Pco Sweies 300level 123
Pco Sweies 300level 123
DONE AT
WRITTEN BY
20181120863
SUBMITTED TO
JANUARY, 2023.
DEDICATION
I dedicate this report to God Almighty, who has given me the privilege to undergo this
industrial training.
I also dedicate this report to my parents, Mr. and Mrs. Humphrey Onuigbo
ACKNOWLEDGEMENT
First off, I want to thank the Almighty God for giving me the grace and the wisdom to write
this report.
I sincerely want to thank my lovely and supporting parents for their support during the period
of my industrial training. I also want to thank my department, Petroleum Engineering; FUTO
and my lecturer who made sure we understood almost all he taught.
I will not forget to appreciate my colleagues for being collaborative throughout the training.
ABSTRACT
Student's Industrial Work Experience Scheme (SIWES) popularly called Industrial training is
a scheme that gives the students of Tertiary Institutions the opportunity to acquire a direct
work experience and also provides them the platform to apply both the theoretical and
practical knowledge acquired in the course of study in a related Industry.
Actually, this report is a summary of my industrial training experience. The crux of the
training was centered on use of bio diesel (from palm kernel oil) to produce oil base mud and
to test the physical properties of the bio diesel.
TABLE OF CONTENTS
COVER PAGE
DEDICATION............................................................................................................................................
ACKNOWLEDGEMENT...........................................................................................................................
ABSTRACT................................................................................................................................................
CHAPTER ONE..........................................................................................................................................
CHAPTER FIVE.......................................................................................................................................
CHAPTER ONE
Student industrial work experience scheme (SIWES) is one of the industrial training funds
(ITF) program, the scheme was designed to give (expose) Nigerian students to the industrial
environment and enable them develop occupational competencies and experiences that
would supplement their theoretical learning and also allow them contribute their quota to
Consequently, SIWES is a planned and structured programme based on stated and specific
career objectives which are geared toward developing the occupational competencies of
participants. In spite of the challenges faced by SIWES in the four decades of its existence,
the Scheme has not only raised consciousness and increased awareness about the need for
training of undergraduate students, but has also helped in the formation of skilled and
competent indigenous manpower which has been manning and managing the technological
resources and industrial sectors of the economy. Participation in SIWES has become a
necessary condition for the award of degrees and diplomas to students graduating from higher
institutions in Nigeria. It is therefore, not in doubt that SIWES is a veritable means or tool for
The main thrust of ITF programmes and services is to stimulate human performance, improve
productivity, and induce value-added production in industry and commerce. Through its
SIWES and Vocational and Apprentice Training Programmes, the Fund also builds capacity
for graduates and youth self-employment, in the context of small scale Industrialization in the
economy. The Industrial Training Fund is a grade ‘A’ parasternal operating under the aegis of
the Federal Ministry of Industry, Trade and Investment. It has been operating for 42 years as
a specialist agency that promotes and encourages the acquisition of industrial and commercial
the practical aspect of their field of study by exposing students to machines and equipment,
professional work methods and ways of safeguarding the work areas and workers in industries
following objectives.
1. To solve the problem of lack of adequate practical skills preparatory for employment
2. To train students on industrial base skills essential for a smooth transition from the
3. To enhance student’s contact for later Job placements and a chance to evaluate
4. The program teaches the students on how to interact effectively with other workers
COMPANY’S PROFILE
At the inception of the School of Engineering and Engineering technology (SEET) in October
1982, the Petrochemical Science and Technology programme was restructured and was
renamed Petroleum Engineering Programme. The programme started at the Lake Nwaebere
Campus which was a temporary site for the University and lectures started in October 1982
led by Engr R. M Aguta. In 1987 the programme was merged with the Chemical Engineering
programme to form the Department of Chemical and Petroleum Engineering. In 1998 the
Department of Chemical and Petroleum Engineering was split into two separate departments
- Chemical Engineering Department and Petroleum Engineering Department and has
remained separate entities to this day.
