J STD 002
J STD 002
IPC/ECA J-STD-002C
                                                      w/Amendment 1
                                                       NOVEMBER 2008
                                                      Supersedes J-STD-002C
                                                         December 2007
     JOINT
 INDUSTRY
STANDARD
       ®
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Notice                                            IPC and ECA Standards and Publications are designed to serve the public interest
                                                  through eliminating misunderstandings between manufacturers and purchasers,
                                                  facilitating interchangeability and improvement of products, and assisting the
                                                  purchaser in selecting and obtaining, with minimum delay, the proper product for
                                                  his particular need. Existence of such Standards and Publications shall not in any
                                                  respect preclude any member or nonmember of IPC or ECA from manufacturing
                                                  or selling products not conforming to such Standards and Publications, nor shall
                                                  the existence of such Standards and Publications preclude their voluntary use by
                                                  those other than IPC or ECA members, whether the standard is to be used either
                                                  domestically or internationally.
                                                  Recommended Standards and Publications are adopted by IPC or ECA without
                                                  regard to whether their adoption may involve patents on articles, materials,
                                                  or processes. By such action, IPC or ECA do not assume any liability to any
                                                  patent owner, nor do they assume any obligation whatever to parties adopting
                                                  the Recommended Standard or Publication. Users are also wholly responsible for
                                                  protecting themselves against all claims of liabilities for patent infringement. The
                                                  material in this joint standard was developed by the IPC Component and Wire
                                                  Solderability Specification Task Group (5-23b) and the ECA Soldering Technology
                                                  Committee (STC).
                                                  ECA                                               IPC
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                                                  Please use the Standard Improvement Form shown at the end of this
                                                  document.
©Copyright 2008. The Electronic Components, Assemblies and Materials Association, Arlington, Virginia, and the IPC, Bannockburn, Illinois,
USA. All rights reserved under both international and Pan-American copyright conventions. Any copying, scanning or other reproduction of
these materials without the prior written consent of the copyright holder is strictly prohibited and constitutes infringement under the Copyright
Law of the United States.
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                                Solderability Tests
                                for Component Leads,
                                Terminations, Lugs,
                                Terminals and Wires
                                             Acknowledgment
Any document involving a complex technology draws material from a vast number of sources. While the principal members
of the IPC Components and Wire Solderability Specification Task Group (5-23b) of the Assembly and Joining Processes
Committee (5-20) and the Electronic Components, Assemblies and Materials Association (ECA) Soldering Technology
Committee (STC) are shown below, it is not possible to include all of those who assisted in the evolution of this joint indus-
try standard. To each of them, the members and staffs of IPC and ECA Associations extend their gratitude.
IPC Assembly & Joining                     Component & Wire Solderability             ECA Soldering
Processes Committee                        Specification Task Group                   Technology Committee
Chair                                      Chair                                      Chair
Leo P. Lambert                             David D. Hillman                           Douglas W. Romm
EPTAC Corporation                          Rockwell Collins                           Texas Instruments Inc.
Vice Chair                                 Vice Chair
Renee J. Michalkiewicz                     Dennis Fritz
Trace Laboratories - East                  MacDermid, Inc.
IPC Component & Wire Solderability Specification Task Group and ECA Soldering Technology Committee
Dr. Donald Abbott, Sensata                 Laya Chen, Microtek (Changzhou)            Shirley He, CEPREI
  Technologies                               Laboratories                             Steven A. Herrberg, Raytheon
David C. Adams, Rockwell Collins           Phillip Chen, L-3 Communications             Systems Company
Dale Albright, Winslow Automation            Electronic Systems                       Dr. Christopher Hunt, National
  aka Six Sigma                            Dr. Beverley Christian, Research In          Physical Laboratory
Greg Alexander, Ascentech, LLC               Motion Limited                           Prakash Kapadia, Celestica
Francis Anglade, Metronelec                Ted Coler, Vishay Dale                       International Inc.
Gail Auyeung, Celestica International      David J. Corbett, Defense Supply           Dr. Christian Klein, Robert Bosch
  Inc.                                       Center Columbus                            GmbH
Chris Ball, Valeo Inc.                     Charles Dal Currier, Ambitech Inc.         Connie M. Korth, Kimball
Mary Carter Berrios, Kemet                 Gordon Davy, Best Manufacturing              Electronics Group
  Electronics                                Practices Center of Excellence           Richard E. Kraszewski, Kimball
James D. Bielick, IBM Corporation          Mary Dinh, Northrop Grumman                  Electronics Group
Joseph Biernacki, Stackpole                  Space Systems Division                   Vijay Kumar, Lockheed Martin
  Electronics, Inc.                        Glenn Dody, Dody Consulting                  Missile & Fire Control
Christine Blair, STMicroelectronics        Richard M. Edgar, Tec-Line Inc.            Mark A. Kwoka, Intersil Corporation
  Inc.                                     Theodore Edwards, Dynaco Corp.             Patrick Kyne, Defense Supply Center
Gerald Leslie Bogert, Bechtel Plant        Robert Furrow, Alcatel-Lucent                Columbus
  Machinery, Inc.                          Gerald Gagnon, Bose Corporation            Harjinder Ladhar, Solectron
Dr. Edwin Bradley, Motorola Inc.                                                        Corporation
                                           Dr. Reza Ghaffarian, Jet Propulsion
Jason Bragg, Celestica International         Laboratory                               Leo P. Lambert, EPTAC Corporation
  Inc.                                     Andrew Giamis, Andrew Corporation          Michael Lauri, IBM
Dr. Peter Bratin, ECI Technology,          Jean Gordon, Fairchild                     Carl Lindquist, SOC America, Inc.
  Inc.                                       Semiconductor                            Laird Macomber, Cornel Dubilier
Michael Cannon, TDK                        Hue T. Green, Lockheed Martin                Electronics
Dennis Cantwell, Printed Circuits            Space Systems Company                    James F. Maguire, Intel Corporation
  Inc.                                     Michael Griffith, KOA Speer                Karun Malhotra, Murata Electronics
Thomas Carroll, Boeing Aircraft &            Electronics, Inc.                        Jack McCullen, Intel Corporation
  Missiles                                 Gerald J. Griswold, Texas                  Len Metzger, Panasonic Industrial
Dr. Srinivas Chada, Medtronic                Instruments, Inc.                          Company
  Microelectronics Center                  Dr. Carol A. Handwerker, Purdue            Renee J. Michalkiewicz, Trace
Calette Chamness, U.S. Army                  University                                 Laboratories - East
  Aviation & Missile Command
                                                                                                                            iii
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Michael Milbrath, BH Electronics        Jim R. Reed, Dell Inc.                 David Toomey, Vishay Sprague
Dr. Kil-Won Moon, NIST                  Chris Reynolds, AVX Corporation           Sanford
David E. Moore, Defense Supply          David Richardson, Vishay               William Lee Vroom, Thomson
  Center Columbus                       John H. Rohlfing, Delphi Electronics      Consumer Electronics
Terry L. Munson, Foresite, Inc.            and Safety                          Karl F. Wengenroth, Enthone Inc. -
Suzanne F. Nachbor, Honeywell           William R. Russell, Raytheon              Cookson Electronics
  Aerospace Minneapolis                    Professional Services LLC           George Wenger, Andrew Corporation
Graham Naisbitt, Gen3 Systems           David F. Scheiner, Kester              Robert Wettermann, BEST Inc.
  Limited                               Jeff Seekatz, Raytheon Company         Vicka White, Honeywell Inc.
Gary Nicholls, Enthone Inc. -           William Sepp, Technic Inc.             Keith Whitlaw, Consultant
  Cookson Electronics                   Joseph L. Sherfick, NSWC Crane         Maureen Williams, NIST
Benny Nilsson, Ericsson AB              Lowell Sherman, Defense Supply         Russell T. Winslow, Winslow
Debora L. Obitz, Trace Laboratories -      Center Columbus                        Automation aka Six Sigma
  East                                  Bradley Smith, Allegro MicroSystems    Jere Wittig, HFK Precision Metal
Gerard A. O’Brien, Solderability           Inc.                                   Stamping Corporation
  Testing & Solutions, Inc.             Paco Solis, Foresite, Inc.             Linda Woody, Lockheed Martin
Stephen Olster, Mini-Systems, Inc.      Roger Su, L-3 Communications              Missile & Fire Control
Michael Paddack, Boeing Company         Fujiang Sun, Huawei Technologies       Yung-Herng Yau, Enthone Inc. -
Dr. J. Lee Parker, JLP                     Co., Ltd.                              Cookson Electronics
Mel Parrish, STI Electronics            Keith Sweatman, Nihon Superior Co.,    Jason Young, Kemet Electronics
Bihari Patel, MacDermid, Inc.              Ltd.                                   Corporation
Michael Pavlov, ECI Technology, Inc.    Michael Toben, Rohm and Haas           Michael W. Yuen, Microsoft
                                           Electronic Materials                   Corporation
John W. Porter, Multicore Solders
  Ltd.                                  Dr. Brian J. Toleno, Henkel            Dr. Adam Zbrzezny, AMD
John M. Radman, Trace                      Corporation
  Laboratories - East
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                                                                  Table of Contents
1     SCOPE ........................................................................ 1       4       TEST PROCEDURES ................................................. 6
1.1         Scope ..................................................................... 1    4.1          Application of Flux ................................................ 6
1.2         Purpose .................................................................. 1     4.2          Visual Acceptance Criteria Tests ............................. 8
1.2.1       Shall and Should .................................................... 1          4.2.1        Test A – Tin/Lead Solder – Solder Bath/Dip and
1.2.2       Document Hierarchy ............................................... 1                          Look Test (Leads, Wires, etc.) ................................ 8
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4.2.7.1.2 Vertical Dipping Device ........................................ 16              4.3.2.4.3 Gauge Repeatability and Reproducibility
                                                                                                     (GR&R) Protocol ................................................. 22
4.2.7.2     Preparation ........................................................... 16
                                                                                           4.3.3        Test G – Tin/Lead Solder – Wetting Balance
4.2.7.3     Procedure ............................................................. 16                  Globule Test ......................................................... 23
4.2.7.4     Evaluation ............................................................ 16     4.3.3.1      Apparatus ............................................................. 23
4.2.7.4.1 Magnification ........................................................ 16        4.3.3.1.1 Dipping Device .................................................... 23
4.2.7.4.2 Accept/Reject Criteria ........................................... 16            4.3.3.2      Materials .............................................................. 23
4.2.8       Test C1 – Lead-free Solder – Wrapped Wires                                     4.3.3.2.1 Flux ..................................................................... 23
            Test (Lugs, Tabs, Terminals, Large Stranded                                    4.3.3.2.2 Solder .................................................................. 23
            Wires) .................................................................. 17
                                                                                           4.3.3.2.3 Test Specimen ...................................................... 23
4.2.8.1     Apparatus ............................................................. 17
                                                                                           4.3.3.3      Procedure ............................................................. 23
4.2.8.1.1 Solder Pot/Bath .................................................... 17
                                                                                           4.3.3.3.1 Temperature of the Solder .................................... 23
4.2.8.1.2 Dipping Device .................................................... 17
                                                                                           4.3.3.3.2 Fluxing ................................................................ 23
4.2.8.2     Preparation ........................................................... 17     4.3.3.3.3 Dipping Angle, Immersion Depth, and
4.2.8.3     Procedure ............................................................. 17               Immersion Rates ................................................... 23
4.2.8.4     Evaluation ............................................................ 17     4.3.3.3.4 Preheat ................................................................. 23
4.2.8.4.1 Magnification ........................................................ 17        4.3.3.4      Evaluation ............................................................ 23
4.2.8.4.2 Accept/Reject Criteria ........................................... 17            4.3.3.4.1 Magnification ........................................................ 23
4.2.9       Test S1 – Lead-free Solder – Surface Mount                                     4.3.3.4.2 Suggested Criteria ................................................ 23
            Process Simulation Test ........................................ 18
                                                                                           4.3.4        Test E1 – Lead-free Solder – Wetting Balance
4.2.9.1     Apparatus ............................................................. 18                  Solder Pot Test (Leaded Components) ................... 26
4.2.9.1.1 Stencil/Screen ....................................................... 18        4.3.4.1      Apparatus ............................................................. 26
4.2.9.1.2 Paste Application Tool .......................................... 18             4.3.4.1.1 Dipping Device .................................................... 26
4.2.9.1.3 Test Substrate ....................................................... 18        4.3.4.2      Preparation ........................................................... 26
