yarn manufacturing. The mini-card test was
                   adopted by the ICCTM in 1988 as the reference method for assessing stickiness [110]. Nev-
                   ertheless, the test method is slow and time consuming, operator dependent and subjec-
                   tive, the results can be influenced by the condition, maintenance and level of cleaning
                   between tests and the relative humidity. Furthermore, the carding machines utilized are
                   no longer readily available and are expensive to purchase [100,110,111].
                      Some Classing facilities, merchants and mills use the pH indicator spray as a screening
                   tool to determine the incidence of stickiness if they suspect the presence of stickiness [110].
                      The various test methods produce different results and, as a consequence, the ITMF Inter-
                   national Committee on Cotton Testing Methods (ICCTM) was conducting Round Trials for
                   Stickiness in 2017 to determine if there are any relationships between the different methods.
                   due to higher labour costs and additional spare parts as saws and blades need to be
                   replaced more regularly [119]. In extreme cases, stickiness can also affect harvesting with
                   the spindle-type harvesters, as sticky deposits will accumulate and clog the spindles caus-
                   ing blockages [101].
                   Figure 15. Sticky cotton causing disruptions during processing on (a) the draw frame creel drive rolls
                   and (b) the drafting section of the draw frame [120].
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                   Figure 16. ITMF stickiness survey results from 1989 to 2016 [18].
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                   3. Seed-coat fragments
                   It has been stated that practically all ginned lint contains seed-coat fragments (SCFs) [123]
                   and that the main source is the chalazal end of the seed – see Figure 17 which is generally
                   not fully developed or is structurally-weak with fibres in this area (possibly immature due
                   to varietal and environmental factors) torn off together with a piece of seed instead of
                   being broken off [124,125]. This leads to the creation of SCFs when the fibre is eventually
                   separated from the seed, consisting mainly of pieces of the chalazal or rounded end of
                   the seed as well as motes (whole immature seeds) which broke during ginning [123].
                   Medium sized motes (1–3 mm in width and 3–5 mm in length), having fibres of medium
                   length attached, contribute to SCFs, due to them becoming fractured during ginning
                   [126].
                       The number of SCFs in ginned cotton can vary by as much as 50%, studies showing
                   that the major factors contributing to their occurrence were cotton variety, crop year and
                   timing of harvest [127–133]. It has further been stated that SCFs are becoming a bigger
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Figure 17. Cotton seed illustrating the position of the Chalazal end (CSIRO).
                   issue, due to increased seed-cotton cleaning during ginning and the fact that spinners
                   require more uniform fibre which is free of foreign matter [134]. Not only do SCFs cause
                   spinning end breakages, but they also cause a deterioration in yarn appearance and
                   increase production costs, being virtually impossible to extract from the bulk of the raw
                   cotton, except at the combing process, because of the tuft of fibres attached to the seed-
                   coat. Hence they are generally incorporated into the yarns as a nep [129,134–136] – see
                   Figure 18. SCFs appear as dark specks on the surface of dyed fabrics, and are generally sur-
                   rounded by immature fibres of lighter colour, which reduce the quality of the final product
                   [135,137,138]. It is for this reason that spinners dread SCFs, with the ITMF Contamination
                   Surveys [18] highlighting the fact that there is a perception amongst spinners that SCFs
                   are a serious and increasing problem. A recent study conducted worldwide in 2016
                   showed that 58% of the participants rated SCFs as a major defect of cotton fibres that
                   affects yarn properties [106]. It has also been stated that cotton-seed oil from SCFs can be
                   associated with stickiness problems encountered during processing [139–142].
                      As would be expected, rotor-spun yarns tend to be less affected by SCFs than ring-spun
                   yarns, due to the fact that the opening roller of the rotor spinning machine removes a sig-
                   nificant amount of trash and SCFs from the input sliver prior to the formation of yarn, and
                   also the fact that the structure of the rotor-spun yarn has the tendency to hide SCFs within
                   the body of the yarn [143]. In one study it was found that the presence of SCFs had a sig-
                   nificant effect on yarn strength, the effect varying with fibre quality. In other words, the
                   presence of SCFs will only have a significant effect on yarn strength if the strength at the
                   point created by the SCFs is less than that at the weakest point, present elsewhere in that
                   yarn segment [144].