The department is currently led by Engr Dr I U Duru as the Head of Department and Engr Dr
Ngozi Nwogwu as the SIWES coordinator who are working tirelessly with the aid of the
other staffs to take the department to greater heights.
SENIOR LECTURERS
Engr. Dr. A. I. B. Ekejiuba
Engr. Dr. C. I. C. Anyadiegwu
Dr. K. C. Igwilo
Engr. Dr. N. C. Izuwa
Engr. Dr. U. I. Duru
Engr. Dr. N. P. Ohia
LECTURER 1
Mr. A. O. Chikwe
Engr. I. M. Onyejekwe
Engr. Dr. A. Kerunwa
Engr. U. J. Obibuike
Engr. E. Egelle
Engr. Dr. A. N. Nwachukwu
Engr. B. Nzeribe
LECTURER 2
Engr. Dr. Mrs N. C. Nwogu
Engr. I. A. Oguamah
Engr. E. O. Mbah
ASSISTANT LECTURERS
Mr. Ibiam
Miss. I. N. Onugha
Mr. P. M. Ikpeka
Mr. F. N. Nwabia
Mr. J. Odoh
Mr. N. Okoli
SAFETY
The safety of lives and equipment are paramount in the industry and thus, treated with
caution just like they say unsafe action +unsafe condition =accident. The company supervisor
briefed us on the safety rules and regulation on my first day of this industrial training.
1. Safety Induction: When starting as a new staff at a company, you need to be equipped with
basic safety s kills for survival in case of necessity, so the new intakes are being trained
"inducted" on the safety rules and they undergo safety training so as to create awareness on
the dangers accompanied with the industry work. Note, those to work on an offshore drilling
rig are required to have a certificate of swimming, so those without it are expected to undergo
a week training so as to learn basic swimming skills in case of any danger when working
2. Personal Protection Equipment (PPE): It involves the tools and equipment required to
perform task in the industry e.g. cover all, goggle, helmet, boots, hand gloves, etc. PPE are
paramount before one could enter the company whether on an official or unofficial visit
CHAPTER THREE
The drilling fluid laboratory provides a wide range of analysis on water-based and oil-based
drilling fluid at standard and HPHT conditions
The objectives of the undergraduate drilling lab course are
Multi mixer, Large volume mixing tank, Pressurized aging cells, Rolled oven, Heated
magnetic stirrer, Centrifuge, Mud balance, Emulsion stability tester, Filtrate analysis
kit, Hydrometer kit, Atmospheric consistometer (Used the check the thickening time of
a cement slurry), Fann viscometers, Variable speed viscometers, Standard filter
press ,HTHP filter press, Sand content kit, Retort kit, Rheometer, PH meter
In the production laboratory, physical properties measurements of H-C are taken according to
the American Petroleum Institute standard (API), such as, fluid density, viscosity, surface
tension, interfacial tension, flash point, vapor pressure, pour point, water content in crude oil,
total salts content of crude oil by conductivity and corrosion.
Centrifuge, Cloud and pour point tester, Heating mantle, Distillation unit, Water bath
Hydrometer.
The flow assurance lab is a laboratory that is more concern with the efficiency of how
hydrocarbon fluids are transmitted economically from the reservoir to the end user over the
life of a project in any environment. Flow assurance analysis is a recognized critical part of
the design and operation of subsea oil/gas systems.