4.2.9.1.4 Lead-Free Reflow Equipment ................................ 18                   4.3.4.3      Procedure ............................................................. 26
4.2.9.2     Preparation ........................................................... 18     4.3.4.4      Evaluation ............................................................ 26
4.2.9.3     Procedure ............................................................. 18     4.3.4.4.1 Magnification ........................................................ 26
4.2.9.4     Evaluation ............................................................ 18     4.3.4.4.2 Accept/Reject Criteria ........................................... 26
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4.3.4.4.3 Gauge Repeatability and Reproducibility                                             Figure 4–3 Solder Dipping Depth for Through-
          (GR&R) Protocol ................................................. 26                           Hole Components ............................................. 9
4.3.5        Test F1 – Lead-free Solder – Wetting Balance                                     Figure 4–4 Leadless Component Immersion Depth ........... 10
             Solder Pot Test (Leadless Components) ................. 27                       Figure 4–5 Illustration of Acceptable Solderable
4.3.5.1      Apparatus ............................................................. 27                  Terminal ......................................................... 11
4.3.5.1.1 Dipping Device .................................................... 27              Figure 4–6 Illustration of Unsolderable Terminal .............. 11
4.3.5.2      Preparation ........................................................... 27       Figure 4–7 Illustration of Acceptable Solderable
4.3.5.3      Procedure ............................................................. 27                  Stranded Wire ................................................ 11
4.3.6.4.2 Suggested Criteria ................................................ 28              Figure B-4 Aid in Evaluation of 5% Allowable Area
                                                                                                         of Pin Holes .................................................. 42
5     NOTES ....................................................................... 29        Figure B-5 Solderability Coverage Guide ......................... 43
5.1          Use of Activated Flux .......................................... 29              Figure C-1 Lead Periphery and Volume for a 132
5.2          Massive Components ............................................ 29                          I/O PQFP ....................................................... 45
5.3          Sampling Plans ..................................................... 29                                             Tables
5.4          Safety Notes ......................................................... 29        Table 1–1       Steam Conditioning Categories for
5.5          Correction for Buoyancy ....................................... 29                               Component Leads and Terminations .................. 2
5.6          Accelerated Steam Conditioning Limitations .......... 29                         Table 3–1       Flux Compositions ........................................... 3
                                                                                              Table 3–2       Steam Temperature Requirements ...................... 4
Appendix        A ...................................................................... 30
                                                                                              Table   3–3     Solderability Test Selection Component Type .... 5
Appendix        B ...................................................................... 39
                                                                                              Table   3–4     Maximum Limits of Solder Bath Contaminant .. 6
Appendix        C ...................................................................... 44
Appendix        D ...................................................................... 46   Table   4–1     Stencil Thickness Requirements ...................... 14
Appendix        E ...................................................................... 47   Table   4–2     Reflow Parameter Requirements ...................... 14
Appendix        F ...................................................................... 48   Table   4–3     Stencil Thickness Requirements ...................... 18
Appendix        G ..................................................................... 50    Table 4–4       Lead-free Reflow Parameter Requirements ...... 18
Appendix        H ...................................................................... 53   Table 4–5       Wetting Balance Parameter and Suggested
                                                                                                              Evaluation Criteria ......................................... 20
                                      Figures
                                                                                              Table 4–6       Dipping Angle and Immersion Depth for
Figure 3–1 Example Reticle ............................................... 4                                  Components (Directly from IEC 60068-2-69) .. 24
Figure 4–1 Dipping Schematic ........................................... 8                    Table 4–7       Wetting Parameters and Suggested
Figure 4–2 Solder Dipping Angle for Surface Mount                                                             Evaluation Criteria ......................................... 25
           Leaded Components ......................................... 9                      Table 3–1       Flux Compositions ......................................... 48
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1.4 Coating Durability The following are guidelines, not       1.7 Contractual Agreement In cases where the stated
specification requirements, for determining the needed         test parameters are inappropriate or insufficient, alternative
level of steam conditioning category assurance (see Table      parameters may be agreed upon between vendor and user.
1–1). The Coating Durability guidelines describe three
broad usage sectors and are not intended to encompass all      2 APPLICABLE DOCUMENTS
possible product use scenarios. The user and vendor need
to agree on the coating durability requirements. Coating       The following documents of the issue currently in effect
Durability Category 3 is the default condition for tin-        form a part of this standard to the extent specified herein.
based finishes.
                                                               2.1 Industry
Category 1 — Minimum Coating Durability Intended for
surfaces that will be soldered within a short period of time
(e.g., up to six months) from the time of testing and are      2.1.1 IPC1
likely to experience a minimum of thermal exposures
                                                               IPC-T-50 Terms and Definitions
before soldering (see 5.6).
Category 2 — Typical Coating Durability Intended for           IPC-TR-464 Accelerated Aging for Solderability Evalua-
surfaces that will be soldered after an extended time from     tions and Addendum
the time of testing and which may see limited thermal
exposures before soldering (see 5.6).                          J-STD-004 Requirements For Soldering Fluxes
Category 3 – Enhanced Coating Durability (default for
                                                               J-STD-005 Requirements for Soldering Pastes
tin-based finishes) Intended for surfaces whose solderabil-
ity may become degraded from storage of longer than six
                                                               J-STD-006 Requirements for Electronic Grade Solder
months or from multiple thermal exposures (see 5.6).
                                                               Alloys and Fluxed and Non-Fluxed Solid Solder for
         Table 1–1 Steam Conditioning Categories               Electronic Soldering Applications
          for Component Leads and Terminations
    Category 1        Category 2            Category 3         IPC-TM-650 Test Methods Manual
     No Steam       1 Hour ± 5 min.      8 hours ± 15 min.
    Conditioning        Steam                 Steam            2.1.2 International Electrotechnical Commission2
    Requirements      Conditioning          Conditioning
1. www.ipc.org
2. www.iec.ch
2
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Dissolution of Component Metallization (Leaching) The          The user’s specific production solder paste product may
loss or removal of metallization from an area on the basis     be used for Test S1 upon agreement between user and
or substrate material after immersion in molten solder.        supplier.
Equilibrium Wetting The degree of wetting in which the
                                                               3.2.2 Flux The flux for tin/lead solderability tests shall
forces of wetting are in equilibrium with the forces of
                                                               be a standard activated rosin flux #1 having a composition
gravity.
                                                               of 25% ± 0.5% by weight of colophony and 0.15% ±
Note: This wetting is visible when the wetting balance         0.01% by weight diethylammonium hydrochloride (CAS
curve flattens out and approaches zero slope (see Figure       660-68-4), in 74.85% ± 0.5% by weight of isopropyl
4–10).                                                         alcohol (see Table 3–1).
Nonwetting, Solder* The partial adherence of molten            The flux for lead-free solderability tests shall be standard
solder to a surface that it has contacted while leaving        activated rosin flux #2 having a composition of 25% ±
some basis metal exposed.                                      0.5% by weight of colophony and 0.39% ± 0.01% by
                                                               weight diethylammonium hydrochloride (CAS 660-68-4),
Pinhole* An imperfection in the form of a small hole that      in 74.61% ± 0.5% by weight of isopropyl alcohol (see
penetrates through a layer of material.                        Table 3–1).
Solderability* The ability of a metal to be wetted by
                                                                              Table 3–1 Flux Compositions
molten solder.
                                                                                                    Composition by
Solder Connection Pinhole* A small hole that penetrates                                             Weight Percent
from the surface of a solder connection to a void of                    Constituent              Flux #1        Flux #2
indeterminate size within the solder connection.               Colophony                         25 ± 0.5       25 ± 0.5
                                                               Diethylammonium Hydrochlo-       0.15 ± 0.01   0.39 ± 0.01
Wetting, Solder* The formation of a relatively uniform,
                                                               ride (CAS 660-68-4)
smooth, unbroken, and adherent film of solder to a basis
                                                               Isopropyl Alcohol (IPA) (CAS      Balance        Balance
metal.                                                         67-63-0)
                                                               Weight of Chlorine as % of           0.2           0.5
3.2 Materials All chemicals shall be of commercial             Solids
grade or better. Fresh solvents shall be used as often as is
necessary to preclude contamination.                           Appendix E: Informative Annex contains a listing of
                                                               industry test flux product sources.
3.2.1 Solder   For tin/lead testing, the solder composition    The flux to be used in preparing the standard copper
shall be Sn60Pb40 or Sn63Pb37 per J-STD-006. The               wrapping wires (see 3.2.4) for tests C and C1 shall
composition of the solder, including contamination levels,     conform to J-STD-004, Type ROL1. This flux shall be
shall be maintained during testing per 3.5.2.                  restricted to the preparation of the standard wrapping
                                                               wires and shall not be used in performing the solderabil-
The composition of the tin/lead solder paste to be used in     ity tests for any of the methods herein.
Test S shall be Sn60Pb40 or Sn63Pb37 for tin/lead per
J-STD-005, mesh size of -325/+500, flux type ROL1. The         3.2.2.1 Flux    Maintenance Standard activated rosin
solder paste shall meet the storage and shelf life require-    fluxes #1 and #2 shall be covered when not in use and
ments of the manufacturer’s specification. The user’s          discarded after eight hours or the flux shall be maintained
specific production solder paste product may be used for       to a specific gravity of 0.843 ± 0.005 at 25 ± 2°C [77 ±
Test S upon agreement between user and supplier.               3.6°F] and discarded after one week of use.
For lead-free testing, the solder composition shall be
                                                               3.2.3 Flux Removal Material used for cleaning flux from
Sn96.5Ag3.0Cu0.5 (SAC305) per J-STD-006. Other lead-
                                                               leads and terminations before solderability evaluations
free solder alloys may be used upon agreement between
                                                               shall be capable of removing visible flux residues (see
user and vendor.
                                                               5.4). The cleaned surface shall exhibit no mechanical
The composition of the lead-free solder paste to be used       damage.
in Test S1 shall be Sn96.5Ag3.0Cu0.5 (SAC305) per
J-STD-005, mesh size of -325/+500, flux type to be             3.2.4 Standard Copper Wrapping Wires The standard
agreed upon between user and vendor. The solder paste          wrapping wires specified in 4.2.3.2 shall be fabricated
shall meet the storage and shelf life requirements of the      from type S, soft or drawn and annealed, uncoated in
manufacturer’s specification. Other lead-free solder pastes    accordance with (CID) A-A-59551 and prepared per the
may be used upon agreement between user and vendor.            following process.
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The nominal diameter of the wrapping wires shall be 0.6               Table 3–2 Steam Temperature Requirements
mm [0.023 in]. The preparation of the wrapping wires                Altitude          Average Local         Steam Tempera-
shall be as follows:                                                                 Boiling Point °C        ture Limits °C
                                                                    0–305 m                100                  93 ± 3
a. Straighten and cut wires into convenient lengths (50
                                                                  305–610 m                99                   92 ± 3
   mm [1.9 in] minimum).
                                                                  610–914 m                98                   91 ± 3
b. Degrease by immersion in an appropriate cleaner (e.g.,
                                                                  914–1219 m               97                   90 ± 3
   isopropyl alcohol) for two minutes.
                                                                 1219–1524 m               96                   89 ± 3
c. Clean in fluoroboric acid 10% HBF4 (by volume), in
                                                                 1524–1829 m               95                   88 ± 3
   water, for five minutes at room temperature with
   agitation. Use caution in handling.                          solder vessel shall be of adequate dimensions to accom-
d. Rinse acid off as follows:                                   modate the specimens and contain sufficient solder to
    1. Two nonheated water rinses (deionized or distilled).     maintain the solder temperature during testing, and to
                                                                prevent exceeding the contamination levels (see 3.5.1 and
    2. Two isopropyl alcohol rinses.
                                                                3.5.2). A minimum of 750 grams of solder should be used.
    3. Air dry.                                                 Note: Precautions should be taken to avoid solder vessel
e. Immerse in flux J-STD-004, Type ROL1.                        damage due to metal erosion when using Lead-free solder
f. Dip in molten solder for five seconds at 245 ± 5°C           alloys.