                      A study of thirteen cotton varieties from three production areas was undertaken to
                   determine the sources of imperfections in fabric, focussing on the three possible sources
                   suspected of giving rise to SCF contamination, namely pieces of the chalazal end, seed
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                   damage and motes. It was found that the relationship between the three suspected areas
                   was poor. The only significant correlations were found between seed diameter and SCF
                   fabric imperfections (r = 0.86) and attachment force (r = 0.40) [145], it being concluded
                   that seeds smaller than 4 mm in diameter may be the major source of fabric SCF imperfec-
                   tions. Another study, involving the 1986 US Regional Cotton Variety Tests, and conducted
                   across the US cotton belt, showed that high nep counts and SCFs can be avoided by using
                   varieties with a low occurrence of immature cottonseed and which have seed diameters
                   greater than 3.73 mm [146]. This was confirmed by a study conducted in 2004, which
                   showed that, although no consistent relationship was found between SCFs and seed
                   diameter, there was a strong indication that cultivars with small seeds (measured in terms
                   of their seed diameter or seed index) did not produce ginned lint containing high levels
                   of SCFs [147–149].
Figure 19. ITMF seed-coat fragment survey results from 1991 to 2016 [18].
                   and foreign matter in the test specimen. Other such instruments include the Premier Evol-
                   vics Pvt. Ltd., aQura instrument which measures the number and size of contaminants
                   and SCFs, the FCT, the Loepfe Labmaster Fibermap and the Mesdan Contest which super-
                   seded the FCT in 2016. These instruments provide results on trash and dust, neps and
                   SCFs and are also used to detect stickiness.
                      The measurement of SCFs through the application of the test methods and instruments
                   referred to above is always carried out ‘off line’, with samples collected then transported
                   to and tested in the laboratory. Online detection and measurement is available, however,
                   to complement the laboratory data; most of the major machinery manufacturers produc-
                   ing carding machines now provide online nep sensors to detect and record the number
                   of neps and SCFs in the card sliver.
                      This classification system allows growers and merchants to better describe and perhaps
                   obtain better premiums for their cotton, and helps spinning mills to establish standards
                   for the whole yarn manufacturing process.
                   4. Conclusion
                   It is clear that the problem of contamination in cotton has by no means been satisfactorily
                   resolved, and that it remains a serious issue. The negative economic, processing and qual-
                   ity impact of such contamination depends on the nature of the contaminant, with plastic
                   or fibrous contaminants currently proving particularly problematic. Although various
TTPR_A_1437008.3d (Standard Sanserif)   (174£248mm) 21-05-2018   9:8
                   automatic detection and removal systems have been developed and installed at various
                   stages of the cotton pipeline, these tend to be expensive and are not 100% effective. Fur-
                   ther development in this area is certainly called for.
                      There can be little doubt that by far the most-effective and lasting way of dealing with
                   the problem of contamination in cotton is to prevent its occurrence at source. Prevention
                   will require regular, and continuously-updated instructional programmes to inform and
                   educate growers, harvesters (both hand and machine-assisted), ginners and cotton-mill
                   processing staff on the damaging effect of cotton contamination, how and where contam-
                   ination occurs and how to combat it, followed by a worldwide effort with a focus on
                   implementation of the necessary measures. The ‘second line of defence’ remains that of
                   detection and elimination of contaminants at the various stages of the cotton processing
                   pipeline; continual advancement in sensor and associated technologies will no doubt lead
                   to the development of new and more effective systems in this respect. Nevertheless,
                   because of the issues associated with actual contaminant removal such as associated loss
                   of fibre, it is unlikely that these alone will ever lead to a perfect solution to the problem;
                   avoiding or at least minimizing contamination at source will remain the most effective
                   and sustainable solution.
                   Acknowledgements
                   The authors thank everyone who has gathered and collected the numerous references used in this pub-
                   lication. The authors also thank everyone for their useful and insightful comments and suggestions.
                   Disclosure statement
                   Any trade names or commercial products mentioned in the publication are solely for the purpose of
                   providing specific information and do not imply recommendation or endorsement by the authors.
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TTPR_A_1437008.3d (Standard Sanserif)   (174£248mm) 21-05-2018   9:8