Centrifuge, Gas chromatograph, Crude oil distillation unit, Distillation unit , Derick,
Pour and cloud point tester.
samples.
of mud rheological
"Viscosity"
properties.
weight.
laboratory.
samples.
in a sample of water-based or
cement systems;
viscosity
10 Sand content kit to determine the volume
fluids.
air
Petropedia defines drilling fluid as a "liquid that is used to facilitate the easy drilling of
wellbores in the earth's surface". It is often used to drill oil or gas wells and even exploration
drillings of wellbores. Collins English Dictionary defines drilling fluid is a "mixture of clays,
water, and chemicals pumped down the drill string while an oil well is being drilled to
lubricate the mechanism, carry away rock cuttings, and maintain pressure so that oil or gas
does not escape to the surface". A suspension of fine-grained mineral matter, usually in
water, circulated in oil-well drilling to cool and lubricate the drill bit, plug up porous
surfaces, etc.
Esabunor O.N.R. defines drilling fluid as a mixture of two or more phases; solid phase is the
bentonite clay; liquid phase could be water, diesel oil, crude oil, or any other synthetic oil;
reactive phase (additives) to enhance the functionality of the drilling fluid. The three phases
are mixed in various proportion to meet specific hole condition. The first person did not
consider the use of additive or chemical to improve the quality of the designed mud (drilling
fluid) while the second person consider the use of chemicals, the third person consider the use
of additives all to improve the quality of the mud to meet specific hole condition.
There are several different types of drilling fluids, based on both their composition and use.
The three key factors that drive decisions about the type of drilling fluid selected for a
Cost.
Technical performance.
Environmental impact.
Selecting the correct type of fluid for the specific conditions is an important part of successful
drilling operations. The basic types of drilling fluid (mud) use in the oil and gas industry are
below:
Water-based fluids (WBFs) are the most widely used systems, and are considered less
expensive than oil-based fluids (OBFs) or synthetic-based fluids (SBFs). The OBFs and SBFs
– also known as invert-emulsion systems – have an oil or synthetic base fluid as the
continuous (or external) phase, and brine as the internal phase. Invert-emulsion systems have
a higher cost per unit than most water-based fluids, so they often are selected when well
conditions call for reliable shale inhibition and/or excellent lubricity. Water-based systems
and invert- emulsion systems can be formulated to tolerate relatively high down hole
temperatures. Pneumatic systems most commonly are implemented in areas where formation
pressures are relatively low and the risk of lost circulation or formation damage is relatively
high. The use of these systems requires specialized pressure-management equipment to help
A properly designed and maintained drilling fluid performs essential functions during well
construction such as transporting cuttings to the surface, preventing well-control issues and
wellbore stability, minimizing formation damage, cooling and lubricating the drill string and
Materials
Beakers, conical flask, measuring cylinder, pipette, hot plate and stirrer, weighing
balance, volumetric flask, separating funnel.
DESCRIPTION
Palm kernel oil contain surfactant (gum) in microscopic quantity, so in other to obtain a pure
oil, I added Orthophosphoric acid and hot water to the palm kernel oil in a process known as
degumming.
Sodium hydroxide acts as catalyst in this reaction and reacts with the alcohol (methanol in
this case) to produce sodium methoxide
The sodium methoxide is now poured into the heated degummed oil and the mixture is
allowed to stand. after some time, the bio-diesel will rise, and they glycerol will settle.
NOTE; since sodium hydroxide acts as catalyst, the main reaction is between the gum oil and
methanol in a process known as trans esterification
PROCEDURE;
Using the 1000ml beaker 900ml of the palm kernel oil was obtained.
3% of the 900ml is the quantity if hot water to be added to the oil.
i.e. 3%*900=27ml of hot water (100 degrees)
0.005% of 900ml is the quantity if acid (75% concentration) to be added to the oil.
0.05/100*900=0.45ml of acid which I approximated to 0.5ml.
Put a beaker containing the oil water and acid on the hot plate and put in the magnetic
stirrer inside.
After it has been properly heated to about 55 degrees and properly stirred, I put off
the hot plate and took the beaker down.
I left the mixture and allowed the gum to settle.
IN PREPARATION OF THE SODIUM METHOXIDE
NaOH comes either in pellet or granular form, in the case the granular NaOH was used.