   [473 ± 9°F] for tin/lead solder alloy. Dip in molten
   solder for five seconds at 255 ± 5°C [491± 9°F] for          3.3.3 Optical Inspection Equipment All test methods
   lead-free solder alloy.                                      requiring visual inspection shall use microscope(s)
                                                                capable of 10X magnification (see individual test meth-
To remove or dissolve the residual flux, wash or rinse per      ods), equipped with reticles, or equivalent, for measure-
3.2.3.                                                          ment. An example of a reticle is shown in Figure 3–1.
Standard wrapping wires will be stored in a clean,              Shadowless lighting shall be suitable for proper inspec-
covered container if not used immediately. The usable life      tion.
of the standard wrapping wires shall not exceed 30 days
after coating.
                                                                             20    15    10      5      0
3.2.5 Water The water to be used for steam condition-
ing purposes shall be distilled or deionized.                                                                  0
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3.3.3.1 Referee     Magnification Referee magnification          Special preparation of leads or terminations, such as
shall be 30X. For fine pitch leaded parts (0.5 mm [0.020         bending or reorientation before test, shall be specified in
in] pitch or less) the referee magnification shall be 70X.       the applicable procurement document. If the insulation on
Referee conditions shall only be used to accept a product        stranded wire must be removed, it shall be done in a
that has been rejected at the inspection magnification.          manner so as not to loosen or damage the individual
                                                                 strands of the wires.
3.3.4 Dipping Equipment Solder dipping devices shall
be mechanical/electro-mechanical and capable of control-         3.4.1.1 Steam Conditioning Categories The user shall
ling the immersion/emersion rates, dwell time and immer-         specify to the vendor, as part of the purchase agreement,
sion depth as specified in 4.2.1 to 4.2.9. Sample holding        the required coating durability (see 1.4). Accelerated
fixtures shall be designed to avoid trapping any excess          steam conditioning shall be performed per Table 1–1.
flux in the fixture and to minimize heat loss and assure         Solderability testing shall be performed per the appropri-
reproducibility of test results.                                 ate test in Table 3–3.
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Specimens shall not be stacked in a manner which                Table 3–4 Maximum Limits of Solder Bath Contaminant
restricts their surface exposure to steam nor shall they be                                                        Maximum Con-
placed closer than 10 mm [0.39 in] from the outer                                      Maximum Con-              tamination Weight
                                                                                      taminant Weight             Percentage Limit
chamber walls, and shall not touch the inner container                                Percentage Limit               Lead-free
walls. In addition, no portion of the specimen shall be          Contaminant          Sn Pb Alloys (1,2)             Alloys (3,4)
less than 40 mm [1.57 in] above the water level.                    Copper                    0.300                      1.000
                                                                      Gold                    0.200                      0.200
3.4.2.1 Post Conditioning Drying After steam condi-                Cadmium                    0.005                      0.005
tioning is complete, specimens shall be immediately                   Zinc                    0.005                      0.005
removed from the chamber and ambient air dried. Solder-            Aluminum                   0.006                      0.006
ability testing shall be performed within 72 hours of
                                                                   Antimony                   0.500                      0.500
removal from the chamber.
                                                                      Iron                    0.020                      0.020
                                                                    Arsenic                   0.030                      0.030
3.4.2.2 Equipment Maintenance Before use, the steam
                                                                    Bismuth                   0.250                      0.250
conditioning apparatus shall have been cleaned with
                                                                     Silver                   0.100                      4.000
deionized or distilled water or hydrogen peroxide to
remove any accumulated residues. This cleaning should be             Nickel                   0.010                      0.010
accomplished within five working days of the condition-               Lead                     N/A                       0.100
ing period.                                                    Notes:
                                                               1. The tin content of the solder shall be maintained within ± 1% of the
                                                                  nominal alloy being used. Tin content shall be tested at the same
                                                                  frequency as testing for copper/gold contamination. The balance of the
3.4.3 Surfaces to be Tested The critical areas of leads
                                                                  bath shall be lead and/or the items listed above.
or terminations intended to be soldered shall be evaluated     2. The total of copper, gold, cadmium, zinc, and aluminum contaminants
for solderability per the test method (see appendix A).           shall not exceed 0.4%. Not applicable to lead-free alloys.
                                                               3. The tin content of the solder shall be maintained within ± 1% of the
This shall include both the bottom termination and                nominal alloy being used. Tin content shall be tested at the same
castellation on chip carriers and on all surfaces intended        frequency as testing for copper/silver concentration. The balance of the
to be soldered on discrete devices. Through-hole leads            bath shall be the items listed above.
                                                               4. Maximum contamination limits are applicable for Sn96.5Ag3.0Cu0.5
that are tested by Method A shall have a 25 mm [0.98 in]          (SAC305) per J-STD-006. Other lead-free solder alloy contamination
portion, or the whole lead if less than 25 mm [0.98 in],          limits may be used upon agreement between user and vendor.
evaluated for solderability (see 4.2.1.4). Test methods
                                                               NOTE: An operating day consists of any eight-hour
shall be selected per Table 3–3.
                                                               period, or any portion thereof, during which the solder is
Surfaces to be tested by Method D shall be completely          liquefied and used.
immersed in molten solder during dipping (see 4.2.4).
                                                               If contamination exceeds the limits specified in Table 3–4,
                                                               then the solder shall be changed and the intervals between
3.5 Solder Bath Requirements                                   analysis shall be shortened. A sampling plan shall be
                                                               developed, implemented, and documented, demonstrating
3.5.1 Solder Temperatures Tin/lead solderability testing       solder contamination limit process control.
shall be done at a solder temperature of 245 ± 5°C [473 ±
9°F]. Lead-free solderability testing shall be done at a       4 TEST PROCEDURES
solder temperature of 255 ± 5°C [491 ± 9°F]. A
temperature of 260 ± 5°C [500 ± 9°F] shall be used for         4.1 Application of Flux Flux per 3.2.2 shall be used.
Test Method D for both tin/lead or lead-free solder alloys.    Leads and terminations shall have flux applied uniformly
                                                               and to cover the surfaces to be tested. The flux shall be at
                                                               room temperature. This section, 4.1, shall apply to all of
3.5.2 Solder Contamination Control The solder in sol-
                                                               the following tests: A, B, C, D, E, F, G, A1, B1, C1, E1,
der baths used for solderability testing shall be chemically
                                                               F1 and G1 but shall not apply to both tests S and S1,
or spectrographically analyzed or replaced each 30 oper-
                                                               which require the use of solder paste and not a separate
ating days. The levels of contamination and Sn content
                                                               flux.
must be within those shown in Table 3–4. The intervals
between analysis may be lengthened if the test results         Axial, radial, and multiple leaded components intended
indicate that the contamination limits are not being           for through-hole mounting shall have their leads
approached. The composition of the lead-free solder,           immersed into the flux approximately perpendicular to the
including contamination levels, shall be maintained during     flux surface. Leaded or leadless components intended for
testing with the silver and copper element levels adjusted     surface mounting shall have their leads or terminations
for alloy requirements.                                        immersed at an angle between 20° and 45° to the flux
6
                     SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
surface. The surfaces to be tested shall be immersed in       may be (but are not required to be) blotted from the
the flux for 5 to 10 seconds. Any droplets of flux that may   surface. The specimens being tested shall be allowed to
form shall be removed by blotting, taking care not to         dry for 5 to 20 seconds before solder immersion, but shall
remove the flux coating from the surfaces to be tested.       not be allowed to dwell above solder-pot (no preheat)
For small passive surface mount devices, the flux droplets    before actual dipping action.
                                                                                                                      7
                            SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
4.2 Visual Acceptance Criteria Tests b) 255 ± 5°C [491 ± 9°F] for lead-free solder testing.
                                            Stop
                                   Start
                                               Termination
                                               to be tested
Dwell Dwell
                                    Flux                                      Solder
                                   Station                                    Station*
IPC-002c-4-1
8
                     SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
                                                      20-45°                        90°
                                                                                            Molten Solder Surface
                                                                                                                IPC-002c-4-2
Figure 4–2 Solder Dipping Angle for Surface Mount Leaded Components
      1.27 mm                                                  1.27 mm
      [0.050 in]                                              [0.050 in]
                                                                           DIP
                                                                                            Molten Solder Surface
IPC-002c-4-3
4.2.1.4.2 Accept/Reject Criteria All leads shall exhibit          surfaces. Anomalies other than dewetting, nonwetting, and
a continuous solder coating free from defects for a               pin holes are not cause for rejection (see Appendices A
minimum of 95% of the critical area of any individual             and B). Exposed terminal metal is allowable on surface
lead. For exposed pad packages the exposed pad surfaces           mount components at the toe end and on the vertical
shall exhibit a continuous solder coating free from defects       surfaces that are either unplated or sheared during
for a minimum of 80% of the critical area of those                component fabrication.
                                                                                                                               9
                          SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
4.2.2 Test B – Tin/Lead Solder – Solder Bath/Dip and         b. The fluxed specimen shall be immersed in the molten
Look Test (Leadless Components) This test is for solder         solder 0.10 mm [0.0039 in] minimum (see Figure 4–4).
bath/dip and look testing of leadless components.               Immerse and withdraw at 25 ± 6 mm [0.984 ± 0.24 in]
                                                                per second and dwell for 5 +0/-0.5 seconds. Massive
4.2.2.1 Apparatus                                               components may require a longer molten solder dwell
4.2.2.1.1 Solder Pot/Bath A solder vessel that meets the        time (see 5.2).
requirements of 3.3.2 shall be used. The solder shall meet   c. After withdrawal, the solder shall be allowed to
the requirements of 3.2.1. Solder bath temperatures and         solidify by air cooling while the specimen is main-
solder contamination control shall be in accordance with        tained in the test attitude.
3.5.1 and 3.5.2.                                             d. Before examination, all terminations shall have all
                                                                visible flux residues removed per 3.2.3.
4.2.2.1.2 Vertical   Dipping Device A mechanical or
electro-mechanical dipping device similar to the device      4.2.2.4 Evaluation
shown in Figure 4–1 shall be used unless otherwise           4.2.2.4.1 Magnification Parts shall be examined at 10X
agreed to between user and vendor. The rate of immer-        using the equipment specified in 3.3.3. For fine pitch
sion, dwell time, and rate of withdrawal shall be within     termination parts (0.5 mm [0.020 in] pitch or less) the
the test limits defined in 4.2.2.3. Surface mount leadless   inspection magnification shall be 30X.
components shall be immersed at an angle to the solder       4.2.2.4.2 Accept/Reject Criteria All terminations shall
surface of 20°- 45° and 90° for discrete chip components     exhibit a continuous solder coating free from defects for a
and exposed pad packages. Other immersion angles may         minimum of 95% of the critical area of any individual
be used if agreed upon between vendor and user.              termination. For exposed pad packages, the exposed pad
                                                             surfaces shall exhibit a continuous solder coating free
4.2.2.2 Preparation Specimen preparation shall be in
                                                             from defects for a minimum of 80% of the critical area of
accordance with 3.4.
                                                             those surfaces. Anomalies other than dewetting, nonwet-
                                                             ting, and pin holes are not cause for rejection (see
4.2.2.3 Procedure
                                                             Appendices A and B). Exposed terminal metal is allow-
a. Dross and burned flux shall be skimmed from the           able on surface mount components at the toe end and on
   surface of the molten solder immediately before dip-      the vertical surfaces that are either unplated or sheared
   ping.                                                     during component fabrication.
                                          20° - 45°
        >
        _ 0.10 mm                                                                          Molten Solder Surface
     [>
      _ 0.00394 in]
IPC-002c-4-4
10
                       SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
4.2.3.1 Apparatus
4.2.3.3 Procedure
                                                                                                                              11
                          SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
4.2.3.4 Evaluation
g. After the dipping process, the part shall be allowed to   In case of dispute, the percent of fillet-length with defects
   cool in air.                                              shall be determined by their actual measurement. See
h. Before examination, all terminations shall have all       Figure B-4 in Appendix B that serves as an aid in the
   visible flux residue removed per 3.2.3.                   evaluation of the 5% allowable defects.
12
                     SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
4.2.4 Test D – Tin/Lead or Lead-Free Solder – Resis-           4.2.4.2 Preparation Specimen preparation shall be in
tance to Dissolution of Metallization Test This test is to     accordance with 3.4.
reveal a susceptibility to loss of solderability due to
either:                                                        4.2.4.3 Procedure
a. Dissolution of metallization over unsolderable base         a. Dross and burned flux shall be skimmed from the
   material (as indicated by loss of wetting), or                 surface of the molten solder immediately before dip-
                                                                  ping.
b. Accumulation of impurities from the basis metal (as
   indicated by dewetting).                                    b. The flux-covered component metallization shall be
                                                                  immersed only once in the molten solder to a minimum
4.2.4.1 Apparatus                                                 depth to completely cover the termination being tested.
                                                               c. The angle of immersion shall be between 20° and 45°.
4.2.4.1.1 Solder Pot/Bath A solder vessel that meets the
requirements of 3.3.2 shall be used. The solder shall meet     d. Immerse and withdraw at a rate of 25 ± 6 mm [0.984
the requirements of 3.2.1. Solder bath temperatures and           ± 0.24 in] per second and dwell for 30 +/- 5 seconds.
solder contamination control shall be in accordance with
                                                               4.2.4.4 Evaluation
3.5.1 and 3.5.2.
                                                               4.2.4.4.1 Magnification Parts shall be examined at 10X
4.2.4.1.2 Dipping Device A mechanical or electrome-            using the equipment specified in 3.3.3. For fine pitch
chanical dipping device similar to the device shown in         components (0.5 mm [0.020 in] pitch or less) the
Figure 4–1 shall be used unless otherwise agreed to            inspection magnification shall be 30X.
between user and vendor. The rate of immersion, dwell
                                                               4.2.4.4.2 Accept/Reject Criteria The criteria for accept-
time, and rate of withdrawal shall be within the test limits
defined in 4.2.4.3.                                            able resistance to leaching/dewetting shall be no more
                                                               than 5% of the solderable metallization exhibiting exposed
4.2.4.1.3 Attitude (Angle of Immersion) All components         underlying, non-wettable base metal or metallization
shall be dipped using a vertical motion to ensure              layers or portions of the ceramic substrate after exposure
complete immersion of the surfaces to be soldered.             to molten solder.
                                                                                                                      13
                                SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
4.2.5 Test S – Tin/Lead Solder – Surface Mount Pro-                      4.2.5.2 Preparation Specimen preparation shall be in
cess Simulation Test This test simulates actual surface                  accordance with 3.4.
mount component performance in a reflow process.
                                                                         4.2.5.3 Procedure
4.2.5.1 Apparatus                                                        a. Place solder paste (per 3.2.1) onto stencil/screen and
                                                                            print the terminal pattern onto the test substrate by
4.2.5.1.1 Stencil/Screen A stencil or screen with pad
                                                                            wiping paste over the stencil/screen in one smooth
geometry openings that is appropriate for the terminals
                                                                            motion using rubber or metal squeegee.
being tested shall be used. Unless otherwise agreed upon
between vendor and user, the nominal stencil thickness                   b. Remove the stencil/screen carefully to avoid smearing
shall be per Table 4–1.                                                     the paste print.
                                                                         c. Verify a paste print equivalent in geometry to the
         Table 4–1 Stencil Thickness Requirements                           terminal of the device to be tested.
     Nominal Stencil
                                                                         d. Place the terminals of the component being tested on
       Thickness                   Component Lead Pitch
                                                                            the solder paste print.
 0.10 mm [0.00394 in]               <0.508 mm [<0.020 in]
 0.15 mm [0.00591 in]         0.508–0.635 mm [0.020–0.025 in]
                                                                         e. Verify component placement by appropriate magnifica-
                                                                            tion.
 0.20 mm [0.00787 in]               >0.635 mm [>0.025 in]
                                                                         f. Place test substrate on applicable reflow equipment and
4.2.5.1.2 Paste Application Tool A rubber or metal
                                                                            conduct reflow process.
squeegee device shall be used to distribute paste across                 g. After reflow, carefully remove substrate with compo-
stencil/screen.                                                             nent(s) and allow to cool to room temperature.
                                                                         h. Remove component(s) from substrate. Component
4.2.5.1.3 Test Substrate A ceramic substrate 0.635 mm
                                                                            leads may adhere slightly to substrate due to flux
[0.025 in] nominal thickness shall be used for testing.
                                                                            residue.
Other non-wettable substrates may be used if agreed upon
between vendor and user.                                                 i. Before examination, all leads shall have all visible flux
                                                                            residues removed per 3.2.3. Care should be exercised
4.2.5.1.4 Tin/lead Reflow Equipment An IR/convection                        in flux residue removal process to not damage leads.
reflow oven, vapor phase reflow system, or oven capable
of reaching the reflow temperature of the tin/lead paste                 4.2.5.4 Evaluation
shall be used. Unless otherwise agreed upon between                      4.2.5.4.1 Magnification Parts shall be examined at 10X
vendor and user the reflow parameters shall be per Table                 using the equipment specified in 3.3.3. For fine pitch
4–2.                                                                     leaded/termination parts (0.5 mm [0.020 in] pitch or less)
                                                                         the inspection magnification shall be 30X.
         Table 4–2 Reflow Parameter Requirements
                                                                         4.2.5.4.2 Accept/Reject Criteria All leads shall exhibit
                        Temperature                    Time              a continuous solder coating free from defects for a
 Vapor Phase              215–219°C              30–60 seconds           minimum of 95% of the critical area of any individual
   Reflow                [419–426°F]             dwell at reflow
                                                                         lead. For exposed pad packages the exposed pad surfaces
                        150–170°C                50–70 seconds           shall exhibit a continuous solder coating free from defects
IR/Convection       [302–338°F] Preheat
    Reflow
                                                                         for a minimum of 80% of the critical area of those
                        215–230°C                50–70 seconds
                    [419–446°F] Reflow                                   surfaces. Anomalies other than dewetting, nonwetting, and
                                                                         pin holes are not cause for rejection (see Appendices A
                          215–230°C             2–5 minutes (until
     Oven                                                                and B). Exposed terminal metal is allowable on surface
                         [419–446°F]            reflow is assured)
Note: Table 4–2 reflow parameter values are for solderability testing    mount components at the toe end and on the vertical
purposes and are not related to moisture sensitivity level reflow test   surfaces that are either unplated or sheared during
parameters.
                                                                         component fabrication.
14
                       SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
4.2.6 Test A1 – Lead-free Solder – Solder Bath/Dip and         b. The fluxed specimen shall be immersed in the molten
Look Test (Leads, Wires, etc.) This test is for solder            solder to within 1.27 mm [0.050 in] of the component
bath/dip and look testing of leaded components, solid             body or to the seating plane (whichever is further from
wires, and stranded wires greater than 0.254 mm [0.01 in]         the component body) for through-hole leaded compo-
minimum.                                                          nents (see Figure 4–3).
                                                               c. Immerse and withdraw at 25 ± 6 mm [0.984 ± 0.24 in]
4.2.6.1 Apparatus
                                                                  per second and dwell for 5 +0/-0.5 seconds (see 5.2).
4.2.6.1.1 Solder Pot/Bath A solder vessel that meets the
                                                               d. After withdrawal, the solder shall be allowed to
requirements of 3.3.2 shall be used. The solder shall meet
                                                                  solidify by air cooling while the specimen is main-
the requirements of 3.2.1. Solder bath temperatures and
                                                                  tained in the test attitude.
solder contamination control shall be in accordance with
3.5.1 and 3.5.2.                                               e. Before examination, all leads shall have all visible flux
                                                                  residues removed per 3.2.3.
4.2.6.1.2 Dipping Device A mechanical or electrome-
chanical dipping device similar to the device shown in
                                                               4.2.6.4 Evaluation
Figure 4–1 shall be used unless otherwise agreed to
between user and vendor. The rate of immersion, dwell          4.2.6.4.1 Magnification Parts shall be examined at 10X
time, and rate of withdrawal shall be within the test limits   using the equipment specified in 3.3.3. For fine pitch
defined in 4.2.6.3. Perpendicularity of through-hole com-      leaded parts (0.5 mm [0.020 in] pitch or less) the
ponent leads to solder surface shall be maintained. Leaded     inspection magnification shall be 30X.
surface mount components shall be immersed at between
20° and 45° (or 90° if agreed upon) to the solder surface      4.2.6.4.2 Accept/Reject Criteria All leads shall exhibit
(see Figure 4–2). This angle shall remain consistent for       a continuous solder coating free from defects for a
any given component type. Wobble, vibration and other          minimum of 95% of the critical area of any individual
extraneous movements shall be minimized.                       lead. For exposed pad packages the exposed pad surfaces
                                                               shall exhibit a continuous solder coating free from defects
4.2.6.2 Preparation Specimen preparation shall be in           for a minimum of 80% of the critical area of those
accordance with 3.4.                                           surfaces. Anomalies other than dewetting, nonwetting, and
                                                               pin holes are not cause for rejection (see Appendices A
4.2.6.3 Procedure
                                                               and B). Exposed terminal metal is allowable on surface
a. Dross and burned flux shall be skimmed from the             mount components at the toe end and on the vertical
   surface of the molten solder immediately before dip-        surfaces that are either unplated or sheared during
   ping.                                                       component fabrication.
                                                                                                                        15
                          SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
4.2.7 Test B1 – Lead-free Solder – Solder Bath/Dip and       b. The fluxed specimen shall be immersed in the molten
Look Test (Leadless Components) This test is for solder         solder 0.10 mm [0.0039 in] minimum (see Figure 4–4).
bath/dip and look testing of leadless components.               Immerse and withdraw at 25 ± 6 mm [0.984 ± 0.24 in]
                                                                per second and dwell for 5 +0/-0.5 seconds. Massive
4.2.7.1 Apparatus                                               components may require a longer molten solder dwell
                                                                time (see 5.2).
4.2.7.1.1 Solder Pot/Bath A solder vessel that meets the
requirements of 3.3.2 shall be used. The solder shall meet   c. After withdrawal, the solder shall be allowed to
the requirements of 3.2.1. Solder bath temperatures and         solidify by air cooling while the specimen is main-
solder contamination control shall be in accordance with        tained in the test attitude.
3.5.1 and 3.5.2.                                             d. Before examination, all terminations shall have all
                                                                visible flux residues removed per 3.2.3.
4.2.7.1.2 Vertical   Dipping Device A mechanical or
electro-mechanical dipping device similar to the device      4.2.7.4 Evaluation
shown in Figure 4–1 shall be used unless otherwise
                                                             4.2.7.4.1 Magnification Parts shall be examined at 10X
agreed to between user and vendor. The rate of immer-
                                                             using the equipment specified in 3.3.3. For fine pitch
sion, dwell time, and rate of withdrawal shall be within
                                                             termination parts (0.5 mm [0.020 in] pitch or less) the
the test limits defined in 4.2.7.3. Surface mount leadless
                                                             inspection magnification shall be 30X.
components shall be immersed at an angle to the solder
surface of 20°- 45° and 90° for discrete chip components     4.2.7.4.2 Accept/Reject Criteria All terminations shall
and exposed pad packages. Other immersion angles may         exhibit a continuous solder coating free from defects for a
be used if agreed upon between vendor and user.              minimum of 95% of the critical area of any individual
                                                             termination. For exposed pad packages, the exposed pad
4.2.7.2 Preparation Specimen preparation shall be in
                                                             surfaces shall exhibit a continuous solder coating free
accordance with 3.4.                                         from defects for a minimum of 80% of the critical area of
                                                             those surfaces. Anomalies other than dewetting, nonwet-
                                                             ting, and pin holes are not cause for rejection (see
4.2.7.3 Procedure
                                                             Appendices A and B). Exposed terminal metal is allow-
a. Dross and burned flux shall be skimmed from the           able on surface mount components at the toe end an on
   surface of the molten solder immediately before dip-      the vertical surfaces that are either unplated or sheared
   ping.                                                     during component fabrication.
16
                       SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
4.2.8 Test C1 – Lead-free Solder – Wrapped Wires Test             wrapping wires specified in 3.2.4 shall be the same
(Lugs, Tabs, Terminals, Large Stranded Wires) This test           size for which the lugs and tabs are designed.
is for wrapped wires testing of lugs, tabs, terminals,
                                                               4.2.8.3 Procedure
stranded wires greater than 1.016 mm [0.040 in] diameter,
and solid wires greater than 1.143 mm [0.045 in]               a. The flux shall be at ambient (room) temperature per
                                                                  3.2.2.
diameter.