Place a paper strip in the electric weighing balance and measure 0.5g of NaOH
Measure 30ml of methanol
Pour the methanol inti the conical flask containing the granular NaOH and stir.
FINAL PROCEDURE
Measure 100ml of the oil (palm kernel oil after all the gum must have settled down)
then heat till it is 65 degrees
Gently pour the methoxide into it
Stir for 1 hour
Pour the mixture into the separating funnel
The biodiesel rises and the triglycerol settle
PRECAUTIONS
The bio-diesel did not separate properly from the glycerol forming soap instead.
This was as a result of the not filtering out the mixture of the gum oil and methoxide
before pouring into the separating funnel.
1. Primary emulsifier
2. Secondary emulsifier
Low recommended oil/water ratio for different mud density
DENSITY (ppg) OIL/WATER RATIO
7-9 60/40
9-11 65/35
11-14 70/30
14-16 75-25
16-19 80/20
19 Above 85/15
MATERIALS NEEDED
1. 222ml of the base oil i.e. palm kernel oil or the synthetic oil.
2. 5gm of lime
3. 6ml of primary emulsifier
4. 3ml of secondary emulsifier
5. Brine solution which is prepared by adding 25gm of CaCl2 to 75ml of water
6. 215 grams of barite
7. Bentonite
Note; the expected weight and oil/water ratio of the oil based mud to be produced are
11.8ppg and 80/20 respectively.
APPARATUS USED
PH= Neutral
CALCULATIONS
i.e. 270-150=120
i.e. 150/2=75
WHEN BIO DIESEL MADE FROM VEGETABLE OIL WAS USED AS BASE FLUID
CALCULATIONS
i.e. 360-163=197
i.e. 163/2=81.5
WHEN BIO DIESEL FROM PALM KERNEL OIL WAS USED AS THE BASE FLUID
PH= Neutral
CALCULATIONS
i.e. 142-150=50
i.e. 92/2=46
AIM: To determine volume of oil, water and solids present in the mud and obtain the
oil/water ratio
In a retort test, a measured sample of fluid is placed in a cup and heated until the liquid
components have been vaporized. The vapors are passed through a condenser and collected in
a graduated cylinder or centrifuge tube that has been calibrated to record the volume of the
condensed liquids at 20°C.
Volume of solids=4.8ml
% of water =100-69.23=30.77
Equal volumes of aniline and oil are stirred continuously in a test tube and heated until the
two merges into a homogeneous solution. Heating is stopped and the tube is allowed to cool.
The temperature at which the two phases separate out is recorded as aniline point.
The aniline point can also be determined by obtaining the temperature at which the base oil
mixes up with the aniline fluid.
PROCEDURE
1. Pour equal volume of the base fluid and the aniline and mix together
2. Check the temperature at which the mixture separates using a thermometer
The aim is the check the tendency of our base fluid of the drilling fluid to attacking the rubber
components of the drilling system
RESULT
The Electrical Stability (ES) meter was used to measure the emulsion breaking voltage.
Emulsion Stability indicates the emulsion and oil wetting qualities of oil-based and
synthetic-based mud samples. The oil mud sample was preheated and poured through a
Marsh Funnel screen into a glass beaker. The mud sample was hand-stirred with the
electrode probe for 10 seconds to help create a uniform composition and temperature.
The ES meter test button was then pressed down automatically applying an increasing
voltage (from 0 to 2000 Volts) across an electrode gap in the probe. The maximum
voltage, and the mud temperature were recorded. The higher the voltage, the more
• Design: A Plan or Drawing produced to show the look and function or working if
a building, garment or another object before it is made (Source: Oxford Dictionary
• There are many Computer Aided Design software used for Engineering Design
but AutoCAD is the most widely used. AutoCAD: Computer Aided Design
software that allows you to draw and edit digital 2D and 3D more quickly and
easily. Invented by John Walker in 1982 and developed and owned by Autodesk.
VIEW FEATURE
This is used to control the visual size of feature or shape while drawing on the
Auto. The visual spectrum can be zoomed, 3D view, orbited, panned etc. To use
the view feature to zoom-in or zoom-out, you place the cursor at the specific point
you want to zoom in or out and use the roller component on the mouse.
TO ZOOM-OUT TOTALLY
• Click enter
• Set Thickness
• Use the modification tools to modify the drawn items until desired shape is
achieved
3-Dimensional Design
Also referred to as 3-D Modeling, used to bring represent 2-D drawings in 3-D
form. In addition to Draw and Modifying Features, it has the Modeling and Solid
editing Features Its view includes the 3-D conceptual and 3-D realistic used to
view 3-D designs and shapes. It has Mesh and Sub-Object options.
Modeling Features
Used to draw 3-D shapes. The consists of the following Shapes features: Box, Cylinder,
Cone, Sphere etc.
3-D Extrude
3-D Revolve
3-D Loft
Benefits of AUTOCAD:
execute and analyze the strength of a building at the design stage level.
In 3D printing: A 3D print has its own advantages for designers, and for this software
AutoCAD in the fashion industry: It has the tools necessary for planning designs for
WORK EXPERIENCE
CONCLUSION
Transesterification is a very sensitive process that requires extreme care as to the nature and
state of the materials used as well as the reaction conditions. The process involves a
straightforward series of chemical reactions, but many things can still go wrong in home (or
laboratory) production setting. Understanding the likely causes of biodiesel failure can help
rescue or at least prevent similar problems in the future. Also, failed biodiesel may
occasionally result in the production of something useful, like soap and lubricant (as
suspected in this work). Recognizing when this happens can prevent the batch from becoming
a total loss. For example, in one of the reaction settings (in this study) the reaction after being
allowed to stay for days did not give any phase separation. In troubleshooting what went
wrong it was observed the container of the NaOH used had some cracks which could have
allowed moisture uptake from the atmosphere. This could also be as a result of not filtering
the methoxide before pouring the mixture into the separating funnel.
During the production of oil base mud from palm kernel (PKO) oil it was observed that the
PKO had better physiochemical properties result. Higher flash points, proving their fire-
resistant capabilities, higher densities and viscosities which reduces cost of mud formulation.
The use of the import function in Auto CAD definitely has some advantages. It can help
to reduce the time it takes to produce the drawings needed in the work environment.
However, if the individual that has created the imported file does not receive credit for
their work, problems may arise in the future. As well, by using the function people may
slowly start to place a lesser value on the intellectual property of others, which will
undoubtedly create future conflict. The use of the import function may also be relied on
heavily in order to create efficiencies within the industry. This could possibly lead to a
decrease in the rate of innovation. It's obvious that the import function has a place in the
building industry, but its use will have to be regulated in order to create a balance
between the negative and the positive effects it creates.
CHALLENGES
1. Intern students should be given ample time suitable for an optimum training
2. Intern students should be paid some allowance
3. I will also recommend that institutions should make provision for student to go on
excursion in various industries aside the IT period which is the only opportunity a
student has and not all may be opportune to get an IT placement
References
1. Alamu, O.J. et al., 2008. Characterization of palm-kernel oil biodiesel produced through
NaOH-catalysed transesterification process. Scientific Research and Essay, 3(7),
pp.308–311.
2. Ananwe, P., Efeovbokhan, V. E., Ayoola, A. A., & Akpanobong, O. (2014). Investigating
Alternatives to Diesel in Oil Based Drilling Mud Formulations Used in the Oil Industry.
Journal of Environmental and Earth Science. 70-77.
5. Craig Summers and Eric Markusen, "Why Good People Do Bad Things: The Case of
Collective Violence", [On-line document], [2005 November] [cited 2008 Oct.12]
Available http://campus.udayton.edu/~richards/Computer%20essays/why%20good
%20people%20do%20....htm