                                                               b. Terminations shall be immersed in the flux to the
                                                                  minimum depth necessary to cover the surface to be
4.2.8.1 Apparatus
                                                                  tested.
4.2.8.1.1 Solder Pot/Bath A solder vessel that meets the       c. The surface to be tested shall be immersed for 5 to 10
requirements of 3.3.2 shall be used. The solder shall meet        seconds and allowed to drain for 10 to 60 seconds.
the requirements of 3.2.1. Solder bath temperatures and        d. The dross and burned flux shall be skimmed from the
solder contamination control shall be in accordance with          surface of the molten solder just before immersing the
3.5.1 and 3.5.2.                                                  terminations in the solder.
                                                               e. Immerse and withdraw at a rate of 25 ± 6 mm [0.984
4.2.8.1.2 Dipping Device A mechanical or electrome-               ± 0.24 in] per second and dwell for 7 ± 0.50 seconds.
chanical dipping device similar to the device shown in
                                                               f. The part shall be attached to a dipping device and the
Figure 4–1 shall be used unless otherwise agreed to
                                                                  flux-covered terminations immersed once in the molten
between user and vendor. The rate of immersion, dwell
                                                                  solder to the same depth specified in 4.2.8.3b.
time, and rate of withdrawal shall be within the test limits
defined in 4.2.8.3. Wobble, vibration, and other extraneous    g. After the dipping process, the part shall be allowed to
movements shall be minimized.                                     cool in air.
                                                               h. Before examination, all terminations shall have all
                                                                  visible flux residue removed per 3.2.3.
4.2.8.2 Preparation Specimen preparation shall be in
accordance with 3.4.                                           4.2.8.4 Evaluation
                                                               4.2.8.4.1 Magnification Parts shall be examined at 10X
a. For application of standard solderable wires for lugs,      using the equipment specified in 3.3.3.
   tabs, terminals, stranded wires greater than 1.016 mm
                                                               4.2.8.4.2 Accept/Reject Criteria The criteria for accept-
   [0.040 in] diameter, and solid wires greater than 1.143
                                                               able solderability of lugs, tabs, terminals, stranded wires
   mm [0.045 in] diameter, all specimens shall have a
                                                               greater than 1.016 mm [0.040 in] diameter, solid wires
   wrap of 1.5 turns of the standard wires around the
                                                               greater than 1.143 mm [0.045 in] diameter are:
   portion of the specimen to be tested.
                                                               a. A minimum of 95% of the total length of fillet between
b. The standard wrapping wires as described in 3.2.4              wrap wires and termination shall be tangent to the
   shall be wrapped in such a manner so that it will not          surface of the termination and be free of anomalies
   move during the solder dip. Examples of this wrap are          such as pinholes.
   shown in Figures 4–5 through 4–8.
                                                               b. A ragged or interrupted tangency line indicates a
c. Special instructions concerning the portion of the             defect.
   specimens to be wrapped shall be specified in the           In case of dispute, the percent of fillet-length with defects
   individual specification, if necessary.                     shall be determined by their actual measurement. See
d. For lugs and tabs designed to accept wires smaller than     Figure B-4 in Appendix B that serves as an aid in the
   0.6 mm [0.024 in] diameter, the standard copper             evaluation of the 5% allowable defects.
                                                                                                                         17
                                SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
4.2.9 Test S1 – Lead-free Solder – Surface Mount                         4.2.9.2 Preparation Specimen preparation shall be in
Process Simulation Test This test simulates actual sur-                  accordance with 3.4.
face mount component performance in a reflow process.
                                                                         4.2.9.3 Procedure
4.2.9.1 Apparatus                                                        a. Place solder paste (see 3.2.1) onto stencil/screen and
                                                                            print the terminal pattern onto the test substrate by
4.2.9.1.1 Stencil/Screen A stencil or screen with pad
                                                                            wiping paste over the stencil/screen in one smooth
geometry openings that is appropriate for the terminals
                                                                            motion using rubber or metal squeegee.
being tested shall be used. Unless otherwise agreed upon
between vendor and user the nominal stencil thickness                    b. Remove the stencil/screen carefully to avoid smearing
shall be per Table 4–3.                                                     the paste print.
                                                                         c. Verify a paste print equivalent in geometry to the
         Table 4–3 Stencil Thickness Requirements                           terminal of the device to be tested.
      Nominal Stencil              Component Lead Pitch
                                                                         d. Place the terminals of the component being tested on
        Thickness
                                                                            the solder paste print.
 0.10 mm [0.00394 in]               <0.508 mm [<0.020 in]
 0.15 mm [0.00591 in]         0.508–0.635 mm [0.020–0.025 in]
                                                                         e. Verify component placement by appropriate magnifica-
                                                                            tion.
 0.20 mm [0.00787 in]               >0.635 mm [>0.025 in]
                                                                         f. Place test substrate on applicable reflow equipment and
4.2.9.1.2 Paste Application Tool A rubber or metal
                                                                            conduct reflow process.
squeegee device shall be used to distribute paste across                 g. After reflow, carefully remove substrate with compo-
stencil/screen.                                                             nent(s) and allow to cool to room temperature.
                                                                         h. Remove component(s) from substrate. Component
4.2.9.1.3 Test Substrate A ceramic substrate 0.635 mm
                                                                            leads may adhere slightly to substrate due to flux
[0.025 in] nominal thickness shall be used for testing.
                                                                            residue.
Other non-wettable substrates may be used if agreed upon
between vendor and user.                                                 i. Before examination, all leads shall have all visible flux
                                                                            residues removed per 3.2.3. Care should be exercised
4.2.9.1.4 Lead-Free Reflow Equipment An IR/convec-                          in flux residue removal process to not damage leads.
tion reflow oven, vapor phase reflow system, or oven
capable of reaching the reflow temperature of the lead-                  4.2.9.4 Evaluation
free paste shall be used. Unless otherwise agreed upon                   4.2.9.4.1 Magnification Parts shall be examined at 10X
between vendor and user the reflow parameters shall be                   using the equipment specified in 3.3.3. For fine pitch
per Table 4–4.                                                           leaded/termination parts (0.5 mm [0.020 in] pitch or less)
                                                                         the inspection magnification shall be 30X.
     Table 4–4 Lead-free Reflow Parameter Requirements
                                                                         4.2.9.4.2 Accept/Reject Criteria All leads shall exhibit
                        Temperature                    Time              a continuous solder coating free from defects for a
 Vapor Phase              217–240°C              45–90 seconds           minimum of 95% of the critical area of any individual
   Reflow                [423–464°F]             dwell at reflow
                                                                         lead. For exposed pad packages, the exposed pad surfaces
                        150–180°C               60–120 seconds           shall exhibit a continuous solder coating free from defects
IR/Convection       [302–356°F] Preheat
    Reflow
                                                                         for a minimum of 80% of the critical area of those
                        230–250°C                30–60 seconds
                    [446–482°F] Reflow                                   surfaces. Anomalies other than dewetting, nonwetting, and
                                                                         pin holes are not cause for rejection (see Appendices A
                          230–250°C             2–5 minutes (until
      Oven                                                               and B). Exposed terminal metal is allowable on surface
                         [446–482°F]            reflow is assured)
Note: Table 4–4 reflow parameter values are for solderability testing    mount components at the toe end and on the vertical
purposes and are not related to moisture sensitivity level reflow test   surfaces that are either unplated or sheared during
parameters.
                                                                         component fabrication.
18
                       SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
4.3 Force Measurement Tests                                    c. Dross and burned flux shall be skimmed from the
                                                                  surface of the molten solder immediately before dip-
4.3.1 Test E – Tin/Lead Solder – Wetting Balance                  ping.
Solder Pot Test (Leaded Components) This test is for
                                                               d. The flux covered termination shall be immersed only
wetting balance testing of leaded components.                     once in the molten solder to a depth of 0.10 mm
                                                                  [0.0039 in].
4.3.1.1 Apparatus A solder meniscus force measuring
                                                               e. The angle of immersion shall be 20° – 45° (see Figure
device (wetting balance) which includes a temperature
                                                                  4–2).
controlled solder pot containing solder per 3.2.1 and
maintained per 3.5.1 and 3.5.2 shall be used. The              f. Immerse and withdraw at 1 mm – 5 mm [0.04 - 0.20
equipment shall have a means of recording force as a              in] per second and dwell for 5 +0/-0.5 seconds.
function of time, such as a chart recorder, data logger, or       Massive components may require a longer solder dwell
computer (see Figure 4–9).                                        time (see 5.2).
                                                       Clamp
             Relative
              Motion                                         Test
                                                          Specimen
                                                 Solder
                                                  Bath         Heater
                                                                                Controls
                                                                                                               IPC-002c-4-9
                                                                                                                              19
                                   SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
          Force / mm                                                                                                            AA
           ( N / mm)
F2 F5
T ime (sec.)
20
                      SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
    Force / mm
     ( N / mm)
                                                                                 AA
F2
                                                                                 F5
                  0                                                                   Time (sec.)
T0
                                                                                                             21
                           SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
4.3.2 Test F – Tin/Lead Solder – Wetting Balance              d. After application of the flux and post dip dwell, the
Solder Pot Test (Leadless Components) This test is for           specimen shall be mounted on the test equipment.
wetting balance testing of leadless components.               e. Dross and burned flux shall be skimmed from the
                                                                 surface of the molten solder immediately before dip-
4.3.2.1 Apparatus A solder meniscus force measuring
                                                                 ping.
device (wetting balance) which includes a temperature
controlled solder pot containing solder per 3.2.1 and         f. The flux covered termination shall be immersed only
maintained per 3.5.1 and 3.5.2 shall be used. The                once in the molten solder to a depth of 0.10 mm
equipment shall have a means of recording force as a             [0.0039 in] minimum.
function of time, such as a chart recorder, data logger, or   g. The angle of immersion shall be per Figure 4–4.
computer (see Figure 4–9).                                    h. A full curve shall be recorded using the equipment
4.3.2.1.1 Dipping Device A mechanical or electrome-
                                                                 specified in 4.3.2.1.
chanical dipping device incorporated in the wetting
                                                              4.3.2.4 Evaluation
balance shall be used. The device shall be preset to
produce an immersion and emersion rate as specified in        4.3.2.4.1 Magnification Parts shall be examined at 10X
4.3.2.3. The specimen dwell time is controlled to the time    using the equipment specified in 3.3.3. For fine pitch
specified in 4.3.2.3.                                         termination parts (0.5 mm [0.020 in] pitch or less) the
                                                              inspection magnification shall be 30X.
4.3.2.2 Preparation Specimen preparation shall be in
                                                              4.3.2.4.2 Accept/Reject Criteria Suggested criteria for
accordance with 3.4.
                                                              solderability evaluation for Test F are listed in Table 4–5.
                                                              Figures 4–10 and 4–11 illustrate the suggested criteria of
4.3.2.3 Procedure
                                                              Table 4–5. In addition, the area of the test sample with
a. Flux per 3.2.2 shall be used and shall be at ambient       fresh solder adhesion shall be greater than the area that
   (room) temperature.                                        was immersed in the solder bath (i.e., the component shall
b. Leads and terminations shall have flux applied uni-        exhibit positive wicking beyond its immersion depth).
   formly and to cover the surfaces to be tested.             4.3.2.4.3 Gauge Repeatability and Reproducibility (GR&R)
c. Immerse and withdraw at 1 mm – 5 mm [0.04 in –             Protocol   Appendix H contains a suggested GR&R
   0.20 in] per second and dwell for 5 +0/-0.5 seconds.       protocol that may be used by the supplier and user to
   Massive components may require a longer solder dwell       ensure that the respective wetting balance equipment are
   time (see 5.2).                                            correctly calibrated.
22
                      SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
4.3.3 Test G – Tin/Lead Solder – Wetting Balance                 4.3.3.3.2 Fluxing A very small amount of flux is care-
Globule Test This test is for wetting balance globule            fully applied to the surface or lead to be tested and the
testing of components.                                           solder globule using a clean cotton tip or bud. No excess
4.3.3.1 Apparatus A solder meniscus force measuring              flux shall be ready to drip off the fluxed part or the excess
device (wetting balance) which includes a temperature            flux must be drained off by carefully touching the lowest
controlled vertical, cylindrical iron shaft shrunk fit into an   point on the surface to be tested with a piece of clean
aluminum housing on which is placed a specific sized             chemical lab filter paper. For this testing, ideally a small
piece of solder. Examples are: a 200 mg piece of solder          amount of flux should be kept in a small container that is
for a 4 mm diameter globule block, a 100 mg piece of             only opened to immerse the cotton tip to wet it with flux.
solder for a 3.2 mm diameter globule block, a 25 mg              The cotton tips should be thrown away and replaced with
piece of solder for a 2 mm globule block or a 5 mg piece         fresh ones every 5 to 10 tests, with all tests done in the
for a 1 mm globule block. The molten solder globule              same testing interval. If testing is interrupted for more
should ideally be replaced after each solderability test, but    than a few minutes, then a new tip should be used.
may be re-used for very small components that do not
remove more than 1% of the solder volume per solder test         4.3.3.3.3 Dipping Angle, Immersion Depth, and Immer-
for up to 5 tests. The equipment shall have a means of           sion Rates The appropriate clip shall be chosen to hold
recording force as a function of time, such as a chart           the part as specified in Table 4–6 and illustrated in Figure
recorder, data logger or computer.                               4–12. Without contaminating the surfaces to be tested, the
                                                                 specimen is mounted in the appropriate clip or other
4.3.3.1.1 Dipping Device A mechanical or electrome-
chanical dipping device incorporated in the wetting              device supplied by the solderability tester manufacturer
balance shall be used. The device shall be preset to             and carefully attached to the machine so as to not damage
produce an immersion and emersion rate as specified in           the transducer or dislodge the component from its orien-
4.3.3.3.3. The specimen dwell time is controlled to the          tation in the clip or other holder. The distance between the
time specified in 4.3.3.3.3.                                     solderable surface of the sample and the solder globule
                                                                 should be fixed. An immersion speed between 1
4.3.3.2 Materials
                                                                 mm/second and 5 mm/second [0.039 in/second and 0.20
4.3.3.2.1 Flux The flux used shall be in accordance with         in/second] should ensure that most test specimens are
3.2.2.                                                           fully immersed. A dwell time of 5 seconds shall be used.
4.3.3.2.2 Solder The solder shall be in accordance with          A dwell time of 10 seconds may be necessary for large
3.2.1. Other alloys may be used upon agreement between           components or components with high thermal mass (see
user and other parties.                                          5.2).
4.3.3.2.3 Test Specimen The test specimen shall either
                                                                 4.3.3.3.4 Preheat The decision to use preheat should be
be a full component or a lead that has been carefully
removed from the component. Ideally the cross-section of         by prior agreement between user and supplier (AABUS).
the component to be dipped is either rectangular, square
or round, to facilitate calculation of the theoretical           4.3.3.4 Evaluation
maximum wetting force. Ideally no burr should be present
but, if they are, generally they will be on the components       4.3.3.4.1 Magnification Magnifications of up to 100X
used in production and should not be removed, as they            may be necessary, for example, to examine components
may actually be the cause of the poor solderability. No          smaller than 0402 chip components.
cleaning of the specimen is allowed. Conditioning, if any,
                                                                 4.3.3.4.2 Suggested     Criteria Prior to any post-test
must be agreed to by the tester and other party in
                                                                 examination, all specimens shall have the flux removed
advance.
                                                                 using a cleaning agent in accordance with 3.2.3. The area
4.3.3.3 Procedure                                                of the test sample with fresh solder adhesion shall be
4.3.3.3.1 Temperature of the Solder The temperature              greater than the area that was immersed in the solder
of the solder is to be stabilized at the required temperature    globule, (i.e. the component shall exhibit positive wetting
for the test before commencing the test. This temperature        beyond its immersion depth). In addition, Table 4–7 lists
shall be per 3.5.1.                                              suggested criteria.
                                                                                                                           23
                                 SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
                Table 4–6 Dipping Angle and Immersion Depth for Components (Directly from IEC 60068-2-69)
                                          Dipping       Figure (See    Immersion       Pin size       Globule
                           a
            Component                     angle b        Fig. 4–12)    depth (mm)       (mm)         weight (mg)      Remarks
                     1005 (0402)       Horizontal or
                                                       2A, 2B                              2              25
                     1608 (0603)       Vertical
Capacitors                                                                 0.10
                     2012 (0805)                                                        3.2 or 4      100 or 200
                                       Horizontal      2A
                     3216 (1206)                                                           4             200
                     1005 (0402)       Vertical        2B
                                                                                           2              25
                     1608 (0603)                       2A, 2B
Resistors                              Horizontal or                       0.10
                     2012 (0805)                                                        3.2 or 4      100 or 200
                                       Vertical        2A,2B,2H c
                     3216 (1206)                                                           4             200
Tantalum
                     Case sizes                             c
capacitors,                            Vertical        2H                  0.10            4             200
                     Ad,B,C,D
LEDs
                     SOT 23, 25,
                     26, 323, 343,                     2D                  0.10            2              25
                     353, 363
                     SOT 89,                                               0.20                                      1 outer pin
                     SOT 223, 523                                                                                    only
                                                       2F
                     Gull wing         20 – 45                             0.25
                     diode
Leaded SMD
                                                                                                                     Remove
                     Any SOIC                                                                                        sufficient
                     VSO QFP,                          2D                  0.20            4             200
                                                                                                                     leads to
                     SOP                                                                                             avoid
                                                                                                                     bridging
                                                                                                                     between
                     PLCC, SOJ         Horizontal      2E                  0.10                                      tested
                                                                                                                     leads
                                                                                                                     Caution
                                                            c
                     QFN               Vertical        2H                  0.10            2              25         from
                                                                                                                     bridging
                     Cylindrical       Horizontal or
                                                       2A, 2B              0.25            4             200
                     SMD               Vertical
                     SOD 80            Vertical        2B                  0.20            4             200
                                                                                                                     Only
                                                                                                                     peripheral
                                                                                                                     balls can
                     Any BGA, CSP                                                                                    be tested,
                                       Horizontal      2G                  0.10            1              10
                     or LGA e                                                                                        and only
                                                                                                                     test down
                                                                                                                     to 1.0 mm
                                                                                                                     pitch
Not recommended for sizes below 1005 (0402).
Bath method is preferred for capacitors 3216 (1206) size.
The recommended dwell time is 5s, except for SOT 89 and SOT 223 components where 10s is recommended.
For Figure 2B, rightward offset distance from the crest of the solder globule shall be 0% to 15% of the pin diameter and shall
avoid leftward offset.
a
     Component names in parentheses, dimensions are expressed in Imperial.
b
     Orientation of the specimen terminals or leads toward the solder surface.
c
     Figure 2H is applicable to the components which do not have electrode toward the solder surface when Figure 2B is applied.
d
     This test may only be applicable with certain test equipment.
e
     This test is recommended only for those balls and bumps that will not melt at the respective temperature and are not
     designed to melt during reflow operation.
24
                     SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
Figure 4–12 Component and Dipping Angle (Directly from IEC 60068-2-69)
                                                                                                                                    25
                           SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
4.3.4 Test E1 – Lead-free Solder – Wetting Balance            d. The flux covered termination shall be immersed only
Solder Pot Test (Leaded Components) This test is for             once in the molten solder to a depth of 0.10 mm
wetting balance testing of leaded components.                    [0.0039 in].
4.3.4.1 Apparatus A solder meniscus force measuring           e. The angle of immersion shall be 20° – 45° (see Figure
device (wetting balance) which includes a temperature            4–2).
controlled solder pot containing solder per 3.2.1 and         f. Immerse and withdraw at 1 mm – 5 mm [0.04 - 0.20
maintained per 3.5.1 and 3.5.2 shall be used. The                in] per second and dwell for 5 +0/-0.5 seconds.
equipment shall have a means of recording force as a             Massive components may require a longer solder dwell
function of time, such as a chart recorder, data logger, or      time (see 5.2).
computer (see Figure 4–9).
4.3.4.1.1 Dipping Device A mechanical or electrome-           4.3.4.4 Evaluation
chanical dipping device incorporated in the wetting
balance shall be used. The device shall be preset to          4.3.4.4.1 Magnification Parts shall be examined at 10X
produce an immersion and emersion rate as specified in        using the equipment specified in 3.3.3. For fine pitch
4.3.4.3. The specimen dwell time is controlled to the time    leaded/termination parts (0.5 mm [0.020 in] pitch or less)
specified in 4.3.4.3. A device to sense contact of the        the inspection magnification shall be 30X.
lead(s) with the molten solder bath shall also be part of
                                                              4.3.4.4.2 Accept/Reject Criteria Suggested criteria for
the fixture or instrument.
                                                              solderability evaluation for Test E1 are listed in Table
4.3.4.2 Preparation Specimen preparation shall be in          4–5. Figures 4–10 and 4–11 illustrate the suggested
accordance with 3.4.                                          criteria of Table 4–5. In addition, the area of the test
                                                              sample with fresh solder adhesion shall be greater than
4.3.4.3 Procedure                                             the area that was immersed in the solder bath (i.e., the
a. Flux per 3.2.2 shall be used. The flux shall be at         component shall exhibit positive wicking beyond its
   ambient (room) temperature.                                immersion depth).
b. Leads and terminations shall have flux applied uni-        4.3.4.4.3 Gauge Repeatability and Reproducibility (GR&R)
   formly and to cover the surfaces to be tested.             Protocol   Appendix H contains a suggested GR&R
c. Dross and burned flux shall be skimmed from the            protocol that may be used by the supplier and user to
   surface of the molten solder immediately before dip-       ensure that the respective wetting balance equipment are
   ping.                                                      correctly calibrated.
26
                       SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
4.3.5 Test F1 – Lead-free Solder – Wetting Balance            d. After application of the flux and post dip dwell, the
Solder Pot Test (Leadless Components) This test is for           specimen shall be mounted on the test equipment.
wetting balance testing of leadless components.               e. Dross and burned flux shall be skimmed from the
                                                                 surface of the molten solder immediately before dip-
4.3.5.1 Apparatus A solder meniscus force measuring
                                                                 ping.
device (wetting balance) which includes a temperature
controlled solder pot containing solder per 3.2.1 and         f. The flux covered termination shall be immersed only
maintained per 3.5.1 and 3.5.2 shall be used. The                once in the molten solder to a depth of 0.10 mm
equipment shall have a means of recording force as a             [0.0039 in] minimum.
function of time, such as a chart recorder, data logger, or   g. The angle of immersion shall be per Figure 4–4.
computer (see Figure 4–9).                                    h. A full curve shall be recorded using the equipment
4.3.5.1.1 Dipping Device A mechanical or electrome-
                                                                 specified in 4.3.5.1.
chanical dipping device incorporated in the wetting
                                                              4.3.5.4 Evaluation
balance shall be used. The device shall be preset to
produce an immersion and emersion rate as specified in        4.3.5.4.1 Magnification Parts shall be examined at 10X
4.3.5.3. The specimen dwell time is controlled to the time    using the equipment specified in 3.3.3. For fine pitch
specified in 4.3.5.3.                                         termination parts (0.5 mm [0.020 in] pitch or less) the
                                                              inspection magnification shall be 30X.
4.3.5.2 Preparation Specimen preparation shall be in
                                                              4.3.5.4.2 Accept/Reject Criteria Suggested criteria for
accordance with 3.4.
                                                              solderability evaluation for Test F1 are listed in Table 4–5.
                                                              Figures 4–10 and 4–11 illustrate the suggested criteria of
4.3.5.3 Procedure
                                                              Table 4–5. In addition, the area of the test sample with
a. Flux per 3.2.2 shall be used and shall be at ambient       fresh solder adhesion shall be greater than the area that
   (room) temperature.                                        was immersed in the solder bath (i.e., the component shall
b. Leads and terminations shall have flux applied uni-        exhibit positive wicking beyond its immersion depth).
   formly and to cover the surfaces to be tested.             4.3.5.4.3 Gauge Repeatability and Reproducibility (GR&R)
c. Immerse and withdraw at 1 mm – 5 mm [0.04 in –             Protocol Appendix H contains a suggested GR&R proto-
   0.20 in] per second and dwell for 5 +0/-0.5 seconds.       col that may be used by the supplier and user to ensure
   Massive components may require a longer solder dwell       that the respective wetting balance equipment are cor-
   time (see 5.2).                                            rectly calibrated.
                                                                                                                        27
                            SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
4.3.6 Test G1 – Lead-free Solder – Wetting Balance               4.3.6.3.2 Fluxing A very small amount of flux is care-
Globule Test This test is for lead-free solder wetting           fully applied to the surface or lead to be tested and the
balance globule testing of components.                           solder globule using a clean cotton tip or bud. No excess
                                                                 flux shall be ready to drip off the fluxed part or the excess
4.3.6.1 Apparatus A solder meniscus force measuring
                                                                 flux must be drained off by carefully touching the lowest
device (wetting balance) which includes a temperature
controlled vertical, cylindrical iron shaft shrunk fit into an   point on the surface to be tested with a piece of clean
aluminum housing on which is placed a specific sized             chemical lab filter paper. For this testing, ideally a small
piece of solder. Examples are: a 200 mg piece of solder          amount of flux should be kept in a small container that is
for a 4 mm diameter globule block, a 25 mg piece for a 2         only opened to immerse the cotton tip to wet it with flux.
mm globule block or a 6.25 mg piece for a 1 mm globule           The cotton tips should be thrown away and replaced with
block. The molten solder globule should ideally be               fresh ones every 5 to 10 tests, with all tests done in the
replaced after each solderability test, but may be re-used       same testing interval. If testing is interrupted for more
for very small components that do not remove more than           than a few minutes, then a new tip should be used.
1% of the solder volume per solder test for up to 5 tests.
                                                                 4.3.6.3.3 Dipping Angle, Immersion Depth, and Immer-
The equipment shall have a means of recording force as a
                                                                 sion Rates The appropriate clip shall be chosen to hold
function of time, such as a chart recorder, data logger or
                                                                 the part as specified in Table 4–6 and illustrated in Figure
computer.
                                                                 4–12. Without contaminating the surfaces to be tested, the
4.3.6.1.1 Dipping Device A mechanical or electrome-              specimen is mounted in the appropriate clip or other
chanical dipping device incorporated in the wetting              device supplied by the solderability tester manufacturer
balance shall be used. The device shall be preset to             and carefully attached to the machine so as to not damage
produce an immersion and emersion rate as specified in           the transducer or dislodge the component from its orien-
4.3.6.3.3. The specimen dwell time is controlled to the          tation in the clip or other holder. The distance between the
time specified in 4.3.6.3.3.                                     solderable surface of the sample and the solder globule
                                                                 should be fixed. An immersion speed between 1
4.3.6.2 Materials
                                                                 mm/second and 5 mm/second [0.039 in/second and 0.20
4.3.6.2.1 Flux The flux used shall be in accordance with         in/second] should ensure that most test specimens are
3.2.2.                                                           fully immersed. A dwell time of 5 seconds shall be used.
4.3.6.2.2 Solder The solder alloy shall be in accordance         A dwell time of 10 seconds may be necessary for large
with 3.2.1. Other alloys may be used upon agreement              components or components with high thermal mass (see
between user and other parties.                                  5.2).
4.3.6.2.3 Test Specimen The test specimen shall either           4.3.6.3.4 Preheat The decision to use preheat should be
be a full component or a lead that has been carefully            as agreed upon between the user and supplier, prior to
removed from the component. Ideally the cross-section of         testing.
the component to be dipped is either rectangular, square
or round, to facilitate calculation of the theoretical
                                                                 4.3.6.4 Evaluation
maximum wetting force. Ideally no burr should be present
but, if they are, generally they will be on the components       4.3.6.4.1 Magnification Magnifications of up to 100X
used in production and should not be removed, as they            may be necessary, for example, to examine components
may actually be the cause of the poor solderability. No          smaller than 0402 chip components.
cleaning of the specimen is allowed. Conditioning, if any,
must be agreed to by the tester and other party, in              4.3.6.4.2 Suggested     Criteria Prior to any post-test
advance.                                                         examination, all specimens shall have the flux removed
                                                                 using a cleaning agent in accordance with 3.2.3. The area
4.3.6.3 Procedure                                                of the test sample with fresh solder adhesion shall be
4.3.6.3.1 Temperature of the Solder The temperature              greater than the area that was immersed in the solder
of the solder is to be stabilized at the required temperature    globule, (i.e. the component shall exhibit positive wetting
for the test before commencing the test. This temperature        beyond its immersion depth). In addition, Table 4–7 lists
shall be per 3.5.1.                                              suggested criteria.
28
                       SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
                                                                                                                              29
                        SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
                                                 Appendix A
                                       Critical Component Surfaces
View 1
                                                                                 T = Lead
                                                                                     Thickness
2 xT
                   View 2
                                                                         C
                                      Se
                                        ati
                                           ng
                                                Pla
                                                   ne
                                                        2x
                                                             T
                                                                                          C
B A
IPC-002c-a-1
30
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IPC-002c-a-2
                                                                                                          31
                         SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
View 1
                                                                         T = Lead
                                                                             Thickness
                                                                                     1 xT
                        Seating Plane
View 2
                            Se
                              ati
                                 ng
                                      Pla
                                         ne
                                               1x
                                                    T
B A (Underside)
IPC-002c-a-3
32
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IPC-002c-a-4
                                                                                                           33
                                SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
             View 1
                                                       T = Lead Thickness
                                                                                    F
                                   Seating Plane
             View 2
                                                                                                       H
                                                         B
                                     Excluded
                Se                                                                           F
                  ati
                     ng
                          Pla
                             ne
                                                  C
                                                                               A (Underside)
                                         1x
                                              T
34
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IPC-002c-a-6
                                                                                                          35
                         SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
IPC-002c-a-7
36
                    SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
IPC-002c-a-8
                                               A, Terminal Underside.
                                               Length L, Width W
IPC-002c-a-9
                                                                                                                      37
                            SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
IPC-002c-a-10
[Critical Surface: Each soldersphere shall have incorporated the solderpaste deposit (uniform, smooth solder with no dewetted
areas)]. With Tests S and S1 – Surface Mount Process Simulation, the component leads shall be wetted in a consistent and unified
manner, with no evidence of surface oxidation anomalies.
38
                     SINGLE USER LICENSE - NOT FOR USE ON A NETWORK OR ONLINE
                                                     Appendix B
                                                   Evaluation Aids
B.1 Evaluation Aids for Tests A, C, A1 and C1                   size defects are also listed. Combinations of these sizes
                                                                can also be totaled easily (see Figure B-1).
B.2 Round Leads The measurement of defects or the
estimation of defect area percentage of the lead total          In considering areas not covered by a continuous, new
surface area, is more difficult with round leads than it is     solder coating and referring to the defined defects illus-
with flat surface rectangular leads. For example, in            trated in Figure B-2, the visible areas of dewetting and
viewing a cylindrical surface such as a round lead, a           nonwetting are applicable directly.
round diameter-sized defect when flat appears oval shaped       An example of what constitutes 5% of the dipped area is:
and narrower in width than the visible surface of the lead      six defects of 0.813 mm [0.032 in] diameter in a 25.4 mm
in the transverse direction, which is half of its circumfer-    [1.0 in] length of a 0.813 mm [0.032 in] diameter (No. 20
ence.                                                           AWG) wires (see Figures B-3, B-4 and B-5}.
To aid the solderability test inspector in estimating the
lead surface percentage after solderability testing, a guide    B.3 Square    Terminations Square terminations shall
sheet for different diameter leads is shown in Figure B-3.      meet the requirements of the solderability coverage guide
When 25.4 mm [1.0 in] of the lead surface of a 0.5 mm           shown in Figure B-5.
[0.02 in] diameter lead is inspected for solder coverage,
10 diameter size defects equal 5% of the total lead surface     B.4 Castellated Terminations Castellated terminations
area. Numbers of half diameter size and quarter diameter        shall meet the same criterion as round leads.
                      Example "A"
                      0.51 mm Dia.
                      Size Area
                                              Example "B"
                                              1/2 of Dia.
                                              Size Area            Example "C"
                                                                   1/4 of Dia.
                                                                   Size Area
             Body
IPC-002c-b-1
                                                                                                                               39
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a) Dewetting b) Nonwetting
c) Pinholes IPC-002c-b-2c
40
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                                                   TERMINAL
                                                 _ROUND_LEAD
                                                  SCALE: 10X
                                         CRITICAL AREA 5% DEFECTIVE
                                      AFTER THE MANNER OF MIL. STD. 202
                                           METHOD 208 FIGURE 208-7
                                    20 UNITS OF 400 DISTRIBUTED RANDOMLY
IPC-002c-b-3
                                                                                                                  41
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IPC-002c-b-4
42
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3 Percent Defects
5 Percent Defects
8 Percent Defects
IPC-002c-b-5
                                                                                                           43
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                                             Appendix C
                              Calculation of Maximum Theoretical Force
Maximum theoretical force is calculated using the proce-       t = Lead height (nominal) = 0.1524 mm
dure of Klein Wassink.1                                        d = Immersion depth = 0.3 mm
Force (Max. Theoretical) = (γ) (P) (cosine β) – (d)(g)         1 = Lead length immersed on bottom side at 20° angle
(V) = [0.4P – 0.08V] mN                                        and 0.3 mm depth = 0.877 mm
where:                                                         m = Lead length immersed on top side at 20° angle and
                                                               0.3 mm depth = 0.458 mm
P = the perimeter of the test specimen in millimeters, i.e.,
                                                               k = Length of solder/lead/air interface along lead side =
the length in millimeters of the solder/printed board or
                                                               0.446 mm
coupon pad (or hole)/air interface as measured at maxi-
mum depth of immersion.                                        2k + 2w = Total length per lead of solder periphery =
                                                               0.892 + 0.508 = 1.4 mm
V= The volume in cubic millimeters of the test specimen
that resides below the solder/board air interface as           P = Total length of periphery per side (33 leads) = 46.2
measured at the maximum depth of immersion.                    mm
γ = Surface tension of solder = 0.4 mN/mm                      Hence:
γ = Surface tension of Pbfree solder = 0.5 mN/mm               Total volume immersed per lead = 0.254 X 0.1524 X
α = Immersion angle of the board to the horizontal             0.458 + 0.5(0.1524 X 0.254 X 0.419) = 0.0177 + 0.0081
surface, i.e., α = 45°                                         = 0.0258 mm3
β = Wetting angle of solder to the board under optimal         Therefore for an 132 I/O QFP, the maximum theoretical
conditions, i.e., β = 0 and therefore the cosine β = 1         wetting force is:
d = Density of solder at 235°C, = 8120 kg/m3 for
                                                               For 33 leads (one side of an 132 I/O QFP) = 33 x 0.0258
Sn60/Pb40 Alloy
                                                               mm3 = 0.85
d = Density of solder at 255°C = 7410 kg/m3 for SAC305
                                                               Maximum Force = (0.4 x 46.2) – (0.08 x 0.85) = 18.41
Alloy
                                                               mN
g = Gravitational constant = 9.8 x 103 mm/s2
                                                               And, for a part of 46.2 mm total periphery:
Periphery and volumes are to be calculated using the           Maximum Force per length of interface = 399 µN/mm
nominal values provided by the device supplier in the
                                                               The force measured on a part in the Set A criteria must
package drawing and the angles and depths of immersion
                                                               therefore be greater than 9.2 mN or 200 µN/mm at F2.
as described in the specification above. The TOTAL
periphery and volume, i.e., the sum of all leads being         Note: All forces are referenced to the corrected zero axis
immersed, is to be used in this calculation.                   and not the zero force line except for the Appendix D
                                                               calculation (parameter AA).
Figure C-1 depicts a sample calculation for 132 I/O QFP.
                                                               1. R. J. Klein Wassink, ‘‘Soldering in Electronics,’’ 2nd
Where:
                                                               Edition, Electrochemical Publications, Ayr, Scotland,
w = Lead width (nominal) = 0.254 mm                            1989, pp 308–309
44
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                                                      m                              α
             Solder Bath Surafce
                                         d
                 t=0.1524                                   l
                         w=0.254
IPC-002c-c-1
Figure C-1 Lead Periphery and Volume for a 132 I/O PQFP
                                                                                                           45
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                                               Appendix D
                                     Calculation of Integrated Value
                                      of Area of the Wetting Curve
The area is calculated using the maximum theoretical        2. The test specimen essentially attains the full maximum
force (see Figure 4.18 or 4.19). Therefore, the area is     theoretical force as it crosses the zero line at two (2)
given as:                                                   seconds and holds that value for the duration of the test,
                                                            i.e., three (3) seconds.
Area = Wetting force x time – Buoyancy x time
                                                              V = Total Volume = 0.4 mm3
Area = (3.0 sec. x Max. Theoretical Force) – 2.0 sec (ρ)
(g) V                                                         Maximum Theoretical Force: 3.97 mN
Area = (3.0 sec. x Max. Theoretical Force) – 2.0 sec x –    Area = (3.0 sec. x 3.97mN) – (2.0 sec. x 0.08 (kg/mm3 x
(8.12 x 10-6 kg/mm3 x 9.8 x 103 mm/s2 x V)                  mm/s2) x 0.4 mm3) = 11.91 mN x seconds – 0.064
                                                            (kg-mm/sec)
The value V is the volume of the test specimen immersed
in the solder bath as calculated in Appendix C. The         Since F= ma, then mN = kg x mm/sec2 or kg =
maximum theoretical force is calculated as per Appendix     mNsec2/mm
C. The following assumptions are made:                      Area = 11.91 mN x seconds – 0.064 (mNsec2/mm) x
                                                            (mm/sec)
1. The maximum buoyancy force holds for the whole two
(2) seconds contributing a negative area of: the buoyancy   Area = 11.91 mN x seconds – 0.064 mN x seconds
force times two (2) seconds.                                Area = 11.85 mN x seconds
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                                                  Appendix E
                                              Informative Annex
E.1 Test Equipment Sources The equipment sources            ability Testing and Solutions Inc., 18 Wildrose Dr.,
described below represent those currently known to the      Edgewood, KY 41017, (859) 331–0598, www.wettingbal-
industry. Users of this document are urged to submit        ance.com
additional source names as they become available, so that
this list can be kept as current as possible.               E.1.4 Steam Conditioning Equipment
                                                            H&H Engineering, Inc., 3612 Wood Duck Circle, Stock-
E.1.1 Tests A, B, C, D, A1, B1, C1, D1
                                                            ton, CA 95206
GEN3 Systems Limited (Formerly Concoat Systems) Unit
B2, Armstrong Mall, Southwood Business Park, Farnbor-       Metronelec, 54, Route de Sartrouville – Le Montreal
ough, Hampshire GU14 0NR England. 011 44 12 5252            78232 Le PECO Cedex, France (USA Distributor: Solder-
1500 www.gen3systems.com                                    ability Testing and Solutions Inc., 18 Wildrose Dr.,
                                                            Edgewood, KY 41017, (859) 331–0598 www.wettingbal-
HMP Soldermatics, P.O. Box 948, Canon City, CO 81215,       ance.com
(719) 275–1531
                                                            Mountaingate Engineering Inc., Campbell, CA 95008,
Malcomtech 26200 Industrial Blvd, Hayward CA 64545,         (408) 866–5100
(510)293–0580, www.malcomtech.com
                                                            Robotic Process Systems Inc., 23301 E. Mission Ave.,
Reef Engineering, Unit 6, Bancrofts Road, South             Liberty Lake, WA 99019, (509) 891–1680
Woodham Ferrers, Essex CM3 5UQ 01245 328123
                                                            Zentek Scientific Systems, 3520 Yale Way, Fremont, CA
Robotic Process Systems Inc., 23301 E. Mission Ave.,        94538, (510) 651–1581
Liberty Lake, WA 99019, (509)891–1680
                                                            E.1.5 Grid Reticles
E.1.2 Tests E, F, E1 & F1
                                                            Bender Associates, 5030 South Mill Avenue, Suite C-2,
Convey AB, Harpsundsvagen 113, S-12458 Bandhagen,
                                                            Tempe, AZ 85252, (602) 820–0900
Sweden 46 (0) 8 99 66 25
GEN3 Systems Limited (Formerly Concoat Systems) Unit        E.2 Test Flux Product Sources The Test Flux product
B2, Armstrong Mall, Southwood Business Park, Farnbor-       sources described below represent those currently known
ough, Hampshire GU14 0NR England. 011 44 12 5252            to the industry. Users of this document are urged to
1500 www.gen3systems.com                                    submit additional product source names as they become
Malcomtech 26200 Industrial Blvd, Hayward CA 64545,         available, so that this list can be kept as current as
(510) 293–0580, www.malcomtech.com                          possible.
Metronelec, 54, Route de Sartrouville – Le Montreal         AIM Solder {www.aimsolder.com} – Standard Flux #1
78232 Le PECO Cedex, France (USA Distributor: Solder-       Product ID: RMA 202–25
ability Testing and Solutions Inc., 18 Wildrose Dr.,        Alpha Metals {www.alphametals.com} – Standard Flux
Edgewood, KY 41017, (859) 331–0598, www.wettingbal-         #2
ance.com
                                                            GEN3 Systems Limited {www.gen3systems.com} – Prod-
Robotic Process Systems Inc., 23301 E. Mission Ave.,        uct ID’s: SMNA – Standard Flux #1: Actiec 2 / –
Liberty Lake, WA 99019, (509)891–1680                       Standard Flux #2: Actiec 5
                                                                                                                  47
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                                             Appendix F
                             J-STD-002/J-STD-003 Activated Solderability
                                Test Flux Rationale Committee Letter
48
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4) Standardization of Solderability Test Flux Composition    compatibility of flux composition requirements between
   on a Global Scale                                         the J-STD-002/003 specification and the IEC specifica-
A second major goal of the J-STD-002/003 solderability       tions is a win-win situation for electronics assemblers and
committees is to develop test methods and standards          component/printed wiring board fabricators.
which promote global standardization for the electronics     A number of the major flux chemistry suppliers have been
industry. The standard activated flux composition selected   queried on the electronics industry’s ability to purchase
and tested by the committees has been utilized in the        the standard activated flux composition, and a positive
International Electrotechnical Commission (IEC) 60068-       response was received. If you have any questions please
2-20 Soldering specification. The IEC specification is       contact the IPC Technical Staff to obtain additional
successfully utilized for solderability testing. Having      answers/clarification.
                                                                                                                     49
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                                      Appendix G
                Graphical Representations: Progression of Solder Wetting
               Curve Parameters As Measured By Wetting Balance Testing
Time 0
                                               F1
                                                                                F2
                      0
                                                    T1               Time (s)        T2
                                                         Buoyancy
Force (mN)
Time 0
                                               F1
                                                                                F2
                       0
                                                    T1               Time (s)        T2
                                                         Buoyancy
Force (mN)
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Time 0 Ta
                                         F1
                                                                           F2
Ta
                   0
                                              T1               Time (s)         T2
                                                    Buoyancy
Force (mN)
Time 0 Ta Tb
                                         F1
                                                                           F2
Ta Tb
                   0
                                              T1               Time (s)         T2
                                                    Buoyancy
Force (mN)
                                                                                               51
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Time 0 Ta Tb T2
                               Fmax
                         2/
                                                                         F1
                           3   Fmax                                                                       F2
Ta Tb
                                 0
                                                                                               Time (s)
                                                  Time to 2/ Fmax
                                                                              T1                               T2
                                                                                    Buoyancy
                                                            3
Force (mN)
                 The net of the parameters measured from the progression of the five steps
                   encountered during the wetting balance testing, as highlighted above:
          Force (mN)
                                                Typical Wetting Curve
          0.8
          0.7
          0.6
          0.5
          0.4
          0.3
          0.2
          0.1
                                                                     F1                                                 F2
                 0
                         Buoyancy
          -0.1
          -0.2
          -0.3
          -0.4
          -0.5
          -0.6
          -0.7
          -0.8
                     0                      1                             2                3          4                    5
                                                                                                                    Time (s)
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                                          Appendix H
                  Test Protocol for Wetting Balance Gauge Repeatability and
                      Reproducibility (GR&R) Using Copper Foil Coupons
 1. All coupons for these tests shall be prepared individu-          d. Immerse the sample immediately into DI water and
    ally just prior to testing. Do NOT batch clean the                  gently agitate for 20 seconds.
    samples.                                                         e. Blot the sample dry as in step ‘‘b’’ above.
 2. Copper foil of 35 microns nominal thickness (‘‘1 oz’’         8. Dip sample into the ‘‘standard activated flux’’ nor-
    copper) shall be used for the test.                              mally used for solderability testing for 5 seconds.
 3. The copper foil shall have NO surface treatment and           9. Holding the samples vertically, blot to remove excess flux.
    is expected to have an oxidized appearance upon              10. Place sample into tool holder.
    receipt from the supplier. Do not use the copper foil if
    it is bright and shiny. This is indicative of surface anti   11. Run the test.
    tarnish treatments being used. Surface treatments/           12. Repeat ten times for each foil width and each test
    preservatives can interfere with the ability to make a           person. It is recommended that three people should be
    consistent ‘‘known good coupon’’ necessary for this              used for the GR&R study.
    test.                                                        13. For ease of data manipulation it is recommended to
 4. The copper foil coupons shall be die cut to ensure               convert the wetting forces obtained into mN/mm of
    repeatability of the samples being tested and shall be           the coupon’s wettable length (perimeter). For
    of the following width dimensions;                               example, the 10 mm wide coupon has a total wettable
                                                                     length (perimeter) = [(2 x 10 mm) + (2 x 0.035 mm)]
    a. 2 mm
                                                                     = 20.07 mm.
    b. 5 mm
                                                                 14. For the ‘‘standard activated’’ flux of nominal 0.2%
    c. 10 mm                                                         activation, the wetting force used for the calculations
 5. Create a file for each foil width and for each                   shall be 0.31 mN/mm. If a more active flux is being
    individual person that is involved performing the                used, a large sample shall be run to obtain the mean
    GR&R.                                                            value and this used for the calculations.
 6. Test parameters shall be:                                    15. Calculate the standard deviation for each of the foil
                                                                     widths and the people running the test.
    a. Solder temperature shall be the as recommended
       for the alloy and the specification being used, i.e.,     16. Multiply the standard deviation value by 6 (this
       for SnPb and ANSI-J-STD-003 it shall be 235 ºC,               represents the plus - minus 3 standard deviations of a
       for ANSI-J-STD-002 it shall be 245 ºC. For SAC                normal distribution)
       305 it shall be 255 ºC, regardless of the specifica-      17. Divide this number by 0.31 and multiply by 100 to
       tion.                                                         obtain a percentage value.
    b. Immersion depth shall be 0.4 mm.                          18. Tabulate the three values per person.
    c. Immersion speed shall be 2 mm/sec.                        19. For an acceptable GR&R, the values obtained should
                                                                     be below 10%.
    d. Dwell time in the solder shall be 10 seconds.
                                                                 20. There should be excellent R&R results with the 10
    e. Immersion angle shall be 90 degrees incident to               mm coupon the first time this protocol is performed
       the solder.                                                   with an increasing spread from test person to test
    f. No preheat shall be used.                                     person when using the smaller coupons. The test may
 7. Sample preparation for the ‘‘known good coupon’’                 need to be repeated or individuals may require some
    shall be as follows:                                             ‘‘practice time’’ prior to running the full GR&R.
    a. Use a tweezers to immerse a foil sample into a            21. In addition to testing the individual, this protocol also
       beaker of Acetone and gently agitate for 20                   tests the machine and will show linearity and any bias
       seconds.                                                      if it exists. Because the wetting forces have been
                                                                     normalized to mN/mm, the readings for each coupon
    b. Remove sample and blot both sides dry with ‘‘Kim              width should be the same. If they are clearly different
       wipes’’ or other suitable lab tissue.                         but the standard deviations produced by the individual
    c. Again using a tweezers, immerse the above sample              test people are below 10%, then there is a problem
       into a 20% v/v Nitric acid/DI water solution and              with the wetting balance and the equipment manufac-
       gently agitate for 20 seconds.                                turer should be notified.
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Address
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